CN117969193A - Jacket needle type convection displacement positive pressure sampling device - Google Patents
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- 238000005070 sampling Methods 0.000 title claims abstract description 430
- 238000006073 displacement reaction Methods 0.000 title claims abstract description 25
- 239000012530 fluid Substances 0.000 claims description 8
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 claims description 5
- 229910052710 silicon Inorganic materials 0.000 claims description 5
- 239000010703 silicon Substances 0.000 claims description 5
- 239000011248 coating agent Substances 0.000 claims description 2
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- 230000009471 action Effects 0.000 abstract description 2
- 239000007789 gas Substances 0.000 description 108
- 101001121408 Homo sapiens L-amino-acid oxidase Proteins 0.000 description 7
- 102100026388 L-amino-acid oxidase Human genes 0.000 description 7
- 101100233916 Saccharomyces cerevisiae (strain ATCC 204508 / S288c) KAR5 gene Proteins 0.000 description 7
- 238000000034 method Methods 0.000 description 6
- 238000004140 cleaning Methods 0.000 description 5
- 238000010586 diagram Methods 0.000 description 4
- 230000000694 effects Effects 0.000 description 4
- 230000008569 process Effects 0.000 description 4
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- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 2
- 230000007547 defect Effects 0.000 description 2
- 238000001514 detection method Methods 0.000 description 2
- 230000014759 maintenance of location Effects 0.000 description 2
- 239000012855 volatile organic compound Substances 0.000 description 2
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 1
- RWSOTUBLDIXVET-UHFFFAOYSA-N Dihydrogen sulfide Chemical compound S RWSOTUBLDIXVET-UHFFFAOYSA-N 0.000 description 1
- 101100012902 Saccharomyces cerevisiae (strain ATCC 204508 / S288c) FIG2 gene Proteins 0.000 description 1
- 229910002092 carbon dioxide Inorganic materials 0.000 description 1
- 239000001569 carbon dioxide Substances 0.000 description 1
- 229910002091 carbon monoxide Inorganic materials 0.000 description 1
- 239000003245 coal Substances 0.000 description 1
- 230000000295 complement effect Effects 0.000 description 1
- 230000002708 enhancing effect Effects 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 238000011010 flushing procedure Methods 0.000 description 1
- 238000004868 gas analysis Methods 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 229910000037 hydrogen sulfide Inorganic materials 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 238000005272 metallurgy Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000002265 prevention Effects 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 231100000331 toxic Toxicity 0.000 description 1
- 230000002588 toxic effect Effects 0.000 description 1
- 238000010407 vacuum cleaning Methods 0.000 description 1
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- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/02—Devices for withdrawing samples
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Abstract
Description
技术领域Technical Field
本发明涉及一种夹套针式对流置换正压采样装置。The invention relates to a jacketed needle type convection displacement positive pressure sampling device.
背景技术Background technique
压罐采样广泛应用于煤矿井下、冶金、隧道工程、炼油厂、环境保护及卫生防疫等领域,以便快速测定现场环境中挥发性有机物(VOCs),有毒有害气体及嗅味气体等(如一氧化碳、二氧化碳、硫化氢)浓度。Pressure tank sampling is widely used in underground coal mines, metallurgy, tunnel engineering, refineries, environmental protection, health and epidemic prevention, etc., in order to quickly determine the concentration of volatile organic compounds (VOCs), toxic and harmful gases and odorous gases (such as carbon monoxide, carbon dioxide, hydrogen sulfide) in the on-site environment.
然而,现有的正压罐采样系统存在诸多缺陷。首先,采样罐的系统设置很难做到实时置换,在气体采样过程中往往只能用加压和抽真空轮流间隔进行,加上采样泵推(压)力有限,多次清洗置换后采样罐内总会有部分残留气体,残留气体的留存将严重影响采样气体的检测精度,且长时间的留存会严重污染采样罐。However, the existing positive pressure tank sampling system has many defects. First, the system setting of the sampling tank is difficult to achieve real-time replacement. During the gas sampling process, it is often only possible to use pressurization and vacuuming alternately. In addition, the sampling pump has limited pushing (pressure) force. After multiple cleaning and replacement, there will always be some residual gas in the sampling tank. The retention of residual gas will seriously affect the detection accuracy of the sampled gas, and long-term retention will seriously pollute the sampling tank.
其次,现有技术中,采样罐虽可进行多次加压抽洗,但抽洗流程往往采用三明治叠加清洗方式,往往无法做到残留气体的完全清除,从而造成后续加压所采气体样品成分的不准确性和干扰,并且采样效率不高,单次采样时间较长,单次采样周期往往达到半小时甚至1小时。Secondly, in the prior art, although the sampling tank can be pressurized and flushed multiple times, the flushing process often adopts a sandwich stacking cleaning method, which often fails to completely remove the residual gas, resulting in inaccuracy and interference in the composition of the gas samples collected by subsequent pressurization. In addition, the sampling efficiency is not high, and the single sampling time is long, with a single sampling cycle often reaching half an hour or even 1 hour.
再次,在正压采样过程中,现有采样泵正压采样流路结构较为复杂,气路部件管路及接口较多,容易漏气受污染,且清洗置换需要频繁手动切换开关阀,导致操作较为复杂。Thirdly, during the positive pressure sampling process, the positive pressure sampling flow path structure of the existing sampling pump is relatively complex, with many gas path components, pipelines and interfaces, which are prone to leakage and contamination, and cleaning and replacement require frequent manual switching of the switch valve, resulting in more complicated operation.
发明内容Summary of the invention
本发明提供一种夹套针式对流置换正压采样装置,有效地解决了现有技术存在的上述缺陷。The present invention provides a jacketed needle type convection displacement positive pressure sampling device, which effectively solves the above-mentioned defects existing in the prior art.
具体而言,本发明提供一种夹套针式对流置换正压采样装置,该装置能够实现置换采样流路和加压采样流路,在所述装置中,连接口经第一管线再经由采样针流体连通至采样罐,该采样罐再经采样针由第二管线后连通至出口,采样泵设置在第一管线或第二管线上,其中,前开关阀设置在第一管线的通路上,后开关阀设置在第二管线的通路上,所述采样针包括内嵌针、外衬管、接口件,内嵌针一端在采样罐的外部与第一管线连通,另一端则伸至采样罐的罐底,接口件环绕于内嵌针并连通于采样罐的顶部开口,外衬管从接口件延伸出来并连通至第二管线,所述装置启动置换采样流路,其中,前开关阀和后开关阀均打开,采样口与连接口固定连接,采样泵将自采样气体泵压入采样口,该采样气体流经第一管线再流经内嵌针后被送至采样罐的罐底,采样气体在采样罐内自下而上形成对流,由此推动采样罐内的原始气体自下而上穿过接口件从外衬管流出,由此,原始气体随同采样气体通过第二管线被吹出出口;随后,所述装置切换成加压采样流路,其中,后开关阀关闭,由此,来自采样口的采样气体输入连接口,该采样气体流经第一管线再流经内嵌针被吹入采样罐,由此在采样罐中进行采样气体的采集累加,采样罐内的采样气体从罐底逐步增进压力升高,当压力增加到特定阈值时,关闭前开关阀。Specifically, the present invention provides a jacketed needle-type convection displacement positive pressure sampling device, which can realize a displacement sampling flow path and a pressurized sampling flow path. In the device, a connecting port is connected to a sampling tank through a first pipeline and then through a sampling needle fluid, and the sampling tank is then connected to an outlet through a second pipeline through the sampling needle. A sampling pump is arranged on the first pipeline or the second pipeline, wherein a front switch valve is arranged on the passage of the first pipeline, and a rear switch valve is arranged on the passage of the second pipeline. The sampling needle comprises an embedded needle, an outer liner, and an interface component. One end of the embedded needle is connected to the first pipeline outside the sampling tank, and the other end extends to the bottom of the sampling tank. The interface component surrounds the embedded needle and is connected to the top opening of the sampling tank. The outer liner extends from the interface component and is connected to the second pipeline. The device starts a displacement sampling flow path, wherein the front switch valve and the rear switch valve are both opened, the sampling port is fixedly connected to the connecting port, the sampling pump presses the self-sampling gas pump into the sampling port, the sampling gas flows through the first pipeline and then through the embedded needle and is sent to the bottom of the sampling tank, the sampling gas forms convection from bottom to top in the sampling tank, thereby pushing the original gas in the sampling tank from bottom to top through the interface part and out of the outer liner, thereby, the original gas is blown out of the outlet through the second pipeline together with the sampling gas; then, the device switches to a pressurized sampling flow path, wherein the rear switch valve is closed, thereby, the sampling gas from the sampling port is input to the connecting port, the sampling gas flows through the first pipeline and then through the embedded needle and is blown into the sampling tank, thereby collecting and accumulating the sampling gas in the sampling tank, the sampling gas in the sampling tank gradually increases in pressure from the bottom of the tank, and when the pressure increases to a specific threshold, the front switch valve is closed.
优选地,所述采样针采用熔融硅惰性化涂覆。Preferably, the sampling needle is inertly coated with molten silicon.
优选地,在第一管线的通路上加装压力表,在加压采样流路的运行过程中,压力表中的读数逐渐增大,一旦压力表中的读数大于特定阈值,则关闭前开关阀促使前开关阀和后开关阀均关闭,由此终止对采样罐的输气。Preferably, a pressure gauge is installed on the passage of the first pipeline. During the operation of the pressurized sampling flow path, the reading in the pressure gauge gradually increases. Once the reading in the pressure gauge is greater than a specific threshold, the front switch valve is closed, causing both the front switch valve and the rear switch valve to close, thereby terminating the gas supply to the sampling tank.
优选地,内嵌针深入到距离采样罐的罐底2-5厘米的位置处。Preferably, the embedded needle is inserted into the sampling tank at a position 2-5 cm from the tank bottom.
本发明还提供一种夹套针式对流置换正压采样装置,该装置能够实现置换采样流路和加压采样流路,在所述装置中,连接口经第一管线再经由第二采样针流体连通至第二采样罐,第二采样针再经由第一采样针联通至第一采样针,第一采样针联通至第一采样罐,第一采样罐再经由第一采样针连通至第二管线,第二管线流体连通至出口,采样泵设置在第一管线或第二管线上,所述第二采样针包括第二内嵌针、第二外衬管、第二接口件,第二内嵌针一端在第二采样罐外部与第一管线连通,另一端则伸至第二采样罐的罐底,第二接口件环绕于第二内嵌针并连通于第二采样罐的顶部开口,第二外衬管从第二接口件延伸出来并连通至第一采样针的第一内嵌针,所述第一采样针包括第一内嵌针、第一外衬管、第一接口件,第一内嵌针一端在第一采样罐外部与第二外衬管连通,另一端则伸至第一采样罐的罐底,第一接口件环绕于第一内嵌针并连通于第一采样罐的顶部开口,第一外衬管从第一接口件延伸出来并连通至第二管线,在第一管线上设置第二前开关阀,在第二采样罐和第一采样罐之间的通路上设置第二后开关阀和第一前开关阀,第二后开关阀相较于第一前开关阀更加靠近第二采样罐,在第二管线上设置第一后开关阀,所述装置启动置换采样流路,其中,第一前开关阀、第一后开关阀、第二前开关阀、第二后开关阀均打开,采样口与连接口固定连接,采样泵将自采样气体泵压入采样口,该采样气体流经第一管线并流经第二内嵌针后被送至第二采样罐的罐底,采样气体在第二采样罐内自下而上形成对流,由此推动第二采样罐内的原始气体自下而上穿过第二接口件从第二外衬管流出,随后,来自第二采样罐的原始气体在采样气体的推动下被推向第一内嵌针,并经过第一内嵌针进入第一采样罐,在第一采样罐的罐底形成自下而上的对流,从而将第二采样罐和第一采样罐中的原始气体均推送经过第一接口件、第一外衬管从而离开第一采样罐,进而沿着第二管线从出口排出,随后,所述装置切换成加压采样流路,其中,将第一后开关阀关闭,采样泵将采样气体泵压入采样口,该采样气体流经第一管线再流经第二内嵌针后被送至第二采样罐的罐底,采样气体在第二采样罐内自下而上形成对流,由此推动第二采样罐内的原始气体自下而上穿过第二接口件从第二外衬管流出,由此在第二采样罐中进行采样气体的采集,然后,第二采样罐内的采样气体从罐底逐步溢至第二内嵌针,进而沿着第二内嵌针流入第一外衬管和第一接口件,进而流入第一采样罐,由此在第一采样罐中也进行采样气体的采集,随后,随着在第一采样罐和第二采样罐中采样气体的采集累加,第一和第二采样罐内的采样气体从罐底逐步增进压力升高,当压力增加到特定阈值时,同时关闭第一前开关阀、第二后开关阀、第二前开关阀。The present invention also provides a jacketed needle-type convection displacement positive pressure sampling device, which can realize a displacement sampling flow path and a pressurized sampling flow path. In the device, the connecting port is connected to the second sampling tank through the first pipeline and then through the second sampling needle fluid, the second sampling needle is then connected to the first sampling needle through the first sampling needle, the first sampling needle is connected to the first sampling tank, the first sampling tank is then connected to the second pipeline through the first sampling needle, the second pipeline fluid is connected to the outlet, the sampling pump is arranged on the first pipeline or the second pipeline, the second sampling needle includes a second embedded needle, a second outer liner, and a second interface component, one end of the second embedded needle is connected to the first pipeline outside the second sampling tank, and the other end extends to the bottom of the second sampling tank, the second interface component surrounds the second embedded needle and is connected to the top opening of the second sampling tank, the second outer liner extends from the second interface component and is connected to The first embedded needle of the first sampling needle, the first sampling needle includes a first embedded needle, a first outer liner, and a first interface component, one end of the first embedded needle is connected to the second outer liner outside the first sampling tank, and the other end extends to the bottom of the first sampling tank, the first interface component surrounds the first embedded needle and is connected to the top opening of the first sampling tank, the first outer liner extends from the first interface component and is connected to the second pipeline, a second front switch valve is arranged on the first pipeline, a second rear switch valve and a first front switch valve are arranged on the passage between the second sampling tank and the first sampling tank, the second rear switch valve is closer to the second sampling tank than the first front switch valve, the first rear switch valve is arranged on the second pipeline, the device starts to replace the sampling flow path, wherein the first front switch valve, the first rear switch valve, the second front switch valve, and the second rear switch valve are all opened, and the sampling port is fixedly connected to the connecting port The sampling pump presses the self-sampling gas pump into the sampling port. The sampling gas flows through the first pipeline and the second embedded needle and is sent to the bottom of the second sampling tank. The sampling gas forms a convection from bottom to top in the second sampling tank, thereby pushing the original gas in the second sampling tank from bottom to top through the second interface and out of the second outer liner. Subsequently, the original gas from the second sampling tank is pushed to the first embedded needle under the push of the sampling gas, and enters the first sampling tank through the first embedded needle, forming a bottom-up convection at the bottom of the first sampling tank, thereby pushing the original gas in the second sampling tank and the first sampling tank through the first interface and the first outer liner to leave the first sampling tank, and then discharged from the outlet along the second pipeline. Subsequently, the device switches to a pressurized sampling flow path, wherein the first rear switch valve is closed, and the sampling pump presses the sampling gas pump into the sampling port. The sampling gas flows through the first pipeline and then through the second embedded needle and is sent to the bottom of the second sampling tank. The sampling gas forms convection from bottom to top in the second sampling tank, thereby pushing the original gas in the second sampling tank from bottom to top through the second interface component and out of the second outer liner tube, thereby collecting the sampling gas in the second sampling tank, and then, the sampling gas in the second sampling tank gradually overflows from the bottom of the tank to the second embedded needle, and then flows along the second embedded needle into the first outer liner tube and the first interface component, and then flows into the first sampling tank, thereby collecting the sampling gas in the first sampling tank, and then, as the sampling gas in the first sampling tank and the second sampling tank is collected cumulatively, the sampling gas in the first and second sampling tanks gradually increases in pressure from the bottom of the tank, and when the pressure increases to a specific threshold, the first front switch valve, the second rear switch valve, and the second front switch valve are closed at the same time.
优选地,所述第一采样针和所述第二采样针采用熔融硅惰性化涂覆。Preferably, the first sampling needle and the second sampling needle are inerted by molten silicon coating.
优选地,在第一管线上加装压力表,随着第一和第二采样罐内逐渐升压,压力表上的读数也逐渐升高,一旦压力表中的读数大于特定阈值,则首先关闭第一前开关阀,完成第一采样罐的气体采样,取出第一采样罐,接着再关闭第二后开关阀和第二前开关阀,完成第二采样罐的气体采样,取出第二采样罐。Preferably, a pressure gauge is installed on the first pipeline. As the pressure in the first and second sampling tanks gradually increases, the reading on the pressure gauge also gradually increases. Once the reading on the pressure gauge is greater than a specific threshold, the first front switch valve is first closed to complete the gas sampling of the first sampling tank and take out the first sampling tank. Then, the second rear switch valve and the second front switch valve are closed to complete the gas sampling of the second sampling tank and take out the second sampling tank.
优选地,第一内嵌针深入到距离第一采样罐的罐底2-5厘米的位置处。Preferably, the first embedded needle penetrates into a position 2-5 cm away from the bottom of the first sampling tank.
优选地,第二内嵌针深入到距离第二采样罐的罐底2-5厘米的位置处。Preferably, the second embedded needle penetrates into a position 2-5 cm away from the bottom of the second sampling tank.
综上,在本发明所提供的夹套针式对流置换正压采样装置,在对采样罐进行气体置换和气体采样时,利用采样针探至采样罐罐底,采样针不仅仅作为气流通道通畅所必不可少的一环,而且巧妙地在采样罐中形成了对流,由此在气体置换阶段通过自下而上的对流作用有效地清除了采样罐中的原始气体,从而有效地对采样罐进行清洁,避免了采样罐受到污染,进一步,在气体采样阶段,采样针的存在可以作为限流缓冲确保气压有序上升而不至于压力瞬间暴涨,由此避免采样罐短时间内承受过大的压力。进一步,采样针还发挥了串联连接的功能,通过采样针的串联连接,有效地将两个及以上采样罐串联起来,从而可以实现两个及以上采样罐在气体置换和气体采样两方面的并行推进和样品备份。In summary, in the jacketed needle type convection displacement positive pressure sampling device provided by the present invention, when performing gas replacement and gas sampling on the sampling tank, the sampling needle is used to probe the bottom of the sampling tank. The sampling needle is not only an indispensable link for the smooth flow of the airflow channel, but also cleverly forms convection in the sampling tank, thereby effectively removing the original gas in the sampling tank through the bottom-up convection effect during the gas replacement stage, thereby effectively cleaning the sampling tank and avoiding contamination of the sampling tank. Further, during the gas sampling stage, the presence of the sampling needle can serve as a current limiting buffer to ensure that the gas pressure rises in an orderly manner without causing an instantaneous pressure surge, thereby avoiding the sampling tank from being subjected to excessive pressure in a short period of time. Furthermore, the sampling needle also plays the role of a series connection. Through the series connection of the sampling needle, two or more sampling tanks are effectively connected in series, so that the parallel advancement and sample backup of two or more sampling tanks in terms of gas replacement and gas sampling can be achieved.
附图说明BRIEF DESCRIPTION OF THE DRAWINGS
为了更清楚地说明本发明实施例或现有技术中的技术方案,以下将对实施例或现有技术描述中所需要使用的附图进行论述,显然,在结合附图进行描述的技术方案仅仅是本发明的一些实施例,对于本领域普通技术人员而言,在不付出创造性劳动的前提下,还可以根据这些附图所示实施例得到其它的实施例及其附图。In order to more clearly illustrate the embodiments of the present invention or the technical solutions in the prior art, the drawings required for use in the embodiments or the description of the prior art will be discussed below. Obviously, the technical solutions described in conjunction with the drawings are only some embodiments of the present invention. For ordinary technicians in this field, other embodiments and their drawings can be obtained based on the embodiments shown in these drawings without paying creative work.
图1示出了根据本发明的夹套针式对流置换正压采样装置的基本结构示意图。FIG1 shows a basic structural schematic diagram of a jacketed needle-type convection displacement positive pressure sampling device according to the present invention.
图2示出了根据本发明的夹套针式对流置换正压采样装置中的采样针的具体构造。FIG. 2 shows the specific structure of the sampling needle in the jacketed needle type convection displacement positive pressure sampling device according to the present invention.
图3示出了根据本发明的夹套针式对流置换正压采样装置中设置两个采样罐的基本结构示意图。FIG3 shows a schematic diagram of the basic structure of two sampling cans arranged in the jacketed needle type convection displacement positive pressure sampling device according to the present invention.
具体实施方式Detailed ways
以下将结合附图对本发明各实施例的技术方案进行清楚完整描述,显然,所描述的实施例仅为本发明的一部分实施例,而不是全部实施例。基于本发明中所述的实施例,本领域普通技术人员在不需要创造性劳动的前提下所得到的所有其它实施例,都在本发明所保护的范围内。The technical solutions of various embodiments of the present invention will be clearly and completely described below in conjunction with the accompanying drawings. Obviously, the described embodiments are only part of the embodiments of the present invention, not all of the embodiments. Based on the embodiments described in the present invention, all other embodiments obtained by ordinary technicians in this field without creative work are within the scope of protection of the present invention.
简而言之,本发明所提供的夹套针式对流置换正压采样装置,可以利用夹套针双腔气路结构和采样泵推(压)力在密闭罐顶部和底部形成压力差,从而让密闭样品罐内部气流快速对流并彻底置换罐瓶体内的残留气体,确保采到的样品特别是背景空气中痕量气体成分的准确性,同时,通过开关阀门和泵的切换,可以实现对罐体的抽真空清洗保存和加压采样保存,增强装置的多功能性及实用性。In short, the jacketed needle convection displacement positive pressure sampling device provided by the present invention can utilize the jacketed needle double-cavity air path structure and the pushing (pressure) force of the sampling pump to form a pressure difference at the top and bottom of the closed tank, thereby allowing the airflow inside the closed sample tank to quickly convect and completely replace the residual gas in the tank body, ensuring the accuracy of the collected samples, especially the trace gas components in the background air. At the same time, by switching the valve and the pump, the vacuum cleaning and pressurized sampling and storage of the tank body can be achieved, enhancing the versatility and practicality of the device.
大体而言,该装置以同一套基本结构并行实现了置换采样流路和加压采样流路,这两个流路在该装置的不同时刻登场,互为逆向又互为补充。下文中,将首先介绍置换采样流路并在此过程中将该装置的大体结构描述清楚。Generally speaking, the device realizes the displacement sampling flow path and the pressurized sampling flow path in parallel with the same basic structure. The two flow paths appear at different times in the device, and are opposite to each other and complement each other. In the following, the displacement sampling flow path will be introduced first and the general structure of the device will be described in the process.
置换采样流路主要作用在于将采样罐以及与采样罐相连的管道中的原始气体“尽可能”排空,从而确保最终采样到的气体正是检测方希望采样到的最大限度反映现场状况的采样气体。对于置换采样流路的介绍,从图1开始。The main function of the replacement sampling flow path is to empty the original gas in the sampling tank and the pipeline connected to the sampling tank "as much as possible", so as to ensure that the gas finally sampled is the sampling gas that the detection party hopes to sample and reflects the on-site conditions to the greatest extent. The introduction of the replacement sampling flow path starts from Figure 1.
图1示出了根据本发明的夹套针式对流置换正压采样装置的基本结构示意图。FIG1 shows a basic structural schematic diagram of a jacketed needle-type convection displacement positive pressure sampling device according to the present invention.
如图1所示,在图1的实施例中由细箭头表示置换采样流路的气体流动方向,在置换采样流路中,采样口通过与之固定的连接口100经第一管线101再经由采样针102流体连通至采样罐103,采样针102再经由第二管线104流体连通至出口105,这其中,在第一管线101中设置采样泵106以控制气流流向。As shown in FIG. 1 , in the embodiment of FIG. 1 , the gas flow direction of the replacement sampling flow path is indicated by a thin arrow. In the replacement sampling flow path, the sampling port is connected to the sampling tank 103 through the first pipeline 101 and then through the sampling needle 102 fluid via the connection port 100 fixed thereto, and the sampling needle 102 is then connected to the outlet 105 through the second pipeline 104 fluid. Among them, a sampling pump 106 is arranged in the first pipeline 101 to control the flow direction of the gas flow.
需要注意的是,采样泵106既可以设置在第一管线101中,也可以设置在第二管线104中。It should be noted that the sampling pump 106 can be disposed in either the first pipeline 101 or the second pipeline 104 .
在置换采样流路的运行时,打开采样泵106将采样口中的采样气体泵推出来,随后流经第一管线101,流过采样针102再流入采样罐103。在采样气体流入采样罐103之后对采样罐103进行气体置换,由此尽可能清除采样罐103内的原始气体。进一步,在采样罐103内,原始气体被采样气体吹送过采样针102再吹入第二管线104直至吹出出口105。When the sampling flow path is replaced, the sampling pump 106 is turned on to pump out the sampled gas in the sampling port, and then the sampled gas flows through the first pipeline 101, flows through the sampling needle 102, and then flows into the sampling tank 103. After the sampled gas flows into the sampling tank 103, the gas in the sampling tank 103 is replaced, thereby removing the original gas in the sampling tank 103 as much as possible. Further, in the sampling tank 103, the original gas is blown by the sampled gas through the sampling needle 102 and then blown into the second pipeline 104 until it is blown out of the outlet 105.
上述置换采样流路的运行,确保了采样罐以及第一和第二管线被彻底清洗,将原始气体的残留量尽可能降低。The operation of the above-mentioned replacement sampling flow path ensures that the sampling tank and the first and second pipelines are thoroughly cleaned, and the residual amount of the original gas is reduced as much as possible.
由上文描述可知,采样针102在置换采样流路运行时使用了两次,即,在采样气体流入采样罐时流经采样针,随后,在原始气体被吹离采样罐时再次流经采样针。As can be seen from the above description, the sampling needle 102 is used twice when the replacement sampling flow path is running, that is, the sample gas flows through the sampling needle when it flows into the sampling tank, and then flows through the sampling needle again when the original gas is blown out of the sampling tank.
为此就需要特别介绍采样针102的构造。图2示出了根据本发明的夹套针式对流置换正压采样装置中的采样针的具体构造。Therefore, it is necessary to introduce the structure of the sampling needle 102. Fig. 2 shows the specific structure of the sampling needle in the jacket needle type convection displacement positive pressure sampling device according to the present invention.
首先需要说明的是,采样针102优选使用熔融硅惰性化涂覆,以增强相关性能。First, it should be noted that the sampling needle 102 is preferably inertly coated with molten silicon to enhance relevant performance.
如图2所示,采样针102包括内嵌针102a、外衬管102b、接口件102c。内嵌针102的一端在采样罐103外部与第一管线101连通,另一端则伸至采样罐103的罐底。接口件102c环绕于内嵌针102a并连通于采样罐103顶部开口。外衬管102b从接口件102c延伸出来并连通至第二管线104。As shown in FIG2 , the sampling needle 102 includes an inner needle 102a, an outer liner 102b, and an interface 102c. One end of the inner needle 102 is connected to the first pipeline 101 outside the sampling tank 103, and the other end extends to the bottom of the sampling tank 103. The interface 102c surrounds the inner needle 102a and is connected to the top opening of the sampling tank 103. The outer liner 102b extends from the interface 102c and is connected to the second pipeline 104.
图1和2中还可见到开关阀108分为前开关阀108a和后开关阀108b,前开关阀108a设置在第一管线101的通路上,后开关阀108b设置在第二管线104的通路上。在置换采样流路运行时,前开关阀108a和后开关阀108b均打开。而在加压采样流路运行时的开关阀108的操作将在后文进行详细介绍。It can also be seen in Figures 1 and 2 that the switch valve 108 is divided into a front switch valve 108a and a rear switch valve 108b, the front switch valve 108a is arranged on the passage of the first pipeline 101, and the rear switch valve 108b is arranged on the passage of the second pipeline 104. When the replacement sampling flow path is in operation, the front switch valve 108a and the rear switch valve 108b are both opened. The operation of the switch valve 108 when the pressurized sampling flow path is in operation will be described in detail later.
基于上文所述的这种结构,在置换采样流路运行时,前后开关阀108a和108b均打开从而不影响流路的畅通,泵推出的采样气体流经第一管线101之后,在内嵌针102a的引导下继续流动,由于内嵌针102a伸至采样罐103的罐底,因此采样气体在内嵌针102a的引导下流入采样罐103的罐底,由此,采样气体就在采样罐103内自下而上形成对流,通过气体对流作用,推动采样罐103内的原始气体自下而上穿过接口件102c从外衬管102b流出,随后,由于外衬管102b与第二管线104连通,因此,从外衬管102b流出的气体将通过第二管线104吹出出口105。Based on the structure described above, when the replacement sampling flow path is running, the front and rear switch valves 108a and 108b are both opened so as not to affect the smooth flow of the flow path. After the sampling gas pushed out by the pump flows through the first pipeline 101, it continues to flow under the guidance of the embedded needle 102a. Since the embedded needle 102a extends to the bottom of the sampling tank 103, the sampling gas flows into the bottom of the sampling tank 103 under the guidance of the embedded needle 102a. As a result, the sampling gas forms convection from bottom to top in the sampling tank 103. Through the effect of gas convection, the original gas in the sampling tank 103 is pushed from bottom to top through the interface 102c and flows out from the outer liner 102b. Subsequently, since the outer liner 102b is connected to the second pipeline 104, the gas flowing out of the outer liner 102b will be blown out of the outlet 105 through the second pipeline 104.
采样针的这一设置对于本发明而言非常重要,如上所述,内嵌针102延伸至罐底,在实际操作中,例如内嵌针深入到距离采样罐的罐底2-5厘米的位置处,通过泵推(压)力的作用,可以快速循环抽离罐体内的所有气体,从而彻底置换气体。This setting of the sampling needle is very important for the present invention. As mentioned above, the embedded needle 102 extends to the bottom of the tank. In actual operation, for example, the embedded needle penetrates into a position 2-5 cm away from the bottom of the sampling tank. Through the action of the pump push (pressure) force, all the gas in the tank can be quickly circulated and extracted, thereby completely replacing the gas.
在置换采样流路的运行完成之后,可快速转至加压采样流路。图1中用粗线箭头表示加压采样流路。在加压采样流路中,首先关闭后开关阀108b,由此在采样罐103中进行采样气体的采集。After the operation of the replacement sampling flow path is completed, the pressurized sampling flow path can be quickly switched. The pressurized sampling flow path is indicated by a bold arrow in Figure 1. In the pressurized sampling flow path, the rear switch valve 108b is first closed, thereby collecting the sample gas in the sampling tank 103.
随着采样罐103内的气压不断增大,采样罐103内的采样气体从罐底逐步递增升压。As the air pressure in the sampling tank 103 continues to increase, the pressure of the sampled gas in the sampling tank 103 gradually increases from the bottom of the tank.
此时,在第一管线101的通路上加装压力表107,尽管此时第二管线104上的后开关阀108b关闭,但由于第一管线101上的前开关阀108a依然打开,因此,第一管线101与采样罐103依然保持连通,因此压力表107上显示的气压仍然能够表征采样罐103中的气压。At this time, a pressure gauge 107 is installed on the passage of the first pipeline 101. Although the rear switch valve 108b on the second pipeline 104 is closed at this time, since the front switch valve 108a on the first pipeline 101 is still open, the first pipeline 101 and the sampling tank 103 are still connected. Therefore, the air pressure displayed on the pressure gauge 107 can still represent the air pressure in the sampling tank 103.
随着采样罐103内的采样气体从罐底逐步递增升压,压力表107的读数也逐渐增大,一旦压力表中的读数大于特定阈值,则关闭前开关阀108a,由此终止对采样罐103的输气。此时,由于前后开关阀均关闭,采样罐103将不再与第一管线101和第二管线104连通,工作人员就可以从容地取走采样罐103供随后采样气体分析之用。As the sample gas in the sampling tank 103 gradually increases in pressure from the bottom of the tank, the reading of the pressure gauge 107 also gradually increases. Once the reading in the pressure gauge is greater than a specific threshold, the front switch valve 108a is closed, thereby terminating the gas supply to the sampling tank 103. At this time, since the front and rear switch valves are closed, the sampling tank 103 will no longer be connected to the first pipeline 101 and the second pipeline 104, and the staff can calmly take away the sampling tank 103 for subsequent sample gas analysis.
图3示出了根据本发明的夹套针式对流置换正压采样装置中设置两个采样罐的基本结构示意图。FIG3 shows a schematic diagram of the basic structure of two sampling cans arranged in the jacketed needle type convection displacement positive pressure sampling device according to the present invention.
如图3所示,采样口固定于连接口100,在置换采样流路的运行时,打开采样泵106将采样口中的采样气体泵推出来,随后流经第一管线101,流过第二采样针202的第二内嵌针202a再流入第二采样罐203。在采样气体流入采样罐203之后对第二采样罐203进行气体置换,由此尽可能清除第二采样罐203内的原始气体。进一步,在第二采样罐203内,原始气体被采样气体吹送过第二采样针202的第二接口件202c和第二外衬管202b。到此为止,配置皆与图1所示实施例类似。As shown in FIG3 , the sampling port is fixed to the connection port 100. When the sampling flow path is replaced, the sampling pump 106 is turned on to pump out the sampled gas in the sampling port, and then the sampled gas flows through the first pipeline 101, flows through the second embedded needle 202a of the second sampling needle 202, and then flows into the second sampling tank 203. After the sampled gas flows into the sampling tank 203, the gas in the second sampling tank 203 is replaced, thereby removing the original gas in the second sampling tank 203 as much as possible. Further, in the second sampling tank 203, the original gas is blown by the sampled gas through the second interface part 202c and the second outer liner 202b of the second sampling needle 202. So far, the configuration is similar to the embodiment shown in FIG1 .
接下来的流路配置则开始与图1所示实施例不同。在图3中,第二外衬管202b将不直接与第二管线104连通,其气流向第一采样罐103连通。具体而言,第一采样罐103配对设置第一采样针102,第一采样针102包括第一内嵌针102a、第一外衬管102b、第一接口件102c。第一内嵌针102a的一端在第一采样罐103外部与第一外衬管102b连通,另一端则伸至第一采样罐103的罐底。第一接口件102c环绕于第一内102a并连通于第一采样罐103顶部开口。第一外衬管102b从第一接口件102c延伸出来并连通至第二管线104。The following flow path configuration begins to differ from the embodiment shown in FIG1 . In FIG3 , the second outer liner tube 202b will not be directly connected to the second pipeline 104 , and its gas flow is connected to the first sampling tank 103 . Specifically, the first sampling tank 103 is paired with a first sampling needle 102 , and the first sampling needle 102 includes a first embedded needle 102a , a first outer liner tube 102b , and a first interface component 102c . One end of the first embedded needle 102a is connected to the first outer liner tube 102b outside the first sampling tank 103 , and the other end extends to the bottom of the first sampling tank 103 . The first interface component 102c surrounds the first inner 102a and is connected to the top opening of the first sampling tank 103 . The first outer liner tube 102b extends from the first interface component 102c and is connected to the second pipeline 104 .
另外,在图3中,在第一管线101上设置第二前开关阀208a,在第二采样罐203和第一采样罐103之间的通路上设置第二后开关阀208b和第一前开关阀108a,第二后开关阀208b相较于第一前开关阀108a更加靠近第二采样罐203,在第二管线104上设置第一后开关阀108b。In addition, in Figure 3, a second front switch valve 208a is set on the first pipeline 101, and a second rear switch valve 208b and the first front switch valve 108a are set on the passage between the second sampling tank 203 and the first sampling tank 103. The second rear switch valve 208b is closer to the second sampling tank 203 than the first front switch valve 108a, and the first rear switch valve 108b is set on the second pipeline 104.
在本实施例中,围绕第一采样罐的配置与第二采样罐基本相同,但第一采样罐的出口(第一外衬管)连通至第二采样罐的入口(第二内嵌针),由此将第一采样罐和第二采样罐串联起来,而第二采样罐的出口(第二外衬管)则作为第二采样罐的出口连通至第二管线104。In this embodiment, the configuration surrounding the first sampling tank is basically the same as that of the second sampling tank, but the outlet of the first sampling tank (first outer liner) is connected to the inlet of the second sampling tank (second embedded needle), thereby connecting the first sampling tank and the second sampling tank in series, and the outlet of the second sampling tank (second outer liner) is connected to the second pipeline 104 as the outlet of the second sampling tank.
由此,在图3的实施例中,在置换采样流路运行时,上述四个开关阀均打开,泵压入的采样气体流经第一管线101之后,在第二内嵌针202a的引导下继续流动,由于第二内嵌针202a伸至第二采样罐203的罐底,因此采样气体在第一内嵌针202a的引导下流入第二采样罐203的罐底,由此,采样气体就在第二采样罐203内自下而上形成对流,通过气体对流作用,推动第二采样罐203内的原始气体自下而上穿过第二接口件202c从第二外衬管202b流出,随后,由于第二外衬管202b与第一内嵌针102a连通,因此,原始气体在采样气体的推动下被推向第一内嵌针102a,并经过第一内嵌针102a进入第一采样罐103,在第一采样罐103罐底形成自下而上的对流,从而彻底清除第一采样罐103中的原始气体,进而原始气体在采样气体的进一步推动下经第一接口件102c、第一外衬管102b离开第一采样罐103,进而沿着第二管线104从出口105排出,由此实现了对串联的两个采样罐的气体置换。Therefore, in the embodiment of FIG. 3 , when the replacement sampling flow path is in operation, the above four switch valves are all opened, and the sampling gas pressed by the pump flows through the first pipeline 101, and then continues to flow under the guidance of the second embedded needle 202a. Since the second embedded needle 202a extends to the bottom of the second sampling tank 203, the sampling gas flows into the bottom of the second sampling tank 203 under the guidance of the first embedded needle 202a. As a result, the sampling gas forms convection from bottom to top in the second sampling tank 203. Through the gas convection effect, the original gas in the second sampling tank 203 is pushed from bottom to top through the second interface 202c and flows out of the second outer liner 202b. Subsequently, since the second outer liner tube 202b is connected to the first embedded needle 102a, the original gas is pushed toward the first embedded needle 102a by the push of the sampling gas, and enters the first sampling tank 103 through the first embedded needle 102a, forming a bottom-up convection at the bottom of the first sampling tank 103, thereby completely removing the original gas in the first sampling tank 103, and then the original gas leaves the first sampling tank 103 through the first interface part 102c and the first outer liner tube 102b under the further push of the sampling gas, and is then discharged from the outlet 105 along the second pipeline 104, thereby realizing the gas replacement of the two sampling tanks connected in series.
在置换采样流路的运行完成之后,可转至加压采样流路。图3中用粗线箭头表示加压采样流路。在加压采样流路中,只需关闭第一后开关阀108b,同时,采样泵106将来自采样口的采样气体经由第一管线101吹入第二采样针202的第二外衬管202b,再经由第二接口件202c从第二采样罐203的罐顶流入第二采样罐203,由此在第二采样罐203中进行采样气体的采集。After the operation of the replacement sampling flow path is completed, it can be switched to the pressurized sampling flow path. The pressurized sampling flow path is indicated by a thick arrow in Figure 3. In the pressurized sampling flow path, it is only necessary to close the first rear switch valve 108b. At the same time, the sampling pump 106 blows the sampling gas from the sampling port into the second outer liner 202b of the second sampling needle 202 through the first pipeline 101, and then flows into the second sampling tank 203 from the tank top of the second sampling tank 203 through the second interface part 202c, thereby collecting the sampling gas in the second sampling tank 203.
随着第二采样罐203内的气压不断增大,第二采样罐203内的采样气体从罐底逐步溢至第二内嵌针202a,进而沿着第二内嵌针202a流入第一外衬管102b和第一接口件102c,进而流入第一采样罐103,由此在第一采样罐103中也进行采样气体的采集。As the air pressure in the second sampling tank 203 continues to increase, the sampling gas in the second sampling tank 203 gradually overflows from the bottom of the tank to the second embedded needle 202a, and then flows along the second embedded needle 202a into the first outer liner tube 102b and the first interface part 102c, and then flows into the first sampling tank 103, thereby collecting the sampling gas in the first sampling tank 103.
而随着第一采样罐103内的气压不断增大,第一采样罐103内的采样气体从罐底逐步递增升压。As the air pressure in the first sampling tank 103 continues to increase, the pressure of the sampled gas in the first sampling tank 103 gradually increases from the bottom of the tank.
此时,在本实施例中,在第一管线101上加装压力表107。随着两个采样罐内逐渐升压,压力表107上的读数也逐渐升高,一旦压力表107中的读数大于特定阈值,则同时关闭第一前开关阀108a、第二后开关阀208b和第二前开关阀208a,完成第一采样罐103和第二采样罐203的气体采样。At this time, in this embodiment, a pressure gauge 107 is installed on the first pipeline 101. As the pressure in the two sampling tanks gradually increases, the reading on the pressure gauge 107 also gradually increases. Once the reading in the pressure gauge 107 is greater than a specific threshold, the first front switch valve 108a, the second rear switch valve 208b and the second front switch valve 208a are closed at the same time, completing the gas sampling of the first sampling tank 103 and the second sampling tank 203.
由此,基本将图1所示实施例和图3所示实施例介绍完毕。在图1所示实施例中,在对采样罐进行气体置换和气体采样时,利用采样针探至采样罐罐底,采样针不仅仅作为气流通道通畅所必不可少的一环,而且巧妙地在采样罐中形成了对流,由此在气体置换阶段通过自下而上的对流作用有效地清除了采样罐中的原始气体,从而有效地对采样罐进行清洁,避免了采样罐受到污染,进一步,在气体采样阶段,采样针的存在可以作为缓冲确保气压有序上升而不至于压力瞬间暴涨,由此避免采样罐短时间内承受过大的压力。Thus, the introduction of the embodiment shown in FIG1 and the embodiment shown in FIG3 is basically completed. In the embodiment shown in FIG1, when the sampling tank is subjected to gas replacement and gas sampling, the sampling needle is used to probe the bottom of the sampling tank. The sampling needle is not only an indispensable link for the smooth flow of the airflow channel, but also cleverly forms convection in the sampling tank, thereby effectively removing the original gas in the sampling tank through the bottom-up convection effect during the gas replacement stage, thereby effectively cleaning the sampling tank and avoiding contamination of the sampling tank. Furthermore, during the gas sampling stage, the presence of the sampling needle can serve as a buffer to ensure that the gas pressure rises in an orderly manner without causing an instantaneous pressure surge, thereby avoiding the sampling tank from being subjected to excessive pressure in a short period of time.
而图3所示实施例中,采样针除了发挥图1中所示功能之外,还发挥了串联连接的功能,通过采样针的串联连接,有效地将两个采样罐串联起来,从而可以实现两个采样罐在气体置换和气体采样两方面的并行推进。由此可见,在图3所示的实施例中,采样针承担了更多的功能。In the embodiment shown in FIG3 , the sampling needle not only plays the role shown in FIG1 , but also plays the role of series connection. Through the series connection of the sampling needle, the two sampling tanks are effectively connected in series, so that the two sampling tanks can be advanced in parallel in terms of gas replacement and gas sampling. It can be seen that in the embodiment shown in FIG3 , the sampling needle has more functions.
以上所述仅为本发明的示例性实施例而已,并不用以限制本发明,凡在本发明的精神和原则之内,所做的任何修改、等同替换、改进等,均应包含在本发明保护的范围之内。The above description is only an exemplary embodiment of the present invention and is not intended to limit the present invention. Any modifications, equivalent substitutions, improvements, etc. made within the spirit and principles of the present invention should be included in the scope of protection of the present invention.
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