CN1425692A - Process for extracting lichee polysaccharide - Google Patents
Process for extracting lichee polysaccharide Download PDFInfo
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- CN1425692A CN1425692A CN 03100544 CN03100544A CN1425692A CN 1425692 A CN1425692 A CN 1425692A CN 03100544 CN03100544 CN 03100544 CN 03100544 A CN03100544 A CN 03100544A CN 1425692 A CN1425692 A CN 1425692A
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- extraction process
- lichee
- enzymolysis
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- polysaccharide
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Abstract
The extraction process of lichee polysaccharide includes the steps of material selection, beating pulp, enzymolysis, filtering to eliminate dregs, seasoning, canning, disinfection, inspection, labeling and packing. Lichee pulp contains rich polysaccharide, protein, vitamins, trace elements and other nutritious components. Lichee has the health functions of invigorating spleen, benefiting liver, promoting the secretion of saliva to relieve thirst, nourishing heart, lowering blood sugar, etc. The present invention utilizes pectase in enzymolysis to make slurry easy to filter and has high activity of the effective component, high yield and high efficiency.
Description
Technical field
The present invention relates to a kind of extraction process of polyose, specifically a kind of extraction process of lichee polysaccharide.
Background technology
Lichee is the distinctive precious fruit of southern china, belongs to the sapindaceous plant fruit, contains abundant polysaccharide, protein, vitamins B, C, calcium, phosphorus, iron microelement in the pulp, reaches the La one methyne ring third stem glycine, organic acid, pectin etc.Traditional Chinese medicine thinks that lichee has very big health care, food therapy value, its warm in nature, sweet acid of distinguishing the flavor of, and tonifying spleen benefit liver promotes the production of body fluid to quench thirst, and nourishes the beneficial heart, and the replenishing essence marrow is enriched blood, raise immunity, lowering blood glucose, subduing swelling and detoxicating, regulating QI to relieve pain; Cure mainly and insufficiency of the spleenly rush down for a long time, stomach cold stomachache, forgetful insomnia, women's weakness, anaemia uterine bleeding and postpartum hemorrhage, tuberculous lymphadenitis etc., lichee has so many benefit, but be confined to ediblely to do, the untapped original taste of fresh litchi pulp.
Rolled up on the 2nd phase " foodstuffs industry science and technology " " development of full lichee sports beverages " article that comrades such as Zheng Zongkun deliver at 2002 the 21st; In the article of " litchi pulp nectar technical study " that comrades such as second phase calendar year 2001 " Shanxi foodstuffs industry " plain boiled water treasured deliver, the content of introducing is general general working method, all not mentioned to adding polygalacturonase in lichee, extract the technology report of polyose.
Summary of the invention
The purpose of this invention is to provide a kind of extraction process of adding the lichee polysaccharide of polygalacturonase.
Task of the present invention is achieved in that a kind of extraction process of lichee polysaccharide, it is characterized in that comprising selecting materials, and making beating, enzymolysis, filter and remove residue, batching, seasoning, tinning, sterilization, cooling, processed finished products is up to the standards, decals, packing encapsulation warehouse-in.Concrete processing step divides following program:
1), select materials: select pollution-free, mildew goes bad, the fresh lichee of damaging by worms, shell, stoning collects pulp;
2), making beating: will weigh up the litchi pulp of certainweight, and be made into magma with hollander;
3) enzymolysis: in magma, add 1.5～3 times 38～48 ℃ hot water by weight; Add 0.2～0.6% polygalacturonase by weight percentage, enzymolysis 30～45 minutes obtains enzymolysis solution;
4), filter and remove residue: enzymolysis solution is inserted in 3000 rev/mins of frame whizzers, and filter and remove residue obtains transition liquid;
5), batching, seasoning: as required by weight percentage,, stir with adding an amount of 0.2～0.8% batching seasonings in the transition liquid;
6), tinning: adapted as required, carry out tinning with large, medium and small different components;
7), sterilization: the tinning finished product is placed in the normal pressure sterilization equipment, carries out disinfection and sterilize about half an hour;
8), cooling, inspection after construction, qualified, decals, vanning warehouse-in are waited to deliver.
Making beating described in the present invention is made becomes the following fineness magma of 100 orders.
Used water is pure water or distilled water or mineral water or deionized water among the present invention.
The alleged per-cent of the present invention occupies add-on, is the weight unit based on gross weight.
Batching described in the present invention, seasoning can add 0.1～0.3% citric acid by weight percentage; 0.1～0.5% sweetener.
In the extraction process step, inspect operation in the middle of being added with in batches by random samples.
Used raw material, work in-process are to buy from the market among the present invention, and polygalacturonase is that BR, the trade mark are that the imported product effect of Fluka is preferable to adopt specification.Equipment used is that Shanghai Medical Apparatus and Instruments Factory produces.The present invention is with the lichee slurries, allocates into and is made into health care, dietotherapy product in food or the drink.
The present invention compares advantage with existing technology; In its extraction process, adopt the enzymolysis process technology, and time, temperature and the enzyme dosage of enzymolysis are provided,, make the lichee slurries except that the characteristics that kept original GOOD TASTE, magma is filtered easily to have ensured the success of enzymolysis; In addition then be the effective ingredient activity that has improved its functional foodstuff, drink, thereby obtain the effect that improves its effect to greatest extent, make food, the drink to incorporate in people's life.
Executing example below by part comes the present invention is further described.
Example 1. is extracted lichee polysaccharide by following processing step.
1), select materials: with free of contamination fresh lichee shell, stoning becomes the pulp raw material.
2), making beating: weigh up certainweight pulp raw material is made the slurries of 80 order left and right sides fineness with hollander magma;
3), enzymolysis: with about 48 ℃ hot water of 3 times of magma addings; Add 0.2～0.6% polygalacturonase, enzymolysis 40 minutes obtains enzymolysis solution;
4), filter and remove residue: enzymolysis solution got rid of with 3000 rev/mins of frame whizzers take off filtration, remove slag after, obtain transition liquid;
5), batching, seasoning: transition liquid is added 0.25～0.3% left and right sides citric acid by weight percentage, and 0.35～0.45% left and right sides sweetener stirs;
6), tinning: adapted on demand, carry out tinning with large, medium and small different components;
7), sterilization: the tinning finished product is placed in the normal pressure sterilization equipment, carries out disinfection and sterilize about half an hour;
8), cooling, inspection after construction, qualified, decals, vanning warehouse-in are waited to deliver.
Example 2 is extracted lichee polysaccharide liquid by following processing step
1), select materials: with free of contamination fresh lichee shell, stoning becomes the pulp raw material;
2), making beating: weigh up certainweight pulp raw material is made the slurries of 70 order left and right sides fineness with hollander magma;
3), enzymolysis: with 43 ℃ of left and right sides hot water of 2 times of magma addings, adding 0.2～0.6% polygalacturonase, enzymolysis obtained enzymolysis solution about 35 minutes;
4), filter and remove residue: enzymolysis solution got rid of with 3000 rev/mins of frame whizzers take off filtration, the back of removing slag, obtain transition liquid;
5), batching, seasoning: transition liquid is added citric acid about 0.1～0.15% by weight percentage, and about 0.1～0.2% sweetener stirs;
6), tinning: adapted on demand, carry out tinning with large, medium and small different components;
7), sterilization: the tinning finished product is placed in the normal pressure sterilization equipment, carries out disinfection and sterilize about half an hour;
8), cooling, inspection after construction, qualified, decals, vanning warehouse-in are waited to deliver.
Example 3 is extracted lichee polysaccharide liquid by following processing step
1), select materials: with free of contamination fresh lichee shell, stoning becomes the pulp raw material.
2), making beating: weigh up certainweight pulp raw material is made the slurries of 60 order left and right sides fineness with hollander magma;
3), enzymolysis: with 38 ℃ of hot water of 1.5 times of magma addings; Add 0.2～0.6% polygalacturonase, enzymolysis obtained enzymolysis solution about 30 minutes;
4), filter and remove residue: enzymolysis solution got rid of with 3000 rev/mins of frame whizzers take off filtration, remove slag after, obtain transition liquid;
5), batching, seasoning: transition liquid is added 0.2～0.25% left and right sides citric acid by weight percentage, and about 0.25～0.3% sweetener stirs;
6), tinning: on demand adapted, carry out tinning with large, medium and small different components;
7), sterilization: the tinning finished product is placed in the normal pressure sterilization equipment, carries out disinfection and sterilize about half an hour;
8), cooling, inspection after construction, qualified, decals, vanning warehouse-in are waited to deliver.
Claims (5)
1, a kind of extraction process of lichee polysaccharide is characterized in that comprising and selects materials, making beating, and enzymolysis, filter and remove residue, batching, seasoning, tinning, sterilization, cooling, inspection after construction, qualified, decals, vanning warehouse-in are waited to deliver; Concrete processing step divides following program:
1), selects materials: select fresh lichee, shell, stoning collects pulp;
2), making beating: will weigh up the litchi pulp of certainweight, and be made into magma with hollander;
3) enzymolysis: in magma, add 1.5～3 times 38～48 ℃ hot water by weight; Add 0.2～0.6% polygalacturonase by weight percentage, enzymolysis 30～45 minutes obtains enzymolysis solution;
4), filter and remove residue: enzymolysis solution is inserted filter and remove residue in 3000 rev/mins of frame whizzers, obtain transition liquid;
5), batching, seasoning: as required by weight percentage, batching, seasonings with adding 0.2～0.8% in the transition liquid stir;
6), tinning: adapted on demand, carry out tinning with large, medium and small different components;
7), sterilization: the tinning finished product is placed in the normal pressure sterilization equipment, and the sterilization that carries out disinfection reached about half an hour;
8), cooling, inspection after construction, qualified, decals, vanning warehouse-in are waited to deliver;
2, according to the extraction process of claims 1 described lichee polysaccharide, it is characterized in that: the making beating described in the invention is made into, is the following fineness magma of 100 orders;
3, according to the extraction process of claims 1 described lichee polysaccharide, it is characterized in that: the batching described in the extraction process, seasoning can add 0.1～0.3% citric acid by weight percentage; 0.1～0.5% sweetener;
4, according to the extraction process of claims 1 described lichee polysaccharide, it is characterized in that: used water is pure water or distilled water or mineral water or deionized water;
5, according to the extraction process of claims 1 described lichee polysaccharide, it is characterized in that in the extraction process step, inspect operation in the middle of being added with in batches by random samples.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 03100544 CN1228347C (en) | 2003-01-16 | 2003-01-16 | Process for extracting lichee polysaccharide |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 03100544 CN1228347C (en) | 2003-01-16 | 2003-01-16 | Process for extracting lichee polysaccharide |
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| Publication Number | Publication Date |
|---|---|
| CN1425692A true CN1425692A (en) | 2003-06-25 |
| CN1228347C CN1228347C (en) | 2005-11-23 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 03100544 Expired - Fee Related CN1228347C (en) | 2003-01-16 | 2003-01-16 | Process for extracting lichee polysaccharide |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1300324C (en) * | 2003-12-12 | 2007-02-14 | 长春工业大学 | Method for extraction and purification of polysaccharide from pilose antler |
| CN1305403C (en) * | 2004-12-16 | 2007-03-21 | 广东省农业科学院农业生物技术研究所 | Preparation method of lichee oral liquid containing intelligence beneficial component |
| CN100543039C (en) * | 2006-04-14 | 2009-09-23 | 中国科学院过程工程研究所 | A kind of longan, the ultrasound-enhanced extraction of lichee polysaccharide and purification process thereof |
| CN100567956C (en) * | 2005-11-30 | 2009-12-09 | 广东省农业科学院农业生物技术研究所 | A kind of lichee polysaccharide Determination on content method |
| CN104292354A (en) * | 2014-11-11 | 2015-01-21 | 济南凯因生物科技有限公司 | Extraction method of litchi polysaccharide |
-
2003
- 2003-01-16 CN CN 03100544 patent/CN1228347C/en not_active Expired - Fee Related
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1300324C (en) * | 2003-12-12 | 2007-02-14 | 长春工业大学 | Method for extraction and purification of polysaccharide from pilose antler |
| CN1305403C (en) * | 2004-12-16 | 2007-03-21 | 广东省农业科学院农业生物技术研究所 | Preparation method of lichee oral liquid containing intelligence beneficial component |
| CN100567956C (en) * | 2005-11-30 | 2009-12-09 | 广东省农业科学院农业生物技术研究所 | A kind of lichee polysaccharide Determination on content method |
| CN100543039C (en) * | 2006-04-14 | 2009-09-23 | 中国科学院过程工程研究所 | A kind of longan, the ultrasound-enhanced extraction of lichee polysaccharide and purification process thereof |
| CN104292354A (en) * | 2014-11-11 | 2015-01-21 | 济南凯因生物科技有限公司 | Extraction method of litchi polysaccharide |
Also Published As
| Publication number | Publication date |
|---|---|
| CN1228347C (en) | 2005-11-23 |
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Granted publication date: 20051123 Termination date: 20120116 |