CN203502259U - Sealed sampling device - Google Patents

Sealed sampling device Download PDF

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Publication number
CN203502259U
CN203502259U CN201320442640.9U CN201320442640U CN203502259U CN 203502259 U CN203502259 U CN 203502259U CN 201320442640 U CN201320442640 U CN 201320442640U CN 203502259 U CN203502259 U CN 203502259U
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China
Prior art keywords
valve
sampling
interface
pipeline
differential
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CN201320442640.9U
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Chinese (zh)
Inventor
吴水生
季向东
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Nantong Sanlian Petrochemical Equipment Manufacture Co Ltd
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Nantong Sanlian Petrochemical Equipment Manufacture Co Ltd
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Abstract

The utility model provides a sealed sampling device which comprises a dual-gear valve, a sample inlet pipeline, a sample outlet pipeline, a nitrogen gas pipeline, a liquid storage tank, a sampling pipeline and a sampling bottle, wherein the dual-gear valve comprises a first three-way valve and a second three-way valve; three ports of the first three-way valve are connected with the sample outlet pipeline, the nitrogen gas pipeline and the liquid storage tank respectively; three ports of the second three-way valve are connected with the sample inlet pipeline, the liquid storage tank and the sampling pipeline respectively; one end, not connected with the second three-way valve, of the sampling pipeline is connected with the sampling bottle; a pressure adjustment valve and a check valve are arranged between the inlet of the nitrogen gas pipeline and the first three-way valve in sequence. According to the design, a sampling process is simplified, the pressure in a sampling process can be adjusted, the safety of operators can be ensured, and a sample can be conveniently taken out.

Description

Enclosed sampling device
Technical field
The utility model relates to the technical field of the industry collection liquids such as petrochemical industry, is specifically related to a kind of sampling apparatus.
Background technology
Closed sampler (liquid phase) is a kind of special sampler that belongs to the collection liquid that the industries such as oil, chemical industry are used, and is a kind of totally-enclosed, easy-operating sampling thief.Current sampling operation process is complicated, operate a plurality of valves and just can complete, complex operation, and easily maloperation; The general steel cylinder that uses is sampled at present, not only heavier, and in laboratory, is difficult to liquid to take out, and needs the specific purpose tools such as supporting corresponding rapid-acting coupling, more loaded down with trivial details.In addition, under high pressure conditions, sampler whole system is parallel to process pipeline, and sampling jar internal pressure is identical with the pressure in process pipeline, to operator, brings unsafe factor; Under this state, a release pipeline need to be set, pressure in system is laid down, could disconnect rapid-acting coupling, but usually this pipeline cannot be set in actual process, nowhere the medium in bleeder line.
Utility model content
The purpose of this utility model is to provide a kind of enclosed sampling device, solves one or more in above-mentioned prior art problem.
According to an aspect of the present utility model, enclosed sampling device is provided, comprise duplicate gear valve, sample inlet pipeline, sample export pipeline, nitrogen pipeline, fluid reservoir, sampling line and sampling jar; Duplicate gear valve comprises the first T-valve, the second T-valve, and three ports of the first T-valve connect respectively sample export pipeline, nitrogen pipeline and fluid reservoir; Three ports of the second T-valve connect respectively sample inlet pipeline, fluid reservoir and sampling line; One end that sampling line is not connected with the second T-valve is connected with sampling jar; Between entrance to the first T-valve of nitrogen pipeline, be also provided with successively pressure regulator valve and non-return valve.This design simplification sampling craft, by pressure regulator valve, can regulate the pressure in sampling process, ensure operating personnel's safety, and be convenient to the taking-up of sample.
In some embodiments, on sample inlet pipeline, be connected with refrigeratory.When sample thief is high-temp liquid, can first by refrigeratory, reduce the temperature of sample.
In some embodiments, duplicate gear valve also comprises gear case, drive bevel gear, the first driven wheel of differential, the second driven wheel of differential, control lever, and the first T-valve comprises first interface, the second interface, the 3rd interface and controls the first valve rod of Spool rotating; The second T-valve comprises the 4th interface, the 5th interface, the 6th interface and controls the second valve rod of Spool rotating; Drive bevel gear, the first driven wheel of differential and the second driven wheel of differential are all located in gear case, and control lever penetrates gearbox wall portion and drive bevel gear is fixed, and the first driven wheel of differential, the second driven wheel of differential all mesh with drive bevel gear; The first valve rod penetrates gearbox wall portion and the first driven wheel of differential is connected and fixed, and the second valve rod penetrates gearbox wall portion and the second driven wheel of differential is connected and fixed; The first interface of the first T-valve, the second interface, the 3rd interface connect respectively nitrogen pipeline, fluid reservoir, sample export pipeline; The 4th interface of the second T-valve, the 5th interface, the 6th interface connect respectively sample inlet pipeline, fluid reservoir, sampling line.This duplicate gear valve can be controlled two T-valve simultaneously, has improved operating efficiency.
In some embodiments, one end that control lever is exposed at gear case outside is provided with operating grip.Rotating operation bar more easily, and need to be by other instruments.
In some embodiments, sampling line is not provided with sampling needle with one end that the second T-valve is connected; Sampling jar bottleneck envelope has barrier film pad.Here the design of sampling needle and barrier film pad match, and in the process of sampling, the method that realizes sampling line and sample thief connection by the saturating barrier film pad of sampling acupuncture is more convenient, has improved sampling efficiency.
In some embodiments, barrier film pad is composited by teflon and silica gel.The barrier film pad of this material still can seal when sampling needle plugs metacneme pad, and energy Reusability, has reduced cost.
In some embodiments, one end that sampling line is provided with sampling needle is fixedly connected with fixed mount; Sampling needle, through the connecting portion of sampling line and sampling needle, is placed in fixed mount; Fixed mount and sampling line are fixedly connected with sheath and and the clasp of sheath activity.Fixed mount is set and is convenient to fixedly sampling jar, avoid in sampling process, because of the loosening connection affecting between sampling line and sampling jar of sampling jar; Fixed mount is designed to mutually detachable fixing sheath and clasp, is convenient to putting into and taking out of sampling jar.
In some embodiments, sampling jar is transparent vial.In sampling process, can be clear that the variation of liquid level, be convenient to sampling operation, prevent that sample from overflowing contaminated environment.
In some embodiments, sampling jar posts blow-out disc.Reduce the risk of vial explosion.
Accompanying drawing explanation
Fig. 1 is the connection diagram of the first embodiment of the present utility model;
Fig. 2 is the connection diagram of the second embodiment of the present utility model;
Fig. 3 is the first embodiment sampling preparation schematic diagram of the present utility model;
Fig. 4,5 is the sampling process schematic diagram of the first embodiment of the present utility model;
Fig. 6 is the first embodiment of the present utility model complete schematic diagram of sampling;
Fig. 7 is the cut-away view of duplicate gear valve;
Fig. 8 is the cut-open view of the first T-valve and the second T-valve under conventional state;
Fig. 9 is the cut-open view of the first T-valve when inputting sample in fluid reservoir and the second T-valve;
The cut-open view of the first T-valve and the second T-valve when Figure 10 is sampling jar sampling;
Figure 11 is the schematic diagram of guidance panel.
Embodiment
Below in conjunction with Figure of description, the utility model is described in more detail.
Embodiment 1:
As shown in Fig. 1,7, the enclosed sampling device that the utility model provides, comprises duplicate gear valve 1, sample inlet pipeline 41, sample export pipeline 43, nitrogen pipeline 42, fluid reservoir 3, sampling line 44 and sampling jar 6;
Wherein, duplicate gear valve 1 comprises the first T-valve 11, the second T-valve 12, gear case 13, drive bevel gear 14, the first driven wheel of differential 15, the second driven wheel of differential 16, control lever 19, the first T-valve 11 comprises that the first valve rod 114, the second T-valve 12 of first interface 111, the second interface 112, the 3rd interface 113 and control Spool rotating comprise the second valve rod 124 of the 4th interface 121, the 5th interface 122, the 6th interface 123 and control Spool rotating;
Drive bevel gear 14, the first driven wheel of differential 15 and the second driven wheel of differential 16 are all positioned at gear case 13, control lever 19 penetrates gear case 13 wall portions and drive bevel gear 14 is fixed by mode one-body molded or that internal and external threads screws, and the first driven wheel of differential 15, the second driven wheel of differential 16 all mesh with drive bevel gear 14;
The first valve rod 114 penetrates gear case 13 wall portions and the first driven wheel of differential 15 is connected and fixed, and the second valve rod 124 penetrates gear case 13 wall portions and the second driven wheel of differential 16 is fixed by mode one-body molded or that internal and external threads screws;
The first interface 111 of the first T-valve 11, the second interface 112, the 3rd interface 113 connect respectively nitrogen pipeline 42, fluid reservoir 3, sample export pipeline 43; The 4th interface 121 of the second T-valve 12, the 5th interface 122, the 6th interface 123 connect respectively described sample inlet pipeline 41, fluid reservoir 3, sampling line 44.One end that sampling line 44 is not connected with the second T-valve 12 is connected with sampling jar 6; Between entrance to the first T-valve 11 of nitrogen pipeline 42, be also provided with successively pressure regulator valve 421 and non-return valve 422.Above-mentioned connected mode all can internal and external threads screw connection.It should be noted that fluid reservoir 3 is connected between the first T-valve 11 and the second T-valve 12.
One end that sampling line 44 is not connected with the second T-valve 12 is connected with sampling needle 51 by one-body molded or tube socket or the internal and external threads mode such as spin; Sampling jar 6 bottleneck envelopes have barrier film pad 71.Barrier film pad 71 is composited by teflon and silica gel.One end that sampling line 44 connects sampling needle 51 is fixedly connected with fixed mount 6, and the connected mode here can be one-body molded, can be also the connection that screws of internal and external threads.Fixed mount 6 is comprised of sheath 61 and clasp 62, and the top of sheath 61 is fixedly connected with sampling line 44, and the lower end of sheath 61 is flexibly connected with clasp 62, removably connects.That mentions here removably connects, and refers to that clasp 62 can be fixing by bolt or bearing pin etc. and sheath 61 realizations more easily.One end of sampling needle 51 is connected with sampling line 44, and the other end, through the connecting portion of sampling line 44 and sampling needle 51, is placed in fixed mount 6.
Under conventional state, the first T-valve 11 and the second T-valve 12 are in the state shown in Fig. 8.Now, the first interface 111 of the first T-valve 11 and the second interface 112 and the 3rd interface 113 are not all communicated with each other; The 4th interface 121 of the second T-valve 12 and the 5th interface 122 and the 6th interface 123 are not communicated with each other.Therefore, sample inlet pipeline 41, sample export pipeline 43, nitrogen pipeline 42, fluid reservoir 3 and sampling line 44 are not all communicated with each other.
As shown in Figure 3, while using the enclosed sampling device collected specimens of the utility model description, change new barrier film pad 71 first to sampling jar 6; Unload clasp 62, sampling jar 6 is put into fixed mount 6 from the lower end of lower jacket 61, and firmly the connection of sampling line 44 and sampling jar 6, to sampling needle 51, until sampling needle 51 punctures barrier film pad 71, is realized in top; Clasp 62 is fixed on sheath 61, realizes fixing sampling jar 6.
As shown in Figure 4, after completing above-mentioned preliminary work, rotating operation bar 19, by the transmission of drive bevel gear 14, drive the first cone follower gear 15 and the second driven wheel of differential 16 to rotate, and then the position of the first T-valve 11 and the second T-valve 12 inner spools is adjusted to state shown in Fig. 9.Now, only the second interface 112 and the 3rd interface 113 connections in the first T-valve 11, first interface 111 is by spool shutoff; Only the 4th interface 121 and the 5th interface 122 connections in the second T-valve 12, the 6th interface 123 is by spool shutoff.Therefore, sample enters from sample inlet pipeline 41, through fluid reservoir 3, flows to sample export pipeline 43.In this process, allow liquid continuous stream through fluid reservoir 3, and postpone a period of time, to guarantee to get representative sample.
As shown in Figure 5, until fluid reservoir 3, be full of after sample, rotary manipulation bar 19, by the transmission of drive bevel gear 14, drive the first cone follower gear 15 and the second driven wheel of differential 16 to rotate, and then the position of the first T-valve 11 and the second T-valve 12 inner spools is adjusted to the state shown in Figure 10.Now, only first interface 111 and the second interface 112 connections in the first T-valve 11, the 3rd interface 113 is by spool shutoff; Only the 5th interface 122 and the 6th interface 123 connections in the second T-valve 12, the 4th interface is by spool shutoff.Therefore, sample export pipeline 43 disconnects and being communicated with fluid reservoir 3, and nitrogen pipeline 42 is communicated with fluid reservoir 3 by the first T-valve 11; Liquid in fluid reservoir 3 enters sampling jar 6 under the promotion of nitrogen, until all samples enters sampling jar 6, and sampler is removed.In this process, can according to actual conditions, regulate the pressure of nitrogen, guarantee carrying out smoothly of sampling.
As shown in Figure 6, after sampling, unload clasp 62, sampling jar 6 is pulled up from sampling needle 51.
In this process, consider that sealing in the sampling jar 6 that has barrier film pad 71 is an airtight space, when sample is when sampling needle 51 splashes into sample thief, air pressure in bottle can hinder splashing into of sample, and then the process of impact sampling, can use the saturating barrier film pad 71 of evacuation needle 52 thorn, the air of sampling jar 6 is discharged outside bottle by evacuation needle 52, guarantee carrying out smoothly of sampling.
Meanwhile, in order to be clear that the variation of liquid level in sampling process, prevent that sample from overflowing contaminated environment, sampling jar 6 is made into transparent vial.In order to make sampling jar 6 reduce the risk of explosion, at sampling jar 6 outer walls, post blow-out disc.
In addition, for handled easily personnel operation, in the outside of gear case 13, by modes such as bolt, bonding or fixings, be fixed with guidance panel 17, the opposing one side of guidance panel 17 and gear case 13 is fixed with state direction board 18 by modes such as bolt, bonding or fixings, and control lever 19 is through guidance panel 17 and state direction board 18.The one end that is exposed at gear case 13 outsides at control lever 19 is fixed with operating grip 10 by welding, the mode such as one-body molded, can drive the rotation of control lever 19 when rotating operation handle 10.As shown in figure 11, under normal conditions, the index line of operating grip 10 points to A point; During to the interior conveying sample of fluid reservoir 3, rotating operation handle 10 to B points; While carrying sample from fluid reservoir 3 is interior to sampling jar 7, rotating operation handle 10 to C points.So, operating personnel, in the process of whole sampling, only need go to relevant position by operating grip 10 by step, can complete whole operation.Whole process is convenient, fast, safety, needn't spend large cost training special messenger to sample, and has also greatly improved sampling efficiency on cost-saving basis.
Embodiment 2:
As shown in Figure 2, when collected sample, during high-temp liquid, need on the basis of embodiment 1, increase refrigeratory 8, this refrigeratory 8 is arranged on sample inlet pipeline 41.When high temp samples enters before fluid reservoir 3 through the second T-valve 12, need elder generation is cooling through subcooler.
More than statement is only optimal way of the present utility model; it should be pointed out that to those skilled in the art, do not departing under the prerequisite of the utility model creation design; can also make some distortion and improvement, within these also should be considered as protection domain of the present utility model.

Claims (8)

1. enclosed sampling device, is characterized in that, comprises duplicate gear valve (1), sample inlet pipeline (41), sample export pipeline (43), nitrogen pipeline (42), fluid reservoir (3), sampling line (44) and sampling jar (7);
Described duplicate gear valve (1) comprises the first T-valve (11), the second T-valve (12), and three ports of described the first T-valve (11) connect respectively described sample export pipeline (43), described nitrogen pipeline (42) and described fluid reservoir (3); Three ports of described the second T-valve (12) connect respectively described sample inlet pipeline (41), fluid reservoir (3) and described sampling line (44); One end that described sampling line (44) is not connected with described the second T-valve (12) is connected with described sampling jar (7); The entrance of described nitrogen pipeline (42) is also provided with pressure regulator valve (421) and non-return valve (422) between described the first T-valve (11).
2. enclosed sampling device according to claim 1, is characterized in that, is connected with refrigeratory (8) on described sample inlet pipeline (41).
3. enclosed sampling device according to claim 1 and 2, it is characterized in that, described duplicate gear valve (1) also comprises gear case (13), drive bevel gear (14), the first driven wheel of differential (15), the second driven wheel of differential (16), control lever (19), and described the first T-valve (11) comprises first interface (111), the second interface (112), the 3rd interface (113) and controls first valve rod (114) of its Spool rotating; Described the second T-valve (12) comprises the 4th interface (121), the 5th interface (122), the 6th interface (123) and controls second valve rod (124) of its Spool rotating;
Described drive bevel gear (14), the first driven wheel of differential (15) and the second driven wheel of differential (16) are all located in described gear case (13), described control lever (19) penetrates gear case (13) wall portion and described drive bevel gear (14) is fixing, and described the first driven wheel of differential (15), the second driven wheel of differential (16) all mesh with described drive bevel gear (14);
Described the first valve rod (114) penetrates gear case (13) wall portion and described the first driven wheel of differential (15) is connected and fixed, and described the second valve rod (124) penetrates gear case (13) wall portion and described the second driven wheel of differential (16) is connected and fixed;
The first interface (111) of described the first T-valve (11), the second interface (112), the 3rd interface (113) connect respectively described nitrogen pipeline (42), fluid reservoir (3), sample export pipeline (43); The 4th interface (121) of described the second T-valve (12), the 5th interface (122), the 6th interface (123) connect respectively described sample inlet pipeline (41), fluid reservoir (3), sampling line (44).
4. enclosed sampling device according to claim 3, is characterized in that, described control lever (19) is exposed at the outside one end of described gear case (13) and is provided with operating grip (10).
5. enclosed sampling device according to claim 3, is characterized in that, one end that described sampling line (44) is not connected with described the second T-valve (2) is provided with sampling needle (51); Described sampling jar (7) bottleneck envelope has barrier film pad (71).
6. enclosed sampling device according to claim 5, is characterized in that, one end that described sampling line (44) is provided with described sampling needle (51) is fixedly connected with fixed mount (6); Described sampling needle (51) is placed in described fixed mount (6); The clasp (62) that described fixed mount (6) is fixedly connected with sheath (61) and is flexibly connected with described sheath (61) with described sampling line (44).
7. enclosed sampling device according to claim 3, is characterized in that, described sampling jar (7) is transparent vial.
8. enclosed sampling device according to claim 7, is characterized in that, described sampling jar (7) posts blow-out disc.
CN201320442640.9U 2013-07-23 2013-07-23 Sealed sampling device Expired - Lifetime CN203502259U (en)

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Cited By (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104006987A (en) * 2014-05-13 2014-08-27 江苏爵格工业设备有限公司 Closed sampling device
CN104155147A (en) * 2014-08-26 2014-11-19 西安石油大学 Sampling container and sampling method used for medium corrosion experiment of oilfield production system
CN105043816A (en) * 2015-09-15 2015-11-11 亚洲硅业(青海)有限公司 Quick connection type closed sampling method
CN106989959A (en) * 2017-06-08 2017-07-28 北京永兴精佳仪器有限公司 A kind of pipeline liquid enclosed sampling method
CN107132074A (en) * 2017-03-24 2017-09-05 中国神华能源股份有限公司 Sampling apparatus
CN108362526A (en) * 2018-04-26 2018-08-03 安策阀门(太仓)有限公司 A kind of aviation fuel sampler
CN109000979A (en) * 2018-09-06 2018-12-14 河南中托力合化学有限公司 A kind of sampling apparatus suitable for fluid reservoir
CN111504734A (en) * 2020-04-30 2020-08-07 江苏星亚迪环境科技有限公司 Low-pressure gas sampler
CN114459832A (en) * 2022-01-11 2022-05-10 中国神华煤制油化工有限公司 Sampling device and chemical system
CN117969193A (en) * 2024-04-02 2024-05-03 北京博赛德科技有限公司 Jacket needle type convection displacement positive pressure sampling device

Cited By (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104006987A (en) * 2014-05-13 2014-08-27 江苏爵格工业设备有限公司 Closed sampling device
CN104155147A (en) * 2014-08-26 2014-11-19 西安石油大学 Sampling container and sampling method used for medium corrosion experiment of oilfield production system
CN105043816A (en) * 2015-09-15 2015-11-11 亚洲硅业(青海)有限公司 Quick connection type closed sampling method
CN105043816B (en) * 2015-09-15 2019-01-04 亚洲硅业(青海)有限公司 A kind of fast-connecting type closed sampling device
CN107132074A (en) * 2017-03-24 2017-09-05 中国神华能源股份有限公司 Sampling apparatus
CN106989959A (en) * 2017-06-08 2017-07-28 北京永兴精佳仪器有限公司 A kind of pipeline liquid enclosed sampling method
CN106989959B (en) * 2017-06-08 2019-07-09 北京永兴精佳仪器有限公司 A kind of pipeline liquid enclosed sampling method
CN108362526B (en) * 2018-04-26 2024-03-15 安策阀门(太仓)有限公司 Aviation oil sampling device
CN108362526A (en) * 2018-04-26 2018-08-03 安策阀门(太仓)有限公司 A kind of aviation fuel sampler
CN109000979A (en) * 2018-09-06 2018-12-14 河南中托力合化学有限公司 A kind of sampling apparatus suitable for fluid reservoir
CN109000979B (en) * 2018-09-06 2024-05-28 河南中托力合化学有限公司 Sampling device suitable for liquid storage tank
CN111504734A (en) * 2020-04-30 2020-08-07 江苏星亚迪环境科技有限公司 Low-pressure gas sampler
CN114459832A (en) * 2022-01-11 2022-05-10 中国神华煤制油化工有限公司 Sampling device and chemical system
CN117969193A (en) * 2024-04-02 2024-05-03 北京博赛德科技有限公司 Jacket needle type convection displacement positive pressure sampling device

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Granted publication date: 20140326