CN1239434C - 类质同像合成的磷酸铵钾固溶体复合肥料及其制备方法 - Google Patents
类质同像合成的磷酸铵钾固溶体复合肥料及其制备方法 Download PDFInfo
- Publication number
- CN1239434C CN1239434C CN 200410073243 CN200410073243A CN1239434C CN 1239434 C CN1239434 C CN 1239434C CN 200410073243 CN200410073243 CN 200410073243 CN 200410073243 A CN200410073243 A CN 200410073243A CN 1239434 C CN1239434 C CN 1239434C
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- CN
- China
- Prior art keywords
- ammonium
- phosphate
- potassium
- isomorphically
- potassium phosphate
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
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- KYAXVUURGCWDJW-UHFFFAOYSA-N [K].P(=O)(O)(O)[O-].[NH4+] Chemical compound [K].P(=O)(O)(O)[O-].[NH4+] KYAXVUURGCWDJW-UHFFFAOYSA-N 0.000 title claims abstract description 21
- 239000003337 fertilizer Substances 0.000 title abstract description 16
- 239000006104 solid solution Substances 0.000 title abstract 4
- 238000000034 method Methods 0.000 title description 14
- 239000002131 composite material Substances 0.000 title 1
- 150000001875 compounds Chemical class 0.000 claims abstract description 23
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 claims abstract description 13
- 239000011591 potassium Substances 0.000 claims abstract description 13
- 229910052700 potassium Inorganic materials 0.000 claims abstract description 13
- 239000000243 solution Substances 0.000 claims abstract description 8
- 238000002360 preparation method Methods 0.000 claims abstract description 7
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 20
- 210000003608 fece Anatomy 0.000 claims description 17
- 239000010871 livestock manure Substances 0.000 claims description 17
- 238000002425 crystallisation Methods 0.000 claims description 13
- 230000008025 crystallization Effects 0.000 claims description 13
- 229910019142 PO4 Inorganic materials 0.000 claims description 12
- LFVGISIMTYGQHF-UHFFFAOYSA-N ammonium dihydrogen phosphate Chemical compound [NH4+].OP(O)([O-])=O LFVGISIMTYGQHF-UHFFFAOYSA-N 0.000 claims description 12
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 claims description 12
- 239000010452 phosphate Substances 0.000 claims description 12
- 239000000126 substance Substances 0.000 claims description 12
- 239000013078 crystal Substances 0.000 claims description 10
- 238000002156 mixing Methods 0.000 claims description 6
- 239000000203 mixture Substances 0.000 claims description 6
- 238000003756 stirring Methods 0.000 claims description 6
- 238000010438 heat treatment Methods 0.000 claims description 5
- 239000012452 mother liquor Substances 0.000 claims description 5
- INQZXVMNJLSCGI-UHFFFAOYSA-M azanium;potassium;hydrogen phosphate Chemical compound [NH4+].[K+].OP([O-])([O-])=O INQZXVMNJLSCGI-UHFFFAOYSA-M 0.000 claims description 4
- 239000000284 extract Substances 0.000 claims description 4
- 239000011259 mixed solution Substances 0.000 claims description 4
- 239000002826 coolant Substances 0.000 claims description 3
- 239000000463 material Substances 0.000 claims description 3
- 238000005303 weighing Methods 0.000 claims description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 abstract description 4
- 235000015097 nutrients Nutrition 0.000 abstract description 4
- 230000001965 increasing effect Effects 0.000 abstract description 3
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 abstract description 2
- 229910052757 nitrogen Inorganic materials 0.000 abstract description 2
- 229910052698 phosphorus Inorganic materials 0.000 abstract description 2
- 239000011574 phosphorus Substances 0.000 abstract description 2
- 235000016709 nutrition Nutrition 0.000 abstract 2
- 230000035764 nutrition Effects 0.000 abstract 2
- 239000007836 KH2PO4 Substances 0.000 abstract 1
- 230000002349 favourable effect Effects 0.000 abstract 1
- 229910000402 monopotassium phosphate Inorganic materials 0.000 abstract 1
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 6
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 4
- GNTDGMZSJNCJKK-UHFFFAOYSA-N divanadium pentaoxide Chemical compound O=[V](=O)O[V](=O)=O GNTDGMZSJNCJKK-UHFFFAOYSA-N 0.000 description 4
- 238000005516 engineering process Methods 0.000 description 4
- 238000004519 manufacturing process Methods 0.000 description 4
- 239000000047 product Substances 0.000 description 4
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 3
- WCUXLLCKKVVCTQ-UHFFFAOYSA-M Potassium chloride Chemical compound [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 description 3
- 229910000147 aluminium phosphate Inorganic materials 0.000 description 3
- 230000004720 fertilization Effects 0.000 description 3
- 150000002500 ions Chemical class 0.000 description 3
- 238000000926 separation method Methods 0.000 description 3
- 238000004176 ammonification Methods 0.000 description 2
- RKTYLMNFRDHKIL-UHFFFAOYSA-N copper;5,10,15,20-tetraphenylporphyrin-22,24-diide Chemical compound [Cu+2].C1=CC(C(=C2C=CC([N-]2)=C(C=2C=CC=CC=2)C=2C=CC(N=2)=C(C=2C=CC=CC=2)C2=CC=C3[N-]2)C=2C=CC=CC=2)=NC1=C3C1=CC=CC=C1 RKTYLMNFRDHKIL-UHFFFAOYSA-N 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 235000021050 feed intake Nutrition 0.000 description 2
- QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 description 2
- 235000021049 nutrient content Nutrition 0.000 description 2
- CHKVPAROMQMJNQ-UHFFFAOYSA-M potassium bisulfate Chemical compound [K+].OS([O-])(=O)=O CHKVPAROMQMJNQ-UHFFFAOYSA-M 0.000 description 2
- CHWRSCGUEQEHOH-UHFFFAOYSA-N potassium oxide Chemical compound [O-2].[K+].[K+] CHWRSCGUEQEHOH-UHFFFAOYSA-N 0.000 description 2
- 229910001950 potassium oxide Inorganic materials 0.000 description 2
- 239000012047 saturated solution Substances 0.000 description 2
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- WZLMXYBCAZZIRQ-UHFFFAOYSA-N [N].[P].[K] Chemical compound [N].[P].[K] WZLMXYBCAZZIRQ-UHFFFAOYSA-N 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 150000001450 anions Chemical class 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 238000001311 chemical methods and process Methods 0.000 description 1
- 238000005285 chemical preparation method Methods 0.000 description 1
- 238000002288 cocrystallisation Methods 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000005755 formation reaction Methods 0.000 description 1
- 239000013505 freshwater Substances 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 238000005469 granulation Methods 0.000 description 1
- 230000003179 granulation Effects 0.000 description 1
- IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 description 1
- 229910000041 hydrogen chloride Inorganic materials 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 230000035800 maturation Effects 0.000 description 1
- 230000000050 nutritive effect Effects 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 239000002367 phosphate rock Substances 0.000 description 1
- PJNZPQUBCPKICU-UHFFFAOYSA-N phosphoric acid;potassium Chemical compound [K].OP(O)(O)=O PJNZPQUBCPKICU-UHFFFAOYSA-N 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
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- Fertilizers (AREA)
Abstract
Description
Claims (5)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN 200410073243 CN1239434C (zh) | 2004-11-08 | 2004-11-08 | 类质同像合成的磷酸铵钾固溶体复合肥料及其制备方法 |
Applications Claiming Priority (1)
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CN 200410073243 CN1239434C (zh) | 2004-11-08 | 2004-11-08 | 类质同像合成的磷酸铵钾固溶体复合肥料及其制备方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN1609062A CN1609062A (zh) | 2005-04-27 |
CN1239434C true CN1239434C (zh) | 2006-02-01 |
Family
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CN 200410073243 Expired - Fee Related CN1239434C (zh) | 2004-11-08 | 2004-11-08 | 类质同像合成的磷酸铵钾固溶体复合肥料及其制备方法 |
Country Status (1)
Country | Link |
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CN (1) | CN1239434C (zh) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
TWI453177B (zh) * | 2007-12-03 | 2014-09-21 | Rotem Amfert Negev Ltd | 以磷酸鉀為基的化合物之製備 |
Families Citing this family (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102320587A (zh) * | 2011-09-14 | 2012-01-18 | 潍坊维源绿色农业科技有限公司 | 磷酸铵钾的制备方法 |
CN110894170A (zh) * | 2018-09-12 | 2020-03-20 | 四川大学 | 碳酸氢铵混晶及其制备方法 |
-
2004
- 2004-11-08 CN CN 200410073243 patent/CN1239434C/zh not_active Expired - Fee Related
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
TWI453177B (zh) * | 2007-12-03 | 2014-09-21 | Rotem Amfert Negev Ltd | 以磷酸鉀為基的化合物之製備 |
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Publication number | Publication date |
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CN1609062A (zh) | 2005-04-27 |
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SE01 | Entry into force of request for substantive examination | ||
C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
ASS | Succession or assignment of patent right |
Owner name: XI'AN JUCHUAN INTERNATIONAL INVESTMENT CO.,LTD. Free format text: FORMER OWNER: SHANXI JUCHUAN FUWANJIA CO., LTD. Effective date: 20091023 |
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Effective date of registration: 20091023 Address after: No. 23, unity South Road, hi tech Zone, Shaanxi, Xi'an Patentee after: Xi'an Juchuan International Investment Co., Ltd. Address before: Xi'an, Shaanxi hi tech Industrial Development Zone, unity South Road, No. 23 (Headquarters) Patentee before: Shaanxi Ju Chuan Fu Wan Jia Stock Company, Ltd. |
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C56 | Change in the name or address of the patentee |
Owner name: XI'AN TONGZE INVESTMENT CO., LTD. Free format text: FORMER NAME: XI'AN JUCHUAN INTERNATIONAL INVESTMENT CO., LTD. |
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CP03 | Change of name, title or address |
Address after: 23 No. 710075, unity South Road, hi tech Industrial Development Zone, Shaanxi, Xi'an Patentee after: Xi'an Tongze Investment Co. Ltd. Address before: 710075, No. 23, unity South Road, hi tech Zone, Shaanxi, Xi'an Patentee before: Xi'an Juchuan International Investment Co., Ltd. |
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CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20060201 Termination date: 20181108 |
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CF01 | Termination of patent right due to non-payment of annual fee |