CN117337988A - Electrolyte solid beverage and preparation method thereof - Google Patents
Electrolyte solid beverage and preparation method thereof Download PDFInfo
- Publication number
- CN117337988A CN117337988A CN202311616562.4A CN202311616562A CN117337988A CN 117337988 A CN117337988 A CN 117337988A CN 202311616562 A CN202311616562 A CN 202311616562A CN 117337988 A CN117337988 A CN 117337988A
- Authority
- CN
- China
- Prior art keywords
- parts
- solid beverage
- electrolyte
- electrolyte solid
- erythritol
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000003792 electrolyte Substances 0.000 title claims abstract description 64
- 235000013361 beverage Nutrition 0.000 title claims abstract description 52
- 239000007787 solid Substances 0.000 title claims abstract description 46
- 238000002360 preparation method Methods 0.000 title claims abstract description 14
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 47
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 30
- 239000000377 silicon dioxide Substances 0.000 claims abstract description 23
- FNAQSUUGMSOBHW-UHFFFAOYSA-H calcium citrate Chemical compound [Ca+2].[Ca+2].[Ca+2].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O.[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O FNAQSUUGMSOBHW-UHFFFAOYSA-H 0.000 claims abstract description 20
- 239000001354 calcium citrate Substances 0.000 claims abstract description 20
- 235000013337 tricalcium citrate Nutrition 0.000 claims abstract description 20
- 239000001506 calcium phosphate Substances 0.000 claims abstract description 19
- QORWJWZARLRLPR-UHFFFAOYSA-H tricalcium bis(phosphate) Chemical compound [Ca+2].[Ca+2].[Ca+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O QORWJWZARLRLPR-UHFFFAOYSA-H 0.000 claims abstract description 19
- 229940078499 tricalcium phosphate Drugs 0.000 claims abstract description 19
- 229910000391 tricalcium phosphate Inorganic materials 0.000 claims abstract description 19
- 235000019731 tricalcium phosphate Nutrition 0.000 claims abstract description 19
- 150000003839 salts Chemical class 0.000 claims abstract description 14
- 235000012239 silicon dioxide Nutrition 0.000 claims abstract description 14
- DATAGRPVKZEWHA-YFKPBYRVSA-N N(5)-ethyl-L-glutamine Chemical compound CCNC(=O)CC[C@H]([NH3+])C([O-])=O DATAGRPVKZEWHA-YFKPBYRVSA-N 0.000 claims description 44
- 239000000463 material Substances 0.000 claims description 44
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 32
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 30
- 239000004386 Erythritol Substances 0.000 claims description 23
- UNXHWFMMPAWVPI-UHFFFAOYSA-N Erythritol Natural products OCC(O)C(O)CO UNXHWFMMPAWVPI-UHFFFAOYSA-N 0.000 claims description 23
- UNXHWFMMPAWVPI-ZXZARUISSA-N erythritol Chemical compound OC[C@H](O)[C@H](O)CO UNXHWFMMPAWVPI-ZXZARUISSA-N 0.000 claims description 23
- 229940009714 erythritol Drugs 0.000 claims description 23
- 235000019414 erythritol Nutrition 0.000 claims description 23
- 229940087559 grape seed Drugs 0.000 claims description 21
- 229940026510 theanine Drugs 0.000 claims description 21
- 239000000843 powder Substances 0.000 claims description 20
- 235000003392 Curcuma domestica Nutrition 0.000 claims description 19
- 235000003373 curcuma longa Nutrition 0.000 claims description 19
- 235000013976 turmeric Nutrition 0.000 claims description 19
- 238000002156 mixing Methods 0.000 claims description 16
- WCUXLLCKKVVCTQ-UHFFFAOYSA-M Potassium chloride Chemical compound [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 claims description 14
- 239000011248 coating agent Substances 0.000 claims description 13
- 238000000576 coating method Methods 0.000 claims description 13
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- 239000003765 sweetening agent Substances 0.000 claims description 12
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- AXZKOIWUVFPNLO-UHFFFAOYSA-N magnesium;oxygen(2-) Chemical compound [O-2].[Mg+2] AXZKOIWUVFPNLO-UHFFFAOYSA-N 0.000 claims description 9
- BJEPYKJPYRNKOW-UHFFFAOYSA-N malic acid Chemical compound OC(=O)C(O)CC(O)=O BJEPYKJPYRNKOW-UHFFFAOYSA-N 0.000 claims description 9
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- BAQAVOSOZGMPRM-QBMZZYIRSA-N sucralose Chemical compound O[C@@H]1[C@@H](O)[C@@H](Cl)[C@@H](CO)O[C@@H]1O[C@@]1(CCl)[C@@H](O)[C@H](O)[C@@H](CCl)O1 BAQAVOSOZGMPRM-QBMZZYIRSA-N 0.000 claims description 9
- 238000004806 packaging method and process Methods 0.000 claims description 7
- 239000001103 potassium chloride Substances 0.000 claims description 7
- 235000011164 potassium chloride Nutrition 0.000 claims description 7
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- GVJHHUAWPYXKBD-UHFFFAOYSA-N (±)-α-Tocopherol Chemical compound OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-UHFFFAOYSA-N 0.000 description 2
- MKYBYDHXWVHEJW-UHFFFAOYSA-N N-[1-oxo-1-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)propan-2-yl]-2-[[3-(trifluoromethoxy)phenyl]methylamino]pyrimidine-5-carboxamide Chemical group O=C(C(C)NC(=O)C=1C=NC(=NC=1)NCC1=CC(=CC=C1)OC(F)(F)F)N1CC2=C(CC1)NN=N2 MKYBYDHXWVHEJW-UHFFFAOYSA-N 0.000 description 2
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Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/105—Plant extracts, their artificial duplicates or their derivatives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
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Abstract
The invention provides an electrolyte solid beverage and a preparation method thereof, belonging to the technical field of solid beverages. The electrolyte solid beverage is added with a plurality of functional components capable of effectively relieving fatigue, and is supplemented with beneficial components such as sugar, salt, electrolyte, trace elements and the like, so that the stability of physiological functions can be maintained in all directions and multiple angles, and the fatigue of organisms can be effectively relieved. In addition, the composite anticaking agent composed of silicon dioxide, calcium citrate and tricalcium phosphate can effectively improve the anticaking performance of the solid beverage and improve the storage stability.
Description
Technical Field
The invention belongs to the technical field of solid beverages, and particularly relates to an electrolyte solid beverage and a preparation method thereof.
Background
In addition to oxygen, water is the most important factor by which humans survive. When the body temperature is raised due to various reasons such as fever, exercise, high temperature and the like, an important way for the body to regulate the body temperature is to reduce the body temperature through sweating, and the conditions all cause the loss of water in the body to be increased, if proper liquid supplement is not obtained, dehydration is caused, electrolyte metabolism disorder is caused, nerve function is influenced, symptoms such as muscle weakness, dysphoria, anxiety and the like appear, and serious dehydration also causes life danger.
At this time, drinking water and electrolyte are added to compensate for the loss of sweat moisture and electrolyte, so as to maintain the physiological function stable. When diarrhea and ingestion of food with diuretic effects is caused, the body loses water and electrolyte through the intestines and urine, and at this time, it is also necessary to increase drinking water and supplement a certain amount of electrolyte to maintain balance of water and electrolyte. Reasonable water and electrolyte supplementing, and also helps to prevent and correct the acid-base balance of body fluid caused by the disturbance of water and electrolyte metabolism.
The water and electrolyte are scientifically proportioned according to the loss condition of the organism, and unreasonable electrolyte supplementation can delay and even be unfavorable for correcting various metabolic disorders and dehydration. The art of maintaining balance of water, electrolyte and acid and alkali is to supplement the beneficial components and inorganic salts in specific types and amounts while drinking water.
Patent (CN 105961933B) discloses a coconut water sports drink containing natural electrolytes, which is prepared from the following components: 0.2 to 2 percent of coconut water, 0.02 to 0.3 percent of acidity regulator, 1 to 8 percent of white granulated sugar, 0.1 to 2 percent of salt lemon juice concentrated main agent, 0.01 to 0.3 percent of edible essence and the balance of RO water; the coconut water is turbid liquid formed by removing shells and concentrating coconuts, contains high natural electrolyte, and can ensure natural health of products and ensure that the products are more natural and fresh in taste; in addition, before mixing and blending the coconut water with the raw materials such as the concentrated main agent of the salt lemon juice, the white granulated sugar, the edible essence and the like, acid treatment, filtration, rapid cooling and centrifugal treatment are carried out to prepare the coconut water clarified liquid with the turbidity of 1-20NTU, and then the coconut water clarified liquid is mixed and blended with other raw materials, so that the phenomenon of precipitation and flocculation of the coconut water sports product in the shelf life can be effectively avoided, and the stability of the product in the shelf life is greatly improved. However, the preparation process of the patent is complex, has single function, and cannot effectively relieve fatigue.
Patent (CN 116636590 a) discloses an electrolyte flavor beverage, which comprises the following raw materials in parts by weight: 10 parts of erythritol, 2 parts of sea salt, 0.9 part of sucralose, 2.5 parts of potassium chloride, 0.6 part of potassium sorbate, 2 parts of citric acid, 1 part of sodium citrate, 0.3 part of zinc gluconate, 0.011 part of vitamin B, 0.28 part of vitamin E, 2 parts of opacifier essence, 2 parts of green lemon essence and secondary ozone RO water. The patent can supplement beneficial components such as electrolyte, vitamins and the like, has the characteristic of low glycemic index, but has single function and can not effectively relieve fatigue.
Therefore, although the electrolyte beverage provided in the prior art can supplement beneficial components such as electrolyte, vitamins, sugar, water and the like and maintain the stability of physiological functions, the electrolyte beverage has relatively single function, and can not effectively relieve the fatigue of a human body while supplementing the beneficial components required by the human body. The functional electrolyte beverage can supplement lost sugar, salt, electrolyte, trace elements and water, improve nerve excitability and human immunity, effectively relieve organism fatigue and is increasingly popular in the market.
Therefore, it is necessary to provide an electrolyte solid beverage which can simultaneously supplement lost sugar, salt, electrolyte, trace elements and moisture and effectively relieve fatigue of the body.
Disclosure of Invention
Aiming at the problems existing in the prior art, the invention provides an electrolyte solid beverage and a preparation method thereof. The electrolyte solid beverage is added with a plurality of functional components capable of effectively relieving fatigue, and is supplemented with beneficial components such as sugar, salt, electrolyte, trace elements and the like, so that the stability of physiological functions can be maintained in all directions and multiple angles, and the fatigue of organisms can be effectively relieved. By adopting the composite anticaking agent composed of silicon dioxide, calcium citrate and tricalcium phosphate, the anticaking performance of the solid beverage can be effectively improved, and the storage stability is improved.
To achieve the above object, in a first aspect, the present invention provides an electrolyte solid beverage comprising the following components: 0.05-0.5 part of turmeric, 0.05-0.5 part of grape seed powder, 0.05-0.2 part of theanine, 15-25 parts of erythritol, 20-30 parts of citric acid, 0.5-2 parts of DL-malic acid, 13-20 parts of salt, 5-25 parts of material A, 4-7 parts of potassium citrate, 4-6 parts of sodium citrate, 0.26-2 parts of potassium chloride, 1-5 parts of an anticaking agent, 0-1.5 parts of a colorant, 0.14-0.35 part of a compound vitamin, 0.01-0.4 part of magnesium oxide, 0.2-1.5 parts of an edible essence and spice and 0.1-0.14 part of taurine;
the material A consists of erythritol with the mass ratio of 934 (60-70) to 200-300, sweetener and water;
the anticaking agent is silicon dioxide, calcium citrate and tricalcium phosphate with the mass ratio of (1-2) to (0.5-1).
The turmeric is rich in curcumin, and researches show that the curcumin has the effects of resisting inflammation, resisting fatigue, protecting kidney, resisting oxidation, promoting immunity, protecting heart, protecting liver function, resisting cancer and the like. The anti-fatigue effect of curcumin may be achieved by modulating PI3K-Akt, cAMP-Creb, cGMP-PKG, PPAR-gamma and adipocyte lipolysis signaling pathways.
The grape seed powder has high content of various vitamins and mineral elements, is rich in procyanidine and linoleic acid, and is a polyphenol compound which takes catechin as a basic structural unit, and researches show that the grape seed procyanidine can prolong the load swimming time of mice, reduce the lactic acid content of the blood of the mice, increase the glycogen content and has remarkable anti-fatigue effect, which is possibly related to the effects of scavenging free radicals and blocking peroxidation of fatty acids by the procyanidine.
Theanine, L-theanine, was originally found to be a unique free amino acid extracted from natural plant tea leaves and was chemically similar to the active substances glutamine, glutamic acid in the brain, and the mechanism of theanine was probably related to the improvement of nervous system function, inhibition of 5-hydroxytryptamine in the brain and promotion of dopamine secretion.
The invention adopts the composite use of turmeric, grape seed powder and tea theanine, can regulate the signal path related to fatigue resistance, block the peroxidation effect of fatty acid and improve the function of nervous system, and plays the role of fatigue resistance in all directions and multiple angles, thereby obviously obtaining ideal fatigue resistance.
In addition, the electrolyte solid beverage is added with liquid essence, spice, potassium citrate and other components easy to absorb moisture, so that the electrolyte solid beverage is easy to absorb moisture and agglomerate. Silica is a common anticaking agent, and GB2760 specifies a limited amount of 1.5g/100g below which it is not effective in anti-caking. According to the invention, the composite anticaking agent consisting of the silicon dioxide, the calcium citrate and the tricalcium phosphate is added, so that the use amount of the anticaking agent can be increased, and the advantages of different types of anticaking agents can be combined, so that the anticaking performance and the storage stability of the electrolyte solid beverage are effectively improved, and the proportion of the silicon dioxide, the calcium citrate and the tricalcium phosphate in the anticaking agent has a great influence on the anticaking performance and the storage stability of the electrolyte solid beverage.
In a preferred embodiment, the sweetener is selected from at least one of sucralose, steviol glycosides, and mogrosides.
In a preferred embodiment, the edible flavor is a liquid flavor.
In a preferred embodiment, the liquid flavor includes at least one of lemon oil, passion fruit flavor, and litchi flavor.
In a preferred embodiment, the material A is obtained by coating the surface of erythritol with a sweetener solution by a fluid bed coating technique after the sweetener solution is dissolved in water.
In a preferred embodiment, the process for the preparation of material a comprises the steps of:
s1, dissolving: dissolving sweetener in water, stirring until completely dissolved;
s2, feeding: throwing erythritol into a fluidized bed, and uniformly distributing;
s3, coating: preheating the fluidized bed, connecting a peristaltic pump, setting the revolution and the pressure of a spray gun, enabling the temperature of the material to reach more than 70 ℃, and spraying and coating;
s4, drying: and after coating, continuing mixing and drying until the water content is less than or equal to 6%, and discharging.
In a preferred embodiment, the number of revolutions in step S3 is 70-110rmp, the lance pressure is 0.18-0.22MPa.
In a second aspect, the present invention provides a method for preparing the aforementioned electrolyte solid beverage, comprising the steps of:
1) Premixing small materials: premixing turmeric, grape seed powder, tea theanine, sodium citrate, compound vitamin, DL-malic acid, potassium citrate, magnesium oxide and colorant to obtain a material B;
2) Total mixing: and (3) uniformly mixing erythritol, citric acid, edible essence and spice and an anticaking agent, adding the material B, the material A and the rest materials, and mixing to prepare the electrolyte solid beverage.
In a preferred embodiment, the premixing time in step 1) is from 5 to 15min; in the step 2), erythritol, citric acid, edible essence and spice and an anticaking agent are mixed for 5-10min, and the mixing time after adding the material B, the material A and the rest materials is 15-35min.
In a preferred embodiment, step 2) is followed by the step of packaging the electrolyte solid beverage produced in step 2); the packaging speed is 40-60 bags/min, and the specification is 2-4 g/bag.
Compared with the prior art, the invention has the technical advantages that:
1. the electrolyte solid beverage is added with a plurality of functional components capable of effectively relieving fatigue, and is supplemented with beneficial components such as sugar, salt, electrolyte, trace elements and the like, so that the stability of physiological functions can be maintained in all directions and multiple angles, and the fatigue of organisms can be effectively relieved.
2. The electrolyte solid beverage of the invention can effectively improve the anti-caking property of the solid beverage and improve the storage stability by adopting the composite anti-caking agent composed of silicon dioxide, calcium citrate and tricalcium phosphate.
3. The invention uses sugar substitutes such as erythritol, sucralose and the like, ensures the taste of the product without adding sugar, has the advantage of low glycemic index, and can be used for people with high blood sugar and people with weight control requirements.
Detailed Description
The following raw material sources are exemplary illustrations:
turmeric: food grade, purchased from curcuma aromatica biological limited in Hebei;
grape seed powder: goods number SH0303, specification 10:1, purchased from Shaanxi Cheng Heng Biotechnology Co., ltd;
salt: dried iodized salt, available from Guangdong salt group Co., ltd;
silica: 1500 mesh, purchased from yang, glas white carbon chemical company, inc;
coloring agent: beta-carotene, model 1%, available from basf (china) limited;
compound vitamins: shuoweili C-22120504, available from Shuoweiwei nutrition technology (Guangzhou) Co., ltd;
flavoring essence and spice: litchi essence, purchased from Guangzhou-name floral fragrance company, inc.;
erythritol: 20-30 mesh, purchased from Jungbunzlauer;
calcium citrate: 1300 mesh, purchased from Jungbunzlauer;
theanine, anhydrous citric acid, potassium citrate, sodium citrate, DL-malic acid, potassium chloride, magnesium oxide, taurine: are commercially available in general.
Example 1
The electrolyte solid beverage of this example consisted of: 0.3 part of turmeric, 0.1 part of grape seed powder, 0.1 part of theanine, 21.99 parts of erythritol (20-30 meshes), 24.5 parts of anhydrous citric acid, 1.5 parts of DL-malic acid, 18 parts of salt, 15 parts of material A, 5 parts of potassium citrate, 5 parts of sodium citrate, 1.5 parts of potassium chloride, 4.4 parts of an anticaking agent, 1 part of a colorant, 0.25 part of compound vitamin, 0.22 part of magnesium oxide, 1 part of edible essence and spice and 0.14 part of taurine;
the material A comprises the following components: 934 parts of erythritol, 66 parts of sucralose and 260 parts of water;
anti-caking agent composition: 1.4 parts of silicon dioxide, 1.6 parts of calcium citrate and 1.4 parts of tricalcium phosphate, namely the silicon dioxide, the calcium citrate and the tricalcium phosphate are adopted in a mass ratio of 1:1.14:1;
the preparation method of the material A comprises the following steps:
s1, dissolving: dissolving sucralose in water, and stirring until the sucralose is completely dissolved;
s2, feeding: throwing erythritol into a fluidized bed, and uniformly distributing;
s3, coating: preheating a fluidized bed for more than 10min, connecting a peristaltic pump, setting the rotating speed to 100rmp and the pressure of a spray gun to 0.22Mpa, starting spraying coating when the temperature of the material reaches more than 70 ℃, and turning off the spray gun, the ejector pin and the peristaltic pump after finishing;
s4, drying: after coating, continuing mixing and drying until the temperature of the material reaches above 70 ℃, sampling and sampling water content which is less than or equal to 6% and is qualified;
s5, shutting down and discharging: closing the airtight seal, manually removing ash (repeatedly opening and closing for several times), disassembling the air inlet pipe, airtight sealing the pressure pipe, taking out the thermometer, and taking out the material to obtain a material A.
The preparation method of the electrolyte solid beverage comprises the following steps:
1) Premixing small materials: premixing turmeric, grape seed powder, tea theanine, sodium citrate, compound vitamin, DL-malic acid, potassium citrate, magnesium oxide and colorant for 10min to obtain a material B;
2) Total mixing: mixing erythritol, citric acid, edible essence and spice, and anticaking agent for 10min to uniformity, adding material B, material A and the rest materials, and mixing for 25min to obtain the electrolyte solid beverage.
3) And (3) packaging: packaging the electrolyte solid beverage prepared in the step 2), wherein the packaging speed is 50 bags/min, and the specification is 4 g/bag.
Example 2
The electrolyte solid beverage of this example consisted of: 0.5 part of turmeric, 0.05 part of grape seed powder, 0.05 part of theanine, 16.43 parts of erythritol (20-30 meshes), 20.3 parts of anhydrous citric acid, 2 parts of DL-malic acid, 20 parts of salt, 25 parts of material A, 4 parts of potassium citrate, 4 parts of sodium citrate, 2 parts of potassium chloride, 3.2 parts of anticaking agent, 1 part of colorant, 0.35 part of compound vitamin, 0.22 part of magnesium oxide, 0.8 part of edible essence and spice and 0.10 part of taurine;
the material A comprises the following components: 934 parts of erythritol, 66 parts of sucralose and 260 parts of water;
anti-caking agent composition: 1 part of silicon dioxide, 1.7 parts of calcium citrate and 0.5 part of tricalcium phosphate, namely silicon dioxide, calcium citrate and tricalcium phosphate with the mass ratio of 1:1.7:0.5 are adopted;
the preparation method of the material A and the preparation process of the electrolyte solid beverage are the same as in the example 1.
Example 3
The electrolyte solid beverage of this example consisted of: 0.1 part of turmeric, 0.5 part of grape seed powder, 0.1 part of theanine, 25 parts of erythritol (20-30 meshes), 26.5 parts of anhydrous citric acid, 0.5 part of DL-malic acid, 13 parts of salt, 15 parts of material A, 6 parts of potassium citrate, 6 parts of sodium citrate, 0.5 part of potassium chloride, 4.3 parts of anticaking agent, 1 part of colorant, 0.35 part of compound vitamin, 0.22 part of magnesium oxide, 0.8 part of edible essence and spice and 0.13 part of taurine;
the material A comprises the following components: 934 parts of erythritol, 66 parts of sucralose and 260 parts of water;
anti-caking agent composition: 1.1 parts of silicon dioxide, 2.2 parts of calcium citrate and 1 part of tricalcium phosphate, namely silicon dioxide, calcium citrate and tricalcium phosphate in a mass ratio of 1:2:0.91 are adopted;
the preparation method of the material A and the preparation process of the electrolyte solid beverage are the same as in the example 1.
Comparative example 1
Example 1 was repeated except that 0.3 part of turmeric, 0.2 part of grape seed powder and 0 part of theanine were used.
Comparative example 2
Example 1 was repeated except that 0.3 part of turmeric, 0 part of grape seed powder and 0.2 part of theanine were used.
Comparative example 3
Example 1 was repeated except that 0.5 part of turmeric, 0 part of grape seed powder and 0 part of theanine were used.
Comparative example 4
Example 1 was repeated except that 0 part of turmeric, 0.25 part of grape seed powder and 0.25 part of theanine were used.
Comparative example 5
Example 1 was repeated except that the anti-caking agent was 1.4 parts of silica alone.
Comparative example 6
Example 1 was repeated except that the anticaking agent was 1.4 parts of silica, 3 parts of calcium citrate, and 0 part of tricalcium phosphate.
Comparative example 7
Example 1 was repeated except that the anticaking agent was 1.4 parts of silica, 0 parts of calcium citrate, and 3 parts of tricalcium phosphate.
Comparative example 8
Example 1 was repeated except that the anti-caking agent was 1.1 parts of silica and 3 parts of calcium carbonate.
Comparative example 9
Example 3 was repeated except that the anticaking agent consisted of 1.1 parts of silica, 1 part of calcium citrate, and 2.2 parts of tricalcium phosphate (i.e., silica, calcium citrate, and tricalcium phosphate in a mass ratio of 1:0.91:2 were used).
Test case
1. Fatigue resistance test
1) Experimental animals and dosing: 80 healthy Kunming male mice of two months of age and weight 22-26g were randomly divided into 8 groups after 1 week of adaptive feeding, and the control group, the example 1-3 group and the comparative example 1-4 group were each intragastrically filled at 8-10 am with the electrolyte solid drink of the example 1-3 group and the comparative example 1-4 group, at a dose of 30g/kg, and the control group was intragastrically filled with the corresponding dose of sucrose, and were continuously dosed for 4 weeks.
2) The test method comprises the following steps: and after the last gastric lavage, a weight which is 5% of the weight of the mouse is tied on the body of the mouse, the mouse is placed in a water pool for carrying out a load swimming test, if the head of the mouse which is immersed in water for 8 seconds cannot float out of the water surface, the water is judged to be exhausted, the time from the water inlet to the exhaustion of the mouse is recorded, namely the exhaustion time, the mouse is killed, and tissues are taken for measuring blood lactic acid and liver glycogen, wherein the blood lactic acid is tested by adopting a whole blood lactic acid test kit (colorimetric method), and the liver glycogen is tested by adopting a liver/muscle glycogen test kit. The test results of the control group, the examples 1 to 3 and the comparative examples 1 to 4 are shown in Table 1, and the elongation, the reduction and the improvement in Table 1 are compared with the control group.
TABLE 1 mouse fatigue test Effect data
Note that: * P < 0.05 compared with the control group
As can be seen from table 1, the electrolyte solid beverage of examples 1 to 3 of the present invention can significantly improve the exhaustion time (97.6% to 106.4% higher than the control group) and the myoglycogen content (57.6% to 63.8% higher than the control group) of the mice, and significantly reduce the blood lactic acid content (43.5% to 49.1% lower than the control group) of the mice, and thus, the electrolyte solid beverage of the present invention has a significant physical fatigue relieving function.
Comparative examples 1-2 only one of grape seed powder and theanine was used in combination with respect to example 1 except turmeric, the time of exhaustion and myoglycogen content of mice were significantly reduced, and the blood lactic acid content of mice was significantly increased, indicating that the combined use of grape seed powder and theanine can better alleviate physical fatigue.
Comparative examples 3-4 used turmeric alone, or grape seed powder and theanine alone, compared to example 1, which used turmeric, grape seed powder and theanine in combination, the time of exhaustion and myoglycogen content of mice were significantly reduced, while the blood lactic acid content of mice was significantly increased, indicating that turmeric, grape seed powder and theanine in combination could better alleviate physical fatigue.
2. Storage stability test
The unpackaged electrolyte solid beverages of examples 1-3 and comparative examples 5-9 were placed in a stability test chamber at a temperature of 42℃and a humidity of 75%, and the presence or absence of caking or swelling was observed every 24 hours, and when caking or swelling was found, the time was recorded, and the storage stability of examples 1-3 and comparative examples 5-9 was continued until the unpackaged solid beverages were left for 40 days.
TABLE 2 storage stability of examples 1-3 and comparative examples 5-9
It can be seen from Table 2 that the solid electrolyte beverages of examples 1 to 3 of the present invention were excellent in storage stability, and the kind and amount of the anticaking agent had a great influence on the stability of the solid electrolyte beverages. In comparative example 5, only 1.4 parts of silicon dioxide is adopted, so that the stability is poor, and the use requirement cannot be met completely; comparative examples 6 to 9 use only one of calcium citrate and tricalcium phosphate in combination with silica, or adjust the amount, or replace calcium citrate and tricalcium phosphate with calcium carbonate, resulted in a significant deterioration in the storage stability of the solid electrolyte beverage.
Finally, it should be noted that the foregoing detailed description is directed to one of the possible embodiments of the present invention, which should not be construed as limiting the scope of the invention, but rather as covering all equivalent embodiments or modifications that may fall within the scope of the invention.
Claims (10)
1. An electrolyte solid beverage, characterized by comprising the following components: 0.05-0.5 part of turmeric, 0.05-0.5 part of grape seed powder, 0.05-0.2 part of theanine, 15-25 parts of erythritol, 20-30 parts of citric acid, 0.5-2 parts of DL-malic acid, 13-20 parts of salt, 5-25 parts of material A, 4-7 parts of potassium citrate, 4-6 parts of sodium citrate, 0.26-2 parts of potassium chloride, 1-5 parts of an anticaking agent, 0-1.5 parts of a colorant, 0.14-0.35 part of a compound vitamin, 0.01-0.4 part of magnesium oxide, 0.2-1.5 parts of an edible essence and spice and 0.1-0.14 part of taurine;
the material A consists of erythritol with the mass ratio of 934 (60-70) to 200-300, sweetener and water;
the anticaking agent is silicon dioxide, calcium citrate and tricalcium phosphate with the mass ratio of (1-2) to (0.5-1).
2. The electrolyte solid beverage of claim 1, wherein the sweetener is selected from at least one of sucralose, steviol glycosides, and mogrosides.
3. The electrolyte solid beverage of claim 1 wherein the flavorant is a liquid flavorant.
4. The electrolyte solid beverage according to claim 3, wherein the liquid flavor comprises at least one of lemon oil, passion fruit flavor, and litchi flavor.
5. The electrolyte solid beverage according to claim 1, wherein the material a is obtained by coating a sweetener solution on the surface of erythritol by a fluidized bed coating technique after the sweetener is dissolved in water to obtain the sweetener solution.
6. The electrolyte solid beverage according to claim 5, wherein the material a preparation process comprises the steps of:
s1, dissolving: dissolving sweetener in water, stirring until completely dissolved;
s2, feeding: throwing erythritol into a fluidized bed, and uniformly distributing;
s3, coating: preheating the fluidized bed, connecting a peristaltic pump, setting the revolution and the pressure of a spray gun, enabling the temperature of the material to reach more than 70 ℃, and spraying and coating;
s4, drying: and after coating, continuing mixing and drying until the water content is less than or equal to 6%, and discharging.
7. The electrolyte solid beverage according to claim 6, wherein the revolution number in step S3 is 70 to 110rmp and the lance pressure is 0.18 to 0.22Mpa.
8. The method for producing an electrolyte solid beverage according to any one of claims 1 to 7, comprising the steps of:
1) Premixing small materials: premixing turmeric, grape seed powder, tea theanine, sodium citrate, compound vitamin, DL-malic acid, potassium citrate, magnesium oxide and colorant to obtain a material B;
2) Total mixing: and (3) uniformly mixing erythritol, citric acid, edible essence and spice and an anticaking agent, adding the material B, the material A and the rest materials, and mixing to prepare the electrolyte solid beverage.
9. The method of claim 8, wherein the premixing time in step 1) is 5-15min; in the step 2), erythritol, citric acid, edible essence and spice and an anticaking agent are mixed for 5-10min, and the mixing time after adding the material B, the material A and the rest materials is 15-35min.
10. The method of claim 9, further comprising the step of packaging the electrolyte solid beverage prepared in step 2) after step 2); the packaging speed is 40-60 bags/min, and the specification is 2-4 g/bag.
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