CN1289658A - Technology for making high-specific-weight alloy parts in different shapes - Google Patents

Technology for making high-specific-weight alloy parts in different shapes Download PDF

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Publication number
CN1289658A
CN1289658A CN 00113684 CN00113684A CN1289658A CN 1289658 A CN1289658 A CN 1289658A CN 00113684 CN00113684 CN 00113684 CN 00113684 A CN00113684 A CN 00113684A CN 1289658 A CN1289658 A CN 1289658A
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China
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temperature
binding agent
under
polyethylene glycol
plasticizer
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CN 00113684
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Chinese (zh)
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CN1119213C (en
Inventor
李益民
李松林
黄伯云
曾舟山
邓忠勇
唐嵘
曲选辉
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YINGJIE HIGH-TECH Co Ltd HUNAN PROV
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YINGJIE HIGH-TECH Co Ltd HUNAN PROV
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Priority to CN 00113684 priority Critical patent/CN1119213C/en
Publication of CN1289658A publication Critical patent/CN1289658A/en
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Publication of CN1119213C publication Critical patent/CN1119213C/en
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Expired - Fee Related legal-status Critical Current

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Abstract

A technology for manufacturing shaped high-specific weight alloy parts includes such steps as mixing W-based powder containing Cu and Ni with binder, injection shaping, degreasing and sintering. Said binder is prepared from polyethene glycol, polyethylene, plasticizer and paraffin through mixing. Its advantages include uniform inner tissue, high density up to 99.5-100%, high mechanical performance and accurate size, high surface finish quality, integral shaping and low cost.

Description

Abnormity high-density alloy machining parts
It is metal powder injection molded to the present invention relates to a kind of usefulness, makes special-shaped high-density alloy machining parts.
The handset vibrator that communication is used, beeper oscillator, deep-sea fishing all is a little special-shaped high specific gravity metal parts with weight etc., requires density even, the dimensional accuracy height.Adopt the technology of powder pressing, produce handset vibrator, because draw ratio is big, density is even everywhere to be not easy to make goods, and it has the step of a 0.2mm simultaneously, needs back processing to obtain.The beeper oscillator has geometrical bodies such as circular arc and through hole, can not once extrude, and also needs following process.And high-density alloy hardness is big, processing difficulties, and the cost height, and be difficult for ensuring the quality of products.
Purpose of the present invention is that a kind of method with powder injection forming will be provided, and produces special-shaped high-density alloy part.
Abnormity high-density alloy machining parts is that the tungsten based powders of cupric 7-1%, nickeliferous 14-2% is mixed with binding agent, is machined to base through injection moulding, degreasing again, sintering.
Introduce the present invention in detail below in conjunction with embodiment.
The preparation of a, binding agent: by weight percentage, taking polyethylene glycol 10-40%, polyethylene 15-40%, plasticizer 1-10%, paraffin 10-74% puts in the vane type batch mixer, mixes hour through 1 under 140-160 ℃ of temperature.
B, batching: the tungsten based powders of binding agent and cupric, nickel, by volume 48-40: 52-60 cooperates, and mixes 1.5 hours under 140 ° of-160 ℃ of temperature in batch mixer.
C, injection moulding: above-mentioned batch mixing is placed in the injection machine, and with 140 °-150 ℃, injection pressure 40-80Mpa under 30 ° of-60 ℃ of conditions of mould temperature, is processed into blank.
D, degreasing: at first blank is put into water and be heated to 40 °-60 ℃, be detained 30 minutes, the polyethylene glycol component in the dissolving binding agent; Then blank is put into debinding furnace, under hydrogen shield, be heated to 260 ℃ with 5 ℃/min speed, the speed with 10 ° of-15 ℃/min is heated to 500 ℃ then.
E, sintering: earlier the degreasing blank is heated to 800 °-900 ℃ and does presintering, place molybdenum wire furnace again, at 1350 °-1400 ℃ of temperature, sintering 90 minutes.
Adhesive preparation of the present invention.
Embodiment 1: taking polyethylene glycol 20%, polyethylene 30%, plasticizer 5%, all the other are paraffin, put in the vane type batch mixer, mix 1 hour under 140 ° of-160 ℃ of temperature.
Embodiment 2: taking polyethylene glycol 10%, polyethylene 15%, plasticizer 1%, all the other are paraffin, put in the vane type batch mixer, mix 1 hour under 140 ° of-160 ℃ of temperature.
Embodiment 3: taking polyethylene glycol 40%, polyethylene 40%, plasticizer 10%, all the other are paraffin, put in the vane type batch mixer, mix 1 hour under 140 ° of-160 ℃ of temperature.
Use the processing profiled high-density alloy part of the present invention, interior tissue is even, and product density can reach 99.5-100%, good mechanical property, and the dimensional accuracy height, surface smoothness is good, and once-forming need not back processing, reduces cost greatly.

Claims (4)

1, a kind of special-shaped high-density alloy machining parts is that the tungsten based powders of cupric 7-1%, nickeliferous 14-2% is mixed with binding agent, is machined to base through injection moulding, and degreasing again, sintering is characterized in that:
The preparation of a, binding agent: by weight percentage, taking polyethylene glycol 10-40%, polyethylene 15-40%, plasticizer 1-10%, paraffin 10-74% puts in the vane type batch mixer, mixes 1 hour under 140 ° of-160 ℃ of temperature;
B, batching: the tungsten based powders of binding agent and cupric, nickel, by volume 48-40: 52-60 cooperates, and mixes 1.5 hours under 140 ° of-160 ℃ of temperature in batch mixer;
C, injection moulding: above-mentioned batch mixing is placed in the injection machine, and with 140 °-150 ℃, injection pressure 40-80Mpa under 30 ° of-60 ℃ of conditions of mould temperature, is processed into blank;
D, degreasing: at first blank is put into water and be heated to 40 °-60 ℃, be detained 30 minutes, the polyethylene glycol component in the dissolving binding agent; Then blank is put into debinding furnace, under hydrogen shield, be heated to 260 ℃ with 5 ℃/min speed, the speed with 10 ° of-15 ℃/min is heated to 500 ℃ then;
E, sintering: earlier the degreasing blank is heated to 800 °-900 ℃ and does presintering, place molybdenum wire furnace again, at 1350 °-1400 ℃ of temperature, sintering 90 minutes.
2, by the described special-shaped high-density alloy machining parts of claim 1, it is characterized in that the preparation of binding agent: taking polyethylene glycol 20%, polyethylene 30%, plasticizer 5%, all the other are paraffin, put in the vane type batch mixer, under 140 ° of-160 ℃ of temperature, mixed 1 hour.
3, by the described special-shaped high-density alloy machining parts of claim 1, it is characterized in that the preparation of binding agent: taking polyethylene glycol 10%, polyethylene 15%, plasticizer 1%, all the other are paraffin, put in the vane type batch mixer, under 140 ° of-160 ℃ of temperature, mixed 1 hour.
4, by the described special-shaped high-density alloy machining parts of claim 1, it is characterized in that the preparation of binding agent: taking polyethylene glycol 40%, polyethylene 40%, plasticizer 10%, all the other are paraffin, put in the vane type batch mixer, under 140 ° of-160 ℃ of temperature, mixed 1 hour.
CN 00113684 2000-09-13 2000-09-13 Technology for making high-specific-weight alloy parts in different shapes Expired - Fee Related CN1119213C (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN 00113684 CN1119213C (en) 2000-09-13 2000-09-13 Technology for making high-specific-weight alloy parts in different shapes

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN 00113684 CN1119213C (en) 2000-09-13 2000-09-13 Technology for making high-specific-weight alloy parts in different shapes

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CN1289658A true CN1289658A (en) 2001-04-04
CN1119213C CN1119213C (en) 2003-08-27

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Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
RU2444418C1 (en) * 2010-06-18 2012-03-10 Российская Федерация, от имени которой выступает Государственная корпорация по атомной энергии "Росатом" (Госкорпорация "Росатом") Method of producing sintered porous articles from tungsten-base pseudoalloy
CN102383016A (en) * 2011-11-02 2012-03-21 中南大学 Microwave sintering and heat treatment method for preparing high-performance tungsten-based high-density alloy
CN102581281A (en) * 2011-12-20 2012-07-18 中国兵器工业第五二研究所 Manufacturing method of mobile phone oscillator
CN104174854A (en) * 2014-07-14 2014-12-03 昆山安泰美科金属材料有限公司 Method for manufacturing miniature tungsten-based alloy part
RU2569287C1 (en) * 2014-05-27 2015-11-20 Федеральное государственное автономное образовательное учреждение высшего профессионального образования "Национальный исследовательский технологический университет "МИСиС" Production of sintered porous tungsten carcass
CN105755312A (en) * 2016-03-30 2016-07-13 山东正诺集团有限公司 Method for preparing titanium-based alloy automobile brake disc material
CN107716932A (en) * 2017-08-21 2018-02-23 柳州科尔特锻造机械有限公司 The method that counterweight peculiar to vessel is prepared with injection molding technology
CN107716929A (en) * 2017-08-21 2018-02-23 柳州科尔特锻造机械有限公司 The forging method of counterweight peculiar to vessel
CN108311695A (en) * 2018-02-13 2018-07-24 沈阳含能金属材料制造有限公司 A kind of decarbonization process of tungsten alloy blank material

Cited By (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
RU2444418C1 (en) * 2010-06-18 2012-03-10 Российская Федерация, от имени которой выступает Государственная корпорация по атомной энергии "Росатом" (Госкорпорация "Росатом") Method of producing sintered porous articles from tungsten-base pseudoalloy
CN102383016A (en) * 2011-11-02 2012-03-21 中南大学 Microwave sintering and heat treatment method for preparing high-performance tungsten-based high-density alloy
CN102383016B (en) * 2011-11-02 2013-04-24 中南大学 Microwave sintering and heat treatment method for preparing high-performance tungsten-based high-density alloy
CN102581281A (en) * 2011-12-20 2012-07-18 中国兵器工业第五二研究所 Manufacturing method of mobile phone oscillator
RU2569287C1 (en) * 2014-05-27 2015-11-20 Федеральное государственное автономное образовательное учреждение высшего профессионального образования "Национальный исследовательский технологический университет "МИСиС" Production of sintered porous tungsten carcass
CN104174854A (en) * 2014-07-14 2014-12-03 昆山安泰美科金属材料有限公司 Method for manufacturing miniature tungsten-based alloy part
CN104174854B (en) * 2014-07-14 2016-08-24 昆山安泰美科金属材料有限公司 A kind of method preparing miniature tungsten-bast alloy part
CN105755312A (en) * 2016-03-30 2016-07-13 山东正诺集团有限公司 Method for preparing titanium-based alloy automobile brake disc material
CN105755312B (en) * 2016-03-30 2017-10-31 山东正诺集团有限公司 A kind of preparation method of titanium-base alloy braking automobile disk material
CN107716932A (en) * 2017-08-21 2018-02-23 柳州科尔特锻造机械有限公司 The method that counterweight peculiar to vessel is prepared with injection molding technology
CN107716929A (en) * 2017-08-21 2018-02-23 柳州科尔特锻造机械有限公司 The forging method of counterweight peculiar to vessel
CN108311695A (en) * 2018-02-13 2018-07-24 沈阳含能金属材料制造有限公司 A kind of decarbonization process of tungsten alloy blank material

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