CN117695174A - Novel plant antiperspirant and deodorant preparation, and preparation method, production device and application thereof - Google Patents
Novel plant antiperspirant and deodorant preparation, and preparation method, production device and application thereof Download PDFInfo
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- CN117695174A CN117695174A CN202311571365.5A CN202311571365A CN117695174A CN 117695174 A CN117695174 A CN 117695174A CN 202311571365 A CN202311571365 A CN 202311571365A CN 117695174 A CN117695174 A CN 117695174A
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- 230000001166 anti-perspirative effect Effects 0.000 title claims abstract description 35
- 239000003213 antiperspirant Substances 0.000 title claims abstract description 35
- 238000002360 preparation method Methods 0.000 title claims abstract description 31
- 239000002781 deodorant agent Substances 0.000 title claims abstract description 28
- 238000004519 manufacturing process Methods 0.000 title claims description 8
- 235000020238 sunflower seed Nutrition 0.000 claims abstract description 29
- 239000000341 volatile oil Substances 0.000 claims abstract description 24
- 241000196324 Embryophyta Species 0.000 claims abstract description 22
- 239000003921 oil Substances 0.000 claims abstract description 22
- 235000019198 oils Nutrition 0.000 claims abstract description 22
- DOOTYTYQINUNNV-UHFFFAOYSA-N Triethyl citrate Chemical compound CCOC(=O)CC(O)(C(=O)OCC)CC(=O)OCC DOOTYTYQINUNNV-UHFFFAOYSA-N 0.000 claims abstract description 13
- 235000018936 Vitellaria paradoxa Nutrition 0.000 claims abstract description 13
- 241001135917 Vitellaria paradoxa Species 0.000 claims abstract description 13
- GVJHHUAWPYXKBD-UHFFFAOYSA-N d-alpha-tocopherol Natural products OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-UHFFFAOYSA-N 0.000 claims abstract description 13
- 229940057910 shea butter Drugs 0.000 claims abstract description 13
- 229960001295 tocopherol Drugs 0.000 claims abstract description 13
- 229930003799 tocopherol Natural products 0.000 claims abstract description 13
- 235000010384 tocopherol Nutrition 0.000 claims abstract description 13
- 239000011732 tocopherol Substances 0.000 claims abstract description 13
- VMYFZRTXGLUXMZ-UHFFFAOYSA-N triethyl citrate Natural products CCOC(=O)C(O)(C(=O)OCC)C(=O)OCC VMYFZRTXGLUXMZ-UHFFFAOYSA-N 0.000 claims abstract description 13
- 235000013769 triethyl citrate Nutrition 0.000 claims abstract description 13
- 239000001069 triethyl citrate Substances 0.000 claims abstract description 13
- GVJHHUAWPYXKBD-IEOSBIPESA-N α-tocopherol Chemical compound OC1=C(C)C(C)=C2O[C@@](CCC[C@H](C)CCC[C@H](C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-IEOSBIPESA-N 0.000 claims abstract description 13
- 241000218691 Cupressaceae Species 0.000 claims abstract description 12
- 241000208152 Geranium Species 0.000 claims abstract description 12
- 229940119170 jojoba wax Drugs 0.000 claims abstract description 12
- WWZKQHOCKIZLMA-UHFFFAOYSA-N octanoic acid Chemical compound CCCCCCCC(O)=O WWZKQHOCKIZLMA-UHFFFAOYSA-N 0.000 claims abstract description 12
- LADGBHLMCUINGV-UHFFFAOYSA-N tricaprin Chemical compound CCCCCCCCCC(=O)OCC(OC(=O)CCCCCCCCC)COC(=O)CCCCCCCCC LADGBHLMCUINGV-UHFFFAOYSA-N 0.000 claims abstract description 12
- 238000010438 heat treatment Methods 0.000 claims description 36
- 235000019864 coconut oil Nutrition 0.000 claims description 14
- 239000003240 coconut oil Substances 0.000 claims description 14
- 240000003183 Manihot esculenta Species 0.000 claims description 11
- 235000016735 Manihot esculenta subsp esculenta Nutrition 0.000 claims description 11
- 229920002472 Starch Polymers 0.000 claims description 11
- 235000019698 starch Nutrition 0.000 claims description 11
- 239000008107 starch Substances 0.000 claims description 11
- 238000003756 stirring Methods 0.000 claims description 10
- 239000000203 mixture Substances 0.000 claims description 6
- 238000009472 formulation Methods 0.000 claims description 5
- 238000002156 mixing Methods 0.000 claims description 5
- 238000005303 weighing Methods 0.000 claims description 5
- 238000005485 electric heating Methods 0.000 claims description 4
- 239000011259 mixed solution Substances 0.000 claims description 4
- 239000000839 emulsion Substances 0.000 claims description 2
- 239000007921 spray Substances 0.000 claims description 2
- 230000000694 effects Effects 0.000 abstract description 5
- 239000000284 extract Substances 0.000 abstract description 2
- 230000000638 stimulation Effects 0.000 abstract 1
- 238000006243 chemical reaction Methods 0.000 description 8
- 238000012360 testing method Methods 0.000 description 6
- 238000004332 deodorization Methods 0.000 description 5
- 241000894006 Bacteria Species 0.000 description 4
- 238000003825 pressing Methods 0.000 description 4
- 230000035900 sweating Effects 0.000 description 4
- 238000000034 method Methods 0.000 description 3
- 230000003020 moisturizing effect Effects 0.000 description 3
- 230000001737 promoting effect Effects 0.000 description 3
- 239000002994 raw material Substances 0.000 description 3
- 239000007787 solid Substances 0.000 description 3
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- 230000003064 anti-oxidating effect Effects 0.000 description 2
- 239000004519 grease Substances 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 230000007774 longterm Effects 0.000 description 2
- 238000002844 melting Methods 0.000 description 2
- 230000008018 melting Effects 0.000 description 2
- 229910052751 metal Inorganic materials 0.000 description 2
- 239000002184 metal Substances 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 239000000843 powder Substances 0.000 description 2
- 230000008569 process Effects 0.000 description 2
- 230000028327 secretion Effects 0.000 description 2
- 239000000243 solution Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 210000004243 sweat Anatomy 0.000 description 2
- 102000008186 Collagen Human genes 0.000 description 1
- 108010035532 Collagen Proteins 0.000 description 1
- 241000233866 Fungi Species 0.000 description 1
- 206010072170 Skin wound Diseases 0.000 description 1
- 241000700605 Viruses Species 0.000 description 1
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- 238000004887 air purification Methods 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- 230000003712 anti-aging effect Effects 0.000 description 1
- 230000000844 anti-bacterial effect Effects 0.000 description 1
- 230000003110 anti-inflammatory effect Effects 0.000 description 1
- 230000001580 bacterial effect Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 229920001436 collagen Polymers 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 230000002708 enhancing effect Effects 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 238000000855 fermentation Methods 0.000 description 1
- 230000004151 fermentation Effects 0.000 description 1
- 239000003906 humectant Substances 0.000 description 1
- 230000000774 hypoallergenic effect Effects 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 239000003112 inhibitor Substances 0.000 description 1
- 230000002401 inhibitory effect Effects 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 230000004060 metabolic process Effects 0.000 description 1
- 244000005700 microbiome Species 0.000 description 1
- 231100000344 non-irritating Toxicity 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- 239000008041 oiling agent Substances 0.000 description 1
- 230000019612 pigmentation Effects 0.000 description 1
- 239000011241 protective layer Substances 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 230000037390 scarring Effects 0.000 description 1
- 210000001732 sebaceous gland Anatomy 0.000 description 1
- 230000037394 skin elasticity Effects 0.000 description 1
- 230000001954 sterilising effect Effects 0.000 description 1
- 238000004659 sterilization and disinfection Methods 0.000 description 1
- 230000002087 whitening effect Effects 0.000 description 1
- 230000029663 wound healing Effects 0.000 description 1
- 230000037303 wrinkles Effects 0.000 description 1
- 229910052725 zinc Inorganic materials 0.000 description 1
- 239000011701 zinc Substances 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/678—Tocopherol, i.e. vitamin E
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/732—Starch; Amylose; Amylopectin; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q15/00—Anti-perspirants or body deodorants
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J4/00—Feed or outlet devices; Feed or outlet control devices
- B01J4/001—Feed or outlet devices as such, e.g. feeding tubes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
- B65D—CONTAINERS FOR STORAGE OR TRANSPORT OF ARTICLES OR MATERIALS, e.g. BAGS, BARRELS, BOTTLES, BOXES, CANS, CARTONS, CRATES, DRUMS, JARS, TANKS, HOPPERS, FORWARDING CONTAINERS; ACCESSORIES, CLOSURES, OR FITTINGS THEREFOR; PACKAGING ELEMENTS; PACKAGES
- B65D83/00—Containers or packages with special means for dispensing contents
- B65D83/0005—Containers or packages provided with a piston or with a movable bottom or partition having approximately the same section as the container
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Chemical & Material Sciences (AREA)
- Epidemiology (AREA)
- Birds (AREA)
- Dermatology (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Emergency Medicine (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Cosmetics (AREA)
Abstract
The invention discloses a novel plant antiperspirant and deodorant preparation which comprises the following components in parts by mass: 0.1-3 parts of caprylic/capric triglyceride, 1-6 parts of sunflower seed oil, 1-12 parts of jojoba oil, 0.1-2 parts of tocopherol, 0.1-3 parts of triethyl citrate, 0.1-3 parts of shea butter, 0.2-5 parts of cypress essential oil and 0.2-6 parts of geranium essential oil. The invention also discloses a preparation device and a preparation method of the novel plant antiperspirant and deodorant preparation. The novel plant antiperspirant and deodorant preparation prepared by the invention has the advantages that all components are natural extracts, the preparation is green and warm and has no stimulation, and the preparation not only has excellent moisture-keeping and skin-care capabilities, but also has the effects of antiperspirant, deodorant, bacteriostasis and the like.
Description
Technical Field
The invention relates to the technical field of pharmaceutical chemical industry, in particular to a novel plant antiperspirant and deodorant preparation, and a preparation method, a production device and application thereof.
Background
In summer, people can not avoid sweating in outdoor activities, and sweat residues on skin and clothes are easy to grow bacteria, so that the bacteria can emit unpleasant smell after short propagation and fermentation. In order to keep oneself and other people pleasant and healthy, people often use antiperspirant to inhibit skin sweating, and antiperspirant is a personal care product for keeping body dry and popular with various people.
Antiperspirant as a modern chemical formulation, the active of antiperspirant is usually various metal salts, such as zinc, iron and aluminum, for example, patent 201780077315.8, 201880078457.0, 201380062201.8, and the antiperspirant active of this metal type is unavoidably irritating to the skin, and the ingredient directly extracted from the plant is rather favored by the consumer under the increasing demands of pure natural, green, nontoxic and hypoallergenic.
Disclosure of Invention
The invention aims to overcome the defects of the prior art and provide a novel plant antiperspirant and deodorant preparation with strong antiperspirant and deodorant capabilities, and a preparation method, a production device and application thereof.
The invention aims at providing a novel plant antiperspirant and deodorant preparation, which comprises the following components in parts by mass: 0.1-3 parts of caprylic/capric triglyceride, 1-6 parts of sunflower seed oil, 1-12 parts of jojoba oil, 0.1-2 parts of tocopherol, 0.1-3 parts of triethyl citrate, 0.1-3 parts of shea butter, 0.2-5 parts of cypress essential oil and 0.2-6 parts of geranium essential oil.
Preferably, the sunflower seed wax also comprises 1-10 parts of sunflower seed wax, 10-30 parts of coconut oil and 5-30 parts of tapioca starch.
The second object of the invention is to provide a preparation method of the novel antiperspirant and deodorant preparation of plants, which comprises the following steps,
(1) Weighing 1-10 parts of sunflower seed wax, 0.1-3 parts of caprylic/capric triglyceride, 10-30 parts of coconut oil, 1-6 parts of sunflower seed oil, 1-12 parts of jojoba oil and 0.1-3 parts of shea butter, mixing, heating at 70-95 ℃, stirring and dissolving;
(2) Adding 0.2-5 parts of cypress essential oil and 0.2-6 parts of geranium essential oil, heating to 70-95 ℃, mixing and stirring uniformly, and dissolving;
(3) 5-30 parts of tapioca starch is weighed and dispersed in the mixed solution, and the mixed solution is stirred uniformly;
(4) Adding 0.1-3 parts of triethyl citrate and 0.1-2 parts of tocopherol, and continuously heating and stirring at 70-95 ℃ to obtain the finished product.
The invention further aims to provide a production device of novel antiperspirant and deodorant preparation for plants, which comprises a feeding barrel, wherein a first feeding port and a second feeding port are arranged at the lower part of the feeding barrel, a first pushing plug, a second pushing plug, a connecting rod and a first pushing rod are arranged in the feeding barrel, two ends of the connecting rod are respectively and fixedly connected with the first pushing plug and the second pushing plug, the first pushing plug and the second pushing plug are respectively and hermetically connected with the inner wall of the feeding barrel in a sliding manner, the first pushing rod pushes the first pushing plug and the second pushing plug to slide up and down along the feeding barrel, a first feeding pipe and a second feeding pipe are arranged outside the feeding barrel, one end of the first feeding pipe is communicated with the first feeding port, a heating device is arranged on the first feeding pipe, the second feeding pipe is communicated with the second feeding port, a third pushing plug and a second pushing rod are arranged in the second feeding port, the first pushing rod pushes the third pushing plug and the second feeding pipe to move left and right along the second feeding pipe.
Preferably, the heating device comprises a jacket, a heating wire and heat conduction oil, the jacket surrounds the first feeding pipe, and the heating wire and the heat conduction oil are located in the jacket.
Preferably, a first heating cavity is arranged in the first pushing plug, a second heating cavity is arranged in the connecting rod, and a third heating cavity is arranged in the second pushing plug.
Preferably, the first feed inlet is located above the second feed inlet.
Preferably, an opening matched with the radian of the feeding cylinder is formed in the end portion of the third pushing plug.
Preferably, the upper surface of the first pushing plug, the upper surface of the second pushing plug and the lower surface of the first pushing plug are both inclined structures.
The invention further protects the application of the novel antiperspirant and deodorant preparation which can be prepared into emulsion, smearing stick or spray.
The invention has the following advantages:
1. the coconut oil has comprehensive antibacterial property, can kill bacteria, viruses, fungi microorganisms and the like, the triethyl citrate has the functions of antioxidation and deodorization, is an odor inhibitor, has the functions of resisting bacteria, inhibiting sweating, astringing and promoting scarring, has the functions of astringing and sterilizing, can balance secretion of sebaceous glands of skin, increases the consistency and softness of products, absorbs excessive grease and moisture, controls secretion of skin grease, enables the skin to keep a fresh and comfortable state, and can inhibit skin sweating when multiple components are combined together, and meanwhile, can inhibit bacterial reproduction and remove malodor emitted by body sweat;
2. the sunflower seed wax and the coconut oil have high melting points and are solid at normal temperature, so that the sunflower seed wax has good film forming property and skin moisturizing property, the hardness and crystal structure of a formula can be improved by adding the sunflower seed wax into the components, and the sunflower seed wax and the coconut oil can be prepared into an antiperspirant stick after being uniformly mixed with various antiperspirant deodorant components, so that the sunflower seed wax is convenient to be smeared on skin;
3. the caprylic/capric triglyceride and the jojoba oil are important oiling agents and humectants in the components; the sunflower seed oil has skin moistening function, anti-inflammatory effect of promoting skin wound healing, and whitening effect; the tocopherol has the effects of enhancing antioxidation, promoting metabolism of skin, preventing pigmentation, improving skin elasticity, moistening skin, caring skin, and resisting aging; the shea butter can form a protective layer on the surface of skin, prevent moisture evaporation, play a role in moisturizing, have an anti-aging role, promote collagen growth after long-term use, enable the skin to be smooth and fine, and reduce wrinkles;
4. the components of the novel plant antiperspirant deodorant preparation are extracted from natural plants, so that the novel plant antiperspirant deodorant preparation is mild, safe and non-irritating, has the excellent moisturizing and skin care capabilities of traditional skin care products, has the effects of antiperspirant, deodorization, bacteriostasis and the like through testing, and is suitable for being made into various products;
5. the preparation method provided by the invention has the advantages that the technical process is simple, the temperature control is reasonable, and the beneficial components in the natural extract can be fully reserved;
6. the invention also provides a feeding device which is suitable for the common feeding of high-melting-point solid, liquid and powder, is also suitable for the direct feeding of other raw materials in the reaction process, can avoid the backflushing of oily gas in a kettle to a feeding pipeline, reduces the amount of gas in the tank from the inside of a reaction tank in the feeding process, and solves the problems that the raw materials are easy to accumulate and block in the pipeline after long-term use of the feeding device.
Drawings
Fig. 1 is a schematic cross-sectional view of the present invention.
In the figure, 1, a feeding cylinder; 2. a first plunger; 3. a connecting rod; 4. a second plunger; 5. a first push rod; 6. a first feed port; 7. a second feed inlet; 8. a first feed tube; 9. a jacket; 10. an electric heating wire; 11. a second feed tube; 12. a third plunger; 13. a second push rod; 14. a third feed inlet; 15. a first heating chamber; 16. a heating plate; 17. an upper press plate; 18. a second heating chamber; 19. a third heating chamber; 20. a heating rod; 21. an opening.
Detailed Description
For the purpose of making the objects, technical solutions and advantages of the embodiments of the present invention more apparent, the technical solutions of the embodiments of the present invention will be clearly and completely described below with reference to the accompanying drawings in the embodiments of the present invention, and it is apparent that the described embodiments are some embodiments of the present invention, but not all embodiments of the present invention. All other embodiments, which can be made by those skilled in the art based on the embodiments of the invention without making any inventive effort, are intended to be within the scope of the invention.
Example 1, comprising the following mass components, 1kg of sunflower seed wax, 10kg of coconut oil, 30kg of tapioca starch, 3kg of caprylic/capric triglyceride, 2kg of sunflower seed oil, 5kg of jojoba oil, 1kg of tocopherol, 1kg of triethyl citrate, 1kg of shea butter, 2kg of cypress essential oil, 6kg of geranium essential oil and 2kg of essence.
Example 2, comprising the following mass components, 10kg of sunflower seed wax, 30kg of coconut oil, 30kg of tapioca starch, 2kg of caprylic/capric triglyceride, 2kg of sunflower seed oil, 5kg of jojoba oil, 3kg of tocopherol, 2kg of triethyl citrate, 2kg of shea butter, 4kg of cypress essential oil, 5kg of geranium essential oil and 1kg of essence.
Example 3, comprising the following mass fractions, sunflower seed wax 5kg, coconut oil 15kg, tapioca starch 15kg, caprylic/capric triglyceride 2kg, sunflower seed oil 4kg, jojoba oil 8kg, tocopherol 0.1kg, triethyl citrate 2kg, shea butter 0.1kg, cypress essential oil 0.2kg, geranium essential oil 0.2kg, essence 0.5kg.
Example 4, comprising the following mass fractions, sunflower seed wax 2kg, coconut oil 20kg, tapioca starch 25kg, caprylic/capric triglyceride 3kg, sunflower seed oil 6kg, jojoba oil 10kg, tocopherol 2kg, triethyl citrate 3kg, shea butter 2kg, cypress essential oil 5kg, geranium essential oil 6kg, essence 0.5kg.
Example 5, comprising the following mass fractions, sunflower seed wax 2kg, coconut oil 10kg, tapioca starch 5kg, caprylic/capric triglyceride 0.1kg, sunflower seed oil 1kg, jojoba oil 1kg, tocopherol 0.1kg, triethyl citrate 0.1kg, shea butter 0.1kg, cypress essential oil 0.2kg, geranium essential oil 0.2kg, essence 0.5kg.
The equipment used by the invention comprises a reaction tank and a feeding device arranged on the reaction tank, wherein the feeding device is shown in figure 1, the feeding device comprises a feeding cylinder 1, a first feeding pipe 8, a second feeding pipe 11, a first oil cylinder and a second oil cylinder, a flange is arranged at the bottom of the feeding cylinder 1, a round first feeding hole 6 and a round second feeding hole 7 are arranged at the lower part of the feeding cylinder 1, a first pushing plug 2, a second pushing plug 4, a connecting rod 3 and a first pushing rod 5 are arranged in the feeding cylinder 1, the first pushing plug 2 and the second pushing plug 4 are respectively and hermetically connected with the inner wall of the feeding cylinder 1 in a sliding manner, the lower surface of the first pushing plug 2 is a conical surface, the upper surface and the lower surface of the second pushing plug 4 are both conical surfaces, the first pushing plug 2 is a cylinder structure with a cavity at the top, an upper pressing plate 17 is arranged in the first pushing plug 2, a first heating cavity 15 is formed between the upper pressing plate 17 and the bottom surface of the first pushing plug 2, the first heating cavity 15 is internally provided with a heating plate 16, the connecting rod 3 is of a hollow tubular structure, the inside of the connecting rod 3 forms a second heating cavity 15, two ends of the connecting rod 3 are respectively connected with the bottom center of the first pushing plug 2 and the top center of the second pushing plug 4 in a threaded plug-in manner, the inside of the second pushing plug 4 is of a cavity structure, the inside of the second pushing plug 4 forms a third heating cavity 19, the second heating cavity 15 and the third heating cavity 19 are internally provided with heating rods 20, the second heating cavity 15 and the third heating cavity 19 are internally provided with heat conduction oil, the bottom end of the first pushing rod 5 is fixedly connected with an upper pressing plate 17, the upper pressing plate 17 is fixedly connected with the first pushing plug 2, the output end of the first oil cylinder pushes the first pushing plug 2 and the second pushing plug 4 to slide up and down along the feeding cylinder 1 through the first pushing rod 5, one end of the first feeding pipe 8 is welded and communicated with the first feeding port 6, the jacket 9 is arranged on the first feeding pipe 8, the jacket 9 surrounds the first feeding pipe 8, an electric heating wire 10 and heat conduction oil are arranged in the jacket 9, the second feeding pipe 11 is obliquely communicated with the second feeding port 7 by 15 degrees, a third pushing plug 12 and a second pushing rod 13 are arranged in the second feeding port 7, the second oil cylinder is fixedly connected through the second pushing rod 13 and pushes the third pushing plug 12 to move left and right along the second feeding pipe 11, a third feeding port 14 is formed in the upper middle of the second feeding pipe 11, the distance between the third feeding port 14 and the second feeding port 7 is smaller than the length of the third pushing plug 12, an opening 21 matched with the radian of the feeding cylinder 1 is formed in the end portion of the second pushing plug 4, the first feeding port 6 is located above the second feeding port 7, and the distance between the first feeding port 6 and the bottom opening of the feeding cylinder 1 is smaller than the height of the first pushing plug 2.
The production method of the novel antiperspirant and deodorant preparation for plants, which is applicable to the raw material components and the using device, comprises the following steps,
(1) Weighing sunflower seed wax, coconut oil and shea butter which are solid at normal temperature according to a proportion, putting caprylic/capric triglyceride, sunflower seed oil and jojoba oil which are liquid at normal temperature into a first feed pipe, heating and melting a jacket, putting the sunflower seed wax, the coconut oil and the shea butter into a reaction tank through a first pushing plug and a second pushing plug, and heating, stirring and dissolving the mixture at 70-95 ℃;
(2) Continuously weighing cypress essential oil and geranium essential oil in corresponding proportions, putting the cypress essential oil and the geranium essential oil into a reaction tank through a first feed pipe, and continuously mixing and stirring uniformly at 70-95 ℃ to dissolve;
(3) The cassava starch with the corresponding proportion is weighed and put into the second feeding pipe through the third feeding hole, the third pushing plug pushes the cassava starch into a cavity between the first pushing plug and the second pushing plug, and the first pushing plug then puts powder into the reaction tank for stirring and dissolving, so that the gas backflushing is prevented from entering the second feeding pipe;
(4) And finally, weighing triethyl citrate and tocopherol with corresponding proportions, putting the triethyl citrate and the tocopherol into a reaction tank through a first feed pipe, and continuously heating and uniformly stirring at 70-95 ℃ to obtain the finished product.
The novel antiperspirant and deodorant preparations prepared according to examples 1 to 5 were subjected to bacteriostasis and deodorization tests according to the experimental method and steps of the "disinfection technical Specification" 2002-2.1.8.2, and the deodorization tests were subjected to experimental tests according to the method for determining the purification effect of QBT 2761-2006 indoor air purification products.
The bacteriostasis test results are as follows
Deodorization test results are as follows
Although the present invention has been described with reference to the foregoing embodiments, it will be apparent to those skilled in the art that modifications may be made to the embodiments described, or equivalents may be substituted for elements thereof, and any modifications, equivalents, improvements and changes may be made without departing from the spirit and principles of the present invention.
Claims (10)
1. The novel plant antiperspirant and deodorant preparation is characterized by comprising the following components in parts by mass: 0.1-3 parts of caprylic/capric triglyceride, 1-6 parts of sunflower seed oil, 1-12 parts of jojoba oil, 0.1-2 parts of tocopherol, 0.1-3 parts of triethyl citrate, 0.1-3 parts of shea butter, 0.2-5 parts of cypress essential oil and 0.2-6 parts of geranium essential oil.
2. A novel antiperspirant and deodorant formulation of claim 1, wherein: also comprises 1-10 parts of sunflower seed wax, 10-30 parts of coconut oil and 5-30 parts of tapioca starch.
3. A process for preparing a novel antiperspirant and deodorant formulation of a plant as claimed in any one of claims 1 or 2, comprising the steps of,
(1) Weighing 1-10 parts of sunflower seed wax, 0.1-3 parts of caprylic/capric triglyceride, 10-30 parts of coconut oil, 1-6 parts of sunflower seed oil, 1-12 parts of jojoba oil and 0.1-3 parts of shea butter, mixing, heating at 70-95 ℃, stirring and dissolving;
(2) Adding 0.2-5 parts of cypress essential oil and 0.2-6 parts of geranium essential oil, heating to 70-95 ℃, mixing and stirring uniformly, and dissolving;
(3) 5-30 parts of tapioca starch is weighed and dispersed in the mixed solution, and the mixed solution is stirred uniformly;
(4) Adding 0.1-3 parts of triethyl citrate and 0.1-2 parts of tocopherol, and continuously heating and stirring at 70-95 ℃ to obtain the finished product.
4. A plant new antiperspirant and deodorant preparation production device according to claim 3, characterized in that: including feed cylinder, feed cylinder's lower part is provided with first feed inlet, second feed inlet, be provided with first plug, second plug, connecting rod, first catch bar in the feed cylinder, the both ends of connecting rod are fixed connection respectively first plug with second plug, first plug with second plug seals sliding connection respectively feed cylinder inner wall, first catch bar promotes first plug with second plug follows feed cylinder slides from top to bottom, feed cylinder is provided with first inlet pipe, second inlet pipe outward, the one end intercommunication of first inlet pipe first feed inlet, be provided with heating device on the first inlet pipe, the second intercommunication the second feed inlet, be provided with third plug, second catch bar in the second feed inlet, the second catch bar promotes the third plug follows the second is left and right sides and is moved, the second is provided with the third inlet pipe.
5. The device for producing a novel antiperspirant and deodorant preparation of plants according to claim 4, which is characterized in that: the heating device comprises a jacket, an electric heating wire and heat conduction oil, wherein the jacket surrounds the first feeding pipe, and the electric heating wire and the heat conduction oil are located in the jacket.
6. The device for producing a novel antiperspirant and deodorant preparation of plants according to claim 4, which is characterized in that: the first heating cavity is arranged in the first pushing plug, the second heating cavity is arranged in the connecting rod, and the third heating cavity is arranged in the second pushing plug.
7. The device for producing a novel antiperspirant and deodorant preparation of plants according to claim 4, which is characterized in that: the first feeding port is located above the second feeding port.
8. The device for producing a novel antiperspirant and deodorant preparation of plants according to claim 4, which is characterized in that: and an opening matched with the radian of the feeding cylinder is formed in the end part of the third pushing plug.
9. The apparatus for producing a novel antiperspirant and deodorant formulation of a plant as claimed in claim 6, wherein: the upper surface of the first pushing plug, the upper surface of the second pushing plug and the lower surface of the second pushing plug are of inclined structures.
10. A novel antiperspirant and deodorant formulation according to claim 1 or 2, which is useful in emulsions, spread sticks or sprays.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202311571365.5A CN117695174A (en) | 2023-11-23 | 2023-11-23 | Novel plant antiperspirant and deodorant preparation, and preparation method, production device and application thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202311571365.5A CN117695174A (en) | 2023-11-23 | 2023-11-23 | Novel plant antiperspirant and deodorant preparation, and preparation method, production device and application thereof |
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| CN117695174A true CN117695174A (en) | 2024-03-15 |
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| CN202311571365.5A Pending CN117695174A (en) | 2023-11-23 | 2023-11-23 | Novel plant antiperspirant and deodorant preparation, and preparation method, production device and application thereof |
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| Country | Link |
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| CN (1) | CN117695174A (en) |
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2023
- 2023-11-23 CN CN202311571365.5A patent/CN117695174A/en active Pending
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