CN1252290A - Health preparation of fresh Chinese angelica and its preparation - Google Patents
Health preparation of fresh Chinese angelica and its preparation Download PDFInfo
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- CN1252290A CN1252290A CN 98120496 CN98120496A CN1252290A CN 1252290 A CN1252290 A CN 1252290A CN 98120496 CN98120496 CN 98120496 CN 98120496 A CN98120496 A CN 98120496A CN 1252290 A CN1252290 A CN 1252290A
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- angelicae sinensis
- radix angelicae
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Abstract
Intermediate fresh Chinese angelica preparation is prepared through the following steps: slicing or crushing washed Chinese angelica roots or leafs into coarse grains; soaking the material in organic solvent at the temperature of -4 deg.C to 37 deg.C for 1-30 days; separating the soaked liquid from the dregs; and separating the extract from organic solvent to obtain the intermediate fresh Chinese angelica preparation while recovering organic solvent. The intermediate fresh Chinese angelica preparation may be further produced into skin-care article and medical health article by adding some supplementary materials. The intermediate fresh Chinese angelica preparation has medical health function greatly superior to the traditional dry Chinese angelica product.
Description
The present invention relates to a kind of skin care (cosmetic) articles for use and medication health article that is classified as primary raw material of working as with aquatic foods.Specifically, providing a kind of intermediate preparation compatibility adjuvant that extracts with bright Radix Angelicae Sinensis makes and has skin and medical treatment articles for use with health role.
Radix Angelicae Sinensis is a Chinese crude drug commonly used in the Chinese medicinal formulae.Traditional Chinese medicine angelica all is the smoke-dried beancurd goods, behind the ripe results of the annual the beginning of October Radix Angelicae Sinensis angelica root, remove earth, dry in the air to half-dried, then two seasons of autumn and winter slowly smoke-dried beancurd make smoke-dried beancurd Radix Angelicae Sinensis medical material.But contained low boiling volatile component (volatile oil) is smoked in the process at Radix Angelicae Sinensis and has nearly all been volatilized in Radix Angelicae Sinensis, and these low boiling volatile components are effective ingredient of the medicine done important in the Radix Angelicae Sinensis.Therefore, traditional Radix Angelicae Sinensis Chinese crude drug essence is only to contain high boiling point volatile oil and other effective ingredient.But the present invention is through a large amount of clinical trial certificates, contains the Radix Angelicae Sinensis that the treatment of Radix Angelicae Sinensis of low boiling volatile oil and health-care effect will be much better than only to contain after the smoke-dried beancurd high boiling point volatile oil and other compositions.
For the Radix Angelicae Sinensis oil goods, normally water steam distillation dry product Radix Angelicae Sinensis or Folium Angelicae Sinensis.Its processing temperature height, and yield is low, and the cost height be difficult for being extracted because of the higher volatile oil component simultaneously, thereby the contained volatile oil component of Radix Angelicae Sinensis oil that this distillation is produced is incomplete, does not particularly contain low boiling volatile oil part.Thereby its therapeuticing and health effect is limited.
The purpose of this invention is to provide a kind of bright Radix Angelicae Sinensis intermediate preparation, is that effective ingredient is aided with other batchings and makes bright Chinese angelica root health preparation and health care goods with this aquatic foods Radix Angelicae Sinensis intermediate preparation.These products contain effective low boiling volatile oil and high boiling point volatile oil and fatty oil in the Radix Angelicae Sinensis, reach other compositions.The medical health care products that more common smoke-dried beancurd product Radix Angelicae Sinensis is made has higher curative effect and health-care effect.
The used raw material of bright angelica sinensis preparations of the present invention is to adopt sophisticated fresh and alive angelica root and at the withered as yet bright Folium Angelicae Sinensis in Radix Angelicae Sinensis period of maturation.Bright angelica sinensis preparations of the present invention is to make by following step:
1. getting bright angelica root and/or leaf cleans back section (thick 1-8mm) or is ground into coarse grain (1-10mm
3) material;
2. use organic solvent, at temperature-4～37 ℃ 1～30 day material of following immersion;
3. isolate the Radix Angelicae Sinensis material after soaking, obtain the organic solvent soak;
4. the organic solvent soak that obtains through step 3 can be directly as bright Radix Angelicae Sinensis intermediate preparation, or Radix Angelicae Sinensis extractum in organic soak is separated with organic solvent, reclaims organic solvent, obtains the bright Radix Angelicae Sinensis oil as bright Radix Angelicae Sinensis intermediate preparation.
In above-mentioned preparation method, but the organic solvent working concentration is ethanol, acetone, ethyl acetate, dichloromethane, the chloroform equal solvent of 10-98%.The use amount of organic solvent gets final product for soaking raw material.Too much organic solvent helps extracting Radix Angelicae Sinensis effective ingredient volatile oil and fatty oil, but is unfavorable for Recovery of Organic Solvent.And the very few effective ingredient that influences in the Radix Angelicae Sinensis raw material of the use amount of organic solvent is extracted fully, therefore, generally by volume is 1～3 times of raw material.Carried out under 1～26 ℃ 1～20 day and soak to be preferably in.
In the preparation of the bright bright angelica sinensis preparations of the present invention, if adopt ethanol to make organic solvent, then the bubble of the organic solvent after organic solvent soaks Radix Angelicae Sinensis liquid can directly use as bright Radix Angelicae Sinensis intermediate preparation.At this moment can save the Separation and Recovery step of organic solvent.
In addition, when in above-mentioned preparation process 4, carrying out the Separation and Recovery organic solvent, can under reduced pressure carry out, be beneficial to Recovery of Organic Solvent for preventing that Radix Angelicae Sinensis volatile oil runs off.These all routinely the separation method of organic solvent carry out.
With the bright angelica sinensis preparations of method for preparing, other adjuvant of compatibility can be mixed with bright Chinese angelica root health preparation of the present invention.These health preparations can be made the skin care articles for use, the treatment and health medicine that also can be made into enriches blood invigorates blood circulation and improve liver, renal function.
Below by embodiment technology of the present invention is given to illustrate in further detail.
The preparation (1) of embodiment 1 bright Radix Angelicae Sinensis intermediate preparation
Get and clean bright angelica root 500g and be cut into about 3mm sheet, put into 1500ml concentration and be in 38% the ethanol (edible ethanol), 15～20 ℃ of airtight immersions 10 days down, immersion process stirring in per 5～6 hours once.Isolate the Radix Angelicae Sinensis raw material and obtain clarifying soak with ethanol liquid through soaking after-filtration, promptly make and contain the Radix Angelicae Sinensis effective ingredient and be not less than the aquatic foods of 2 weight (as follows) % when middle preparation (1).
The preparation (2) of embodiment 2 bright Radix Angelicae Sinensis intermediate preparation
The bright Radix Angelicae Sinensis 500g that is cut into the 1.5mm sheet that gets with embodiment 1 puts in the 1000ml dichloromethane, soaks 5 days under 10～15 ℃ of following airtight conditions, separates the Radix Angelicae Sinensis residue, gets the dichloromethane soak.The decompression separation dichloromethane, bright Radix Angelicae Sinensis volatile oil, for effective ingredient greater than 75% bright Radix Angelicae Sinensis intermediate preparation (2).
The preparation (3) of embodiment 3 bright Radix Angelicae Sinensis intermediate preparation
Get bright Folium Angelicae Sinensis 2000g and pulverize that extruding leaches fiber and residue gets bright Folium Angelicae Sinensis liquid.Gained liquid 500ml is put among the chloroform 200ml, stir, airtight immersion is after 3 days under 15～20 ℃, bright Folium Angelicae Sinensis liquid is separated with chloroform, and the reclaim under reduced pressure chloroform gets volatile oil, with 95% washing with alcohol extract, separate residue, decompression separation ethanol again must contain effective composition greater than 65% bright Radix Angelicae Sinensis intermediate preparation (3).
The preparation (4) of embodiment 4 bright Radix Angelicae Sinensis intermediate preparation
Get with the bright Radix Angelicae Sinensis 300g of the chopping of embodiment 1 and with the serosity 200g of embodiment 3 by embodiment 3 described methods, make and contain effective composition greater than 70% bright Radix Angelicae Sinensis intermediate preparation (4).
The preparation of embodiment 5 bright Radix Angelicae Sinensis skin care water
With the bright Radix Angelicae Sinensis intermediate preparation (1) that embodiment 1 makes, the compatibility Chinese medicine extraction with other adjuvant, be deployed into transparency liquid and promptly get bright Radix Angelicae Sinensis skin care water.One of its concrete prescription is:
Bright Radix Angelicae Sinensis intermediate preparation (1): 250ml (being equivalent to Radix Angelicae Sinensis effective ingredient 5g approximately);
Radix Ginseng extractive solution: 100ml;
Radix Angelicae Dahuricae extracting solution: 100ml;
Glycerol: 20g;
Spice: an amount of; Add distilled water and obtain product to 1000ml.
The preparation of the available embodiment of bright Radix Angelicae Sinensis intermediate preparation (1) (2)～(4) replaces in the above-mentioned bright Radix Angelicae Sinensis skin care water, makes to contain in the Radix Angelicae Sinensis effective ingredient (1000ml) to be no less than 5g.For the benefit of bright Radix Angelicae Sinensis volatile oil dissolving adds a little ethanol and will add other adjuvant again after the bright Radix Angelicae Sinensis volatile oil dissolving earlier when preparation.
If producing liquid, senior natural perfume material of adding and Lac regis apis can make bright Radix Angelicae Sinensis beauty wash and the beautiful skin water of bright Radix Angelicae Sinensis royal jelly in the bright Radix Angelicae Sinensis skin care water.
Embodiment 6 bright Radix Angelicae Sinensis cleansing milk
The senior detergent of bright Radix Angelicae Sinensis intermediate preparation (3) compatibility, spice that embodiment 3 is made are made viscid Emulsion and are promptly got bright Radix Angelicae Sinensis cleansing milk.One of its concrete prescription is:
Preparation (3): 3g (being equivalent to Radix Angelicae Sinensis effective ingredient 2g) is returned in the bright centre of working as;
Laurel acidic group sodium sulfate: 4.8g;
Laurel acidic group thioether: 4.0g;
Fatty acid distribution of coconut oil diethylamide: 4.0g
Spice: an amount of; Add distilled water and obtain product to 100g.
The bright angelica sinensis preparations compatibility detergent that makes with the present invention, spice etc. also can obtain containing other articless for washing of bright Radix Angelicae Sinensis, carry out the effect that bathing all can be received skin care with this product.Be used for this class articles for use Radix Angelicae Sinensis content of effective more preferably greater than 1%.
Detergent and adjuvant that bright Radix Angelicae Sinensis intermediate preparation compatibility adapts also can be made into bright Radix Angelicae Sinensis shampoo and bright Radix Angelicae Sinensis fancy soap.
Embodiment 7 bright Radix Angelicae Sinensis freckle-removing creams
Bright Radix Angelicae Sinensis intermediate preparation (2) the compatibility adjuvant that embodiment 2 is made is made cream and is promptly got bright Radix Angelicae Sinensis freckle-removing cream.One of its concrete prescription is:
Preparation (2): 4g (being equivalent to Radix Angelicae Sinensis effective ingredient 3g) is returned in the bright centre of working as;
Semen Myristicae acid isopropyl ester: 15g
Stearic acid: 5g
Hexadecylic acid: 5g
Arlacel-60: 2.5g
Tween 80: 1.3g
Antiseptic: an amount of
Spice: an amount of; Add distilled water and obtain product to 100g.
Return the preparation compatibility adjuvant can obtain bright Radix Angelicae Sinensis freckle-removing cream with aquatic foods of the present invention when the centre, its bright Radix Angelicae Sinensis content of effective should be greater than 3%, and obtained product can be got tangible clinical effectiveness.
The sun-proof fragrant white lead of embodiment 8 bright Radix Angelicae Sinensis
Bright Radix Angelicae Sinensis intermediate preparation (4) compatibility plant UV absorbent and filler that embodiment 4 is made can be that one of concrete prescription of the sun-proof fragrant white lead of bright Radix Angelicae Sinensis is:
Bright angelica sinensis preparations (4): 2.6g (being equivalent to Radix Angelicae Sinensis effective ingredient 2g);
Plant ultraviolet absorbent: 0.3g
Interior bean hat isopropyl propionate: 1.1g
Squalane: 1.2g
Titanium dioxide powder: 26.8g
Mica powder: 36.0g
Spice: an amount of; Add distilled water and obtain product to 100g.
When preparing with the sun-proof fragrant white lead of above-mentioned bright Radix Angelicae Sinensis, available bright Radix Angelicae Sinensis intermediate preparation of the present invention (1), (2) or (3) replace intermediate preparation (4), and the Radix Angelicae Sinensis effective ingredient should be greater than 2% in the prepared sun-proof powder.
Embodiment 9 bright Radix Angelicae Sinensis volatile oil soft gelatin capsules
With embodiment 2 made bright Radix Angelicae Sinensis intermediate preparation (2) add ethanol (95%) make with extra care bright Radix Angelicae Sinensis refined volatile oil.This volatile oil contains bright Radix Angelicae Sinensis effective ingredient greater than 85%.With this refining bright Radix Angelicae Sinensis volatile oil, make the soft gelatin capsule that living ball contains bright Radix Angelicae Sinensis effective ingredient 0.05～0.2g by system fish liver oil capsule and technical process, promptly get bright Radix Angelicae Sinensis volatile oil soft gelatin capsule of the present invention.
Embodiment 10 bright Radix Angelicae Sinensis Fructus Hippophae electuaries
With embodiment 3 prepared bright angelica sinensis preparations (3), adjuvants such as bright Fructus Hippophae condensed cream of compatibility and sucrose after making with extra care once more with ethanol, technology can make bright Radix Angelicae Sinensis Fructus Hippophae electuary routinely, contains the Radix Angelicae Sinensis effective ingredient more than 3% in this electuary approximately.Rare system more than 10 times after, get final product drinkable bright Radix Angelicae Sinensis Oral Liquid Fructus Hippophae.
In the foregoing description 5～10, except that bright Radix Angelicae Sinensis intermediate preparation (1)～(4) that bright Radix Angelicae Sinensis intermediate preparation employing embodiment 1～4 is produced, all technology and condition are carried out routinely for compatibility adjuvant among each embodiment and preparation method.Only require to make the amount that contains the Radix Angelicae Sinensis effective ingredient that is necessary in the goods, just can receive ideal health care and therapeutic effect.Further specify effect of the present invention below by clinical practice.
1. " bright Radix Angelicae Sinensis skin care water " is to the skin effect of wrinkled skin
Wash one's hands at every turn, behind the face, taking advantage of and wetly can make the face and the hands of rimose in 3～6 days, reach the natural, ecological of softness delicacy with bright wet being coated with bright Radix Angelicae Sinensis skin care water.Particularly bright Radix Angelicae Sinensis skin care water also has good especially effect to the crowfoot cracks of intractable foot.Be coated with the dead bark at the bottom of this product rear foot, washed off by water logging especially easily.Every day foot is embathed super wet being coated with in back and use once bright Radix Angelicae Sinensis skin care water, just can make the thick keratinization dead bark of sole skin of obstinate crowfoot cracks in 3～8 days.Washed the capable person by water logging, and recover soft intact normal condition.
After, foot bath in 1～7 day once is coated with once bright Radix Angelicae Sinensis skin care water after whenever washing, dry and wear socks again, impels the dead bark of keratinization, constantly separates with normal skin timely, is come off and embathe at any time smoothly, makes the sole skin, keeps normal ecological thin thickness.The skin of the foot of obstinate crowfoot cracks can not be made like this,, just normal ecology can be kept forever as long as moisten down the uninterrupted of bright Radix Angelicae Sinensis skin care water.
Be coated with bright Radix Angelicae Sinensis skin care water and the reference substance that is coated with the identical adjuvant made from smoke-dried beancurd product Radix Angelicae Sinensis " skin water ", the skin effect contrast of the obstinate crowfoot cracks of foot is seen Table 1
Table 1 is coated with the contrast table of bright Radix Angelicae Sinensis skin care water to foot crowfoot cracks effect
| Grouping | Number on probation | Be coated with crowfoot cracks in 12 days and finish the healing number | Be coated with 12 days healing rates (%) |
| Bright Radix Angelicae Sinensis skin care water group | ??66 | 56 | ?84.8 |
| " skin water " group of dried Radix Angelicae Sinensis | ??32 | 6 | ?18.7 |
2. the disappear effect of senile plaque of bright Radix Angelicae Sinensis freckle-removing cream
" the bright Radix Angelicae Sinensis freckle-removing cream " produced with bright Radix Angelicae Sinensis is coated on the senile plaque skin, senile plaque disappeared or the effect of coming off in 1-2 month; But " the Radix Angelicae Sinensis cream " with the identical adjuvant of traditional smoke-dried beancurd product Radix Angelicae Sinensis compatibility is made then do not produce the senile plaque effect of disappearing.See Table 2
The bright Radix Angelicae Sinensis freckle-removing cream of the table 2 senile plaque effect table that disappears
| Grouping | Be coated with the number of using | Be coated with the time (my god) | Number takes effect | Effective percentage (%) |
| Bright Radix Angelicae Sinensis freckle-removing cream | 28 | 30 | 17 | 60.7 |
| Dried Radix Angelicae Sinensis " cream " group | 12 | 30 | 0 | - |
By the statistical result of above-mentioned clinical trial as can be known, variously contain bright Radix Angelicae Sinensis goods and have good health protection and therapeutic effect by what bright angelica sinensis preparations of the present invention institute compatibility obtained.
Claims (9)
1. bright Radix Angelicae Sinensis intermediate preparation is characterized in that prepared according to the following steps:
(1) gets and cut thick 1～8mm sheet or be ground into coarse grain 1～10mm after bright angelica root is cleaned
3Material, or bright Folium Angelicae Sinensis squeezed out the juice material;
(2) use organic solvent, at temperature-4～37 ℃ 1～30 day material of following immersion;
(3) isolate the Radix Angelicae Sinensis material after the immersion, obtain the organic solvent soak;
(4) Radix Angelicae Sinensis extractum in organic soak is separated with organic solvent, reclaim organic solvent, obtain bright Radix Angelicae Sinensis intermediate preparation.
2. according to the described bright Radix Angelicae Sinensis intermediate preparation of claim 1, it is characterized in that organic solvent used in the preparation process is ethanol, acetone, ethyl acetate, dichloromethane or chloroform.
3. according to the described bright angelica sinensis preparations of claim 1, it is characterized in that in the preparation process with concentration being 10～98% ethanol, and when using ethanol as organic solvent, isolating the organic solvent soak that the Radix Angelicae Sinensis material obtains after the immersion, directly is bright Radix Angelicae Sinensis intermediate preparation.
4. bright Radix Angelicae Sinensis skin care water it is characterized in that being is main effective ingredient by the described bright Radix Angelicae Sinensis intermediate preparation of claim 1, and bright Radix Angelicae Sinensis effective ingredient is no less than 5g in 1000ml.
5. bright Radix Angelicae Sinensis cleansing milk it is characterized in that being is main effective ingredient by the described bright Radix Angelicae Sinensis intermediate preparation of claim 1, and the Radix Angelicae Sinensis active constituent content is greater than 1 weight %.
6. bright Radix Angelicae Sinensis freckle-removing cream it is characterized in that being is main effective ingredient by the described bright Radix Angelicae Sinensis intermediate preparation of claim 1, and the Radix Angelicae Sinensis active constituent content is greater than 3 weight %.
7. sun-proof fragrant white lead of bright Radix Angelicae Sinensis it is characterized in that being is main effective ingredient by the described bright Radix Angelicae Sinensis intermediate preparation of claim 1, and the Radix Angelicae Sinensis active constituent content is greater than 2 weight %.
8. bright Radix Angelicae Sinensis volatile oil soft gelatin capsule is characterized in that being is main effective ingredient by the described bright Radix Angelicae Sinensis intermediate preparation of claim 1, and to contain the Radix Angelicae Sinensis effective ingredient among every ball 2g be 0.05-0.2g.
9. bright Radix Angelicae Sinensis Fructus Hippophae electuary it is characterized in that being is main effective ingredient by the described bright Radix Angelicae Sinensis intermediate preparation of claim 1, and the Radix Angelicae Sinensis active constituent content is greater than 3 weight %.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN98120496A CN1081929C (en) | 1998-10-28 | 1998-10-28 | Health preparation of fresh Chinese angelica and its preparation |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN98120496A CN1081929C (en) | 1998-10-28 | 1998-10-28 | Health preparation of fresh Chinese angelica and its preparation |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1252290A true CN1252290A (en) | 2000-05-10 |
| CN1081929C CN1081929C (en) | 2002-04-03 |
Family
ID=5226774
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN98120496A Expired - Lifetime CN1081929C (en) | 1998-10-28 | 1998-10-28 | Health preparation of fresh Chinese angelica and its preparation |
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| Country | Link |
|---|---|
| CN (1) | CN1081929C (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102144677A (en) * | 2011-04-06 | 2011-08-10 | 中国药文化研究会 | Angelica sinensis health care oil, preparation method and application of angelica sinensis health care oil |
| CN102764220A (en) * | 2012-08-10 | 2012-11-07 | 启东市通洋机电有限公司 | Chinese medicinal herb facial cleanser |
| CN105248456A (en) * | 2015-11-30 | 2016-01-20 | 南京中医药大学 | Traditional Chinese medicine extract having Ditylenchus destructor Thorne resisting activity and application thereof |
| CN109464321A (en) * | 2018-11-12 | 2019-03-15 | 江苏千药堂国医研究院有限公司 | A kind of traditional Chinese medicine extract composition and application |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1014025B (en) * | 1987-12-22 | 1991-09-25 | 金珍玉 | Manufacturing method of voltile oil containing 50% chinese angelica |
-
1998
- 1998-10-28 CN CN98120496A patent/CN1081929C/en not_active Expired - Lifetime
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102144677A (en) * | 2011-04-06 | 2011-08-10 | 中国药文化研究会 | Angelica sinensis health care oil, preparation method and application of angelica sinensis health care oil |
| CN102764220A (en) * | 2012-08-10 | 2012-11-07 | 启东市通洋机电有限公司 | Chinese medicinal herb facial cleanser |
| CN105248456A (en) * | 2015-11-30 | 2016-01-20 | 南京中医药大学 | Traditional Chinese medicine extract having Ditylenchus destructor Thorne resisting activity and application thereof |
| CN109464321A (en) * | 2018-11-12 | 2019-03-15 | 江苏千药堂国医研究院有限公司 | A kind of traditional Chinese medicine extract composition and application |
Also Published As
| Publication number | Publication date |
|---|---|
| CN1081929C (en) | 2002-04-03 |
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