CN1471820A - Insecticide producing method by cartap pesticide devil liquor and its products and use method - Google Patents
Insecticide producing method by cartap pesticide devil liquor and its products and use method Download PDFInfo
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- CN1471820A CN1471820A CNA021383049A CN02138304A CN1471820A CN 1471820 A CN1471820 A CN 1471820A CN A021383049 A CNA021383049 A CN A021383049A CN 02138304 A CN02138304 A CN 02138304A CN 1471820 A CN1471820 A CN 1471820A
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- insecticide
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- waste liquid
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Abstract
A process for preparing the insecticide from the waste liquid of cartap includes such steps as determining the content of active component in the waste dliquid, regulating the content of cartap to 6%, mixing it with sodium hydroxide, reacting for 2-3 hr, and adding less nitrone as penetrant and raw imidacloprid. Its advantages are high effect and low cost.
Description
Technical field
The present invention relates to a kind ofly utilize method that the cartap pesticide waste liquid makes insecticide and with the pesticide product of this method acquisition and the usage of this insecticide.
Background technology
It is about 6% waste liquid that the cartap pesticide producing can produce concentration, must be through handling before the discharging, and its processing cost is very high, has increased the weight of the burden of pesticide producing producer.And on the other hand, for insect pests such as aphelenchoides besseyi disease, rice leaf roller, the production cost of existing pesticide product is generally higher.
Summary of the invention
Technical problem to be solved by this invention is, a kind of insecticide that is used for preventing and treating insect pests such as aphelenchoides besseyi disease, rice leaf roller that can utilize the manufacturing of cartap pesticide waste liquid is provided, it is compared with existing existing this insecticides better prevention effect and lower cost, also reduces the processing cost of cartap pesticide waste liquid simultaneously.
The method that the present invention makes insecticide with the cartap pesticide waste liquid is: after at first the cartap pesticide waste liquid being carried out active ingredient chemical examination mensuration, regulate the content of cartap in the waste liquid, make it reach 6% steady concentration, pour into reactor reaction 2～3 hours after pressing deployed 6% cartap pesticide waste liquid and the abundant mixing and stirring of sodium hydroxide then, make liquid PH value reach 5, after finishing, reaction adds an amount of penetrant azone, also can add a small amount of 96% the former medicine of Imidacloprid again, pour out packing again, be finished product.
The composition proportion of pesticide product of the present invention is: 1～3 part of 93～96 parts of 6% cartap pesticide waste liquid (weight portion, down with), 2～4 parts in sodium hydroxide, azone, 0～1 part of 96% the former medicine of Imidacloprid.
The method that insecticide of the present invention is used for preventing and treating the aphelenchoides besseyi disease is: insecticide of the present invention is picked up vernalization to showing money or valuables one carries unintentionally with 500 times～3000 times aqueous solution seed soaking after 48～60 hours, sowing then.
The method that insecticide of the present invention is used for preventing and treating rice leaf folder is: spray after insecticide of the present invention is blended into an amount of water with the dosage of every mu of 300ml～500ml.
The method that insecticide of the present invention is used for preventing and treating cabbage caterpillar is: spray after insecticide of the present invention is blended into an amount of water with the dosage of every mu of 150ml～500ml.
Insecticide of the present invention is used for the anti-method that eliminates aphis and is: spray after insecticide of the present invention is blended into an amount of water with the dosage of every mu of 100ml～200ml.
The present invention is owing to utilized the waste liquid of producing agricultural chemicals to make insecticide, its technology is simple, convenient, has saved pesticide producing producer carries out purified treatment and discharging to waste liquid huge spending.Pesticide product insecticidal effect of the present invention is remarkable simultaneously, can reach or cross existing similar pesticide product, and its cost is significantly less than the common insecticides product.Wherein, can reach more than 90%, save cost more than 80% than conventional control medicament to the control efficiency of aphelenchoides besseyi disease; Control efficiency to rice leaf folder can reach more than 90%, saves cost 40% than conventional control medicament; Control efficiency to the vegetables cabbage caterpillar can reach 83%, saves 1.4 times of costs than the control medicament of routine; Control efficiency to vegetable aphid can reach more than 99%.
Embodiment
Embodiment one: (one) insecticide manufacture method: after earlier the cartap pesticide waste liquid being carried out active ingredient chemical examination mensuration, regulate the content of cartap in the waste liquid, make it reach 6% steady concentration.Get 97 parts of this soups and sodium hydroxide again and mix the back reactor internal reaction 2～3 hours for about 2 parts.The penetrant azone that adds 1 part after reaction is finished.(2) insecticidal formulation: 97 parts of 6% cartap pesticide waste liquids, 2 parts in sodium hydroxide, 1 part of azone.(3) insecticide using method: (1) is mixed with 2000 times of aqueous solution to the control of aphelenchoides besseyi disease with insecticide of the present invention, soaks seed rice after 48 hours, and the vernalization that drains away the water can be sowed to showing money or valuables one carries unintentionally; (2) to the control of rice leaf folder,, convert 50 kilograms of sprayings of water with the dosage of insecticide of the present invention according to 400 milliliters every mu.
Embodiment two: (one) insecticide manufacture method: after earlier the cartap pesticide waste liquid being carried out active ingredient chemical examination mensuration, regulate the content of cartap in the waste liquid, make it reach 6% steady concentration.Get 96 parts of this soups and sodium hydroxide again and mix the back reactor internal reaction 2～3 hours for about 2 parts.1 part of the former medicine of Imidacloprid of 1 part of back adding penetrant azone and 96% is finished in reaction.(2) insecticidal formulation: 96 parts of 6% cartap pesticide waste liquids, 2 parts in sodium hydroxide, 1 part of azone, 1 part of Imidacloprid.(3) insecticide using method: (1) with the dosage of insecticide of the present invention according to 150 milliliters every mu, converts 50 kilograms of sprayings of water to the control of vegetables cabbage caterpillar; (2) to the control of vegetable aphid,, convert 50 kilograms of sprayings of water with the dosage of insecticide of the present invention according to 100 milliliters every mu.Provide contrast experiment's data of embodiment of the invention practical effect below:
(1) to the control efficiency such as the following table of aphelenchoides besseyi disease:
| Handle | Repeat | Sick cave number | The diseased plant number | Diseased plant rate % | The diseased plant rate % that goes down |
| 1000 times of aqueous solution of insecticide of the present invention | ????1 | ????4 | ????4 | ????0.39 | ????86.14 |
| ????2 | ????4 | ????5 | ????0.49 | ||
| ????3 | ????2 | ????2 | ????0.20 | ||
| ????4 | ????4 | ????4 | ????0.39 | ||
| On average | ????3.5 | ????3.75 | ????0.37 | ||
| 2000 times of aqueous solution of insecticide of the present invention | ????1 | ????3 | ????3 | ????0.29 | ????84.27 |
| ????2 | ????6 | ????6 | ????0.59 | ||
| ????3 | ????2 | ????3 | ????0.29 | ||
| ????4 | ????4 | ????5 | ????0.49 | ||
| On average | ????3.75 | ????4.25 | ????0.42 | ||
| 3000 times of aqueous solution of insecticide of the present invention | ????1 | ????6 | ????6 | ????0.59 | ????79.77 |
| ????2 | ????4 | ????4 | ????0.39 | ||
| ????3 | ????8 | ????8 | ????0.78 | ||
| ????4 | ????4 | ????4 | ????0.39 | ||
| On average | ????5.5 | ????5.5 | ????0.54 | ||
| 6000 times of aqueous solution of 98% Padan's pulvis | ????1 | ????13 | ????8 | ????0.78 | ????79.03 |
| ????2 | ????3 | ????4 | ????0.39 | ||
| ????3 | ????8 | ????9 | ????0.88 | ||
| ????4 | ????3 | ????2 | ????0.20 | ||
| On average | ????6.75 | ????5.75 | ????0.56 | ||
| Blank (CK) | ????1 | ????9 | ????12 | ????1.18 | ????-- |
| ????2 | ????19 | ????20 | ????1.96 | ||
| ????3 | ????23 | ????41 | ????4.02 | ||
| ????4 | ????17 | ????36 | ????3.53 | ||
| On average | ????17 | ????27.25 | ????2.67 |
(2) to the control efficiency such as the following table of rice leaf folder: (behind the medicine 4 days)
| Handle | Repeat | The hundred caves bundle number of sheets | The residual worm amount in hundred caves | Significance | |||
| Number | Compare CK-% | Number | Compare CK-% | ????0.05 | ????0.01 | ||
| Insecticide 200ml/ mu of the present invention | ????1 | ????30 | ????34.8 | ????10 | ????58.3 | ????a | ????A |
| ????2 | ????60 | ????23.1 | ????12 | ????64.7 | |||
| ????3 | ????32 | ????38.5 | ????10 | ????50 | |||
| ????4 | ????36 | ????43.7 | ????6 | ????78.6 | |||
| On average | ????39.5 | ????34.2 | ????9.5 | ????64.1 | |||
| Insecticide 300ml/ mu of the present invention | ????1 | ????22 | ????52.2 | ????4 | ????83.3 | ????b | ????B |
| ????2 | ????26 | ????66.6 | ????8 | ????76.5 | |||
| ????3 | ????22 | ????57.7 | ????6 | ????70 | |||
| ????4 | ????18 | ????71.9 | ????8 | ????71.6 | |||
| On average | ????22 | ????63.3 | ????6.5 | ????75.4 | |||
| Insecticide 400ml/ mu of the present invention | ????1 | ????12 | ????73.9 | ????2 | ????91.7 | ????c | ????C |
| ????2 | ????16 | ????79.5 | ????6 | ????82.3 | |||
| ????3 | ????12 | ????77.0 | ????2 | ????90 | |||
| ????4 | ????6 | ????90.6 | ????0 | ????100 | |||
| On average | ????11.5 | ????80.8 | ????2.5 | ????90.6 | |||
| 18% dimehypo water solution 250ml/ mu | ????1 | ????24 | ????47.8 | ????4 | ????83.3 | ????c | ????C |
| ????2 | ????28 | ????64.1 | ????4 | ????88.2 | |||
| ????3 | ????10 | ????80.7 | ????4 | ????80 | |||
| ????4 | ????12 | ????81.2 | ????2 | ????92.9 | |||
| On average | ????18.5 | ????69.2 | ????3.5 | ????86.8 | |||
| Blank (CK) | ????1 | ????46 | ????/ | ????24 | |||
| ????2 | ????78 | ????/ | ????34 | ||||
| ????3 | ????52 | ????/ | ????20 | ||||
| ????4 | ????64 | ????/ | ????28 | ||||
| On average | ????60 | ????/ | ????26.5 | ||||
(3) to control efficiency such as the following table of cabbage caterpillar:
| Make with medicament | Preparation (gram/mu) | Radix (head/strain) before the medicine | Behind the medicine 3 days | Behind the medicine 7 days | ||
| Borer population (head/strain) alive | Proofread and correct preventive effect (%) | Borer population (head/strain) alive | Proofread and correct preventive effect (%) | |||
| Insecticide of the present invention | ????100 | ????12.10 | ????0.50 | ??97.74 | ????9.05 | ????74.85 |
| ????150 | ????11.80 | ????0.25 | ??98.84 | ????6.75 | ????81.09 | |
| ????200 | ????12.65 | ????0.10 | ??96.62 | ????6.20 | ????83.91 | |
| 95% cartap WP | ????19.47 | ????11.45 | ????0.70 | ??96.32 | ????16.40 | ????52.14 |
| 2.5% decis EC | ????30 | ????11.45 | ????0.50 | ??97.57 | ????12.05 | ????63.15 |
| Blank | ????-- | ????6.35 | ????11.35 | ??-- | ????19.15 | ????-- |
(4) to the control efficiency such as the following table of vegetable aphid:
| Make with medicament | Preparation (gram/mu) | Radix (head/strain) before the medicine | Behind the medicine 3 days | Behind the medicine 7 days | ||
| Borer population (head/strain) alive | Proofread and correct preventive effect (%) | Borer population (head/strain) alive | Proofread and correct preventive effect (%) | |||
| Insecticide of the present invention | ????100 | ????45.90 | ????2.50 | ????97.61 | ????2.15 | ??99.01 |
| ????150 | ????43.60 | ????0.50 | ????99.49 | ????0.55 | ??99.56 | |
| ????200 | ????51.40 | ????0.40 | ????99.56 | ????0.30 | ??99.86 | |
| 10% Imidacloprid WP | ????10 | ????38.0 | ????0.50 | ????99.38 | ????1.35 | ??98.53 |
| Blank | ????-- | ????32.75 | ????65.55 | ????-- | ????119.95 | ??-- |
Claims (7)
1, a kind of method of making insecticide with the cartap pesticide waste liquid, it is characterized in that: after at first the cartap pesticide waste liquid being carried out active ingredient chemical examination mensuration, regulate the content of cartap in the waste liquid, make it reach 6% steady concentration, pour into reactor reaction 2～3 hours after getting deployed 6% cartap pesticide waste liquid and the abundant mixing and stirring of sodium hydroxide then, make liquid PH value reach 5, add an amount of penetrant azone after reaction is finished, pour out packing again.
2, the method with cartap pesticide waste liquid manufacturing insecticide according to claim 1 is characterized in that: the former medicine of Imidacloprid of adding a small amount of 96% before soup is poured out packing.
3, a kind of insecticide, its prescription is: 1～3 part of 93～96 parts of 6% cartap pesticide waste liquid (weight portion, down with), 2～4 parts in sodium hydroxide, azone, 0～1 part of 96% the former medicine of Imidacloprid.
4, a kind of method with the described insecticide control aphelenchoides besseyi of claim 3 disease is characterized in that: this insecticide is picked up vernalization to showing money or valuables one carries unintentionally with 500 times～3000 times aqueous solution seed soaking after 48～60 hours, sowing then.
5, a kind of method with claim 3 described insecticide control rice leaf folder is characterized in that: spray after this insecticide is blended into an amount of water with the dosage of every mu of 300ml～500ml.
6, a kind of method with claim 3 described insecticide control vegetables cabbage caterpillar is characterized in that: spray after this insecticide is blended into an amount of water with the dosage of every mu of 150ml～500ml.
7, a kind of method with claim 3 described insecticide control aphid is characterized in that: spray after this insecticide is blended into an amount of water with the dosage of every mu of 100ml～200ml.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 02138304 CN1197457C (en) | 2002-09-17 | 2002-09-17 | Insecticide producing method by cartap pesticide devil liquor and its products and use method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 02138304 CN1197457C (en) | 2002-09-17 | 2002-09-17 | Insecticide producing method by cartap pesticide devil liquor and its products and use method |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1471820A true CN1471820A (en) | 2004-02-04 |
| CN1197457C CN1197457C (en) | 2005-04-20 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 02138304 Expired - Fee Related CN1197457C (en) | 2002-09-17 | 2002-09-17 | Insecticide producing method by cartap pesticide devil liquor and its products and use method |
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| CN (1) | CN1197457C (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2008049264A1 (en) * | 2006-10-23 | 2008-05-02 | Zhenjiangshi Agriculture Research Institute | A method of preparing a pesticide from cartap waste liquid and its product as well as its use |
| CN102626096A (en) * | 2012-03-22 | 2012-08-08 | 江苏省绿盾植保农药实验有限公司 | Particulate agent for controlling Nilaparvata lugens prepared from pesticide waste liquid, and preparation method thereof |
| CN107836460A (en) * | 2017-11-22 | 2018-03-27 | 江苏邦盛生物科技有限责任公司 | A kind of Pesticidal combination and its application containing cartap and imidacloprid |
| CN108184846A (en) * | 2018-01-18 | 2018-06-22 | 四川龙蟒福生科技有限责任公司 | A kind of gibberellic acid missible oil and preparation method thereof |
-
2002
- 2002-09-17 CN CN 02138304 patent/CN1197457C/en not_active Expired - Fee Related
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2008049264A1 (en) * | 2006-10-23 | 2008-05-02 | Zhenjiangshi Agriculture Research Institute | A method of preparing a pesticide from cartap waste liquid and its product as well as its use |
| CN102626096A (en) * | 2012-03-22 | 2012-08-08 | 江苏省绿盾植保农药实验有限公司 | Particulate agent for controlling Nilaparvata lugens prepared from pesticide waste liquid, and preparation method thereof |
| CN107836460A (en) * | 2017-11-22 | 2018-03-27 | 江苏邦盛生物科技有限责任公司 | A kind of Pesticidal combination and its application containing cartap and imidacloprid |
| CN107836460B (en) * | 2017-11-22 | 2021-04-13 | 江苏邦盛生物科技有限责任公司 | Insecticidal composition containing cartap and imidacloprid and application thereof |
| CN108184846A (en) * | 2018-01-18 | 2018-06-22 | 四川龙蟒福生科技有限责任公司 | A kind of gibberellic acid missible oil and preparation method thereof |
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| Publication number | Publication date |
|---|---|
| CN1197457C (en) | 2005-04-20 |
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Assignee: Jiangsu Lvdun Plant Protection Pesticide Experiment Co., Ltd. Assignor: Zhenjiang Agricultural Science Academy Contract fulfillment period: 2008.10.6 to 2018.10.5 contract change Contract record no.: 2008320001133 Denomination of invention: Insecticide producing method by cartap pesticide devil liquor and its products and use method Granted publication date: 20050420 License type: Exclusive license Record date: 20081212 |
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Free format text: EXCLUSIVE LICENSE; TIME LIMIT OF IMPLEMENTING CONTACT: 2008.10.6 TO 2018.10.5; CHANGE OF CONTRACT Name of requester: JIANGSU PROVINCE LVDUNZHIBAO AGRICULTURE CHEMICAL Effective date: 20081212 |
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| C19 | Lapse of patent right due to non-payment of the annual fee | ||
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