CN117101253A - Preparation process of natural plant organic liquid - Google Patents
Preparation process of natural plant organic liquid Download PDFInfo
- Publication number
- CN117101253A CN117101253A CN202210531936.1A CN202210531936A CN117101253A CN 117101253 A CN117101253 A CN 117101253A CN 202210531936 A CN202210531936 A CN 202210531936A CN 117101253 A CN117101253 A CN 117101253A
- Authority
- CN
- China
- Prior art keywords
- organic liquid
- natural plant
- plant organic
- membrane
- solution
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000007788 liquid Substances 0.000 title claims abstract description 52
- 238000002360 preparation method Methods 0.000 title claims abstract description 13
- 239000012528 membrane Substances 0.000 claims abstract description 39
- RSWGJHLUYNHPMX-UHFFFAOYSA-N Abietic-Saeure Natural products C12CCC(C(C)C)=CC2=CCC2C1(C)CCCC2(C)C(O)=O RSWGJHLUYNHPMX-UHFFFAOYSA-N 0.000 claims abstract description 37
- KHPCPRHQVVSZAH-HUOMCSJISA-N Rosin Natural products O(C/C=C/c1ccccc1)[C@H]1[C@H](O)[C@@H](O)[C@@H](O)[C@@H](CO)O1 KHPCPRHQVVSZAH-HUOMCSJISA-N 0.000 claims abstract description 37
- KHPCPRHQVVSZAH-UHFFFAOYSA-N trans-cinnamyl beta-D-glucopyranoside Natural products OC1C(O)C(O)C(CO)OC1OCC=CC1=CC=CC=C1 KHPCPRHQVVSZAH-UHFFFAOYSA-N 0.000 claims abstract description 37
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 24
- 238000000108 ultra-filtration Methods 0.000 claims abstract description 21
- 238000001728 nano-filtration Methods 0.000 claims abstract description 13
- 238000001914 filtration Methods 0.000 claims abstract description 11
- 238000001223 reverse osmosis Methods 0.000 claims abstract description 8
- 238000003756 stirring Methods 0.000 claims abstract description 7
- 239000011148 porous material Substances 0.000 claims description 6
- 238000004519 manufacturing process Methods 0.000 claims 9
- 238000000034 method Methods 0.000 abstract description 8
- 239000000126 substance Substances 0.000 abstract description 8
- 238000004821 distillation Methods 0.000 abstract description 6
- 239000000047 product Substances 0.000 abstract description 6
- 239000003795 chemical substances by application Substances 0.000 abstract description 3
- 230000003750 conditioning effect Effects 0.000 abstract description 3
- 239000002994 raw material Substances 0.000 abstract description 3
- 230000001954 sterilising effect Effects 0.000 abstract description 3
- 238000004140 cleaning Methods 0.000 abstract description 2
- 238000007670 refining Methods 0.000 abstract description 2
- 208000017520 skin disease Diseases 0.000 abstract description 2
- 239000004480 active ingredient Substances 0.000 abstract 1
- 230000001877 deodorizing effect Effects 0.000 abstract 1
- 239000012263 liquid product Substances 0.000 abstract 1
- 238000002156 mixing Methods 0.000 abstract 1
- 239000000243 solution Substances 0.000 description 42
- 230000000694 effects Effects 0.000 description 4
- 238000005374 membrane filtration Methods 0.000 description 3
- 238000012545 processing Methods 0.000 description 3
- 239000011550 stock solution Substances 0.000 description 3
- 241000282414 Homo sapiens Species 0.000 description 2
- 238000009835 boiling Methods 0.000 description 2
- 238000004332 deodorization Methods 0.000 description 2
- 238000011161 development Methods 0.000 description 2
- 230000007613 environmental effect Effects 0.000 description 2
- 239000012467 final product Substances 0.000 description 2
- 235000015073 liquid stocks Nutrition 0.000 description 2
- 238000012827 research and development Methods 0.000 description 2
- 230000000087 stabilizing effect Effects 0.000 description 2
- 238000004659 sterilization and disinfection Methods 0.000 description 2
- 239000013543 active substance Substances 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 238000012271 agricultural production Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 239000011344 liquid material Substances 0.000 description 1
- 229920002521 macromolecule Polymers 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000004806 packaging method and process Methods 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/02—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping in boilers or stills
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D36/00—Filter circuits or combinations of filters with other separating devices
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D61/00—Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
- B01D61/02—Reverse osmosis; Hyperfiltration ; Nanofiltration
- B01D61/025—Reverse osmosis; Hyperfiltration
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D61/00—Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
- B01D61/14—Ultrafiltration; Microfiltration
- B01D61/145—Ultrafiltration
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Water Supply & Treatment (AREA)
- Nanotechnology (AREA)
- Separation Using Semi-Permeable Membranes (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The invention discloses a preparation process of natural plant organic liquid, which comprises the steps of reduced pressure distillation, ultrafiltration, RO reverse osmosis, stirring and filtering, wherein the reduced pressure distillation is realized by a rotary evaporator, a water bath kettle and a water circulation vacuum pump, ultrafiltration treatment is carried out by an ultrafiltration membrane, RO reverse osmosis treatment is carried out by an RO membrane or a nanofiltration membrane, and rosin solution is added for mixing and filtering to obtain the natural plant organic liquid. The natural plant organic liquid refining process has high treatment efficiency, is easy to construct and convenient for engineering application, can effectively remove tar and macromolecular harmful substances in the organic liquid, simultaneously effectively retains active ingredients in the organic liquid, has the tar content close to 0 after treatment, almost does not detect macromolecular harmful substances, obviously improves the chromaticity reduction and the transparency of the organic liquid, finally forms a relatively stable, clear and transparent organic liquid product, and provides a safe and stable raw material for developing plant conditioning agents, sterilizing and deodorizing agents, products for treating skin diseases, skin cleaning and the like by utilizing the organic liquid in the future.
Description
Technical Field
The invention belongs to the technical field of organic liquid preparation, and particularly relates to a preparation process of natural plant organic liquid.
Background
In recent years, the world economy continues to develop at a high speed, a large number of artificially synthesized chemicals corresponding to the world economy are applied to the fields of environment, agriculture and health, secondary pollution and side effects are endangering the health of human beings continuously, natural plant organic liquid is extracted from plants and is rich in active substances with plant conditioning, sterilization and deodorization and skin cleaning, because the natural organic liquid is applied to agricultural production and environmental management, but the organic liquid contains part of tar which is difficult to remove, and the direct application can cause adverse effects on the environment, biology and human health, so that tar and macromolecular harmful substances in the plant organic liquid need to be removed effectively.
At present, the method for removing tar in organic liquid is mainly a filtering method, but researches show that the method has low tar removing efficiency, particularly has almost no removing effect on low molecular tar, and the filtering method is carried out under normal pressure, and has the advantages of slower filtering process and low efficiency.
Disclosure of Invention
The invention aims to provide a preparation process of natural plant organic liquid, which aims to solve the problems in the background technology.
In order to achieve the above purpose, the present invention provides the following technical solutions: a preparation process of natural plant organic liquid comprises the following steps:
s1: distilling under reduced pressure;
s2: ultrafiltration;
s3: RO reverse osmosis;
s4: stirring;
s5: and (5) filtering.
Preferably, the step S1 is realized by a rotary evaporator, a water bath kettle and a water circulation vacuum pump.
Preferably, the working temperature of the water bath kettle is 60-80 ℃, and the working pressure of the water circulation vacuum pump is 0.08-0.1MPa.
Preferably, the S2 is achieved by an ultrafiltration membrane.
Preferably, the pore size of the ultrafiltration membrane is 0.01um.
Preferably, the S3 is implemented by any one of RO membrane and nanofiltration membrane.
Preferably, the RO membrane and nanofiltration membrane have a pore size of 0.1nm.
Preferably, the refined solution after the treatment of S3 is added with a rosin solution and then enters the treatment step of S4.
Preferably, the rosin solution is prepared from medical rosin, and 5-50 mL (5 per mill-5%) of rosin solution is added into 1L of refined solution.
Preferably, the step S5 is to treat the refined solution and rosin solution mixed by the step S4 to obtain natural plant organic solution.
The invention has the technical effects and advantages that: according to the characteristic of different boiling points of substances, the natural plant organic liquid stock solution is subjected to reduced pressure distillation, macromolecule tar is separated from micromolecular natural organic substances, so that purer refined solution can be obtained, the refined solution obtained through reduced pressure distillation is subjected to ultrafiltration through an ultrafiltration membrane to obtain ultrafiltrate, the ultrafiltrate is subjected to RO membrane or nanofiltration membrane to obtain finished refined solution, the finished product natural plant organic liquid is obtained after being treated by rosin solution, and the finished product natural plant organic liquid is packaged and stored by a plastic barrel and is used as a main raw material for deep development of the final product;
the rosin solution is prepared from medical rosin, so that natural components in the organic liquid are not influenced, and the rosin solution has a stabilizing effect on active components in the organic liquid;
the refining process of the natural plant organic liquid is easy to construct and convenient to apply, tar in the organic liquid can be effectively removed, a basic raw liquid material is provided for the research and development of products such as plant conditioning agents for agricultural use, sterilization and deodorization for environmental use, skin disease treatment for health use and the like, and the dosage of rosin can be adjusted according to the actual conditions of different plant organic liquids.
Drawings
FIG. 1 is a schematic illustration of the preparation process of the present invention.
Detailed Description
The following description of the embodiments of the present invention will be made clearly and completely with reference to the accompanying drawings, in which it is apparent that the embodiments described are only some embodiments of the present invention, but not all embodiments.
Example 1
A preparation process of natural plant organic liquid comprises the following steps:
s1: distilling under reduced pressure;
s2: ultrafiltration;
s3: RO reverse osmosis;
s4: stirring;
s5: and (5) filtering.
Specifically, the S1 is realized through a rotary evaporator, a water bath kettle and a water circulation vacuum pump.
Specifically, the working temperature of the water bath kettle is 60 ℃, and the working pressure of the water circulation vacuum pump is 0.08MPa.
Specifically, the S2 is realized by an ultrafiltration membrane.
Specifically, the aperture of the ultrafiltration membrane is 0.01um.
Specifically, the S3 is realized through any one of an RO membrane and a nanofiltration membrane.
Specifically, the pore diameters of the RO membrane and the nanofiltration membrane are 0.1nm.
Specifically, the refined solution after the treatment of S3 is added with rosin solution and then enters the treatment step of S4.
Specifically, the rosin solution is prepared from medical rosin, and 5 mL rosin solution is added into 1L of refined liquid.
Specifically, the S5 is used for processing the refined solution and the rosin solution mixed by the S4 to obtain the natural plant organic solution.
Example 2
A preparation process of natural plant organic liquid comprises the following steps:
s1: distilling under reduced pressure;
s2: ultrafiltration;
s3: RO reverse osmosis;
s4: stirring;
s5: and (5) filtering.
Specifically, the S1 is realized through a rotary evaporator, a water bath kettle and a water circulation vacuum pump.
Specifically, the working temperature of the water bath kettle is 70 ℃, and the working pressure of the water circulation vacuum pump is 0.09MPa.
Specifically, the S2 is realized by an ultrafiltration membrane.
Specifically, the aperture of the ultrafiltration membrane is 0.01um.
Specifically, the S3 is realized through any one of an RO membrane and a nanofiltration membrane.
Specifically, the pore diameters of the RO membrane and the nanofiltration membrane are 0.1nm.
Specifically, the refined solution after the treatment of S3 is added with rosin solution and then enters the treatment step of S4.
Specifically, the rosin solution is prepared from medical rosin, and 40 mL rosin solution is added into 1L of refined liquid.
Specifically, the S5 is used for processing the refined solution and the rosin solution mixed by the S4 to obtain the natural plant organic solution.
Example 3
A preparation process of natural plant organic liquid comprises the following steps:
s1: distilling under reduced pressure;
s2: ultrafiltration;
s3: RO reverse osmosis;
s4: stirring;
s5: and (5) filtering.
Specifically, the S1 is realized through a rotary evaporator, a water bath kettle and a water circulation vacuum pump.
Specifically, the working temperature of the water bath kettle is 80 ℃, and the working pressure of the water circulation vacuum pump is 0.1MPa.
Specifically, the S2 is realized by an ultrafiltration membrane.
Specifically, the aperture of the ultrafiltration membrane is 0.01um.
Specifically, the S3 is realized through any one of an RO membrane and a nanofiltration membrane.
Specifically, the pore diameters of the RO membrane and the nanofiltration membrane are 0.1nm.
Specifically, the refined solution after the treatment of S3 is added with rosin solution and then enters the treatment step of S4.
Specifically, the rosin solution is prepared from medical rosin, and 50 mL rosin solution is added into 1L of refined liquid.
Specifically, the S5 is used for processing the refined solution and the rosin solution mixed by the S4 to obtain the natural plant organic solution.
Specifically, according to the preparation process of the natural plant organic liquid, according to the characteristics of different boiling points of substances, a rotary evaporator, a water bath kettle and a water circulation vacuum pump are used for carrying out reduced pressure distillation on the natural plant organic liquid stock solution, so that macromolecular tar is separated from micromolecular natural organic substances, purer refined liquid can be obtained preliminarily, and separated impurity waste liquid is removed;
ultrafiltering the distilled liquid obtained by reduced pressure distillation through an ultrafiltration membrane to obtain ultrafiltrate, performing reverse osmosis treatment on the ultrafiltrate through an RO membrane or a nanofiltration membrane to obtain refined liquid bodies, packaging and storing the refined liquid bodies in a plastic barrel to serve as main raw materials for deep development of final products, wherein rosin solution is prepared from medical rosin, the influence of the rosin solution on natural components of the refined liquid bodies is avoided to the greatest extent, the rosin solution has a stabilizing effect on active components in organic liquid, and the refined liquid is added with the rosin solution to obtain the final product natural plant organic liquid after stirring and filtering;
the process is easy to construct and convenient to apply, tar in the organic liquid can be effectively removed, the content of the tar after treatment is extremely low, a basic stock solution material can be provided for the research and development of products in the fields of agriculture, environment and health, and the dosage of the rosin solution is determined according to the actual use environment.
The foregoing is only a preferred embodiment of the invention, but the scope of the invention is not limited thereto, and any person skilled in the art who is in the field of the invention can apply equivalent substitution or modification to the technical solution and the inventive concept according to the invention within the scope of the invention.
Claims (10)
1. The preparation process of the natural plant organic liquid is characterized by comprising the following steps of:
s1: distilling under reduced pressure;
s2: ultrafiltration;
s3: RO reverse osmosis;
s4: stirring;
s5: and (5) filtering.
2. The process for preparing natural plant organic liquid according to claim 1, wherein: the S1 is realized by a rotary evaporator, a water bath kettle and a water circulation vacuum pump.
3. The process for preparing natural plant organic liquid according to claim 2, wherein: the working temperature of the water bath kettle is 60-80 ℃, and the working pressure of the water circulation vacuum pump is 0.08-0.1MPa.
4. The process for preparing natural plant organic liquid according to claim 1, wherein: the S2 is realized by an ultrafiltration membrane.
5. The process for preparing natural plant organic liquid according to claim 4, wherein: the aperture of the ultrafiltration membrane is 0.01um.
6. The process for preparing natural plant organic liquid according to claim 1, wherein: the S3 is realized through any one of an RO membrane and a nanofiltration membrane.
7. The process for preparing natural plant organic liquid according to claim 6, wherein: the pore diameters of the RO membrane and the nanofiltration membrane are 0.1nm.
8. The process for preparing natural plant organic liquid according to claim 1, wherein: and (3) adding rosin solution into the refined solution processed in the step (S3), and then entering the step (S4).
9. The process for preparing natural plant organic liquid according to claim 8, wherein: the rosin solution is prepared from medical rosin, and 5-50 mL (5 per mill-5%) rosin solution is added into 1L refined solution.
10. The process for preparing natural plant organic liquid according to claim 1, wherein: and S5, treating the refined solution and the rosin solution mixed in the step S4 to obtain the natural plant organic solution.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202210531936.1A CN117101253A (en) | 2022-05-17 | 2022-05-17 | Preparation process of natural plant organic liquid |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202210531936.1A CN117101253A (en) | 2022-05-17 | 2022-05-17 | Preparation process of natural plant organic liquid |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN117101253A true CN117101253A (en) | 2023-11-24 |
Family
ID=88798929
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202210531936.1A Pending CN117101253A (en) | 2022-05-17 | 2022-05-17 | Preparation process of natural plant organic liquid |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN117101253A (en) |
-
2022
- 2022-05-17 CN CN202210531936.1A patent/CN117101253A/en active Pending
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| US5356811A (en) | Method of processing stabilized aloe vera gel obtained from the whole aloe vera leaf | |
| CN107155305A (en) | The high concentration collagen preparation method used as medical material | |
| CN106576602A (en) | Preparation process of full-nutrient sea-buckthorn essence stock solution | |
| CN106336060A (en) | Mountain spring water production process | |
| CN101779628B (en) | Method for preparing gallic acid aquiculture sanitizer and product thereof | |
| CN117101253A (en) | Preparation process of natural plant organic liquid | |
| CN103289967A (en) | Extraction method for extracting superoxide dismutase from shenzhou grass | |
| CN103626885A (en) | Clean production method of Pulullan | |
| CN105012581A (en) | Fresh aloe antibacterial composite, application and preparing method of fresh aloe antibacterial composite | |
| CN1258450A (en) | Natural plant disinfectant and its preparation | |
| CN108774283B (en) | Method for preparing tea saponin by coupling high-voltage pulse electric field and biological enzymolysis | |
| CN1096456C (en) | Process for continuously extracting glycitin, olegose and saponin | |
| CN109601821A (en) | One kind having anti-microbial property essential oil smell minimizing technology | |
| US10487824B2 (en) | Method of making a hydrolyzed collagen gel | |
| CN100352461C (en) | External-use medicine for treating leucoderma and its preparing method | |
| CN107233361A (en) | The preparation method of propolis | |
| CN107397177A (en) | A kind of processing method of fresh safe sweet-scented osmanthus honey | |
| CN1742757A (en) | Glossy ganoderma polysaccharide and preparing method | |
| CN115252883A (en) | Composite liquid dressing formula for rapidly repairing and sterilizing body surface injury | |
| CN116251379A (en) | Process for removing ginkgolic acid from ginkgo leaf extract | |
| CN1733229A (en) | Method for processing aloe gel 20:1 concentrated juice used for cosmetic | |
| CN108992497A (en) | A kind of disinfectant liquid for skin and preparation method thereof | |
| CN116898761A (en) | Plant essential oil skin disinfectant and preparation method thereof | |
| CN110468159A (en) | A kind of method and the antibiotic extracted enzymatic hydrolysis natural plants and prepare broad-spectrum antibiotic | |
| CN113208024A (en) | Method for preparing bamboo water from fresh bamboo cellulose powder and application of bamboo water |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication |