CN1500858A - Health caring fancy soap and preparing method thereof - Google Patents
Health caring fancy soap and preparing method thereof Download PDFInfo
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- CN1500858A CN1500858A CNA021448337A CN02144833A CN1500858A CN 1500858 A CN1500858 A CN 1500858A CN A021448337 A CNA021448337 A CN A021448337A CN 02144833 A CN02144833 A CN 02144833A CN 1500858 A CN1500858 A CN 1500858A
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Abstract
The health toilet soap is made with glossy ganoderma powder, propolis, lanoline, titania powder, EDTA-2NA, urea, menthol, soap essence, soap grain and life activating energy composition. The life activating energy composition consists of sodium silicate, sodium aluminate, sodium oxide, sodium thiosulfate, germanium dioxide, potassium carbonate, glucose, white sugar, gold nitrate and silver thiosulfate. The health toilet soap has the health effects of sterilizing, bacteriostasis, resisting senility and cleaning skin.
Description
Technical Field
The invention relates to a skin-care washing product, in particular to a health-care perfumed soap and a preparation method thereof.
Background
Perfumed soaps as washing products havea long history and are mainly used for decontamination, cleaning, hand washing, face washing and bath. Some perfumed soaps with emphasized functions are on the market in recent years, but most of them have single functions (such as sulfur soap, bath soap and the like), and some of them have potential damage effects on skin cuticle and deep cells after long-term use.
Disclosure of Invention
In view of the above problems, the present invention aims to provide a health soap which has no side effect on human body, can clean skin and can recover skin, and a preparation method thereof.
The technical scheme of the invention is as follows:
the health-care perfumed soap comprises soap granules, traditional Chinese medicines and a life activation energy compound, and is prepared from the following components in parts by weight:
1-5 parts of ganoderma lucidum powder, 1-5 parts of propolis, 0.5-5 parts of lanolin, 0.1-0.8 part of titanium dioxide, 5-10 parts of urea, 0.1-0.8 part of EDTA-2Na0.1, 1-5 parts of menthol, 1-4 parts of soap essence, 70-90 parts of soap granules and 0.5-2.0 parts of a life activation energy compound;
wherein the composition by weight of the living body activation energy complex is:
7.0-10.0 g of sodium silicate, 0.5-2.0 g of sodium aluminate, 2.0-4.0 g of sodium oxide, 0.5-1.5 g of sodium thiosulfate, 2.0-4.0 g of germanium dioxide, 0.5-1.5 g of potassium carbonate, 2.5-5.0 g of glucose (purity 85-99.5%), 8.0-15.0 g of white sugar (purity 85-99%), 1010ml of gold nitrate with concentration of 6.5-10.4 g/L and 60-65 mml of silver thiosulfate with concentration of 29.68-48.24 g/L;
the living body activation energy compound is prepared by the following method:
1) preparation of solution 1
Taking 7.0-10.0 g of sodium silicate, 0.5-2.0 g of sodium aluminate, 2.0-4.0 g of sodium oxide, 0.5-1.5 g of sodium thiosulfate, 2.0-4.0 g of germanium dioxide, 0.5-1.5 g of potassium carbonate, 2.5-5.0 g of glucose (purity 85% -99.5%) and 8.0-15.0 g of white sugar (purity 85% -99%), respectively dissolving the raw materials in 200ml of purified water at 20-40 ℃, and then mixing the solutions together to obtain a solution 1; wherein; taking only the supernatant of the germanium dioxide solution;
2) preparation of solution 2
Adding 5.0-8.0 g of gold ore powder into a crucible, and heating to 1100 ℃ to melt the gold ore powder; adding the molten gold into 1000ml of purified water, stirring the mixture evenly, adding 10ml of nitric acid into the mixture, and forming a yellowish gold nitrate solution, namely solution 2, in the prepared mixed solution at the temperature of 40-50 ℃;
3) preparation of solution 3
Dissolving 2.0-3.0 g of silver nitrate in 10-15 ml of purified water at normal temperature, and dissolving 3.0-4.0 g of sodium chloride in 50ml of purified water; mixing the two solutions to generate white silver chloride precipitate, separating the precipitate, washing with purified water for 3 times, and adding 2 parts of water, 3 parts of the precipitate and 4g of sodium thiosulfate into the separated silver chloride; heating the mixture at 30-40 ℃ for 25-35 minutes while stirring to fully dissolve silver chloride to obtain a colorless and tasteless silver thiosulfate solution, namely solution 3;
4) mixing the solution 1, the solution 2 and the solution 3, and standing at room temperature for more than 72 hours to obtain a transparent colorless liquid living body activation energy compound.
The health soap is prepared by the following steps:
1) weighing the components of the soap, crushing the ganoderma lucidum powder, the propolis, the urea and the menthol into fine powder, and sieving the fine powder by a sieve with more than 100 meshes for later use;
2) diluting the living body activation energy compound into colorless, tasteless and transparent liquid at a ratio of 1: 200-500 for later use;
3) putting 50-60 ℃ vacuum-dried soap particles (with water content of 1.0-12.5% and fatty acid content of more than 65-85%) (see fine chemical handbook, edited by Zhou academic Master of Zhou Xue Kong.), adding Ganoderma powder, molten lanolin (JSCI-II), titanium dioxide (GB-2440-91), propolis (see Shenqi propolis therapy edited by Liu Fuhai), menthol, soap essence (QB1507-92) and life activation energy compound, continuously stirring (no less than 30 minutes), grinding (35-45 ℃), pressing into bars (with soap particle temperature of 35-55 ℃ and water content of 10.5-12.5%), and blocking to obtain 5-180 g toilet soap.
The invention has the following advantages:
1. the formula of the invention adopts ganoderma lucidum powder (ganoderma lucidum spore powder prepared by adopting a special wall breaking technology). The ganoderma lucidum powder contains various microelements such as double-stranded ribonucleic acid, ergosterol, organic germanium and polysaccharide, and has the unique effects of improving the immunologic function of a human body, increasing the SOD (superoxide dismutase) generation amount of the human body, eliminating free radicals, regulating endocrine, improving the closure degree of cell membranes, improving the physiological function of cells, protecting cell tissues from being damaged by the free radicals, inducing the generation of interferon, resisting virus and the like.
2. The formula of the invention adopts propolis which contains multiple amino acids such as VB1, VPP, VA protogen, enzyme and polysaccharide and more than 20 precious trace elements including potassium, zinc, iron, phosphorus, cobalt, chromium, manganese, selenium, titanium, zirconium, strontium and the like; 38 elements necessary for living of organisms, and 34 elements in the propolis.
3. Propolis has broad-spectrum antibacterial effect. It can inhibit and kill more than 100 kinds of bacteria, fungous virus and protozoa. It also has effects in promoting organism epidemic prevention, improving blood circulation, promoting granulation growth, promoting wound healing, moistening, relieving itching, deodorizing, and preventing sunburn.
4. The invention comprehensively utilizes the effective components of the ganoderma lucidum powder and the propolis and the special effects of the compound of the activation energy of the living body (wherein the special effects of the ganoderma lucidum powder and the propolis are firstly applied to perfumed soaps and washing products), and the invention has the effects of skin health care, chapping prevention, pruritus resistance, freckle removal, wrinkle removal, acne removal, skin activity recovery, prevention and killing of harmful microorganisms (bacteria, viruses and mites) on the surface layer and the deep layer, improves the microcirculation of skin tissues, strengthens the nutrient balance between skin cells and soft tissues and promotes the metabolism between skin cells and tissues.
5. The active energy complex of living body in active ion state prepared by the present invention has stronger radioactivity than that of powdered bioceramic far infrared prepared by the conventional process, because atoms for radiating far infrared, such as gold, silver and silicon, exist in active ion state for more effectively radiating far infrared.
6. Since the living body-activating energy complex prepared by the present invention is coated or impregnated in a liquid (aqueous form) into various products, it can be uniformly absorbed into or coated on the surface of the products, making the products more effective in emitting far infrared rays.
7. The silver ion living body activation energy compound prepared by the invention can slowly release oxygen, so that the heat resistance, flexibility and wear resistance of the product can be enhanced.
8. The compound prepared by the invention does not freeze even if the activation energy of the living body is at the temperature of 15 ℃ below zero, is colorless and tasteless, and always keeps radioactivity, does not decompose and does not denature.
9. The compound of living body activation energy prepared by the invention can be only used in vitro, can also directly act on skin and in vivo, and can be dispersed in various carriers, and has good adhesive strength and adhesive rate.
10. The compound has the functions of ultraviolet resistance and deodorization, and can enhance the immune function, hematopoietic function, anti-tumor function and anti-apoptosis function of human bodies, decompose harmful substances, regulate internal secretion, reduce blood sugar and blood fat (kill viruses such as HTV, HBV, HCV and the like in vitro) and have the functions of disinfection and sterilization because the basic side ions generate kinetic energy.
11. The far infrared ray is one kind of electromagnetic wave, and after being absorbed by human body, the far infrared ray can make water molecule in body produce resonance and increase internal energy of molecule (ii) a The energy of the energy comes from far infrared photons (4e) emitted by an anionic base substance, so that biological macromolecules such as protein and the like can be activated, and biological cells are in high-level vibration dynamics; because the biological cells generate resonance effect, far infrared photon energy can be transmitted to a deeper part of the skin of a human body, the temperature of the deep part of the skin rises, and the generated heat is emitted from inside to outside; the strength of the action makes capillary vessel dilate, promotes blood circulation, strengthens metabolism among tissues, increases regeneration capacity of the tissues and improves immunity of the organism.
Detailed Description
Example 1
Taking 70g of soap granules, 5g of lanolin, 5g of ganoderma lucidum powder, 5g of propolis, 10g of urea, 5g of menthol, 4g of soap essence, 0.8g of titanium dioxide, 0.8g of EDTA-2Na and a life activation energy compound: 1.0 g;
pulverizing Ganoderma powder, propolis, urea, and Mentholum (oven dried at low temperature) into fine powder, sieving with 100 mesh sieve, placing soap granules dried at 50 deg.C under vacuum into batch mixer, adding melted lanolin, titanium dioxide, EDTA-2Na, urea, Ganoderma powder, propolis, Mentholum, soap essence, and living body activation energy compound, stirring continuously (30 min), grinding (35 deg.C), pressing into bar (the soap granule temperature is 35 deg.C, water content is 10.5%), and making into soap blocks of 80 g.
Example 2
Taking 90g of soap particles, 0.5g of lanolin, 1g of ganoderma lucidum powder, 1g of propolis, 5g of urea, 1g of menthol, 1g of soap essence, 0.1g of titanium dioxide, 0.1g of EDTA-2Na0.1g and 1.0g of a life activation energy compound;
pulverizing Ganoderma powder, propolis, urea, and Mentholum into fine powder, sieving with 100 mesh sieve, collecting 55 deg.C vacuum dried soap granules, placing into batch mixer, adding melted lanolin, titanium dioxide, EDTA-2Na, urea, Ganoderma powder, propolis, Mentholum, essence, and living body activation energy compound, stirring (35 min), grinding (40 deg.C), pressing (soap granule temperature 55 deg.C, water content 11.5%, and making into 125g soap block.
Example 3
Taking 85g of soap granules, 3.0g of lanolin, 3g of ganoderma lucidum powder, 3g of propolis, 7g of urea, 3g of menthol, 2g of soap essence, 0.4g of titanium dioxide, 0.4g of EDTA-2Na and 1.0g of a life activation energy compound;
pulverizing Ganoderma powder, propolis, urea, and Mentholum into fine powder, sieving with 100 mesh sieve, adding 60 deg.C vacuum dried soap granules into batch mixer, adding melted lanolin, titanium dioxide, EDTA-2Na, urea, Ganoderma powder, propolis, Mentholum, essence, and compound of living body activation energy, stirring (40 min), grinding (45 deg.C), pressing into blocks (soap granule temperature 55 deg.C, water content 12.5%), and making into 100g soap.
The health-care perfumed soap prepared by the embodiment can be used for skin care, chapping prevention, spot removal, wrinkle removal, acne removal, pruritus prevention and microorganism (bacteria, viruses and mites) prevention and killing besides being used as a hand washing, face washing and bathing product.
The soap product can be in any form of solid, powder, liquid, paste, milk or lotion.
Example 4
Preparation of a living body activation energy complex:
1) preparation of solution 1
Taking 7.0g of sodium silicate, 0.5g of sodium aluminate, 2.0g of sodium oxide, 0.5g of sodium thiosulfate, 2.0g of germanium dioxide, 0.5g of potassium carbonate, 2.5g of glucose (purity 85%) and 8.0g of white sugar (purity 85%), respectively dissolving the components in 200ml of purified water at 25 ℃, mixing the solutions together, and taking only supernatant of the germanium dioxide solution to obtain a solution 1;
2) preparation of solution 2
5.0g of gold ore powder was charged into a crucible and heated to 1100 ℃ to melt it. Adding the molten gold into 800ml of purified water, stirring the mixture evenly, putting the mixture into a large beaker, adding 8ml of nitric acid into the beaker, and forming a yellowish gold nitrate solution by the prepared mixed solution at 40 ℃ to obtain a solution 2;
3) preparation of solution 3
2.0g of silver nitrate was dissolved in 10ml of purified water and 3.0g of sodium chloride was dissolved in 50ml of purified water at room temperature. When the above two solutions were mixed together, a white silver chloride precipitate appeared, the precipitate was separated, washed with purified water 3 times, and 2 parts of water, 3 parts of the precipitate and 3.0g of sodium thiosulfate were added to the separated silver chloride. Heating the mixture at 30 deg.C for 25 min while stirring to dissolve silver chloride completely to obtain a colorless and odorless silver thiosulfate solution, to obtain solution 3;
4) the solution 1, the solution 2 and the solution 3 are mixed evenly and placed for more than 72 hours at normal temperature to prepare a transparent colorless liquid living body activation energy compound.
Example 5
Preparation of a living body activation energy complex:
1) preparation of solution 1
Taking 8.5g of sodium silicate, 1.0g ofsodium aluminate, 3.0g of sodium oxide, 1.0g of sodium thiosulfate, 3.0g of germanium dioxide, 1.0g of potassium carbonate, 3.5g of glucose (with the purity of more than 90%) and 11.0g of white sugar (with the purity of more than 90%), respectively dissolving the components in 200ml of purified water at the temperature of 35 ℃, mixing the solutions together, and only taking the supernatant of the germanium dioxide solution to obtain a solution 1;
2) preparation of solution 2
6.5g of gold ore powder was charged into a crucible and heated to 1150 ℃ to melt it. Adding the molten gold into 1000ml of purified water, stirring the mixture evenly, putting the mixture into a large beaker, adding 9ml of nitric acid into the beaker, and forming a yellowish gold nitrate solution by the prepared mixed solution at 45 ℃ to obtain a solution 2;
3) preparation of solution 3
2.5g of silver nitrate was dissolved in 12.5ml of purified water and 3.5g of sodium chloride was dissolved in 50ml of purified water at room temperature. When the two solutions were mixed together, a white silver chloride precipitate appeared, the precipitate was separated, washed with purified water 3 times, and 2 parts of water, 3 parts of the precipitate and 3.5g of sodium thiosulfate were added to the separated silver chloride. Heating the mixture at 35 deg.C for 30 min while stirring to dissolve silver chloride completely to obtain a colorless and odorless silver thiosulfate solution, to obtain solution 3;
(4) the solution 1, the solution 2 and the solution 3 are mixed evenly and placed for more than 72 hours at normal temperature to prepare a transparent colorless liquid living body activation energy compound.
Example 6
Preparation of a living body activation energy complex:
1) preparation of solution 1
Taking 10.0g of sodium silicate, 2.0g of sodium aluminate, 4.0g of sodium oxide, 1.5g of sodium thiosulfate, 4.0g of germanium dioxide, 1.5g of potassium carbonate, 5.0g (purity 99.5%) of glucose and 15.0g (purity 99%) of white sugar as raw materials, respectively dissolving the components in 200ml of purified water at 40 ℃, mixing the solutions together, and only taking supernatant of the germanium dioxide solution to obtain a solution 1;
2) preparation of solution 2
8.0g of gold ore powder was charged into a crucible and heated to 1180 ℃ to melt it. Adding the molten gold into 1200ml of purified water, stirring the mixture evenly, putting the mixture into a large beaker, adding 10ml of nitric acid into the beaker, and forming a yellowish chloroauric acid solution from the prepared mixed solution at 50 ℃ to obtain a solution 2;
3) preparation of solution 3
3.0g of silver nitrate was dissolved in 15ml of purified water and 4.0g of sodium chloride was dissolved in 50ml of purified water at room temperature. When the above two solutions were mixed together, a white silver chloride precipitate appeared, the precipitate was separated, washed with purified water 3 times, and 2 parts of water, 3 parts of the precipitate and 4.0g of sodium thiosulfate were added to the separated silver chloride. Heating the mixture at 40 deg.C for 35 min while stirring to dissolve silver chloride completely to obtain a colorless and odorless silver thiosulfate solution, to obtain solution 3;
4) the solution 1, the solution 2 and the solution 3 are mixed evenly and placed for more than 72 hours at normal temperature to prepare a transparent colorless liquid living body activation energy compound.
Performance determination of the living body activation energy complex:
A. far infrared ray radioactivity and radiation intensity:
polyester synthetic fibers, which are commonly used as a liner of pants, were immersed in the liquid obtained in example 4 above for 60 seconds, dried and then measured by a JIT-E500 apparatus under the conditions: the resolution was 1/6cm, and the integral number was 20. MCT indicator, temperature 35 ℃; as a result, the emission intensity was 68.5 to 80% at a wavelength of 4.0 to 6.0 μm and exceeded 80% at a wavelength of 8.0 μm.
B. Antibacterial effect
100ml of the liquid obtained in example 4 above was mixed with 20L of purified water, and a wool fibre with a diameter of 30cm x 30cm was soaked for 60 seconds, dried and tested in the presence of staphylococcus aureus at 25 ℃ and showed a reduction in viable microbial biomass of 76.8% within 24 hours.
C. Ultraviolet ray blocking experiment
The instrument is a UV spectrometer, and the result shows that the average blocking rate of the instrument is 98% at the wavelength of 200-400 mu m and 84% at the wavelength of 300-400 mu m, which are harmful to human bodies.
D. Antistatic experiment
The instrument is KSK0555, B method; relative humidity at 20 ℃ of 65%, the polyester synthetic fibers were soaked for 60 seconds with the liquid from example 4 above and compared with untreated fibers, and the results of rubbing were:
friction voltage (V) | Static reduction (%) | |
Untreated cotton specimen | 520 | 0 |
Treated cotton specimen | 18 | 96.5 |
Claims (5)
1. A health soap is characterized in that: the composition is prepared from the following components in parts by weight:
1-5 parts of ganoderma lucidum powder, 1-5 parts of propolis, 0.5-5 parts of lanolin, 0.1-0.8 part of titanium dioxide, 0.1-0.8 part of EDTA-2NA, 5-10 parts of urea, 1-5 parts of menthol, 1-4 parts of soap essence, 70-90 parts of soap granules and 0.5-2.0 parts of a life activation energy compound;
wherein the composition by weight of the living body activation energy complex is:
7.0-10.0 g of sodium silicate, 0.5-2.0 g of sodium aluminate, 2.0-4.0 g of sodium oxide, 0.5-1.5 g of sodium thiosulfate, 2.0-4.0 g of germanium dioxide, 0.5-1.5 g of potassium carbonate, 2.5-5.0 g of glucose with the purity of 85-99.5%, 8.0-15.0 g of white sugar with the purity of 85-99%, 1010ml of gold nitrate with the concentration of 6.5-10.4 g/L and 60-65 ml of silver thiosulfate with the concentration of 29.68-48.24 g/L.
2. The health soap as claimed in claim 1, wherein: the toilet soap product is in a solid state, a powder state, a liquid state, a paste, a milk or a dew.
3. A method for preparing a health soap according to claim 1, which comprises: the health soap is prepared by the following steps:
1) weighing the components of the soap according to the weight, crushing the ganoderma lucidum powder, the propolis, the urea and the menthol into fine powder, and sieving the fine powder by a sieve of more than 100 meshes for later use;
2) diluting the living body activation energy compound into colorless, tasteless and transparent liquid at a ratio of 1: 200-500 for later use;
3) adding ganoderma lucidum powder, melted lanolin, titanium dioxide, propolis, menthol, soap essence and a life activation energy compound into soap granules with the water content of 1.0-12.5% and the fatty acid content of more than 65-85% under stirring, continuously stirring for no less than 30 minutes, grinding, pressing into bars, and forming into blocks to obtain the fancy soaps with various weights.
4. A living body activation energy complex, comprising: the composition is prepared from the following components in parts by weight: 7.0-10.0 g of sodium silicate, 0.5-2.0 g of sodium aluminate, 2.0-4.0 g of sodium oxide, 0.5-1.5 g of sodium thiosulfate, 2.0-4.0 g of germanium dioxide, 0.5-1.5 g of potassium carbonate, 2.5-5.0 g of glucose with the purity of 85-99.5%, 8.0-15.0 g of white sugar with the purity of 85-99%, 1010ml of gold nitrate with the concentration of 6.5-10.4 g/L and 60-65 ml of silver thiosulfate with the concentration of 29.68-48.24 g/L.
5. A method for preparing the living body activationenergy complex of claim 4, comprising the following steps:
1) preparation of solution 1
Taking 7.0-10.0 g of sodium silicate, 0.5-2.0 g of sodium aluminate, 2.0-4.0 g of sodium oxide, 0.5-1.5 g of sodium thiosulfate, 2.0-4.0 g of germanium dioxide, 0.5-1.5 g of potassium carbonate, 2.5-5.0 g of glucose with the purity of 85-99.5% and 8.0-15.0 g of white sugar with the purity of 85% and 99% as raw materials, respectively dissolving the raw materials in 200ml of purified water at the temperature of 20-40 ℃, mixing the solutions together, and only taking supernatant of the germanium dioxide solution to obtain a solution 1;
2) preparation of solution 2
5.0-8.0 g of gold ore powder is added into a crucible and heated to 1100 ℃ to be melted. Adding the molten gold into 1000ml of purified water, stirring, adding 10ml of nitric acid into the purified water, and forming a yellowish gold nitrate solution in the prepared mixed solution at the temperature of 40-50 ℃ to obtain a solution 2;
3) preparation of solution 3
Dissolving 2.0-3.0 g of silver nitrate in 10-15 ml of purified water at normal temperature, and dissolving 3.0-4.0 g of sodium chloride in 50ml of purified water; separating the precipitate, washing, and adding 2 parts of water, 3 parts of the precipitate and 4g of sodium thiosulfate into the separated silver chloride; heating the mixture at 30-40 ℃ for 25-35 minutes while stirring to fully dissolve silver chloride to obtain a colorless and tasteless silver thiosulfate solution 3;
4) the solution 1, the solution 2 and the solution 3 are mixed evenly and placed for more than 72 hours at normal temperature to prepare a transparent colorless liquid living body activation energy compound.
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CN 02144833 CN1261557C (en) | 2002-11-15 | 2002-11-15 | Health caring fancy soap and preparing method thereof |
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CN 02144833 CN1261557C (en) | 2002-11-15 | 2002-11-15 | Health caring fancy soap and preparing method thereof |
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CN1261557C CN1261557C (en) | 2006-06-28 |
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Cited By (8)
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CN102504984A (en) * | 2011-11-01 | 2012-06-20 | 包头市红卫日用化工有限公司 | Dual-color synthetic soap and preparation method thereof |
CN103371182A (en) * | 2012-04-13 | 2013-10-30 | 上海维来新材料有限公司 | Double-complexing nanosilver polymer liquid antibacterial agent and preparation method thereof |
CN103409252A (en) * | 2013-08-21 | 2013-11-27 | 烟台九州燃油燃气节能科技有限公司 | Germanium-enriched frosted essential oil soap |
CN103820250A (en) * | 2014-02-23 | 2014-05-28 | 谭俊昌 | Skin care soap containing Spina Gleditsiae and Mythic Fungus, and its making method |
CN104312795A (en) * | 2014-10-31 | 2015-01-28 | 无锡优创生物科技有限公司 | Refreshing soap |
CN104312796A (en) * | 2014-10-31 | 2015-01-28 | 无锡优创生物科技有限公司 | Preparation method of soap for refreshing |
JP2016516861A (en) * | 2013-04-16 | 2016-06-09 | ユニリーバー・ナームローゼ・ベンノートシヤープ | Bar soap with improved antibacterial activity |
CN107638430A (en) * | 2017-09-30 | 2018-01-30 | 李明玉 | Organochlorine Pesticide Residues treatment fluid and preparation method thereof |
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2002
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Cited By (9)
Publication number | Priority date | Publication date | Assignee | Title |
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CN102504984A (en) * | 2011-11-01 | 2012-06-20 | 包头市红卫日用化工有限公司 | Dual-color synthetic soap and preparation method thereof |
CN103371182A (en) * | 2012-04-13 | 2013-10-30 | 上海维来新材料有限公司 | Double-complexing nanosilver polymer liquid antibacterial agent and preparation method thereof |
JP2016516861A (en) * | 2013-04-16 | 2016-06-09 | ユニリーバー・ナームローゼ・ベンノートシヤープ | Bar soap with improved antibacterial activity |
US10370622B2 (en) | 2013-04-16 | 2019-08-06 | Conopco, Inc. | Soap bar having enhanced antibacterial activity |
CN103409252A (en) * | 2013-08-21 | 2013-11-27 | 烟台九州燃油燃气节能科技有限公司 | Germanium-enriched frosted essential oil soap |
CN103820250A (en) * | 2014-02-23 | 2014-05-28 | 谭俊昌 | Skin care soap containing Spina Gleditsiae and Mythic Fungus, and its making method |
CN104312795A (en) * | 2014-10-31 | 2015-01-28 | 无锡优创生物科技有限公司 | Refreshing soap |
CN104312796A (en) * | 2014-10-31 | 2015-01-28 | 无锡优创生物科技有限公司 | Preparation method of soap for refreshing |
CN107638430A (en) * | 2017-09-30 | 2018-01-30 | 李明玉 | Organochlorine Pesticide Residues treatment fluid and preparation method thereof |
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