CN1281675C - Water-proof liquid rubber - Google Patents
Water-proof liquid rubber Download PDFInfo
- Publication number
- CN1281675C CN1281675C CN 200410062252 CN200410062252A CN1281675C CN 1281675 C CN1281675 C CN 1281675C CN 200410062252 CN200410062252 CN 200410062252 CN 200410062252 A CN200410062252 A CN 200410062252A CN 1281675 C CN1281675 C CN 1281675C
- Authority
- CN
- China
- Prior art keywords
- rubber
- antiager
- tenderizer
- styrene
- promotor
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
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- 229920001971 elastomer Polymers 0.000 title claims description 22
- 239000005060 rubber Substances 0.000 title claims description 22
- 239000007788 liquid Substances 0.000 title claims description 12
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 24
- 229920003048 styrene butadiene rubber Polymers 0.000 claims abstract description 22
- 239000000945 filler Substances 0.000 claims abstract description 14
- 239000004709 Chlorinated polyethylene Substances 0.000 claims description 19
- 239000012190 activator Substances 0.000 claims description 19
- 229920001084 poly(chloroprene) Polymers 0.000 claims description 19
- 229920001897 terpolymer Polymers 0.000 claims description 11
- FPAFDBFIGPHWGO-UHFFFAOYSA-N dioxosilane;oxomagnesium;hydrate Chemical group O.[Mg]=O.[Mg]=O.[Mg]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O FPAFDBFIGPHWGO-UHFFFAOYSA-N 0.000 claims description 7
- XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical group [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 claims description 5
- 235000012204 lemonade/lime carbonate Nutrition 0.000 claims description 4
- 238000002360 preparation method Methods 0.000 claims description 4
- 239000002994 raw material Substances 0.000 claims description 4
- 238000003756 stirring Methods 0.000 claims description 4
- -1 antiager Substances 0.000 claims description 3
- 238000012856 packing Methods 0.000 claims description 3
- 239000002904 solvent Substances 0.000 claims description 3
- YXIWHUQXZSMYRE-UHFFFAOYSA-N 1,3-benzothiazole-2-thiol Chemical compound C1=CC=C2SC(S)=NC2=C1 YXIWHUQXZSMYRE-UHFFFAOYSA-N 0.000 claims description 2
- 239000006096 absorbing agent Substances 0.000 claims description 2
- KUAZQDVKQLNFPE-UHFFFAOYSA-N thiram Chemical compound CN(C)C(=S)SSC(=S)N(C)C KUAZQDVKQLNFPE-UHFFFAOYSA-N 0.000 claims description 2
- 229960002447 thiram Drugs 0.000 claims description 2
- 239000011787 zinc oxide Substances 0.000 claims description 2
- KMNUDJAXRXUZQS-UHFFFAOYSA-L zinc;n-ethyl-n-phenylcarbamodithioate Chemical compound [Zn+2].CCN(C([S-])=S)C1=CC=CC=C1.CCN(C([S-])=S)C1=CC=CC=C1 KMNUDJAXRXUZQS-UHFFFAOYSA-L 0.000 claims description 2
- 238000000034 method Methods 0.000 abstract description 4
- 230000003712 anti-aging effect Effects 0.000 abstract description 3
- 239000004902 Softening Agent Substances 0.000 abstract 1
- 239000003086 colorant Substances 0.000 abstract 1
- 230000007613 environmental effect Effects 0.000 abstract 1
- 239000003973 paint Substances 0.000 abstract 1
- 239000000203 mixture Substances 0.000 description 12
- 238000004078 waterproofing Methods 0.000 description 12
- 238000009472 formulation Methods 0.000 description 10
- 239000000047 product Substances 0.000 description 9
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 6
- 239000000463 material Substances 0.000 description 6
- 238000010276 construction Methods 0.000 description 5
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 description 3
- 239000002253 acid Substances 0.000 description 3
- 230000032683 aging Effects 0.000 description 3
- 239000003513 alkali Substances 0.000 description 3
- AXCZMVOFGPJBDE-UHFFFAOYSA-L calcium dihydroxide Chemical compound [OH-].[OH-].[Ca+2] AXCZMVOFGPJBDE-UHFFFAOYSA-L 0.000 description 3
- 239000000920 calcium hydroxide Substances 0.000 description 3
- 229910001861 calcium hydroxide Inorganic materials 0.000 description 3
- 229910017604 nitric acid Inorganic materials 0.000 description 3
- 238000003556 assay Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000004566 building material Substances 0.000 description 1
- 150000001924 cycloalkanes Chemical class 0.000 description 1
- 230000002950 deficient Effects 0.000 description 1
- 230000002939 deleterious effect Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000002708 enhancing effect Effects 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 238000003933 environmental pollution control Methods 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 238000007689 inspection Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000002086 nanomaterial Substances 0.000 description 1
- 231100000614 poison Toxicity 0.000 description 1
- 230000007096 poisonous effect Effects 0.000 description 1
- 230000002787 reinforcement Effects 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Landscapes
- Compositions Of Macromolecular Compounds (AREA)
- Sealing Material Composition (AREA)
Abstract
The present invention discloses waterproof paint which is made of epdm, styrene-butadiene rubber, a solidifying agent, a softening agent, an accelerant, a vulcanizing agent, an anti-aging agent and a filler. The product of the present invention belongs to an environmental protection type product and can be made into products of various colors. The present invention has the advantages of simple use method, low cost, wide application range and strong adaptability.
Description
Technical field
The present invention relates to a kind of material of construction, particularly relate to a kind of water-proof liquid rubber.
Background technology
In the existing various water-proof material, major part is not an environment-friendly type, distributes various to poisonous, the deleterious gas of human body.And all there is unsatisfactory place in the water-proof material of those environment-friendly types in performance and use, as costs an arm and a leg, uses trouble etc.
Summary of the invention
The objective of the invention is to overcome prior art defective, a kind of environment-friendly type, water-proof liquid rubber easy to use are provided.
The present invention realizes by following technical solution.
The formulation by weight of water-proof liquid rubber of the present invention is difference according to the difference of using the position.Specific as follows:
1, uses when the building surface waterproofing work: terpolymer EP rubber 15-20 part, styrene-butadiene rubber(SBR) 5-10 part, chlorinatedpolyethylene 0-5 part, chloroprene rubber 0-5 part, activator 0.1-0.5 part, tenderizer 5-10 part, promotor 0.2-0.5 part, vulcanizing agent 0.2-0.4 part, antiager 0.1-0.2 part, filler 20-30 part.
When 2, using under construction layer waterproofing work: styrene-butadiene rubber(SBR) 15-20 part, chlorinatedpolyethylene 5-10 part, chloroprene rubber 0-5 part, activator 0.1-0.5 part, tenderizer 5-10 part, promotor 0.2-0.5 part, vulcanizing agent 0.2-0.4 part, antiager 0.1-0.2 part, filler 20-30 part.
3, use when building bottom or filleting waterproofing work: styrene-butadiene rubber(SBR) 10-15 part, chloroprene rubber 10-15 part, chlorinatedpolyethylene 0-5 part, activator 0.1-0.5 part, tenderizer 5-10 part, promotor 0.2-0.5 part, vulcanizing agent 0.2-0.4 part, antiager 0.1-0.2 part, filler 20-30 part.
Wherein, terpolymer EP rubber, styrene-butadiene rubber(SBR), chlorinatedpolyethylene, chloroprene rubber are the main body compositions, and other compositions are ancillary components.
Described activator comprises zinc oxide, 2-benzothiazolyl mercaptan etc.; Tenderizer comprises the cycloalkanes wet goods; Promotor comprises cyclohexyl-2-[4-morpholinodithio sulphenamide, tetramethyl-thiuram disulfide, zinc-ethylphenyl dithiocarbamate etc.; Antiager comprises UV light absorber UV-9 etc.; Filler comprises talcum powder and lime carbonate etc.
Terpolymer EP rubber is mainly used in anti-aging; Chlorinatedpolyethylene is mainly used in enhancing intensity; Chloroprene rubber is mainly used in and strengthens cohesiveness and stretching force; Styrene-butadiene rubber(SBR) is mainly used in and strengthens intensity and elasticity.
For reaching more than the different application target prescription proportioning flexibly: can add terpolymer EP rubber, nano material and antiager as need reinforcement anti-aging effect; As adding chlorinatedpolyethylene to the requirement of strength height; As the big chloroprene rubber added of need unit elongation; As the big styrene-butadiene rubber(SBR) added of need intensity; Added promotor and the vulcanizing agent short as the need curing time.
Make material hold-time length material can be made the first and second two components, the first component is added promotor and is not added vulcanizing agent by said ratio, and the second component is added vulcanizing agent and do not added promotor by system.In use two components are mixed and stir evenly.
The preparation method of water-proof liquid rubber of the present invention is as follows:
(1) the petrolic solvent oil with 4-8 times of weight dissolves terpolymer EP rubber, styrene-butadiene rubber(SBR), chloroprene rubber and chlorinatedpolyethylene by force;
(2) add ancillary components such as various activators, tenderizer, promotor, vulcanizing agent, antiager, filler;
(3) stir packing under the normal temperature.
Beneficial effect of the present invention is embodied in the following aspects:
1, product of the present invention belongs to environmentally friendly machine, and is free from environmental pollution;
2, can make versicolor product, beautify the environment;
3, using method is simple, and hand labor intensity is little;
4, raw material is extensive, and is with low cost, good in economic efficiency;
5, have wide range of applications, adaptability is strong.
Embodiment
Further specify the present invention below by specific embodiment.
Use in the building surface waterproofing work [embodiment 1]
Formulation by weight is: terpolymer EP rubber 15, styrene-butadiene rubber(SBR) 5, activator 0.1-0.5, tenderizer 5-10, ZNO 0.1, tenderizer 5, px 0.2, vulcanizing agent 0.2, antiager 0.1, talcum powder 20.
The preparation method is as follows:
(1) dissolves terpolymer EP rubber, styrene-butadiene rubber(SBR) by force with No. 100 petrolic solvent oil of 80-160 part;
(2) add ancillary components such as various activators, tenderizer, promotor, vulcanizing agent, antiager, filler;
(3) this product is white liquid with no taste, can be modulated into shades of colour by adding various tinting materials according to user's needs during actual production;
(4) stir packing under the normal temperature.
Using method: product of the present invention is poured on the building surface that needs waterproof, adopts existing dauber to make it be close to metope or ground gets final product.
Use in the building surface waterproofing work [embodiment 2]
Formulation by weight is: terpolymer EP rubber 20, styrene-butadiene rubber(SBR) 10, chlorinatedpolyethylene 5, chloroprene rubber 5, M 0.5, tenderizer 10, cz 0.5, vulcanizing agent 0.4, antiager 0.2, lime carbonate 30.
Use in the building surface waterproofing work [embodiment 3]
Formulation by weight is: terpolymer EP rubber 18, styrene-butadiene rubber(SBR) 8, chlorinatedpolyethylene 0.5, chloroprene rubber 0.5, activator 0.35, tenderizer 8, promotor 0.35, vulcanizing agent 0.3, antiager 0.15, filler 25.
The product that makes is through detecting, and the result is as follows:
Tensile strength＞1.65MPI
Low temperature flexibility (40 ℃) is qualified
Unit elongation 500%
Acid resistance 10% nitric acid, sulfuric acid soak 7 days no changes
Alkali resistance 10% calcium hydroxide soaks 7 days no changes
Thermal ageing (168 hours) stretching strength retentivity 〉=80%
[embodiment 4] use layer waterproofing work under construction
Formulation by weight is: styrene-butadiene rubber(SBR) 15, chlorinatedpolyethylene 5, chloroprene rubber 0.5, activator 0.1, tenderizer 5, tmtd 0.2, vulcanizing agent 0.2, antiager 0.1, talcum powder 20.
[embodiment 5] use layer waterproofing work under construction
Formulation by weight is: styrene-butadiene rubber(SBR) 18, chlorinatedpolyethylene 8, chloroprene rubber 3.5, activator 0.45, tenderizer 8, tmtd 0.35, vulcanizing agent 0.3, antiager 0.15, talcum powder 25.
The product that makes is through detecting, and the result is as follows:
Tensile strength＞1.60MPI
Low temperature flexibility (40 ℃) is qualified
Unit elongation 450%
Acid resistance 10% nitric acid, sulfuric acid soak 6 days no changes
Alkali resistance 10% calcium hydroxide soaks 6 days no changes
Thermal ageing (168 hours) stretching strength retentivity 〉=80%
[embodiment 6] use layer waterproofing work under construction
Formulation by weight is: styrene-butadiene rubber(SBR) 20, chlorinatedpolyethylene 10, chloroprene rubber 5, activator 0.5, tenderizer 10, tmtd 0.5, vulcanizing agent 0.4, antiager 0.2, talcum powder 30.
Use in building bottom or filleting waterproofing work [embodiment 7]
Formulation by weight is: styrene-butadiene rubber(SBR) 10, chloroprene rubber 10, chlorinatedpolyethylene 0.5, activator 0.1, tenderizer 5, promotor 0.2, vulcanizing agent 0.2, antiager 0.1, lime carbonate 20.
Using method: water it in expansion joint that is filled in buildings or embedding is added in main building seam.
Use in building bottom or filleting waterproofing work [embodiment 8]
Formulation by weight is: styrene-butadiene rubber(SBR) 13, chloroprene rubber 12, chlorinatedpolyethylene 4.5, activator 0.25, tenderizer 7, promotor 0.35, vulcanizing agent 0.3, antiager 0.15, filler 25.
The product that makes is through detecting, and the result is as follows:
Tensile strength＞1.55MPI
Low temperature flexibility (40 ℃) is qualified
Unit elongation 520%
Acid resistance 10% nitric acid, sulfuric acid soak 6 days no changes
Alkali resistance 10% calcium hydroxide soaks 6 days no changes
Thermal ageing (168 hours) stretching strength retentivity 〉=80%
Use in building bottom or filleting waterproofing work [embodiment 9]
Formulation by weight is: styrene-butadiene rubber(SBR) 15, chloroprene rubber 15, chlorinatedpolyethylene 5, activator 0.5, tenderizer 10, promotor 0.5, vulcanizing agent 0.4, antiager 0.2, talcum powder 30.
Embodiment 2-9 preparation method is with embodiment 1.
Product is through the check of building materials quality supervision and inspection station, Beijing, and the result is as follows:
| Sequence number | Interventions Requested | Standard-required (salable product) | Assay | This conclusion |
| 1 | TVOC(S)，g/l | ≤600 | 265 | Meet |
| 2 | Benzene (S), g/kg | ≤5 | 0.2 | Meet |
Prove that it meets the index request among the GB 50325-2001 " civil building engineering indoor environmental pollution control standard ".
Claims (5)
1, a kind of water-proof liquid rubber is made by the raw material of following weight part: terpolymer EP rubber 15-20 part, styrene-butadiene rubber(SBR) 5-10 part, chlorinatedpolyethylene 0-5 part, chloroprene rubber 0-5 part, activator 0.1-0.5 part, tenderizer 5-10 part, promotor 0.2-0.5 part, vulcanizing agent 0.2-0.4 part, antiager 0.1-0.2 part, filler 20-30 part.
2, a kind of water-proof liquid rubber is made by the raw material of following weight part: styrene-butadiene rubber(SBR) 15-20 part, chlorinatedpolyethylene 5-10 part, chloroprene rubber 0-5 part, activator 0.1-0.5 part, tenderizer 5-10 part, promotor 0.2-0.5 part, vulcanizing agent 0.2-0.4 part, antiager 0.1-0.2 part, filler 20-30 part.
3, a kind of water-proof liquid rubber is made by the raw material of following weight part: styrene-butadiene rubber(SBR) 10-15 part, chloroprene rubber 10-15 part, chlorinatedpolyethylene 0-5 part, activator 0.1-0.5 part, tenderizer 5-10 part, promotor 0.2-0.5 part, vulcanizing agent 0.2-0.4 part, antiager 0.1-0.2 part, filler 20-30 part.
4, according to claim 1 or 2 or 3 described water-proof liquid rubbers, it is characterized in that: described activator is selected from zinc oxide, the 2-benzothiazolyl mercaptan any; Tenderizer is meant naphthenic oil; Promotor is selected from N-cyclohexyl-2-[4-morpholinodithio sulphenamide, tetramethyl-thiuram disulfide, the zinc-ethylphenyl dithiocarbamate any; Antiager is meant UV light absorber UV-9; Filler is selected from talcum powder or the lime carbonate any.
5, the preparation method of water-proof liquid rubber according to claim 1 comprises the steps:
(1) the petrolic solvent oil with 4-8 times of weight dissolves terpolymer EP rubber, styrene-butadiene rubber(SBR), chloroprene rubber and chlorinatedpolyethylene by force;
(2) add activator, tenderizer, promotor, vulcanizing agent, antiager, filler;
(3) stir packing under the normal temperature.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200410062252 CN1281675C (en) | 2004-07-02 | 2004-07-02 | Water-proof liquid rubber |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200410062252 CN1281675C (en) | 2004-07-02 | 2004-07-02 | Water-proof liquid rubber |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1587310A CN1587310A (en) | 2005-03-02 |
| CN1281675C true CN1281675C (en) | 2006-10-25 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 200410062252 Expired - Fee Related CN1281675C (en) | 2004-07-02 | 2004-07-02 | Water-proof liquid rubber |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN1281675C (en) |
Families Citing this family (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100381494C (en) * | 2005-12-30 | 2008-04-16 | 何霖 | Trielement ethyl butyric rubber waterproofing coiled material and production process thereof |
| CN100357348C (en) * | 2005-12-30 | 2007-12-26 | 何霖 | Trielement ethyl propylric rubber waterproofing coiled material and production process thereof |
| CN101089039B (en) * | 2006-06-12 | 2010-11-24 | 深圳市迅特科技有限公司 | Chlorinated polyethylene-neoprene mixed polymer |
| CN101113262B (en) * | 2007-09-14 | 2011-12-07 | 北京立高科技有限公司 | EPT rubber waterproofing paint and process for preparing the same |
| CN101284970B (en) * | 2008-05-30 | 2010-07-28 | 王丹 | Waterproof coating material |
| CN104761829A (en) * | 2015-03-28 | 2015-07-08 | 安徽同丰橡塑工业有限公司 | Acid-alkali resistant rubber material formula |
| CN106085016A (en) * | 2016-07-18 | 2016-11-09 | 安徽朗凯奇建材有限公司 | Heat-insulating waterproof coating of butadiene-styrene rubber a kind of of clay alteration and preparation method thereof |
| CN105949850A (en) * | 2016-07-18 | 2016-09-21 | 安徽朗凯奇建材有限公司 | Antiseptic butadiene styrene rubber heat-insulating waterproof coating and preparation method thereof |
| CN106085017A (en) * | 2016-07-18 | 2016-11-09 | 安徽朗凯奇建材有限公司 | A kind of heat-insulating waterproof coating of butadiene-styrene rubber not chapped and preparation method thereof |
| CN105949849A (en) * | 2016-07-18 | 2016-09-21 | 安徽朗凯奇建材有限公司 | Nanometer aluminum oxide modified butadiene styrene rubber heat-insulation waterproof coating and preparation method thereof |
| CN105949887A (en) * | 2016-07-18 | 2016-09-21 | 安徽朗凯奇建材有限公司 | High-brightness butadiene-styrene-rubber heat-insulation and waterproof coating and preparing method thereof |
| CN105949888A (en) * | 2016-07-18 | 2016-09-21 | 安徽朗凯奇建材有限公司 | Glass fiber reinforced butadiene styrene rubber heat insulation and water prevention coating and preparation method thereof |
| CN106085015A (en) * | 2016-07-18 | 2016-11-09 | 安徽朗凯奇建材有限公司 | Heat-insulating waterproof coating of butadiene-styrene rubber a kind of of durable antibiotic and preparation method thereof |
| CN107805393A (en) * | 2017-11-06 | 2018-03-16 | 张永宏 | The surfacing of Electrostatic Absorption film production mould |
-
2004
- 2004-07-02 CN CN 200410062252 patent/CN1281675C/en not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| CN1587310A (en) | 2005-03-02 |
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| TR01 | Transfer of patent right |
Effective date of registration: 20090206 Address after: Ma Village East of Chengguan Town, Beijing, Fangshan District Patentee after: Beijing Jianguo Weiye Waterproof Material Co., Ltd. Address before: Xin Yang Xiang Wang Ping Cun, Hunan City, Liling Province Patentee before: Yang Tailong |
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| ASS | Succession or assignment of patent right |
Owner name: BEIJING CITY JIANGUOWEIYE WATERPROOF MATERIALS CO. Free format text: FORMER OWNER: YANG TAILONG Effective date: 20090206 |
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Granted publication date: 20061025 Termination date: 20100702 |