CN117405624A - Terahertz near-field imaging system measurement method with precision superior to 10 nanometers - Google Patents
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Abstract
Description
技术领域Technical field
一种精度优于10纳米的太赫兹近场成像系统测量方法,属于太赫兹近场系统成像领域,具体涉及太赫兹近场系统精度测量。A terahertz near-field imaging system measurement method with an accuracy better than 10 nanometers belongs to the field of terahertz near-field system imaging and specifically involves the accuracy measurement of terahertz near-field systems.
背景技术Background technique
太赫兹近场成像系统是基于原子力显微镜系统,在原子力探针的针尖上耦合一定功率的太赫兹波进入待测样品内部,利用太赫兹波的穿透性和原子力探针针尖的衍射性,对待测样品的表面和内部同时实现的高分辨率的成像功能。太赫兹近场成像系统的成像精度一般为纳米级精度,具体为几十纳米精度,常取决于探针针尖的尖端的曲率半径,否则成像图形会失真。例如探针针尖的曲率半径为40纳米,那成像精度一般为40纳米,随着针尖的使用,针尖磨损曲率半径变为50纳米,那么成像精度为50纳米。原子力显微镜探针针尖的制作比较复杂,如果尖端曲率半径过小,在使用时和样品间作用力会导致针尖磨损。理论上探针针尖曲率半径可以做到很小,突破40纳米完全可以实现,但是对制作工艺、成本、使用条件提出很高要求,不利于推广使用。一般探针针尖曲率半径为40纳米,导致太赫兹近场成像系统的精度难以突破40纳米。The terahertz near-field imaging system is based on the atomic force microscope system. A terahertz wave of a certain power is coupled to the tip of the atomic force probe into the interior of the sample to be measured. The penetrating property of the terahertz wave and the diffraction property of the atomic force probe tip are used to treat the The high-resolution imaging function is realized simultaneously on the surface and inside of the measured sample. The imaging accuracy of a terahertz near-field imaging system is generally nanometer-level, specifically tens of nanometers, and often depends on the radius of curvature of the tip of the probe tip, otherwise the imaging pattern will be distorted. For example, if the radius of curvature of the probe tip is 40 nanometers, the imaging accuracy is generally 40 nanometers. As the tip is used, the tip wears and the radius of curvature becomes 50 nanometers, then the imaging accuracy is 50 nanometers. The production of the atomic force microscope probe tip is relatively complicated. If the tip curvature radius is too small, the force acting between the tip and the sample during use will cause tip wear. Theoretically, the radius of curvature of the probe tip can be very small, and a breakthrough of 40 nanometers is completely achievable. However, it places high requirements on the manufacturing process, cost, and usage conditions, which is not conducive to popularization and use. Generally, the radius of curvature of the probe tip is 40 nanometers, making it difficult for the accuracy of the terahertz near-field imaging system to exceed 40 nanometers.
随着科技的发展,如半导体芯片工艺突破到11纳米甚至7纳米,需要一种测量手段达到优于10纳米的精度,扫描电子显微镜是其中的一种选择,但是扫描电子显微镜在使用时需要抽真空和镀导电膜,影响待测样品的性能。太赫兹近场成像系统可直接无处理的在大气环境下进行成像无需进行特殊处理,但需要优化测量方法,提高测量精度到优于10纳米精度,满足半导体工艺发展的需要。With the development of science and technology, such as the breakthrough of semiconductor chip technology to 11 nanometers or even 7 nanometers, a measurement method is needed to achieve an accuracy better than 10 nanometers. Scanning electron microscope is one of the options, but scanning electron microscope requires extraction when used. Vacuum and conductive film plating affect the performance of the sample to be tested. The terahertz near-field imaging system can directly perform imaging in the atmospheric environment without special processing, but it needs to optimize the measurement method and improve the measurement accuracy to better than 10 nanometers to meet the needs of semiconductor process development.
发明内容Contents of the invention
为解决太赫兹近场系统成像精度依托原子力显微镜探针针尖精度,难以突破40纳米的成像精度的问题。本发明利用太赫兹近场成像系统中太赫兹波穿透性的特点,根据太赫兹近场成像逐点扫成像的原理,在固定扫描范围内,增加扫描点的数量,提高成像系统的精度,可优于10纳米。In order to solve the problem that the imaging accuracy of the terahertz near-field system relies on the accuracy of the atomic force microscope probe tip, it is difficult to break through the imaging accuracy of 40 nanometers. This invention utilizes the penetrability characteristics of terahertz waves in the terahertz near-field imaging system, and based on the principle of point-by-point scanning of terahertz near-field imaging, increases the number of scanning points within a fixed scanning range and improves the accuracy of the imaging system. Can be better than 10 nanometers.
本发明内容是利用太赫兹近场成像系统中太赫兹波的穿透性特点,采取逐点扫描成像保持精度和分辨率的方式,增加扫描点的数量提高精度,利用太赫兹近场成像中的太赫兹波成像,逐点扫描后内部太赫兹波可以穿透待测样品并反馈到接收进行成像,摆脱进行成像精度依靠原子力显微镜的探针针尖精度问题。根据太赫兹波逐点扫描成像的原理,选择固定的扫描范围,增加扫描点的数量,可以获得精度优于10纳米以上的测量方法。The content of the present invention is to utilize the penetrating characteristics of terahertz waves in the terahertz near-field imaging system, adopt a point-by-point scanning imaging method to maintain accuracy and resolution, increase the number of scanning points to improve accuracy, and utilize the terahertz near-field imaging system to maintain accuracy and resolution. Terahertz wave imaging, after point-by-point scanning, the internal terahertz wave can penetrate the sample to be measured and be fed back to the receiver for imaging, eliminating the problem of imaging accuracy that relies on the probe tip accuracy of the atomic force microscope. According to the principle of point-by-point scanning imaging of terahertz waves, by selecting a fixed scanning range and increasing the number of scanning points, a measurement method with an accuracy better than 10 nanometers can be obtained.
本发明提供一种精度优于10纳米的太赫兹近场成像系统测量方法,包括以下步骤:The present invention provides a terahertz near-field imaging system measurement method with an accuracy better than 10 nanometers, which includes the following steps:
步骤一,选择曲率半径为40纳米的探针;Step 1: Select a probe with a curvature radius of 40 nanometers;
步骤二,利用太赫兹近场成像系统逐点扫描成像,设置扫描参数;Step 2: Use the terahertz near-field imaging system to scan point by point and set the scanning parameters;
步骤三,逐点扫描后太赫兹波穿透待测样品并反馈到接收进行成像,成像图为内部成像图。Step 3: After point-by-point scanning, the terahertz wave penetrates the sample to be tested and is fed back to the receiver for imaging. The imaging picture is the internal imaging picture.
进一步,太赫兹系统的太赫兹源功率最少为50毫瓦以上。Furthermore, the terahertz source power of the terahertz system is at least 50 milliwatts.
进一步,步骤二中设置扫描参数的方法为,扫描范围为a纳米,扫描点数为n个,在扫描范围a固定的情况下,可增加扫描点数n的值,或在扫描点数n固定的情况下,降低扫描范围a的值,在内部成像图中,设置a/n小于10纳米。Furthermore, the method of setting the scanning parameters in step 2 is as follows: the scanning range is a nanometer and the number of scanning points is n. When the scanning range a is fixed, the value of the scanning point n can be increased, or when the scanning point number n is fixed , reduce the value of the scanning range a, and set a/n to less than 10 nanometers in the internal imaging map.
具体的,一种精度优于10纳米的太赫兹近场成像系统测量方法,利用太赫兹近场成像系统逐点扫描成像的原理和太赫兹波穿透性的特点,逐点扫描成像保持成像系统的精度和分辨率。针尖的太赫兹波穿透性摆脱针尖曲率半径对精度误差,利用太赫兹近场成像中太赫兹波穿透成像,逐点扫描后太赫兹波可穿透内部并反馈到外部进行接收成像,摆脱太赫兹近场成像中探针针尖成像限制系统成像精度的问题。根据太赫兹波逐点成像中没有探针针尖结构尺寸限制成像精度的问题,理论上增加扫描点的数量,可无限提高成像系统的精度。考虑到逐点扫描电机精度、信号传输时间延时等,在一定扫描范围内,适当增加扫描点的数量,在目前太赫兹近场成像系统中可提高成像精度从40纳米到10纳米。Specifically, a measurement method for a terahertz near-field imaging system with an accuracy better than 10 nanometers uses the principle of point-by-point scanning imaging of the terahertz near-field imaging system and the characteristics of the penetrability of terahertz waves. The point-by-point scanning imaging maintains the imaging system accuracy and resolution. The terahertz wave penetrability of the tip gets rid of the precision error caused by the tip curvature radius. The terahertz wave penetration imaging in terahertz near-field imaging is used. After point-by-point scanning, the terahertz wave can penetrate the interior and be fed back to the outside for reception and imaging. The problem of probe tip imaging in terahertz near-field imaging limits the imaging accuracy of the system. According to the point-by-point imaging of terahertz waves, there is no problem that the size of the probe tip structure limits the imaging accuracy. In theory, increasing the number of scanning points can infinitely improve the accuracy of the imaging system. Taking into account the point-by-point scanning motor accuracy, signal transmission time delay, etc., within a certain scanning range, appropriately increasing the number of scanning points can improve the imaging accuracy from 40 nanometers to 10 nanometers in the current terahertz near-field imaging system.
本发明具有以下有益效果:The invention has the following beneficial effects:
本发明专利的优点是工艺简单(相对于电子显微镜而言)、成本低(利用40纳米精度的探针,成本比10纳米精度探针大大降低)、操作简单,可推广应用到10纳米半导体工艺制程中。The advantages of the patented invention are simple process (compared to electron microscopy), low cost (using a 40-nanometer precision probe, the cost is much lower than a 10-nanometer precision probe), simple operation, and can be applied to 10-nanometer semiconductor processes In process.
附图说明Description of the drawings
图1是针尖端太赫兹波进入样品内部示意图;Figure 1 is a schematic diagram of the needle tip terahertz wave entering the interior of the sample;
图2是扫描范围内扫描点示意图;Figure 2 is a schematic diagram of scanning points within the scanning range;
图3是采取此测量方法成像精度图。Figure 3 is a chart of imaging accuracy using this measurement method.
其中图1中:1是探针,2是待测样品,3是太赫兹波进入的方向,4是进入样品后的太赫兹波返回方向。In Figure 1: 1 is the probe, 2 is the sample to be measured, 3 is the direction in which the terahertz wave enters, and 4 is the return direction of the terahertz wave after entering the sample.
具体实施方式Detailed ways
下面结合附图和实施例对本发明进一步说明。The present invention will be further described below in conjunction with the accompanying drawings and examples.
一种精度优于10纳米的太赫兹近场成像系统测量方法,利用太赫兹近场成像系统逐点扫描成像的原理和太赫兹波穿透性的特点,太赫兹近场成像中太赫兹波穿透成像,逐点扫描后太赫兹波可穿透内部并反馈到外部进行接收成像,摆脱太赫兹近场成像中探针针尖成像限制系统成像精度的问题。在一定扫描范围内,增加扫描点的数量,可提高成像系统的精度。在目前太赫兹近场成像系统中可使用40纳米的探针,将成像精度从40纳米提高到10纳米。A measurement method for a terahertz near-field imaging system with an accuracy better than 10 nanometers. It uses the principle of point-by-point scanning imaging of the terahertz near-field imaging system and the characteristics of the terahertz wave penetration. In terahertz near-field imaging, the terahertz wave penetrates Transparent imaging, after point-by-point scanning, the terahertz wave can penetrate the interior and be fed back to the outside for reception and imaging, getting rid of the problem of probe tip imaging in terahertz near-field imaging that limits the imaging accuracy of the system. Within a certain scanning range, increasing the number of scanning points can improve the accuracy of the imaging system. In current terahertz near-field imaging systems, 40-nanometer probes can be used to increase imaging accuracy from 40 nanometers to 10 nanometers.
太赫兹穿透性,太赫兹近场成像系统在原子力探针的尖端耦合一定功率的太赫兹波,在近场成像工作时,如图1所示,太赫兹波在探针1尖端向下方待测样品2方向传播,即太赫兹波进入的方向3,如图1所示。太赫兹近场成像系统中的太赫兹源功率要足够强,最少为50毫瓦,功率过小导致探针处的太赫兹波能量小,难以穿透待测样品。太赫兹波穿透待测样品后,其中有部分太赫兹波向探针方向传播,即进入样品后的太赫兹波返回方向4,如图1中所示,此时太赫兹波携带一定的待测样品信息,和探针携带的近场信息共同传递到成像系统中,可同时进行表面和内部的成像。太赫兹波的信号主要表现在内部成像方面。Terahertz penetration, the terahertz near-field imaging system couples a certain power of terahertz waves at the tip of the atomic force probe. When working in the near-field imaging, as shown in Figure 1, the terahertz wave waits downward at the tip of probe 1. The measured sample propagates in direction 2, which is the direction 3 where the terahertz wave enters, as shown in Figure 1. The power of the terahertz source in the terahertz near-field imaging system must be strong enough, at least 50 milliwatts. If the power is too small, the energy of the terahertz wave at the probe will be small, making it difficult to penetrate the sample to be measured. After the terahertz wave penetrates the sample to be measured, part of the terahertz wave propagates toward the probe, that is, the terahertz wave returns in the direction 4 after entering the sample, as shown in Figure 1. At this time, the terahertz wave carries a certain amount of radiation to be measured. The measured sample information and the near-field information carried by the probe are jointly transmitted to the imaging system, which can perform surface and internal imaging at the same time. The signal of terahertz wave is mainly manifested in internal imaging.
逐点扫描成像,太赫兹近场成像系统成像的特点是利用逐点扫描特点,如图2所示,扫描范围为方形,扫描点数为扫描完成一行时的总点数,扫描的点数和扫描行数相同。在太赫兹近场成像中,探针的成像为表面图,如扫描点数过多,相邻两点距离小于探针曲率半径,会导致表面图像失真,得不到真实图形。太赫兹波穿透的成像由于没有探针结构尺寸的限制,内部图像不存在失真现象。Point-by-point scanning imaging. The imaging characteristic of the terahertz near-field imaging system is the use of point-by-point scanning characteristics. As shown in Figure 2, the scanning range is square, the number of scanning points is the total number of points when scanning a line, the number of points scanned and the number of scanned lines. same. In terahertz near-field imaging, the imaging of the probe is a surface image. If there are too many scanning points and the distance between two adjacent points is less than the radius of curvature of the probe, the surface image will be distorted and the real image will not be obtained. Since there is no restriction on the size of the probe structure in the imaging of terahertz wave penetration, there is no distortion in the internal image.
扫描设置,在进行扫描时,设置扫描参数,如扫描范围为a纳米,扫描点数为n个,在扫描范围a固定的情况下,可增加扫描点数n的值,或在扫描点数n固定的情况下,降低扫描范围a的值。太赫兹近场成像的表面成像图设置要保证a/n大于40纳米(探针的曲率半径)。在内部成像图中,设置a/n小于10纳米,这样利用逐点扫描和太赫兹的穿透性,保证在内部成像图中成像精度优于10纳米。Scan setting, when scanning, set the scanning parameters, such as the scanning range is a nanometer and the number of scanning points is n. When the scanning range a is fixed, the value of the scanning point n can be increased, or when the scanning point n is fixed Next, reduce the value of scan range a. The surface imaging map setting for terahertz near-field imaging must ensure that a/n is greater than 40 nanometers (radius of curvature of the probe). In the internal imaging map, set a/n to less than 10 nanometers, so that point-by-point scanning and the penetration of terahertz are used to ensure that the imaging accuracy in the internal imaging map is better than 10 nanometers.
试验举例,如图3所示,对硅基样品进行内部成像,a/n=1.965,在内部成像图中采取剖面线测量,其中有尖峰的两个标注点的距离为3.93纳米,已经优于10纳米精度。在图中还存在比两个标注点距离小的尖峰,它们的精度优于3.93纳米。As an example of the test, as shown in Figure 3, internal imaging of a silicon-based sample was performed, a/n = 1.965, and cross-section line measurements were taken in the internal imaging diagram. The distance between the two marked points with sharp peaks was 3.93 nanometers, which is already better than 10nm accuracy. There are also sharp peaks smaller than the distance between the two labeled points in the figure, and their accuracy is better than 3.93 nanometers.
一种精度优于10纳米的太赫兹近场成像系统测量方法,利用太赫兹近场成像系统逐点扫描成像的原理和太赫兹波穿透性的特点,通过设置扫描参数,在近场成像内部成像图中,利用40纳米的探针实现优于10纳米的成像精度。本发明专利具有工艺简单(相对于电子显微镜而言)、成本低(利用40纳米精度的探针,成本比10纳米精度探针大大降低)、操作简单的优点,可推广应用到10纳米半导体工艺制程中。A measurement method for a terahertz near-field imaging system with an accuracy better than 10 nanometers. It uses the principle of point-by-point scanning imaging of the terahertz near-field imaging system and the characteristics of the penetrability of terahertz waves. By setting the scanning parameters, inside the near-field imaging In the imaging picture, a 40-nanometer probe is used to achieve imaging accuracy better than 10 nanometers. The patented invention has the advantages of simple process (compared to an electron microscope), low cost (using a 40-nanometer precision probe, the cost is much lower than a 10-nanometer precision probe), and simple operation, and can be applied to 10-nanometer semiconductor processes. In process.
本领域的技术人员容易理解,以上所述仅为本发明的较佳实施例而已,并不用以限制本发明,凡在本发明的精神和原则之内所作的任何修改、等同替换和改进等,均应包含在本发明的保护范围之内。It is easy for those skilled in the art to understand that the above descriptions are only preferred embodiments of the present invention and are not intended to limit the present invention. Any modifications, equivalent substitutions and improvements, etc., made within the spirit and principles of the present invention, All should be included in the protection scope of the present invention.
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