CN1390920A - Male tussah chrysalis oil and its preparing process - Google Patents
Male tussah chrysalis oil and its preparing process Download PDFInfo
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- CN1390920A CN1390920A CN 01114061 CN01114061A CN1390920A CN 1390920 A CN1390920 A CN 1390920A CN 01114061 CN01114061 CN 01114061 CN 01114061 A CN01114061 A CN 01114061A CN 1390920 A CN1390920 A CN 1390920A
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Abstract
A male tussach moth oil is prepared from male tussach moth through removing wings, drying at 30-60 deg.C until its water content is 8-13%, pulverizing by 20-60 meshes, and supercritical CO2 extracting. Its advantages are rich active substances and no content of solvent.
Description
The present invention relates to a kind of male tussah chrysalis oil and method for making thereof.
The tussah male silkworm moth (hereinafter to be referred as male Bombycis mori) of not mating as yet eat in state-owned long history, be considered as a kind of tonic of preciousness period by imperial family as far back as Tang, Song.Modern scientific research shows, cytochrome C, vitamin B12, nicotinic acid, α-ecdyson, β-ecdyson, male hormone, brain hormones, neotonin, class sexual hormoue (cover ketone, estradiol), prostaglandin(PG) or the like multiple biologically active substance is arranged in the male Bombycis mori body, the biological effect of these biologically active substances is very big, has fabulous invigorating the liver and kidney, establishing-Yang and anti-aging effects.Utilize the intravital biologically active substance of male Bombycis mori to can be made into plurality kinds of health care food or medicine,, need the intravital biologically active substance of male Bombycis mori is extracted for making things convenient for pharmacy.In the prior art, useful wine extracts as the method for solvent soaking, after the extraction of steeping in wine bubble, the intravital biologically active substance of male Bombycis mori is dissolved in the solvent liquor, be difficult to and separated from solvent, limited the application of the intravital biologically active substance of male Bombycis mori in the deep processing of preparation plurality kinds of health care food or medicine after extracting.
The objective of the invention is in order to overcome above-mentioned deficiency, propose a kind of male tussah chrysalis oil and method for making thereof that the intravital biologically active substance of male Bombycis mori is extracted and separates.
The present invention is achieved using the following method.
Product male tussah chrysalis oil of the present invention is the light yellow oil matter that is rich in biologically active substance for preparing with following method,
1, male Bombycis mori is removed wing, become the male Bombycis mori body;
2, the male Bombycis mori body is dried to the dried male Bombycis mori body of water content 8～13% under 30～60 ℃ of temperature;
3, dried male Bombycis mori body is ground into 20～60 purpose male Bombycis mori powder;
4, the male Bombycis mori powder is extracted with the carbon dioxide upercritical fluid extraction method, obtain being rich in the light yellow oil matter of biologically active substance, the carbon dioxide upercritical fluid extraction extraction conditions is: extracting pressure: 15～30MPa, extraction temperature: 31～45 ℃, extraction entrainment agent: edible ethanol, the ratio of carbonic acid gas weight rate and entrainment agent weight rate: 20～50: 1, flash trapping stage pressure 8～12Mpa, 30～40 ℃ of flash trapping stage temperature, secondary separating pressure 5～6MPa, 35～45 ℃ of secondary separation temperatures.
The method for making of product male tussah chrysalis oil of the present invention is:
1, male Bombycis mori is removed wing, become the male Bombycis mori body;
2, the male Bombycis mori body is dried to the dried male Bombycis mori body of water content 8～13% under 30～60 ℃ of temperature;
3, dried male Bombycis mori body is ground into 20～60 purpose male Bombycis mori powder;
4, the male Bombycis mori powder is extracted with the carbon dioxide upercritical fluid extraction method, obtain being rich in biologically active substance light yellow oil matter, the carbon dioxide upercritical fluid extraction extraction conditions is: extracting pressure: 15～30MPa, extraction temperature: 31～45 ℃, extraction entrainment agent: edible ethanol, the ratio of carbonic acid gas weight rate and entrainment agent weight rate: 20～50: 1, flash trapping stage pressure 8～12MPa, 30～40 ℃ of flash trapping stage temperature, secondary separating pressure 5～6MPa, 35～45 ℃ of secondary separation temperatures.
Product of the present invention is to extract from the male tussah chrysalis body and the isolated biologically active substance light yellow oil matter that is rich in the method for carbon dioxide upercritical fluid extraction, do not contain solvent in the product that extracts, when being used for deep processing and pharmacy and nutritive food, easily.
Below in conjunction with embodiment, the present invention is further illustrated.
Embodiment 1
Product male tussah chrysalis oil of the present invention is the light yellow oil matter that is rich in biologically active substance for preparing with following method,
1, male Bombycis mori is removed wing, become the male Bombycis mori body;
2, the male Bombycis mori body is dried to the dried male Bombycis mori body of water content 8～13% under 50 ℃ of temperature;
3, dried male Bombycis mori body is ground into 30 purpose male Bombycis mori powder;
4, the male Bombycis mori powder is extracted with the carbon dioxide upercritical fluid extraction method, obtain being rich in the light yellow oil matter of biologically active substance, the carbon dioxide upercritical fluid extraction extraction conditions is: extracting pressure: 25MPa, extraction temperature: 37 ℃, extraction entrainment agent: edible ethanol, the ratio of carbonic acid gas weight rate and entrainment agent weight rate: 25: 1, flash trapping stage pressure 10MPa, 35 ℃ of flash trapping stage temperature, secondary separating pressure 5MPa, 40 ℃ of secondary separation temperatures.
The carbon dioxide upercritical fluid extraction extraction conditions also can be: extracting pressure: 22MPa, extraction temperature: 33 ℃, extraction entrainment agent: edible ethanol, the ratio of carbonic acid gas weight rate and entrainment agent weight rate: 30: 1, flash trapping stage pressure 9MPa, 33 ℃ of flash trapping stage temperature, secondary separating pressure 5MPa, 37 ℃ of secondary separation temperatures.
The carbon dioxide upercritical fluid extraction extraction conditions also can be: extracting pressure: 27MPa, extraction temperature: 40 ℃, extraction entrainment agent: edible ethanol, the ratio of carbonic acid gas weight rate and entrainment agent weight rate: 40: 1, flash trapping stage pressure 11MPa, 37 ℃ of flash trapping stage temperature, secondary separating pressure 6MPa, 43 ℃ of secondary separation temperatures.
The carbon dioxide upercritical fluid extraction extraction conditions also can be: extracting pressure: 29MPa, extraction temperature: 42 ℃, extraction entrainment agent: edible ethanol, the ratio of carbonic acid gas weight rate and entrainment agent weight rate: 45: 1, flash trapping stage pressure 10MPa, 38 ℃ of flash trapping stage temperature, secondary separating pressure 6MPa, 44 ℃ of secondary separation temperatures.
Embodiment 2
The method for making of product male tussah chrysalis oil of the present invention is:
1, male Bombycis mori is removed wing, become the male Bombycis mori body;
2, the male Bombycis mori body is dried to the dried male Bombycis mori body of water content 8～13% under 50 ℃ of temperature;
3, dried male Bombycis mori body is ground into 30 purpose male Bombycis mori powder;
4, the male Bombycis mori powder is extracted with the carbon dioxide upercritical fluid extraction method, obtain being rich in the light yellow oil matter of biologically active substance, the carbon dioxide upercritical fluid extraction extraction conditions is: extracting pressure: 25MPa, extraction temperature: 37 ℃, extraction entrainment agent: edible ethanol, the ratio of carbonic acid gas weight rate and entrainment agent weight rate: 25: 1, flash trapping stage pressure 10MPa, 35 ℃ of flash trapping stage temperature, secondary separating pressure 5MPa, 40 ℃ of secondary separation temperatures.
The carbon dioxide upercritical fluid extraction extraction conditions also can be: extracting pressure: 22MPa, extraction temperature: 33 ℃, extraction entrainment agent: edible ethanol, the ratio of carbonic acid gas weight rate and entrainment agent weight rate: 30: 1, flash trapping stage pressure 9MPa, 33 ℃ of flash trapping stage temperature, secondary separating pressure 5MPa, 37 ℃ of secondary separation temperatures.
The carbon dioxide upercritical fluid extraction extraction conditions also can be: extracting pressure: 27MPa, extraction temperature: 40 ℃, extraction entrainment agent: edible ethanol, the ratio of carbonic acid gas weight rate and entrainment agent weight rate: 40: 1, flash trapping stage pressure 11MPa, 37 ℃ of flash trapping stage temperature, secondary separating pressure 6MPa, 43 ℃ of secondary separation temperatures.
The carbon dioxide upercritical fluid extraction extraction conditions also can be: extracting pressure: 29MPa, extraction temperature: 42 ℃, extraction entrainment agent: edible ethanol, the ratio of carbonic acid gas weight rate and entrainment agent weight rate: 45: 1, flash trapping stage pressure 10MPa, 38 ℃ of flash trapping stage temperature, secondary separating pressure 6MPa, 44 ℃ of secondary separation temperatures.
Claims (8)
1. male tussah chrysalis oil is characterized in that: be the light yellow oil matter that is rich in biologically active substance for preparing with following method,
(1) as yet not the tussah male silkworm moth of mating remove wing, become the male Bombycis mori body;
(2) the male Bombycis mori body is dried to the dried male Bombycis mori body of water content 8～13% under 30～60 ℃ of temperature;
(3) dried male Bombycis mori body is ground into 20～60 purpose male Bombycis mori powder;
(4) the male Bombycis mori powder is extracted with the carbon dioxide upercritical fluid extraction method, obtain being rich in the light yellow oil matter of biologically active substance, the carbon dioxide upercritical fluid extraction extraction conditions is: extracting pressure: 15～30MPa, extraction temperature: 31～45 ℃, extraction entrainment agent: edible ethanol, the ratio of carbonic acid gas weight rate and entrainment agent weight rate: 20～50: 1, flash trapping stage pressure 8～12MPa, 30～40 ℃ of flash trapping stage temperature, secondary separating pressure 5～6MPa, 35～45 ℃ of secondary separation temperatures.
2. by the described male tussah chrysalis oil of claim 1, it is characterized in that: described carbon dioxide upercritical fluid extraction extraction conditions is: extracting pressure: 22MPa, extraction temperature: 33 ℃, the ratio of carbonic acid gas weight rate and entrainment agent weight rate: 30: 1, flash trapping stage pressure 9MPa, 33 ℃ of flash trapping stage temperature, secondary separating pressure 5MPa, 37 ℃ of secondary separation temperatures.
3. by the described male tussah chrysalis oil of claim 1, it is characterized in that: described carbon dioxide upercritical fluid extraction extraction conditions is: extracting pressure: 27MPa, extraction temperature: 40 ℃, the ratio of carbonic acid gas weight rate and entrainment agent weight rate: 40: 1, flash trapping stage pressure 11MPa, 37 ℃ of flash trapping stage temperature, secondary separating pressure 6MPa, 43 ℃ of secondary separation temperatures.
4. by the described male tussah chrysalis oil of claim 1, it is characterized in that: described carbon dioxide upercritical fluid extraction extraction conditions is: extracting pressure: 29MPa, extraction temperature: 42 ℃, the ratio of carbonic acid gas weight rate and entrainment agent weight rate: 45: 1, flash trapping stage pressure 10MPa, 38 ℃ of flash trapping stage temperature, secondary separating pressure 6MPa, 44 ℃ of secondary separation temperatures.
5. the method for making of a male tussah chrysalis oil is characterized in that:
(1) as yet not the tussah male silkworm moth of mating remove wing, become the male Bombycis mori body;
(2) the male Bombycis mori body is dried to the dried male Bombycis mori body of water content 8～13% under 30～60 ℃ of temperature;
(3) dried male Bombycis mori body is ground into 20～60 purpose male Bombycis mori powder;
(4) the male Bombycis mori powder is extracted with the carbon dioxide upercritical fluid extraction method, obtain being rich in the light yellow oil matter of biologically active substance, the carbon dioxide upercritical fluid extraction extraction conditions is: extracting pressure: 15～30MPa, extraction temperature: 31～45 ℃, extraction entrainment agent: edible ethanol, the ratio of carbonic acid gas weight rate and entrainment agent weight rate: 20～50: 1, flash trapping stage pressure 8～12MPa, 30～40 ℃ of flash trapping stage temperature, secondary separating pressure 5～6MPa, 35～45 ℃ of secondary separation temperatures.
6. press the method for making of the described male tussah chrysalis oil of claim 5, it is characterized in that: described carbon dioxide upercritical fluid extraction extraction conditions is: extracting pressure: 22MPa, extraction temperature: 33 ℃, the ratio of carbonic acid gas weight rate and entrainment agent weight rate: 30: 1, flash trapping stage pressure 9MPa, 33 ℃ of flash trapping stage temperature, secondary separating pressure 5MPa, 37 ℃ of secondary separation temperatures.
7. press the method for making of the described male tussah chrysalis oil of claim 5, it is characterized in that: described carbon dioxide upercritical fluid extraction extraction conditions is: extracting pressure: 27MPa, extraction temperature: 40 ℃, the ratio of carbonic acid gas weight rate and entrainment agent weight rate: 40: 1, flash trapping stage pressure 11MPa, 37 ℃ of flash trapping stage temperature, secondary separating pressure 6MPa, 43 ℃ of secondary separation temperatures.
8. press the method for making of the described male tussah chrysalis oil of claim 5, it is characterized in that: described carbon dioxide upercritical fluid extraction extraction conditions is: extracting pressure: 29MPa, extraction temperature: 42 ℃, the ratio of carbonic acid gas weight rate and entrainment agent weight rate: 45: 1, flash trapping stage pressure 10MPa, 38 ℃ of flash trapping stage temperature, secondary separating pressure 6MPa, 44 ℃ of secondary separation temperatures.
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| Application Number | Priority Date | Filing Date | Title |
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| CN 01114061 CN1132923C (en) | 2001-06-13 | 2001-06-13 | Male tussah chrysalis oil and its preparing process |
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| CN 01114061 CN1132923C (en) | 2001-06-13 | 2001-06-13 | Male tussah chrysalis oil and its preparing process |
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Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1304543C (en) * | 2004-02-04 | 2007-03-14 | 徐华 | Natural silkworm, silkworm pupa protein oil preparation process |
| JP2008528579A (en) * | 2005-01-31 | 2008-07-31 | ドン ファ ファーム インダストリー カンパニー リミテッド | Pharmaceutical composition for the treatment of renal disorders and health foods containing herbal extracts |
| CN101967425A (en) * | 2010-10-15 | 2011-02-09 | 王朝臣 | Process and system for preparing oak silkworm male moth oil by ultrasound-enhanced super-critical carbon dioxide (CO2) extraction |
| CN101530432B (en) * | 2009-04-10 | 2011-04-27 | 山东省蚕业研究所 | Method for producing degreased concentrated solution of tussah male moth |
| CN102362620A (en) * | 2011-10-24 | 2012-02-29 | 天津渤海职业技术学院 | Antheraea pernyi oil microencapsulation preparation process |
| CN101117612B (en) * | 2006-08-01 | 2012-06-20 | 西安市轻工业研究所 | Edible insect oil and production method and use thereof |
| CN101744838B (en) * | 2008-12-22 | 2012-09-12 | 吉林农业大学 | Method for preparing tussah moth oil |
| CN104434990A (en) * | 2014-11-17 | 2015-03-25 | 江西省蚕桑茶叶研究所 | Male silkworm moth oil micro-emulsion |
| CN108124964A (en) * | 2017-12-11 | 2018-06-08 | 长春三真实业有限公司 | A kind of establishing-Yang male silk moth milk tablet |
-
2001
- 2001-06-13 CN CN 01114061 patent/CN1132923C/en not_active Expired - Fee Related
Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1304543C (en) * | 2004-02-04 | 2007-03-14 | 徐华 | Natural silkworm, silkworm pupa protein oil preparation process |
| JP2008528579A (en) * | 2005-01-31 | 2008-07-31 | ドン ファ ファーム インダストリー カンパニー リミテッド | Pharmaceutical composition for the treatment of renal disorders and health foods containing herbal extracts |
| CN101117612B (en) * | 2006-08-01 | 2012-06-20 | 西安市轻工业研究所 | Edible insect oil and production method and use thereof |
| CN101744838B (en) * | 2008-12-22 | 2012-09-12 | 吉林农业大学 | Method for preparing tussah moth oil |
| CN101530432B (en) * | 2009-04-10 | 2011-04-27 | 山东省蚕业研究所 | Method for producing degreased concentrated solution of tussah male moth |
| CN101967425A (en) * | 2010-10-15 | 2011-02-09 | 王朝臣 | Process and system for preparing oak silkworm male moth oil by ultrasound-enhanced super-critical carbon dioxide (CO2) extraction |
| CN102362620A (en) * | 2011-10-24 | 2012-02-29 | 天津渤海职业技术学院 | Antheraea pernyi oil microencapsulation preparation process |
| CN104434990A (en) * | 2014-11-17 | 2015-03-25 | 江西省蚕桑茶叶研究所 | Male silkworm moth oil micro-emulsion |
| CN108124964A (en) * | 2017-12-11 | 2018-06-08 | 长春三真实业有限公司 | A kind of establishing-Yang male silk moth milk tablet |
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|---|---|
| CN1132923C (en) | 2003-12-31 |
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