CN1290730A - Process for preparing pepper oil resin - Google Patents
Process for preparing pepper oil resin Download PDFInfo
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- CN1290730A CN1290730A CN 00130396 CN00130396A CN1290730A CN 1290730 A CN1290730 A CN 1290730A CN 00130396 CN00130396 CN 00130396 CN 00130396 A CN00130396 A CN 00130396A CN 1290730 A CN1290730 A CN 1290730A
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- oil resin
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Abstract
Paper after beign crushed in extracted with two or more organic solvents and is obtained a brown liquid product after the chemical solvents are separated through distillation. The pepper oil resin contains certain amount of piperinee, pepper oil and other concentrated chemical components. It is used as fragrant and pungent additive for wine and seasoning, nutritious additive for functional beverage, natural preservative for instant noodles and meat product, etc.
Description
The present invention relates to a kind of thing pepper oleoresin extracting method or technology.
Pepper oleoresin be by pepper through pulverizing, use the organic solvent lixiviate again, isolate the product that obtains after the organic solvent then.Pepper oleoresin has concentrated piperic nutrition and medicinal component, gives off a strong fragrance, and is keeping the distinctive fragrance of pepper, local flavor and pungent, is widely used in drink (food) product processing industry, can be used as the spice additive of drink (food) product, fresh-keeping and sanitas.Can be antibacterial, improve food fragrance, short gastrointestinal peristalsis, accelerate blood circulation.Be a kind of important food, meat additive, as allotment spices as sausage, can food, soup, sauce, beverage and ardent spirits etc.Also be specially adapted to modulate the spices of oriental odor flavor.Country's being in great demand such as Japan, France, Eastern Europe and Latin America to the pepper oleoresin product.Middle-size and small-size food processing plant is to using the pepper resin also interested gradually.
Traditional pepper oleoresin extraction process is the single solvents that use in leaching process more, and leaching yield is lower, and need repeat many times, and this process operation is more numerous and diverse.
The object of the present invention is to provide a kind of pepper oleoresin extracting method thing, this method can improve the extraction yield and the separating effect of pepper oleoresin, reduce and extract pepper oleoresin extraction cost (ratio for input and output is about 2: 1), and gained pepper oleoresin quality better.
The objective of the invention is to adopt following method and step to realize: the black/white pepper dry fruit of learning from else's experience selected is ground into the pepper powder of certain particle size with it; Get the pepper powder of pulverizing, add two or more mixed organic solvents, after the mechanical stirring, solid powder is separated with liquid mixture; With distilling in resulting all vat liquors (liquid mixture) adding still kettle, isolate organic solvent wherein; Steam after the organic solvent, the gained enriched material is the pepper oleoresin that contains the higher proportion piperine.
The present invention compared with prior art, it is simple to have technology, the pepper oleoresin extraction rate obviously is improved, and has reduced pepper oleoresin lixiviate cost (ratio for input and output is about 2: 1), and gained pepper oleoresin quality better.
Below in detail most preferred embodiment of the present invention is described.
1, piperic is pulverized.The black/white pepper dry fruit of learning from else's experience selected is ground into certain particle size (＜2mm) pepper powder.
2, the organic solvent lixiviate of pepper powder.Get the pepper powder of pulverizing, add two or more blended organic solvent (ratio of organic solvent and pepper powder is 1: 1～6: 1), under 25 ℃～40 ℃ temperature, under intermittence or continuously stirring effect, through certain hour (t=1～6 hour) afterwards, solid powder (impurity in the pepper) is separated with liquid mixture, separation method can be following method two or more combine: press filtration, suction filtration, membrane filtration and chromatographic separation.Again repeatedly (greater than 2 times) repeat above step, the oleo-resinous that contains in pepper extracts and to finish.
3, the distillation of vat liquor.With distilling in above-mentioned resulting all vat liquors adding still kettles, isolate organic solvent wherein.This process can be air distillation, or underpressure distillation, or the rectifying of multistage column plate.Steam after the organic solvent, the spissated product of gained is pepper oleoresin.
Embodiment 1
Getting 100Kg Qionghai white pepper and being ground into particle diameter is 80 purpose pepper powders, add 300Kg with ethanol and acetone in 1: 1 ratio then and carry out lixiviate, stirred 5 minutes in per 30 minutes, adopted membrane filtration to carry out separating of solid powder and liquid phase later in 2 hours in conjunction with suction filtration.Repeat lixiviate and separating process 4 times.Air distillation is carried out in all vat liquors merging, after steaming organic solvent fully, can be obtained more than the enriched material pepper oleoresin 10Kg.
Embodiment 2
Getting 100Kg Qionghai piper nigrum and being ground into particle diameter is 60 purpose pepper powders, add 200Kg with ethanol and ethyl acetate in 2: 1 ratio then and carry out lixiviate, continuously stirring in the leaching process adopted membrane filtration to carry out separating of solid powder and liquid phase in conjunction with suction filtration later in 1 hour.Repeat lixiviate and separating process 4 times.Underpressure distillation is carried out in all vat liquors merging, after steaming organic solvent fully, can be obtained more than the enriched material pepper oleoresin 15Kg.
Pepper oleoresin extract that the present invention is made and edible oil by 8%～10% mixed after, make flavouring hot pepper oil.This flavouring hot pepper oil has the unique former fragrance of pepper, local flavor and pungent, can be directly edible as seasonings.Also can be used as cooking sauce.With the pepper oleoresin that the present invention makes, the ratio with 3%～5% can reach fresh-keeping and the rot-resistant effect as natural fresh-keeping, the sanitas of meat product, has also increased the local flavor of meat product simultaneously.The pepper oleoresin that the present invention makes can add in the drinks goods in 1% ratio, can be made into the pepper wine of other tool local flavor.This pepper wine has health care, resisting cold, functions such as wind-damp dispelling.
Annotate: the above ratio all is weight percentage.
Claims (7)
1. process for preparing pepper oil resin, this method may further comprise the steps successively: the black/white pepper dry fruit of learning from else's experience selected is ground into the pepper powder of certain particle size with it; Get the pepper powder of pulverizing, add two or more mixed organic solvents, after the mechanical stirring, solid powder is separated with liquid mixture; With distilling in resulting all vat liquors (liquid mixture) adding still kettle, isolate organic solvent wherein; Steam after the organic solvent, the gained enriched material is the pepper oleoresin that contains the higher proportion piperine.
2. process for preparing pepper oil resin according to claim 1 is characterized in that said ground pepper particle diameter less than 2mm, and pepper can be piper nigrum or white pepper.
3. process for preparing pepper oil resin according to claim 1, the ratio that it is characterized in that described mixed organic solvents and pepper powder is 1: 1～6: 1.
4. process for preparing pepper oil resin according to claim 1 is characterized in that organic solvent with after the pepper powder mixes, under 25 ℃～40 ℃ temperature, intermittently or continuously stirring 1～6 hour.
5. process for preparing pepper oil resin according to claim 1 is characterized in that it can be combining of following two or more method that solid powder and liquid mixture are carried out isolating method: press filtration, suction filtration, membrane filtration and chromatographic separation.
6. process for preparing pepper oil resin according to claim 1 is characterized in that used organic solvent includes ethanol, methyl alcohol, acetone, ether, ethyl acetate, ethylene dichloride, benzene and chloroform.
7. process for preparing pepper oil resin according to claim 1 is characterized in that the mechanical stirring mode can be intermittently or continuously stirring.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN00130396A CN1128194C (en) | 2000-11-03 | 2000-11-03 | Process for preparing pepper oil resin |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN00130396A CN1128194C (en) | 2000-11-03 | 2000-11-03 | Process for preparing pepper oil resin |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1290730A true CN1290730A (en) | 2001-04-11 |
| CN1128194C CN1128194C (en) | 2003-11-19 |
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ID=4594155
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN00130396A Expired - Fee Related CN1128194C (en) | 2000-11-03 | 2000-11-03 | Process for preparing pepper oil resin |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN1128194C (en) |
Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101928463A (en) * | 2010-07-08 | 2010-12-29 | 天津春发食品配料有限公司 | Method for preparing black pepper oil resin |
| CN102260594A (en) * | 2011-08-01 | 2011-11-30 | 晨光生物科技集团股份有限公司 | Method for extracting black pepper essence oil and black pepper essence oil resin from black paper |
| CN102487998A (en) * | 2011-12-13 | 2012-06-13 | 海南师范大学 | Method for refreshing cowpeas by using piperine ethanol-water solution |
| CN102793135A (en) * | 2012-08-07 | 2012-11-28 | 海南尊鳌科技开发有限公司 | Method for extracting pepper oleoresin, product and method for producing product |
| CN102925283A (en) * | 2012-10-23 | 2013-02-13 | 中国热带农业科学院香料饮料研究所 | Preparation method of pepper oleoresin |
| CN101669552B (en) * | 2009-08-24 | 2013-02-20 | 天津春发生物科技集团有限公司 | Seasoning oil containing sesame oil, natural essential oil and oleoresin |
| CN103005008A (en) * | 2013-01-08 | 2013-04-03 | 中国热带农业科学院香料饮料研究所 | Pepper flavored oil and method for preparing same |
| CN103039931A (en) * | 2013-01-08 | 2013-04-17 | 中国热带农业科学院香料饮料研究所 | Pepper oil resin and preparation method thereof |
| CN109875109A (en) * | 2019-01-30 | 2019-06-14 | 湖北中烟工业有限责任公司 | A kind of cigarette preparation method of allspice oil resin and its application in cigarette |
| US20200115663A1 (en) * | 2018-10-16 | 2020-04-16 | Golden Spice Liquors LLC | Beverage compositions and methods of making and using the same |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1069677C (en) * | 1998-12-05 | 2001-08-15 | 海南大学 | Liquidambar extract preparing method |
-
2000
- 2000-11-03 CN CN00130396A patent/CN1128194C/en not_active Expired - Fee Related
Cited By (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101669552B (en) * | 2009-08-24 | 2013-02-20 | 天津春发生物科技集团有限公司 | Seasoning oil containing sesame oil, natural essential oil and oleoresin |
| CN101928463B (en) * | 2010-07-08 | 2012-09-12 | 天津春发生物科技集团有限公司 | Method for preparing black pepper oil resin |
| CN101928463A (en) * | 2010-07-08 | 2010-12-29 | 天津春发食品配料有限公司 | Method for preparing black pepper oil resin |
| CN102260594A (en) * | 2011-08-01 | 2011-11-30 | 晨光生物科技集团股份有限公司 | Method for extracting black pepper essence oil and black pepper essence oil resin from black paper |
| CN102487998A (en) * | 2011-12-13 | 2012-06-13 | 海南师范大学 | Method for refreshing cowpeas by using piperine ethanol-water solution |
| CN102793135A (en) * | 2012-08-07 | 2012-11-28 | 海南尊鳌科技开发有限公司 | Method for extracting pepper oleoresin, product and method for producing product |
| CN102925283A (en) * | 2012-10-23 | 2013-02-13 | 中国热带农业科学院香料饮料研究所 | Preparation method of pepper oleoresin |
| CN102925283B (en) * | 2012-10-23 | 2014-01-22 | 中国热带农业科学院香料饮料研究所 | Preparation method of pepper oleoresin |
| CN103005008A (en) * | 2013-01-08 | 2013-04-03 | 中国热带农业科学院香料饮料研究所 | Pepper flavored oil and method for preparing same |
| CN103039931A (en) * | 2013-01-08 | 2013-04-17 | 中国热带农业科学院香料饮料研究所 | Pepper oil resin and preparation method thereof |
| CN103005008B (en) * | 2013-01-08 | 2014-01-15 | 中国热带农业科学院香料饮料研究所 | Pepper flavored oil and method for preparing same |
| US20200115663A1 (en) * | 2018-10-16 | 2020-04-16 | Golden Spice Liquors LLC | Beverage compositions and methods of making and using the same |
| CN109875109A (en) * | 2019-01-30 | 2019-06-14 | 湖北中烟工业有限责任公司 | A kind of cigarette preparation method of allspice oil resin and its application in cigarette |
Also Published As
| Publication number | Publication date |
|---|---|
| CN1128194C (en) | 2003-11-19 |
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