CN1186113C - 半干式电晕放电烟气净化方法及装置 - Google Patents
半干式电晕放电烟气净化方法及装置 Download PDFInfo
- Publication number
- CN1186113C CN1186113C CNB021101426A CN02110142A CN1186113C CN 1186113 C CN1186113 C CN 1186113C CN B021101426 A CNB021101426 A CN B021101426A CN 02110142 A CN02110142 A CN 02110142A CN 1186113 C CN1186113 C CN 1186113C
- Authority
- CN
- China
- Prior art keywords
- corona discharge
- flue gas
- ammonium salt
- pole plate
- fume
- Prior art date
Links
- 238000004140 cleaning Methods 0.000 title claims abstract description 12
- 238000001035 drying Methods 0.000 title claims description 13
- 238000000034 methods Methods 0.000 title description 7
- 239000000047 products Substances 0.000 claims abstract description 30
- 150000003863 ammonium salts Chemical class 0.000 claims abstract description 20
- 238000001694 spray drying Methods 0.000 claims abstract description 16
- QGZKDVFQNNGYKY-UHFFFAOYSA-N ammonia Chemical compound data:image/svg+xml;base64,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 data:image/svg+xml;base64,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 N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims abstract description 10
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- 239000003546 flue gases Substances 0.000 claims description 40
- UGFAIRIUMAVXCW-UHFFFAOYSA-N carbon monoxide Chemical compound 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- 230000035695 Efflux Effects 0.000 description 1
- PDCNZSPWVGYKGD-UHFFFAOYSA-O [NH4+].[S+2] Chemical compound 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[NH4+].[S+2] PDCNZSPWVGYKGD-UHFFFAOYSA-O 0.000 description 1
- 239000000443 aerosols Substances 0.000 description 1
- 238000003915 air pollution Methods 0.000 description 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N carbon Chemical compound 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Classifications
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Abstract
本发明提供了一种半干式电晕放电烟气净化方法及装置。将含有SO2和NOX的高温烟气引入喷雾干燥塔内增湿降温，然后引入电晕放电烟气净化器，施加高电压，并加入氨气，发生电晕流光放电，产生强氧化性自由基，自由基引发的化学反应将SO2和NOX转化为固体铵盐颗粒，并从烟气中分离出来，收集在极板(或管)上，净化后的洁净烟气经烟囱排放。向电晕放电净化器供水，在极板(或管)上形成水膜，清洗反应产物，清洗液循环使用。将清洗产物溶液喷入喷雾干燥塔，在使烟气增湿降温的同时，蒸发干燥形成较大的铵盐颗粒，加以回收。
Description
技术领域
本发明涉及一种电晕放电净化烟气中SO2和NOX的方法和装置。
背景技术
随着经济的发展，煤和石油等矿物燃料消耗急剧增加，其燃烧产生的SO2、NOX等造成了严重的大气污染，人们一直在不断探索技术更先进、更经济的脱除方法。80年代，人们提出了脉冲电晕放电低温等离子体烟气净化技术，2001年第9届全国电除尘学术会及第1届全国脱硫学术会论文“脉冲电晕等离子体烟气脱硫工业中试装置”介绍了一种脉冲放电烟气脱硫技术方案，整个工艺过程为干式，采用ns级窄脉冲供电，施加电压高，电晕能耗较高。另外，由于产物颗粒细小，烟气又进行了增湿，在电晕放电反应器和产物收集电除尘中易造成极板粘结现象，影响反应器和产物收集电除尘的供电，降低脱硫、脱硝和产物收集效果，甚至使烟气净化系统不能连续稳定运行。
发明内容
本发明的目的就是提供一种提高脱硫效率、降低能耗、解决产物粘结问题的电晕放电净化烟气SO2和NOX的方法及装置。
本发明解决其技术问题采用的技术方案是发明了一种半干式电晕放电烟气净化方法，利用氨喷射和高压电晕放电、喷雾干燥，将SO2和NOX转化为铵盐，并加以回收，用做化肥。包括以下步骤：将烟气引入增湿降温喷雾干燥塔，使烟气冷却到烟气饱和绝热温度至80℃之间，烟气湿度增加到5～15％范围之内；增湿降温后的烟气进入电晕放电烟气净化器，同时加入氨气，施加上直流叠加交流、高频或脉冲高电压，发生电晕流光放电，在烟气氛围中形成低温等离子体，产生强氧化性自由基O、OH、HO2等，这些自由基引发的反应，在有氨参与的条件下，将SO2和NOX最终转化为微米级的固体铵盐颗粒，依靠静电捕集作用，将铵盐颗粒从气流中分离出来，收集到极板上，净化后的烟气经烟囱排放；给电晕放电烟气净化器极板供水，在极板上形成水膜，清洗收集到的反应产物铵盐，清洗液从净化器底部流入贮液槽，循环使用；抽取一部分产物铵盐溶液喷入增湿降温喷雾干燥塔，一方面水分蒸发用于烟气增湿降温，同时液滴蒸发干燥形成较大的固体铵盐颗粒，加以回收。
实现上述方法的一种半干式电晕放电烟气净化装置，包括一个增湿降温喷雾干燥塔和由烟道相连接的电晕放电烟气净化器。增湿降温喷雾干燥塔将SO2和NOX净化产物铵盐溶液分散为雾滴，同时由干燥塔顶部旋转引入烟气，雾滴与烟气混合发生传质传热过程，蒸发结晶成30～120μm的固体颗粒，随气流旋转过程中在惯性分离和重力作用下，从干燥塔底部分离出来。在产物溶液雾滴蒸发干燥的同时，使烟气增湿降温。产物溶液的雾化，可以采用压力式雾化器，也可以采用旋转式雾化器，或气流式雾化器。
电晕放电烟气净化器具有发生脱硫脱硝化学反应和收集反应产物双重作用。将经过增湿降温的烟气引入净化器，由加氨系统加入氨气，同时施加高电压，在电晕放电氧化和氨气协同作用下，将SO2和NOX转化为铵盐气溶胶颗粒，产物颗粒被电晕放电产生的离子荷电，在静电力作用下，被收集到极板上，从而实现烟气净化。电极结构可以采用线—板式，也可以采用线—筒式。供电可以采用直流、直流叠加交流、高频、脉冲等高压电源，在电晕放电净化器下面布置一个贮液槽，有一供液泵从中抽取溶液经管道送至安装在电晕放电净化器上部的布水器，布水器有喷嘴或溢流槽向电晕放电净化器极板供水，在极板表面形成水膜，清洗极板上收集的反应产物铵盐，清洗液从电晕放电烟气净化器底部流入贮液槽，循环使用。供液泵将一部分产物溶液送至增湿降温喷雾干燥塔作为烟气增湿降温介质，同时完成反应产物蒸发干燥，造粒回收。
本发明的有益效果是：脱硫脱硝和产物收集相结合，节省专门的产物收集过程及装置；采用湿式水膜清洗产物，可提高脉冲放电脱硫、脱硝中的异相反应作用；SO2、NOX和NH3在电晕风作用下，随气流向极板移动，溶于水膜，进一步发生脱除反应；解决了产物粘结问题；反应器极板、极线清洁，供电系统运行稳定，放电状况良好；产物收集效率高，可以减小净化装置尺寸；减少氨和产物铵盐外排，避免产生二次污染；在产物溶液喷雾干燥过程中，雾滴与烟气传质效果好，氧气和SO2、NOX可进入雾滴液膜中，氧气溶解有利于将产物中的亚硫酸铵转化为硫铵，稳定产物，同时也可发生直接的脱硫、脱硝化学反应。综上所述，本发明提供的脱硫、脱硝方法，可提高净化效率，减少能耗，提高运行可靠性。在经济指标上，可缩小净化装置尺寸，降低供电级别，减少电源成本，从而降低脱硫投资和运行成本。
附图说明
附图1是本发明技术方案的流程图，其中，1为增湿降温喷雾干燥塔，2为喷雾干燥塔供液泵，3为加氨喷嘴，4为补水管路，5为贮液槽，6为电晕放电烟气净化器，7为净化器供液泵。
附图2是湿式水膜清洗产物循环系统示意图，其中，8为管道，9为形成水膜的布水器，10为电晕放电净化器极板。
具体实施案例下面结合附图，对本发明实施技术方案做进一步描述。
含有SO2和NOX的高温烟气从顶部入口进入增湿降温喷雾干燥塔(1)，采用压力雾化方式喷入雾化液滴，使烟气温度降至60～80℃，湿度增加至10％左右。然后烟气进入电晕放电烟气净化器(6)，净化器有4个电场，采用线板式结构，同极间距300mm，在净化器入口，由加氨喷嘴(3)按NH3与SO2化学计量比略低于1∶1加入氨气，净化器(6)前两个电场施加ns级100～125kV脉冲高电压，后两个电场施加器加上50～70kV直流电压，发生脉冲电晕放电，将SO2和NOX转化为铵盐颗粒，并捕集下来，净化后的洁净烟气经烟囱排入大气。在电晕放电净化器下面设置贮液槽(5)，供液泵(7)将其中的水经管道(8)抽至设在净化器上部的布水器(9)，布水器(9)的喷嘴向极板喷雾，在极板(10)上形成水膜，水膜向下流动，产物溶解到水膜中，随水膜流入贮液槽(5)，清洗液用供液泵(7)再打到电晕放电净化器(6)上，循环使用。干燥塔供液泵(2)从贮液槽(5)中抽取部分产物清洗液送至增湿降温喷雾干燥塔(1)，雾化蒸发干燥，形成较大的铵盐产物颗粒，从干燥塔底部取出，用做化肥。
Claims (2)
1.一种半干式电晕放电烟气净化方法，包括以下步骤：A.将高温烟气引入增湿降温喷雾干燥塔，将烟气温度降至饱和绝热温度至80℃之间，烟气湿度增至5～15％；B.将增湿降温后的烟气引入电晕放电烟气净化器，同时加入氨气，施加直流叠加交流、高频或脉冲高电压，发生电晕流光放电，产生强氧化性自由基，自由基引发的反应，将SO2和NOX转化为铵盐，铵盐在静电力的作用下被捕集在极板上；C.向电晕放电净化器极板供水，在极板上形成水膜，清洗极板上收集的铵盐，清洗液从电晕放电净化器底部流入贮液槽，循环使用；D.从贮液槽抽取部分反应产物铵盐溶液，喷入增湿降温喷雾干燥塔，一方面用于烟气增湿降温，同时蒸发干燥，形成较大铵盐颗粒，加以回收。
2.一种实施权利要求1所述方法的装置，它包括一个增湿降温喷雾干燥塔和由烟道相连接的电晕放电烟气净化器，其特征是：电晕放电净化器采用直流叠加交流、高频或脉冲高电压供电，脱硫脱硝的同时捕集产物，在其下面布置一个贮液槽，有一供液泵从中抽取溶液经管道送至安装在电晕放电净化器上部的布水器，布水器喷嘴或溢流槽向电晕放电净化器极板供水，在极板表面形成清洗水膜，清洗极板上收集的反应产物铵盐，清洗液从电晕放电净化器底部流入贮液槽，循环使用。供液泵另有管道接至增湿降温喷雾干燥塔。
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| JP3775417B2 (ja) * | 2004-02-09 | 2006-05-17 | ダイキン工業株式会社 | 放電装置及び空気浄化装置 |
| KR101139217B1 (ko) * | 2011-10-06 | 2012-05-15 | (주)안성정기 | 혼소배출가스 고도처리용 동시복합처리장치 |
| CN102814113A (zh) * | 2012-08-13 | 2012-12-12 | 河南绿源新星环保设备有限公司 | 一种半干式氨法脱硫新工艺 |
| CN105396441B (zh) * | 2015-10-28 | 2017-10-13 | 山西晋浙环保科技有限公司 | 一种低温省煤器和双极性高压流光放电联用烟气净化方法 |
| CN105268309A (zh) * | 2015-12-04 | 2016-01-27 | 杭州杭联热电有限公司 | 一种半干法脉冲等离子体烟气净化系统 |
| CN107233785A (zh) * | 2016-03-29 | 2017-10-10 | 苏州迈沃环保工程有限公司 | 利用超高压低温等离子体进行废气脱硫脱硝的方法及系统 |
| CN105833718B (zh) * | 2016-04-14 | 2019-12-03 | 中国石油大学(北京) | 一种等离子体协同催化剂的脱硝系统及其处理方法 |
| CN106215697A (zh) * | 2016-08-26 | 2016-12-14 | 江苏中圣高科技产业有限公司 | 一种负载离子液体催化剂的氨法联合脱硫脱硝方法及装置 |
| CN111473388A (zh) * | 2018-06-21 | 2020-07-31 | 洪学文 | 一种油烟净化器 |
| CN109821655A (zh) * | 2019-01-29 | 2019-05-31 | 湖南大学 | 一种新型静电除尘装置 |
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