CN1261557C - Health caring fancy soap and preparing method thereof - Google Patents
Health caring fancy soap and preparing method thereof Download PDFInfo
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- CN1261557C CN1261557C CN 02144833 CN02144833A CN1261557C CN 1261557 C CN1261557 C CN 1261557C CN 02144833 CN02144833 CN 02144833 CN 02144833 A CN02144833 A CN 02144833A CN 1261557 C CN1261557 C CN 1261557C
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Abstract
The present invention discloses a health care fancy soap which comprises the compositions by weight of 1 to 5 portions of glossy ganoderma powder, 1 to 5 portions of propolis, 0.5 to 5 portions of lanolin, 0.1 to 0.8 portion of titanium white powder, 0.1 to 0.8 portion of EDTA-2NA, 5 to 10 portions of carbamide, 1 to 5 portions of menthol, 1 to 4 portions of soap essence, 70 to 90 portions of soap curd and 0.5 to 2.0 portions of biomass activation energy composite. The biomass activation energy composite contains 7.0-to 10.0 g of sodium silicate, 0.5 to 2.0g of sodium aluminate, 2.0 to 4.0g of sodium oxide, 0.5 to 1.5g of sodium thiosulfate, 2.0 to 4.0g of germanium dioxide, 0.5 to 1.5g of potassium carbonate, 2.5 to 5.0g of dextrose, 8.0 to 15.0g of white sugar, 1010 ml of aurum nitric acid and 60 to 65 ml of silver thiosulfate. The fancy soap has the advantages of germ removal, germ inhibition, age resistance, skin cleanness and health care.
Description
Technical field
The present invention relates to a kind of skin care articles for washing, especially a kind of health care fancy soap and preparation method thereof.
Background technology
As the perfumed soap of articles for washing, existing long history, its effect mostly is decontamination, cleans, washes one's hands, washes one's face, bathing.Some emphasizes the perfumed soap of function, in recent years appearing on the market more, but mostly be simple function (as sulfur soap, bath soap etc.), some life-time service has potential injury effect to keratoderma and deep layer cell.
Summary of the invention
At the problems referred to above, the object of the present invention is to provide a kind of human body to be had no side effect, can cleaning skin, but health care fancy soap of rehabilitation skin and preparation method thereof again.
Technical solution of the present invention is as follows:
Health care fancy soap comprises neat soap, Chinese medicine and life entity activation energy mixture, and prepares by following parts by weight:
1～5 part of Ganoderma powder, 1～5 part of propolis, 0.5～5 part in lanolin, 0.1～0.8 part of titanium dioxide, 5～10 parts in urea, 0.1～0.8 part of EDTA-2Na (disodium ethylene diamine tetraacetate), 1～5 part of mentha camphor, 1～4 part of soap compound, 70～90 parts of neat soaps, 0.5～2.0 part of life entity activation energy mixture;
The weight of wherein said life entity activation energy mixture consists of:
Water glass 7.0～10.0g, sodium aluminate 0.5～2.0g, sodium oxide 2.0～4.0g, Sulfothiorine 0.5～1.5g, germanium dioxide 2.0～4.0g, salt of wormwood 0.5～1.5g, glucose 2.5～5.0g (purity 85%～99.5%), white sugar 8.0～15.0g (purity 85%～99%), concentration are that nitric acid gold 1010ml, the concentration of 6.5～10.4g/L is silver thiosulfate 60～65ml of 29.68～48.24g/L;
Described life entity activation energy mixture adopts following method preparation:
1) preparation solution 1
Get sodium silicate raw material 7.0～10.0g, sodium aluminate 0.5～2.0g, sodium oxide 2.0～4.0g, Sulfothiorine 0.5～1.5g, germanium dioxide 2.0～4.0g, salt of wormwood 0.5～1.5g, glucose 2.5～5.0g (purity 85%～99.5%), white sugar 8.0～15.0g (purity 85%～99%), under 20 ℃～40 ℃, be dissolved in respectively in the 200ml pure water, then described solution is mixed, get solution 1; Wherein, Germanium dioxide solution is only got its supernatant liquor;
2) preparation solution 2
5.0～8.0g gold mine powder is added in the crucible, be heated to 1100 ℃ and make its fusing; The gold of fusing is added to is stirred to even back in the 1000ml pure water to wherein adding 10ml nitric acid, the mixed solution of making forms a kind of yellowish nitric acid gold solutions, ie in solution 2 down at 40～50 ℃;
3) preparation solution 3
Under the normal temperature 2.0～3.0g Silver Nitrate is dissolved in 10～15ml pure water, 3.0～4.0g sodium-chlor is dissolved in the 50ml pure water; Above-mentioned two solution are mixed white silver nitride precipitation just occurred, isolates throw out, with purified rinse water 3 times, 2 parts of water, 3 parts of throw outs and 4g Sulfothiorine is added in the isolated silver chloride again; This mixture heated 25～35 minutes down at 30 ℃～40 ℃, heated while stirring so that silver chloride fully dissolves, and obtained a kind of silver thiosulfate solution of colorless and odorless, ie in solution 3;
4), place above the liquid life entity activation energy mixture of just making a kind of clear, colorless in 72 hours at normal temperatures with above-mentioned solution 1, solution 2 and solution 3 mixings.
Above-mentioned health care fancy soap prepares as follows:
1) take by weighing weight by above-mentioned perfumed soap component, Ganoderma powder, propolis, urea, mentha camphor are ground into fine powder and cross 100 above mesh sieves, and be stand-by:
2) life entity activation energy mixture is diluted to 1: 200～500 colorless and odorless transparent liquids, stand-by;
3) (moisture is 1.0～12.5% to get 50～60 ℃ of vacuum drying neat soaps, in fatty acid content (more than 65～85%) (method for making see " fine chemistry industry handbook Zhou Xueliang chief editor) the intermittent type spice machine of packing into (or BDM spice machine), add Ganoderma powder, the lanolin (JSCI-II) of fusing, titanium dioxide (GB-2440-91), propolis (seeing Liu Fuhai chief editor " magical propolis therapy " for details), mentha camphor, soap compound (QB1507-92), life entity activation energy mixture also constantly stirs (must not be less than 30 minutes), grind (35～45 ℃), press strip (35～55 ℃ of neat soap temperature, water content is 10.5～12.5%, become piece), make the perfumed soap of multiple weight such as 5～180g.
The present invention has following advantage:
1. adopted Ganoderma powder (Ganoderma spore powder that adopts special wall breaking technology to produce) in the prescription of the present invention.Various trace elements such as the double stranded RNA that contains in the Ganoderma powder, ergosterol, organic germanium and polysaccharide; can improve body immune function; improve human body SOD growing amount; eliminate free radical, endocrine regulation, the sealing degree of raising cytolemma; improve the cell physiological function; unique effects such as protection cell tissue is not subjected to radical damage, induces the generation Interferon, rabbit, and is antiviral.
2. adopt propolis in the prescription among the present invention, contained V in the propolis
Bl, V
PP, V
A is formerEtc. multiple amino acids, enzyme and polysaccharide and 20, plant valuable trace element more, comprise potassium, zinc, iron, phosphorus, cobalt, chromium, manganese, selenium, titanium, zirconium, strontium etc.; The necessary 38 kinds of elements of biological existence just have 34 kinds more than in the propolis.
3. propolis has broad-spectrum antibacterial action.It can suppress and kill 100 various bacteria, mycovirus and protozoon.Also can promote biological human body epidemic prevention ability, improve blood circulation, promote the granulation growth, accelerating wound healing, and have moist, antipruritic, deodorization, function such as sun-proof.
4. the special efficacy of the effective ingredient of integrated use Ganoderma powder of the present invention, propolis and the life entity activation energy mixture (special efficacy of Ganoderma powder and propolis wherein, first Application in perfumed soap and articles for washing), act on the skin care maintenance, anti-chap, antipruritic, removing beverage, anti-wrinkle, the acne of dispelling, recover skin vitality, prevent and kill the harmful microorganism (bacterium, virus and acarid) of top layer and deep layer, improve the skin histology microcirculation, strengthen the nutritive equilibrium between skin cells and the soft tissue, promote the metabolism between the skin cell tissue.
5. the life entity activation energy mixture that exists with the activating ion attitude of the present invention's preparation is stronger than the powdered biological pottery far infrared radioactivity of traditional technology preparation, because of having the atom of emitting far infrared ray, be to exist with activating ion attitude that can more effective emitting far infrared ray as gold and silver and silicon.
6. the life entity activation energy mixture for preparing owing to the present invention wraps quilt or soaks into various products with liquid (watery), so it can be absorbed product equably or the bag quilt arrives product surface, makes more effectively emitting far infrared ray of this product.
7. the middle silver of the present invention's preparation can slowly discharge oxygen from life entity activation energy mixture, so can strengthen thermotolerance, snappiness and the wear resistance of product.
8. even the life entity activation energy mixture of the present invention preparation does not freeze under～15 ℃ of temperature yet, and colorless and odorless, keep radioactivity always, do not decompose, unchangeability.
9. the life entity activation energy mixture of the present invention preparation only can be used for externally, also can directly act in skin and the body, and be dispersed in the various carriers, and good adhesion strength and adhesive rate are arranged.
10. the life entity activation energy mixture of the present invention's preparation also has uvioresistant, deodorization functions, because its alkaline secondary ion generation kinetic energy, can strengthen the human immunologic function, hemopoietic function, anti-tumor function, anti-apoptotic function, decomposing harmful substances, endocrine regulation, hypoglycemic, reducing blood-fat (in viruses such as killing in vitro HTV, HBV, HCV) tool sterilization.
11. far infrared rays is electromagnetic a kind of, after far infrared rays is absorbed by the body, can make water molecules generation resonance in the body, increases internal energy of molecular promptly
Its energy comes from the far infrared photon (4e) of negatively charged ion base thing emission, thereby but biomacromolecules such as activation of protein make biological cell be in high level vibrations attitude; Because biomass cells produces resonance effect, the far infrared photon can be able to be delivered to the subcutaneous darker part of human body, the subcutaneous deep temperature rises, and the warm of generation distributed from inside to outside; This action intensity makes telangiectasis, stimulates circulation, and strengthens the metabolism between each tissue, increases the regenerative power of tissue, improves the immunological competence of human body, and the present invention has adopted this far infrared rays technology just, thereby plays medical care effect.
Embodiment
Embodiment 1
Get neat soap 70g, lanolin 5g, Ganoderma powder 5g, propolis 5g, urea 10g, mentha camphor 5g, soap compound 4g, titanium dioxide 0.8g, EDTA-2Na0.8g, life entity activation energy mixture: 1.0g;
Ganoderma powder, propolis, urea, mentha camphor (oven drying at low temperature) are ground into fine powder cross 100 mesh sieves, 50 ℃ of vacuum drying neat soaps are encased in the intermittent type spice machine, (temperature is 35 ℃), press strip (35 ℃ of neat soap temperature are ground in the lanolin, titanium dioxide, EDTA-2Na, urea, Ganoderma powder, propolis, mentha camphor, soap compound, life entity activation energy mixture and continuous stir (30 minutes) that add fusing subsequently, water content is 10.5%), become piece, make the heavy perfumed soap of 80g.
Embodiment 2
Get neat soap 90g, lanolin 0.5g, Ganoderma powder 1g, propolis 1g, urea 5g, mentha camphor 1g, soap compound 1g, titanium dioxide 0.1g, EDTA-2Na 0.1g, life entity activation energy mixture 1.0g;
Ganoderma powder, propolis, urea, mentha camphor are ground into fine powder cross 100 mesh sieves, get 55 ℃ of vacuum drying neat soaps, be encased in the batch agitator, the back adds lanolin, titanium dioxide, EDTA-2Na, urea, Ganoderma powder, propolis, mentha camphor, essence, the life entity activation energy mixture of fusing, and constantly stirring (35 minutes), grind (40 ℃ of temperature), (55 ℃ of neat soap temperature, water content are 11.5% to press strip; ), become piece, make the heavy perfumed soap of 125g.
Embodiment 3
Get neat soap 85g, lanolin 3.0g, Ganoderma powder 3g, propolis 3g, urea 7g, mentha camphor 3g, soap compound 2g, titanium dioxide 0.4g, EDTA-2Na 0.4g, life entity activation energy mixture 1.0g;
Ganoderma powder, propolis, urea, mentha camphor are ground into fine powder cross 100 mesh sieves, other gets 60 ℃ of vacuum drying neat soaps and is encased in the intermittent type spice machine, the back adds lanolin, titanium dioxide, EDTA-2Na, urea, Ganoderma powder, propolis, mentha camphor, essence, the life entity activation energy mixture of fusing, and constantly stirring (40 minutes), grind (temperature is 45 ℃), (55 ℃ of neat soap temperature, water content are 12.5% to press strip; Become piece, make the perfumed soap of 100g.
The health care fancy soap that the foregoing description makes except that as washing one's hands, wash one's face, the bath article, still can be used for skin care, is anti-ly chapped, removing beverage, anti-wrinkle, the acne of dispelling, the effect of antipruritic, prevention and killing microorganisms (bacterium, virus and acarid).
That above-mentioned perfumed soap goods can be is solid-state, any form in the powder attitude, liquid state, cream, breast, dew.
Embodiment 4
The preparation of life entity activation energy mixture:
1) preparation solution 1
Get sodium silicate raw material 7.0g, sodium aluminate 0.5g, sodium oxide 2.0g, Sulfothiorine 0.5g, germanium dioxide 2.0g, salt of wormwood 0.5g, glucose 2.5g (purity 85%), white sugar 8.0g (purity 85%), each composition is dissolved in the 200ml pure water under 25 ℃ respectively, then these solution are mixed, but germanium dioxide solution is only got its supernatant liquor, gets solution 1;
2) preparation solution 2
5.0g gold mine powder is added in the crucible, be heated to 1100 ℃ and make its fusing.The gold that will melt is put in the large beaker after being added to and being stirred to evenly in the 800ml pure water again, adds 8ml nitric acid again in beaker, and the mixed solution of making forms a kind of yellowish nitric acid gold solution down at 40 ℃, gets solution 2;
3) preparation solution 3
Under the normal temperature 2.0g Silver Nitrate is dissolved in the 10ml pure water, 3.0g sodium-chlor is dissolved in the 50ml pure water.Above-mentioned two solution are mixed white silver nitride precipitation just occurred, isolates throw out, with purified rinse water 3 times, 2 parts of water, 3 parts of throw outs and 3.0g Sulfothiorine is added in the isolated silver chloride again.This mixture heated 25 minutes down at 30 ℃, heated while stirring so that silver chloride fully dissolves, and obtained a kind of silver thiosulfate solution of colorless and odorless, got solution 3;
4) above-mentioned solution 1, solution 2 and solution 3 mixings are placed at normal temperatures above the liquid life entity activation energy mixture of just making a kind of clear, colorless in 72 hours.
Embodiment 5
The preparation of life entity activation energy mixture:
1) preparation solution 1
Get sodium silicate raw material 8.5g, sodium aluminate 1.0g, sodium oxide 3.0g, Sulfothiorine 1.0g, germanium dioxide 3.0g, salt of wormwood 1.0g, glucose 3.5 (purity is more than 90%), white sugar 11.0g (purity is more than 90%), each composition is dissolved in the 200ml pure water under 35 ℃ respectively, then these solution are mixed, but germanium dioxide solution is only got its supernatant liquor, gets solution 1;
2) preparation solution 2
6.5g gold mine powder is added in the crucible, be heated to 1150 ℃ and make its fusing.The gold that will melt is put in the large beaker after being added to and being stirred to evenly in the 1000ml pure water again, adds 9ml nitric acid again in beaker, and the mixed solution of making forms a kind of yellowish nitric acid gold solution down at 45 ℃, gets solution 2;
3) preparation solution 3
Under the normal temperature 2.5g Silver Nitrate is dissolved in the 12.5ml pure water, 3.5g sodium-chlor is dissolved in the 50ml pure water.Above-mentioned two solution are mixed white silver nitride precipitation just occurred, isolates throw out, with purified rinse water 3 times, 2 parts of water, 3 parts of throw outs and 3.5g Sulfothiorine is added in the isolated silver chloride again.This mixture heated 30 minutes down at 35 ℃, heated while stirring so that silver chloride fully dissolves, and obtained a kind of silver thiosulfate solution of colorless and odorless, got solution 3;
(4) above-mentioned solution 1, solution 2 and solution 3 mixings are placed at normal temperatures above the liquid life entity activation energy mixture of just making a kind of clear, colorless in 72 hours.
Embodiment 6
The preparation of life entity activation energy mixture:
1) preparation solution 1
Get sodium silicate raw material 10.0g, sodium aluminate 2.0g, sodium oxide 4.0g, Sulfothiorine 1.5g, germanium dioxide 4.0g, salt of wormwood 1.5g, glucose 5.0g (purity 99.5%), white sugar 15.0g (purity 99%), each composition is dissolved in the 200ml pure water under 40 ℃ respectively, then these solution are mixed, but germanium dioxide solution is only got its supernatant liquor, gets solution 1;
2) preparation solution 2
8.0g gold mine powder is added in the crucible, be heated to 1180 ℃ and make its fusing.The gold that will melt is put in the large beaker after being added to and being stirred to evenly in the 1200ml pure water again, adds 10ml nitric acid again in beaker, and the mixed solution of making forms a kind of yellowish chlorauric acid solution down at 50 ℃, gets solution 2;
3) preparation solution 3
Under the normal temperature 3.0g Silver Nitrate is dissolved in the 15ml pure water, 4.0g sodium-chlor is dissolved in the 50ml pure water.Above-mentioned two solution are mixed white silver nitride precipitation just occurred, isolates throw out, with purified rinse water 3 times, 2 parts of water, 3 parts of throw outs and 4.0g Sulfothiorine is added in the isolated silver chloride again.This mixture heated 35 minutes down at 40 ℃, heated while stirring so that silver chloride fully dissolves, and obtained a kind of silver thiosulfate solution of colorless and odorless, got solution 3;
4) above-mentioned solution 1, solution 2 and solution 3 mixings are placed at normal temperatures above the liquid life entity activation energy mixture of just making a kind of clear, colorless in 72 hours.
The performance measurement of life entity activation energy mixture:
A. far infrared radioactivity and intensity of radioactivity:
With the polyethylene terephthalate of Chang Zuowei trousers lining with above-mentioned example 4 soaked with liquid 60 seconds, dry back is measured with the JIT-E500 instrument, condition is: resolving power is 1/6cm, the integration number is 20.The MCT telltale, 35 ℃ of temperature; The result is 68.5～80% for intensity of radioactivity when wavelength is 4.0～6.0 μ m, surpasses 80% when wavelength is 8.0 μ m.
B. anti-microbial effect
The liquid 100ml that above-mentioned example 4 is got mixes with the pure water of 20L, with a diameter is that the 30cm*30cm hair fibre soaked 60 seconds with it, and dry back is at 25 ℃, and staphylococcus aureus experimentizes under existing, in 24 hours, the result shows that the microbial biomass of survival has reduced 76.8%.
C. ultraviolet blocking experiment
Instrument is the UV spectrograph, and the result is on average blocking-up rate of 300～400 μ m 84% for human body there being the on average blocking-up rate of wavelength 200～400 μ m 98% of harm at wavelength.
D. antistatic experiment
Instrument is KSK0555, the B method; 20 ℃ of relative humidity 65% were handled polyethylene terephthalate and untreated comparison in 60 seconds with the soaked with liquid that above-mentioned example 4 gets, and friction results is:
| Friction voltage (V) | Static reduces (%) | |
| Untreated cotton sample | 520 | 0 |
| Cotton sample after the processing | 18 | 96.5 |
Claims (4)
1. health care fancy soap is characterized in that: by weight, formulated by following composition:
1～5 part of Ganoderma powder, 1～5 part of propolis, 0.5～5 part in lanolin, 0.1～0.8 part of titanium dioxide, 0.1～0.8 part of disodium ethylene diamine tetraacetate, 5～10 parts in urea, 1～5 part of mentha camphor, 1～4 part of soap compound, 70～90 parts of neat soaps, 0.5～2.0 part of life entity activation energy mixture;
The weight of wherein said life entity activation energy mixture consists of:
Water glass 7.0～10.0g, sodium aluminate 0.5～2.0g, sodium oxide 2.0～4.0g, Sulfothiorine 0.5～1.5g, germanium dioxide 2.0～4.0g, salt of wormwood 0.5～1.5g, purity are that 85%～99.5% glucose 2.5～5.0g, purity are that white sugar 8.0～15.0g of 85%～99%, nitric acid gold 1010ml, the concentration that concentration is 6.5～10.4g/L are silver thiosulfate 60～65ml of 29.68～48.24g/L.
2. health care fancy soap according to claim 1 is characterized in that: the form of described perfumed soap goods is solid-state, powder attitude, liquid state, cream, breast or reveals.
3. the preparation method of the described health care fancy soap of claim 1, it is characterized in that: above-mentioned health care fancy soap prepares as follows:
1) take by weighing by each components by weight percent of perfumed soap, Ganoderma powder, propolis, urea, mentha camphor are ground into fine powder and cross 100 mesh sieves, and be stand-by;
2) life entity activation energy mixture is diluted to 1: 200～500 colorless and odorless transparent liquids, stand-by;
3) water intaking branch content is 1.0～12.5%, fatty acid content 65～85% above neat soaps, stir Ganoderma powder, propolis, urea, mentha camphor and step 2 after the lanolin, titanium dioxide, soap compound and the step 1) that add fusing are down pulverized) the life entity activation energy mixture that obtained and constantly stirring, time must not be less than 30 minutes, grind, press strip becomes piece, makes the perfumed soap of various weight.
4. according to the preparation method of the health care fancy soap of claim 3, it is characterized in that: the preparation process of described life entity activation energy mixture is:
1) preparation solution 1
Get glucose 2.5～5.0g, purity 85%～99% white sugar 8.0～15.0g of sodium silicate raw material 7.0～10.0g, sodium aluminate 0.5～2.0g, sodium oxide 2.0～4.0g, Sulfothiorine 0.5～1.5g, germanium dioxide 2.0～4.0g, salt of wormwood 0.5～1.5g, purity 85%～99.5%, under 20 ℃～40 ℃, be dissolved in respectively in the 200ml pure water, then these solution are mixed, but germanium dioxide solution is only got its supernatant liquor, gets solution 1;
2) preparation solution 2
5.0～8.0g gold mine powder is added in the crucible, be heated to 1100 ℃ and make its fusing.The gold that will melt is added to and stirs in the 1000ml pure water to wherein adding 10ml nitric acid again, and the mixed solution of making forms a kind of yellowish nitric acid gold solution down at 40～50 ℃, gets solution 2;
3) preparation solution 3
Under the normal temperature 2.0～3.0g Silver Nitrate is dissolved in 10～15ml pure water, 3.0～4.0g sodium-chlor is dissolved in the 50ml pure water; Isolate throw out, flushing is added to 2 parts of water, 3 parts of throw outs and 4g Sulfothiorine in the isolated silver chloride again; This mixture heated 25～35 minutes down at 30 ℃～40 ℃, heated while stirring so that silver chloride fully dissolves, and obtained a kind of silver thiosulfate solution 3 of colorless and odorless;
4) above-mentioned solution 1, solution 2 and solution 3 mixings are placed at normal temperatures above the liquid life entity activation energy mixture of just making a kind of clear, colorless in 72 hours.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 02144833 CN1261557C (en) | 2002-11-15 | 2002-11-15 | Health caring fancy soap and preparing method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 02144833 CN1261557C (en) | 2002-11-15 | 2002-11-15 | Health caring fancy soap and preparing method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1500858A CN1500858A (en) | 2004-06-02 |
| CN1261557C true CN1261557C (en) | 2006-06-28 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 02144833 Expired - Fee Related CN1261557C (en) | 2002-11-15 | 2002-11-15 | Health caring fancy soap and preparing method thereof |
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Families Citing this family (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102504984A (en) * | 2011-11-01 | 2012-06-20 | 包头市红卫日用化工有限公司 | Dual-color synthetic soap and preparation method thereof |
| CN103371182A (en) * | 2012-04-13 | 2013-10-30 | 上海维来新材料有限公司 | Double-complexing nanosilver polymer liquid antibacterial agent and preparation method thereof |
| EP2986698B1 (en) | 2013-04-16 | 2019-04-03 | Unilever Plc. | Soap bar having enhanced antibacterial activity |
| CN103409252A (en) * | 2013-08-21 | 2013-11-27 | 烟台九州燃油燃气节能科技有限公司 | Germanium-enriched frosted essential oil soap |
| CN103820250A (en) * | 2014-02-23 | 2014-05-28 | 谭俊昌 | Skin care soap containing Spina Gleditsiae and Mythic Fungus, and its making method |
| CN104312795A (en) * | 2014-10-31 | 2015-01-28 | 无锡优创生物科技有限公司 | Refreshing soap |
| CN104312796A (en) * | 2014-10-31 | 2015-01-28 | 无锡优创生物科技有限公司 | Preparation method of soap for refreshing |
| CN107638430A (en) * | 2017-09-30 | 2018-01-30 | 李明玉 | Organochlorine Pesticide Residues treatment fluid and preparation method thereof |
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2002
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