CN117414328A - Antioxidant and oil-controlling powder cake composition and preparation method thereof - Google Patents
Antioxidant and oil-controlling powder cake composition and preparation method thereof Download PDFInfo
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- CN117414328A CN117414328A CN202311554967.XA CN202311554967A CN117414328A CN 117414328 A CN117414328 A CN 117414328A CN 202311554967 A CN202311554967 A CN 202311554967A CN 117414328 A CN117414328 A CN 117414328A
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- powder
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- oil
- composition
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- 239000000843 powder Substances 0.000 title claims abstract description 171
- 230000003078 antioxidant effect Effects 0.000 title claims abstract description 60
- 239000003963 antioxidant agent Substances 0.000 title claims abstract description 59
- 239000000203 mixture Substances 0.000 title claims abstract description 32
- 238000002360 preparation method Methods 0.000 title abstract description 11
- 229910052500 inorganic mineral Inorganic materials 0.000 claims abstract description 31
- 239000011707 mineral Substances 0.000 claims abstract description 31
- 239000011159 matrix material Substances 0.000 claims abstract description 30
- 239000002270 dispersing agent Substances 0.000 claims abstract description 29
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 26
- 238000000227 grinding Methods 0.000 claims abstract description 25
- -1 DPPH free radical Chemical class 0.000 claims abstract description 20
- 239000002994 raw material Substances 0.000 claims abstract description 15
- 239000000853 adhesive Substances 0.000 claims abstract description 12
- 230000001070 adhesive effect Effects 0.000 claims abstract description 12
- 239000002245 particle Substances 0.000 claims description 41
- 238000003756 stirring Methods 0.000 claims description 25
- 238000002156 mixing Methods 0.000 claims description 22
- 239000000463 material Substances 0.000 claims description 17
- 150000004676 glycans Chemical class 0.000 claims description 16
- 229920001282 polysaccharide Polymers 0.000 claims description 16
- 239000005017 polysaccharide Substances 0.000 claims description 16
- 239000004205 dimethyl polysiloxane Substances 0.000 claims description 12
- 229920000435 poly(dimethylsiloxane) Polymers 0.000 claims description 12
- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 claims description 12
- 229920002554 vinyl polymer Polymers 0.000 claims description 12
- 239000011230 binding agent Substances 0.000 claims description 11
- 238000010521 absorption reaction Methods 0.000 claims description 10
- 238000000034 method Methods 0.000 claims description 10
- 238000001694 spray drying Methods 0.000 claims description 10
- 239000011148 porous material Substances 0.000 claims description 9
- 239000000243 solution Substances 0.000 claims description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 8
- IIZPXYDJLKNOIY-JXPKJXOSSA-N 1-palmitoyl-2-arachidonoyl-sn-glycero-3-phosphocholine Chemical class CCCCCCCCCCCCCCCC(=O)OC[C@H](COP([O-])(=O)OCC[N+](C)(C)C)OC(=O)CCC\C=C/C\C=C/C\C=C/C\C=C/CCCCC IIZPXYDJLKNOIY-JXPKJXOSSA-N 0.000 claims description 7
- 229910021578 Iron(III) chloride Inorganic materials 0.000 claims description 7
- 241000133231 Marshallia caespitosa Species 0.000 claims description 7
- 238000001816 cooling Methods 0.000 claims description 7
- 238000010438 heat treatment Methods 0.000 claims description 7
- RBTARNINKXHZNM-UHFFFAOYSA-K iron trichloride Chemical compound Cl[Fe](Cl)Cl RBTARNINKXHZNM-UHFFFAOYSA-K 0.000 claims description 7
- 102000008186 Collagen Human genes 0.000 claims description 6
- 108010035532 Collagen Proteins 0.000 claims description 6
- XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 claims description 6
- 239000007864 aqueous solution Substances 0.000 claims description 6
- 229920001436 collagen Polymers 0.000 claims description 6
- 150000001875 compounds Chemical class 0.000 claims description 6
- 239000002105 nanoparticle Substances 0.000 claims description 6
- 238000003825 pressing Methods 0.000 claims description 6
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims description 5
- 238000005520 cutting process Methods 0.000 claims description 5
- 238000003760 magnetic stirring Methods 0.000 claims description 5
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 claims description 5
- IXPNQXFRVYWDDI-UHFFFAOYSA-N 1-methyl-2,4-dioxo-1,3-diazinane-5-carboximidamide Chemical group CN1CC(C(N)=N)C(=O)NC1=O IXPNQXFRVYWDDI-UHFFFAOYSA-N 0.000 claims description 3
- 239000004698 Polyethylene Substances 0.000 claims description 3
- 229920002472 Starch Polymers 0.000 claims description 3
- 229940073609 bismuth oxychloride Drugs 0.000 claims description 3
- BWOROQSFKKODDR-UHFFFAOYSA-N oxobismuth;hydrochloride Chemical compound Cl.[Bi]=O BWOROQSFKKODDR-UHFFFAOYSA-N 0.000 claims description 3
- 229920000573 polyethylene Polymers 0.000 claims description 3
- 235000010413 sodium alginate Nutrition 0.000 claims description 3
- 239000000661 sodium alginate Substances 0.000 claims description 3
- 229940005550 sodium alginate Drugs 0.000 claims description 3
- 239000008107 starch Substances 0.000 claims description 3
- 235000019698 starch Nutrition 0.000 claims description 3
- 239000011787 zinc oxide Substances 0.000 claims description 3
- BRPQOXSCLDDYGP-UHFFFAOYSA-N calcium oxide Chemical compound [O-2].[Ca+2] BRPQOXSCLDDYGP-UHFFFAOYSA-N 0.000 claims description 2
- 239000000292 calcium oxide Substances 0.000 claims description 2
- ODINCKMPIJJUCX-UHFFFAOYSA-N calcium oxide Inorganic materials [Ca]=O ODINCKMPIJJUCX-UHFFFAOYSA-N 0.000 claims description 2
- FBAFATDZDUQKNH-UHFFFAOYSA-M iron chloride Chemical compound [Cl-].[Fe] FBAFATDZDUQKNH-UHFFFAOYSA-M 0.000 claims description 2
- MSRJTTSHWYDFIU-UHFFFAOYSA-N octyltriethoxysilane Chemical compound CCCCCCCC[Si](OCC)(OCC)OCC MSRJTTSHWYDFIU-UHFFFAOYSA-N 0.000 claims description 2
- 229960003493 octyltriethoxysilane Drugs 0.000 claims description 2
- KKCBUQHMOMHUOY-UHFFFAOYSA-N sodium oxide Chemical compound [O-2].[Na+].[Na+] KKCBUQHMOMHUOY-UHFFFAOYSA-N 0.000 claims description 2
- 229910001948 sodium oxide Inorganic materials 0.000 claims description 2
- XOLBLPGZBRYERU-UHFFFAOYSA-N tin dioxide Chemical compound O=[Sn]=O XOLBLPGZBRYERU-UHFFFAOYSA-N 0.000 claims description 2
- 229910001887 tin oxide Inorganic materials 0.000 claims description 2
- VXUYXOFXAQZZMF-UHFFFAOYSA-N titanium(IV) isopropoxide Chemical compound CC(C)O[Ti](OC(C)C)(OC(C)C)OC(C)C VXUYXOFXAQZZMF-UHFFFAOYSA-N 0.000 claims 2
- 230000000694 effects Effects 0.000 abstract description 12
- 210000002374 sebum Anatomy 0.000 abstract description 12
- 230000008030 elimination Effects 0.000 abstract description 7
- 238000003379 elimination reaction Methods 0.000 abstract description 7
- 239000006185 dispersion Substances 0.000 abstract description 5
- 238000001179 sorption measurement Methods 0.000 abstract description 5
- 238000005282 brightening Methods 0.000 abstract description 2
- 230000003647 oxidation Effects 0.000 abstract description 2
- 238000007254 oxidation reaction Methods 0.000 abstract description 2
- 238000009472 formulation Methods 0.000 abstract 1
- 230000000052 comparative effect Effects 0.000 description 13
- 235000013870 dimethyl polysiloxane Nutrition 0.000 description 10
- 238000004090 dissolution Methods 0.000 description 6
- 238000012360 testing method Methods 0.000 description 5
- 230000008859 change Effects 0.000 description 3
- 239000002537 cosmetic Substances 0.000 description 3
- 239000004519 grease Substances 0.000 description 3
- 230000028327 secretion Effects 0.000 description 3
- 239000002390 adhesive tape Substances 0.000 description 2
- 238000004220 aggregation Methods 0.000 description 2
- 230000002776 aggregation Effects 0.000 description 2
- 230000004888 barrier function Effects 0.000 description 2
- MGJZITXUQXWAKY-UHFFFAOYSA-N diphenyl-(2,4,6-trinitrophenyl)iminoazanium Chemical compound [O-][N+](=O)C1=CC([N+](=O)[O-])=CC([N+]([O-])=O)=C1N=[N+](C=1C=CC=CC=1)C1=CC=CC=C1 MGJZITXUQXWAKY-UHFFFAOYSA-N 0.000 description 2
- 238000002474 experimental method Methods 0.000 description 2
- 235000021588 free fatty acids Nutrition 0.000 description 2
- TUJKJAMUKRIRHC-UHFFFAOYSA-N hydroxyl Chemical compound [OH] TUJKJAMUKRIRHC-UHFFFAOYSA-N 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 238000005303 weighing Methods 0.000 description 2
- 229920000663 Hydroxyethyl cellulose Polymers 0.000 description 1
- 239000004354 Hydroxyethyl cellulose Substances 0.000 description 1
- 206010020751 Hypersensitivity Diseases 0.000 description 1
- 240000007594 Oryza sativa Species 0.000 description 1
- 235000007164 Oryza sativa Nutrition 0.000 description 1
- 208000026935 allergic disease Diseases 0.000 description 1
- 230000007815 allergy Effects 0.000 description 1
- 229940099583 aluminum starch octenylsuccinate Drugs 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 239000008367 deionised water Substances 0.000 description 1
- 229910021641 deionized water Inorganic materials 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 235000013312 flour Nutrition 0.000 description 1
- 235000019447 hydroxyethyl cellulose Nutrition 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 230000002045 lasting effect Effects 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 231100000957 no side effect Toxicity 0.000 description 1
- 238000000643 oven drying Methods 0.000 description 1
- 230000000149 penetrating effect Effects 0.000 description 1
- 239000002504 physiological saline solution Substances 0.000 description 1
- 235000009566 rice Nutrition 0.000 description 1
- 230000037307 sensitive skin Effects 0.000 description 1
- 230000036555 skin type Effects 0.000 description 1
- 238000007711 solidification Methods 0.000 description 1
- 230000008023 solidification Effects 0.000 description 1
- 230000000638 stimulation Effects 0.000 description 1
Classifications
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/20—Halogens; Compounds thereof
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- A—HUMAN NECESSITIES
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/27—Zinc; Compounds thereof
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/35—Ketones, e.g. benzophenone
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- A61K8/553—Phospholipids, e.g. lecithin
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- A61K8/89—Polysiloxanes
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- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/12—Face or body powders for grooming, adorning or absorbing
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/41—Particular ingredients further characterized by their size
- A61K2800/412—Microsized, i.e. having sizes between 0.1 and 100 microns
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- Fats And Perfumes (AREA)
- Cosmetics (AREA)
Abstract
The invention provides an antioxidant and oil-controlling powder cake composition and a preparation method thereof, wherein the powder cake composition comprises the following raw materials in parts by weight: 25-55 parts of biological matrix powder, 35-75 parts of active mineral powder, 2-5 parts of anti-caking agent, 8-12 parts of antioxidant, 5-8 parts of dispersing agent and 2-4 parts of adhesive; the preparation method of the powder by S1, the dispersion of S2, the secondary grinding of S3, the preparation of the powder cake by S4 and the like are combined with the formulation of the composition, the prepared powder cake has better oxidation resistance and oil control effect, prevents the skin after makeup from being oxidized and dullness, achieves the effects of brightening and even skin color, has strong oil adsorption capacity, has a matte texture, effectively removes the oily light on the face, has the DPPH free radical elimination rate of 74.0-78.9%, has the hydroxyl free radical elimination rate of 65.1-68.9%, has the oil control efficiency of 95.9% and has the sebum resistance score of 10 minutes, and is a popular product.
Description
Technical Field
The invention relates to the technical field of cosmetics, in particular to an antioxidant and oil-controlling powder cake composition and a preparation method thereof.
Background
The world of the 80 th century has entered an era of advanced development of science and technology, and people need to work with high efficiency, live in a fast pace, and at the same time, simplify the requirements for cosmetic procedures, and demand versatility for the performance of products. Therefore, some developed countries have proposed a cake with both foundation effect and make-up function, and the cake is made of fine powder through pressing into cake-shaped cosmetics, so that the cake is fine and smooth, and can help users make up and prevent the change of makeup caused by interference of external factors. And the powder cake can also lighten the skin color, cover the face blemish and fill the uneven places of the face. The skin of human body can easily secrete grease in daily state, only foundation make-up with foundation make-up liquid, carefully drawn makeup can slide along with grease secretion over time, or the eyeground, face frequency can appear foundation, eye shadow, blush's spot. The existing powder cake is not fine enough in texture, is easy to accumulate on the surface of skin or generate a floating powder phenomenon, and is more easy to cause oil skin caking especially aiming at the skin types of oil skin, mixed oil skin and oil sensitive skin. Meanwhile, the extensibility of part of the powder cake is poor, uneven make-up effect is easy to appear after the powder cake is used, and the uniformity and the adherence of the powder cake are poor. Some powder cakes are easy to make-up or easy to oxidize and appear dull after being used, and especially under hot and humid climates, the requirements of users on long-time lasting make-up effect cannot be met.
Disclosure of Invention
In view of the above, the present invention provides an antioxidant and oil-controlling cake composition and a preparation method thereof, which solve the above problems.
The technical scheme of the invention is realized as follows: an antioxidant and oil-controlling powder cake composition: the material comprises the following raw materials in parts by weight: 25-55 parts of biological matrix powder, 35-75 parts of active mineral powder, 2-5 parts of anti-caking agent, 8-12 parts of antioxidant, 5-8 parts of dispersing agent and 2-4 parts of adhesive; the biological matrix powder is Qiya seed powder, silk powder and puffball powder with the mass ratio of (2.5-6.9) to (10.5-15.2) to (0.4-1.9); the dispersing agent is a compound of algal polysaccharide and ferric chloride.
Further, the material comprises the following raw materials in parts by weight: the material comprises the following raw materials in parts by weight: 40 parts of biological matrix powder, 55 parts of active mineral powder, 3 parts of anti-caking agent, 10 parts of antioxidant, 7 parts of dispersing agent and 3 parts of adhesive.
Further, the active mineral powder is selected from any one or a combination of more of zinc oxide, bismuth oxychloride, titanium oxide, tin oxide, calcium oxide and sodium oxide, the particle size range is less than 90um, and the active mineral powder contains 2-10% of quasi-nano particles with the pore diameter within the range of 100-900 nm.
Further, the anti-caking agent is any one or a combination of a plurality of starch octenyl aluminum succinate, vinyl polydimethylsiloxane, triisostearyl titanate isopropyl ester and triisostearyl titanate isopropyl ester.
Further, the antioxidant consists of (22-50): 10-30): 18-37, hydrogenated lecithin and alpha-anisone.
Further, the dispersing agent is prepared by adding 3-5 times of water into algal polysaccharide for dissolution to obtain an algal polysaccharide aqueous solution, adding ferric chloride solution with the molar concentration of 2-6mol/L, stirring and mixing, heating to 70-90 ℃ and continuing stirring for 1-3 hours, cooling, separating and purifying to obtain the algal polysaccharide-iron compound.
Further, the binder is selected from sodium alginate, polyethylene, vinyl polydimethylsiloxane or triethoxy octyl silane.
Further, the preparation method of the antioxidant and oil-controlling powder cake composition comprises the following steps:
s1, preparing powder: mixing and stirring the biological matrix powder and an anti-caking agent, and grinding for 2-4 hours at the temperature of 30-50 ℃ and the magnetic stirring rotation speed of 250-400rpm to obtain powder with the particle size of 0.4-0.6 mm;
s2, dispersing: mixing the active mineral powder with the powder obtained in the step S1 and an antioxidant to obtain a mixed material, adding a dispersing agent, and uniformly dispersing for 30-50min under the ultrasonic condition to obtain a dispersed powder;
s3, secondary grinding: placing the dispersed powder into a grinder, grinding under the pressure of 40-50kPa and the cutting rate of 3-8um/s, grinding for 15-20min to obtain powder with the particle size of 0.2-0.4mm, and spray drying and curing to obtain oil absorption particles;
s4, preparing a powder cake: mixing the oil absorption particles with binder, stirring, and pressing in a mold to obtain antioxidant and oil-controlling powder cake.
Further, the ultrasonic power of the S2 is 300-800W, and the frequency is 20-60KHz.
Further, the inlet temperature of the S3 spray drying is 80-120 ℃, the outlet temperature is 50-90 ℃, the feeding speed is 150-250mL/h, and the flow rate of compressed air is 400-700L/h.
Compared with the prior art, the invention has the beneficial effects that:
the invention uses biological matrix powder, active mineral powder and the like to prepare the powder cake which is mixed according to the ratio, has better oxidation resistance and oil control effect, prevents the skin from being oxidized and dulled after makeup, achieves the effects of brightening and even skin color, has strong ability of absorbing grease, has matt texture, and effectively removes the oily light on the face;
wherein the biological matrix powder is combined with the anti-caking agent, the anti-caking agent can eliminate or reduce electrostatic effect, reduce the adsorption force among particles, ensure that the powder keeps good fluidity, and simultaneously, the anti-caking agent can react with moisture in the air to form a film covered on the surfaces of the powder particles to prevent moisture from penetrating, thereby reducing the caking of the biological matrix powder; the biological matrix powder can form an adsorption layer on the surface of the skin, adsorb free fatty acid in the skin and quickly flocculate to inhibit sebum secretion;
the raw materials combine chemical bonds on particles among the biological matrix powder, the active mineral powder and the antioxidant through the dispersing agent to form a barrier layer among stable particles, prevent aggregation of the particles and change the surface charge property, so that the dispersion is realized, and the powder is more uniform; the secondary grinding ensures that the powder is finer and finer, can be orderly adhered to pores on the surface of the skin, can better adsorb sebum in the pores, is more skin-friendly, and ensures that the skin makeup resistance is longer.
Detailed Description
In order to better understand the technical content of the present invention, the following provides specific examples to further illustrate the present invention.
The experimental methods used in the embodiment of the invention are conventional methods unless otherwise specified.
Materials, reagents, and the like used in the examples of the present invention are commercially available unless otherwise specified.
The embodiment of the invention proves that the invention has no side effects such as allergy, stimulation and the like through experiments such as spot patches in hospitals.
Example 1
An antioxidant and oil-controlling powder cake composition: the material comprises the following raw materials in parts by weight: 25-55 parts of biological matrix powder, 35 parts of active mineral powder, 2 parts of anti-caking agent, 8 parts of antioxidant, 5 parts of dispersing agent and 2 parts of adhesive;
the biological matrix powder is Qiya seed powder, silk powder and puffball powder with the mass ratio of 2.5:10.5:0.4;
the active mineral powder is selected from zinc oxide with particle diameter less than 90um, wherein the active mineral powder contains quasi-nano-level particles with pore diameter of 100-900nm of 2-10%;
the anti-caking agent is aluminum starch octenyl succinate;
the antioxidant comprises end-lacking collagen, hydrogenated lecithin and alpha-anisone in a mass ratio of 22:10:18;
the dispersing agent is prepared by adding water with the mass being 3 times that of algal polysaccharide to dissolve to obtain an aqueous algal polysaccharide solution, adding ferric chloride solution with the molar concentration of 2mol/L, stirring and mixing, heating to 70 ℃ in a volume ratio of 3:12, continuously stirring for 1h, cooling, separating and purifying to obtain an algal polysaccharide-ferric compound;
the binder is selected from sodium alginate or polyethylene.
Example 2
An antioxidant and oil-controlling powder cake composition: the material comprises the following raw materials in parts by weight: 55 parts of biological matrix powder, 75 parts of active mineral powder, 5 parts of anti-caking agent, 12 parts of antioxidant, 8 parts of dispersing agent and 4 parts of adhesive;
the biological matrix powder is Qiya seed powder, silk powder and puffball powder with the mass ratio of 6.9:15.2:1.9;
the active mineral powder is selected from bismuth oxychloride with the particle size range smaller than 90um, wherein the active mineral powder contains 2-10% of quasi-nano particles with the pore diameter within the range of 100-900 nm;
the anti-caking agent is vinyl polydimethylsiloxane;
the antioxidant comprises end-lacking collagen, hydrogenated lecithin and alpha-anisone in a mass ratio of 50:30:37;
the dispersing agent is prepared by adding 5 times of water into algal polysaccharide for dissolution to obtain an aqueous solution of algal polysaccharide, adding an iron chloride solution with the molar concentration of 6mol/L, stirring and mixing, heating to 90 ℃ in a volume ratio of 9:20, continuously stirring for 3 hours, cooling, separating and purifying to obtain an algal polysaccharide-iron compound;
the adhesive is vinyl polydimethylsiloxane.
Example 3
An antioxidant and oil-controlling powder cake composition: the material comprises the following raw materials in parts by weight: 40 parts of biological matrix powder, 55 parts of active mineral powder, 3 parts of anti-caking agent, 10 parts of antioxidant, 7 parts of dispersing agent and 3 parts of adhesive;
the biological matrix powder is Qiya seed powder, silk powder and puffball powder with the mass ratio of 4.5:12.3:1.2;
the active mineral powder is selected from titanium oxide with the particle size range less than 90um, wherein the active mineral powder contains 2-10% of quasi-nano particles with the pore diameter in the range of 100-900 nm;
the anti-caking agent is vinyl polydimethylsiloxane;
the antioxidant comprises end-lacking collagen, hydrogenated lecithin and alpha-anisone in a mass ratio of 35:20:28;
the dispersing agent is prepared by adding water with the mass of 4 times into algal polysaccharide to dissolve to obtain an aqueous solution of algal polysaccharide, adding ferric chloride solution with the molar concentration of 4mol/L, stirring and mixing, heating to 80 ℃ in a volume ratio of 7:16, continuously stirring for 2 hours, cooling, separating and purifying to obtain an algal polysaccharide-ferric compound;
the binder is selected from vinyl polydimethyl siloxane;
the following preparation methods were employed for the above examples 1-3:
s1, preparing powder: mixing and stirring the biological matrix powder and an anti-caking agent, and grinding for 3 hours at a grinding temperature of 40 ℃ and a magnetic stirring rotating speed of 350rpm to obtain powder with a particle size of 0.5 mm;
s2, dispersing: mixing the active mineral powder with the powder obtained in the step S1 and an antioxidant to obtain a mixed material, adding a dispersing agent, uniformly dispersing for 40min under ultrasonic conditions, and obtaining a dispersed powder, wherein the ultrasonic power is 500W and the frequency is 40 KHz;
s3, secondary grinding: putting the dispersed powder into a grinder, grinding the powder into powder with the particle size of 0.3mm, wherein the grinding pressure is 45kPa, the cutting rate is 5um/s, grinding the powder for 18min to obtain powder with the particle size of 0.3mm, and then performing spray drying and solidification, wherein the inlet temperature of spray drying is 100 ℃, the outlet temperature is 70 ℃, the feeding speed is 200mL/h, and the compressed air flow rate is 600L/h to obtain oil absorption particles;
s4, preparing a powder cake: mixing the oil absorption particles with binder, stirring, and pressing in a mold to obtain antioxidant and oil-controlling powder cake.
Example 4
An antioxidant and oil-controlling powder cake composition: the material comprises the following raw materials in parts by weight: 40 parts of biological matrix powder, 55 parts of active mineral powder, 3 parts of anti-caking agent, 10 parts of antioxidant, 7 parts of dispersing agent and 3 parts of adhesive;
the biological matrix powder is Qiya seed powder, silk powder and puffball powder with the mass ratio of 4.5:12.3:1.2;
the active mineral powder is selected from titanium oxide with the particle size range less than 90um, wherein the active mineral powder contains 2-10% of quasi-nano particles with the pore diameter in the range of 100-900 nm;
the anti-caking agent is vinyl polydimethylsiloxane;
the antioxidant comprises end-lacking collagen, hydrogenated lecithin and alpha-anisone in a mass ratio of 35:20:28;
the dispersing agent is prepared by adding water with the mass of 4 times into algal polysaccharide to dissolve to obtain an aqueous solution of algal polysaccharide, adding ferric chloride solution with the molar concentration of 4mol/L, stirring and mixing, heating to 80 ℃ in a volume ratio of 7:16, continuously stirring for 2 hours, cooling, separating and purifying to obtain an algal polysaccharide-ferric compound;
the binder is selected from vinyl polydimethyl siloxane;
the above examples employed the following preparation methods:
s1, preparing powder: mixing and stirring the biological matrix powder and an anti-caking agent, and grinding for 2-4 hours at the temperature of 30 ℃ and the magnetic stirring rotating speed of 250rpm to obtain powder with the particle size of 0.4 mm;
s2, dispersing: mixing the active mineral powder with the powder obtained in the step S1 and an antioxidant to obtain a mixed material, adding a dispersing agent, uniformly dispersing for 30min under ultrasonic conditions, and obtaining a dispersed powder, wherein the ultrasonic power is 300W and the frequency is 20 KHz;
s3, secondary grinding: the dispersion powder is put into a grinder, ground into powder with the particle size of 0.2mm, the grinding pressure is 40kPa, the cutting rate is 3um/s, grinding is carried out for 15min, the powder with the particle size of 0.2mm is obtained, then the powder is solidified by spray drying, the inlet temperature of spray drying is 80 ℃, the outlet temperature is 50 ℃, the feeding speed is 150mL/h, and the compressed air flow rate is 400L/h, so as to obtain oil absorption particles;
s4, preparing a powder cake: mixing the oil absorption particles with binder, stirring, and pressing in a mold to obtain antioxidant and oil-controlling powder cake.
Example 5
An antioxidant and oil-controlling powder cake composition: the material comprises the following raw materials in parts by weight: 40 parts of biological matrix powder, 55 parts of active mineral powder, 3 parts of anti-caking agent, 10 parts of antioxidant, 7 parts of dispersing agent and 3 parts of adhesive;
the biological matrix powder is Qiya seed powder, silk powder and puffball powder with the mass ratio of 4.5:12.3:1.2;
the active mineral powder is selected from titanium oxide with the particle size range less than 90um, wherein the active mineral powder contains 2-10% of quasi-nano particles with the pore diameter in the range of 100-900 nm;
the anti-caking agent is vinyl polydimethylsiloxane;
the antioxidant comprises end-lacking collagen, hydrogenated lecithin and alpha-anisone in a mass ratio of 35:20:28;
the dispersing agent is prepared by adding water with the mass of 4 times into algal polysaccharide to dissolve to obtain an aqueous solution of algal polysaccharide, adding ferric chloride solution with the molar concentration of 4mol/L, stirring and mixing, heating to 80 ℃ in a volume ratio of 7:16, continuously stirring for 2 hours, cooling, separating and purifying to obtain an algal polysaccharide-ferric compound;
the binder is selected from vinyl polydimethyl siloxane;
the above examples employed the following preparation methods:
s1, preparing powder: mixing and stirring the biological matrix powder and an anti-caking agent, and grinding for 4 hours at a grinding temperature of 50 ℃ and a magnetic stirring rotating speed of 400rpm to obtain powder with a particle size of 0.6 mm;
s2, dispersing: mixing the active mineral powder with the powder obtained in the step S1 and an antioxidant to obtain a mixed material, adding a dispersing agent, uniformly dispersing for 50min under ultrasonic conditions, and obtaining a dispersed powder, wherein the ultrasonic power is 800W and the frequency is 60 KHz;
s3, secondary grinding: the dispersion powder is put into a grinder, ground into powder with the particle size of 0.4mm, the grinding pressure is 50kPa, the cutting rate is 8um/s, grinding is carried out for 20min, the powder with the particle size of 0.4mm is obtained, then the powder is solidified by spray drying, the inlet temperature of the spray drying is 120 ℃, the outlet temperature is 90 ℃, the feeding speed is 250mL/h, and the compressed air flow rate is 700L/h, thus obtaining oil absorption particles;
s4, preparing a powder cake: mixing the oil absorption particles with binder, stirring, and pressing in a mold to obtain antioxidant and oil-controlling powder cake.
Comparative example 1
The comparison example is different from example 3 in that an antioxidant and oil-controlling powder cake composition comprises the following raw materials in parts by weight: 15 parts of biological matrix powder, 25 parts of active mineral powder, 1 part of anti-caking agent, 15 parts of antioxidant, 10 parts of dispersing agent and 1 part of adhesive.
Comparative example 2
The difference between this comparative example and example 3 is that the bio-based powder in the antioxidant and oil controlling compact composition was replaced with starch and rice flour in a mass ratio of 4.5:12.3.
Comparative example 3
This comparative example differs from example 3 in that the dispersant in an antioxidant, oil control compact composition is an equivalent amount of hydroxyethyl cellulose.
Comparative example 4
This comparative example differs from example 3 in that no antioxidant is added to an antioxidant, oil-controlling compact composition.
1. Antioxidant Capacity test
The cakes and the commercially available cakes prepared by the compositions and methods of examples 1-5 and comparative examples 1-4 were divided into 10 groups of three parallel tests, and the cakes were diluted 10 times and measured by DPPH radical elimination rate and hydroxyl radical elimination rate:
as can be seen from the above table, the compact composition of the present invention has a certain antioxidant capacity, a DPPH radical elimination rate of 74.0 to 78.9% and a hydroxyl radical elimination rate of 65.1 to 68.9%, wherein the effect of example 3 is the best, and compared with comparative example 4, it is demonstrated that the antioxidant is added to the compact composition of the present invention to have a more remarkable effect on the elimination of DPPH radicals and hydroxyl radicals, and in comparative examples 1 to 3, it is demonstrated that the proportion, the bio-matrix powder, and the dispersant have a certain effect on the overall antioxidant effect.
2. Oil control performance
The pressed powders and commercially available pressed powders prepared in examples 1 to 5 and comparative examples 1 to 4 were divided into 10 groups of 3 parallel tests according to the above-mentioned method;
1. oil control: adhesive tape was attached to a clean slide and weighed m 0 Smearing proper amount of powder cake on adhesive tape, oven drying, and weighing m 1 . Immersing the powder cake sample in 0.9% physiological saline, stirring for 30min, rinsing with deionized water, drying, and weighing m 2 。
Oil control (%) = (m) 2 -m 0 )/(m 1 -m 0 )×100；
2. Sebum resistance test: 1g of foundation sample is taken and placed on a black-and-white plate, a flat foundation film is coated and coated, an equal amount of artificial simulated sebum is dripped on the coating film, the black-and-white plate is inclined at 45 ℃, the sebum naturally flows down, the integrity of a chalk film is observed, and the test standard is that:
| status of | Score value |
| The dissolution area of the foundation by artificial sebum is 71-100% | 1-3 minutes |
| The dissolution area of the foundation by artificial sebum is 30-70% | 4-6 minutes |
| The dissolution area of the foundation by artificial sebum is less than 30 percent | 7-10 min |
The results are shown in the following table:
from the results, the powder cake provided by the invention has the advantages that the oil control effect is synergistically exerted through the combination of the raw materials, the oil control efficiency reaches 95.9%, the sebum resistance score is 10 minutes, the dissolution area of the powder foundation by artificial sebum is less than 30%, and compared with comparative example 2, the example group shows that the biological matrix powder has better adsorption capacity, can form an adsorption layer on the surface of skin, can adsorb free fatty acid in the skin and flocculate rapidly, inhibit sebum secretion and prevent oil from being pulled out; compared with comparative example 3, the dispersing agent of the present invention forms a barrier layer between stable particles by bonding with chemical bonds on the powder particles, prevents aggregation of the particles, and simultaneously reacts with ions on the surfaces of the particles to change the surface charge properties, so that the particles are charged and mutually repelled, thereby realizing dispersion and making the powder more uniform.
The foregoing description of the preferred embodiments of the invention is not intended to be limiting, but rather is intended to cover all modifications, equivalents, alternatives, and improvements that fall within the spirit and scope of the invention.
Claims (10)
1. An antioxidant and oil control powder cake composition is characterized in that: the material comprises the following raw materials in parts by weight: 25-55 parts of biological matrix powder, 35-75 parts of active mineral powder, 2-5 parts of anti-caking agent, 8-12 parts of antioxidant, 5-8 parts of dispersing agent and 2-4 parts of adhesive; the biological matrix powder is Qiya seed powder, silk powder and puffball powder with the mass ratio of (2.5-6.9) to (10.5-15.2) to (0.4-1.9); the dispersing agent is a compound of algal polysaccharide and ferric chloride.
2. An antioxidant, oil control compact composition as defined in claim 1, wherein: the material comprises the following raw materials in parts by weight: the material comprises the following raw materials in parts by weight: 40 parts of biological matrix powder, 55 parts of active mineral powder, 3 parts of anti-caking agent, 10 parts of antioxidant, 7 parts of dispersing agent and 3 parts of adhesive.
3. An antioxidant, oil control compact composition as defined in claim 1, wherein: the active mineral powder is selected from any one or more of zinc oxide, bismuth oxychloride, titanium oxide, tin oxide, calcium oxide and sodium oxide, has a particle size range of less than 90um, and contains 2-10% of quasi-nanoscale particles with a pore diameter of 100-900 nm.
4. An antioxidant, oil control compact composition as defined in claim 1, wherein: the anti-caking agent is starch octenyl aluminum succinate, vinyl polydimethylsiloxane, triisostearyl isopropyl titanate or any one or a combination of a plurality of the triisostearyl isopropyl titanate.
5. An antioxidant, oil control compact composition as defined in claim 1, wherein: the antioxidant consists of (22-50) end-lacking collagen (10-30) and (18-37) hydrogenated lecithin and alpha-anisone in a mass ratio.
6. An antioxidant, oil control compact composition as defined in claim 1, wherein: the dispersing agent is prepared by adding 3-5 times of water into algal polysaccharide to dissolve to obtain an aqueous solution of algal polysaccharide, adding an iron chloride solution with the molar concentration of 2-6mol/L, stirring and mixing, heating to 70-90 ℃ and continuing stirring for 1-3 hours, cooling, separating and purifying to obtain an algal polysaccharide-iron compound.
7. An antioxidant, oil control compact composition as defined in claim 1, wherein: the binder is selected from sodium alginate, polyethylene, vinyl polydimethylsiloxane or triethoxy octyl silane.
8. The method for preparing the antioxidant and oil-controlling powder cake composition as claimed in claim 1, wherein the method comprises the following steps: the method comprises the following steps:
s1, preparing powder: mixing and stirring the biological matrix powder and an anti-caking agent, and grinding for 2-4 hours at the temperature of 30-50 ℃ and the magnetic stirring rotation speed of 250-400rpm to obtain powder with the particle size of 0.4-0.6 mm;
s2, dispersing: mixing the active mineral powder with the powder obtained in the step S1 and an antioxidant to obtain a mixed material, adding a dispersing agent, and uniformly dispersing for 30-50min under the ultrasonic condition to obtain a dispersed powder;
s3, secondary grinding: placing the dispersed powder into a grinder, grinding under the pressure of 40-50kPa and the cutting rate of 3-8um/s, grinding for 15-20min to obtain powder with the particle size of 0.2-0.4mm, and spray drying and curing to obtain oil absorption particles;
s4, preparing a powder cake: mixing the oil absorption particles with binder, stirring, and pressing in a mold to obtain antioxidant and oil-controlling powder cake.
9. The method for preparing the antioxidant and oil-controlling powder cake composition as claimed in claim 1, wherein the method comprises the following steps: the ultrasonic power of the S2 is 300-800W, and the frequency is 20-60KHz.
10. The method for preparing the antioxidant and oil-controlling powder cake composition as claimed in claim 1, wherein the method comprises the following steps: the inlet temperature of the S3 spray drying is 80-120 ℃, the outlet temperature is 50-90 ℃, the feeding speed is 150-250mL/h, and the flow rate of compressed air is 400-700L/h.
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