CN117017883A - Deoiling shampoo and preparation method thereof - Google Patents

Deoiling shampoo and preparation method thereof Download PDF

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CN117017883A
CN117017883A CN202311080536.4A CN202311080536A CN117017883A CN 117017883 A CN117017883 A CN 117017883A CN 202311080536 A CN202311080536 A CN 202311080536A CN 117017883 A CN117017883 A CN 117017883A
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extract
parts
shampoo
degreasing
gentiana macrophylla
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CN117017883B (en
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黄广文
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Guangzhou Dichen Biotechnology Co ltd
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Guangzhou Dichen Biotechnology Co ltd
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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783—Angiosperms [Magnoliophyta]
    • A61K8/9794—Liliopsida [monocotyledons]
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783—Angiosperms [Magnoliophyta]
    • A61K8/9789—Magnoliopsida [dicotyledons]
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00—Preparations for care of the hair
    • A61Q5/008—Preparations for oily hair
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00—Preparations for care of the hair
    • A61Q5/02—Preparations for cleaning the hair
    • G—PHYSICS
    • G06—COMPUTING; CALCULATING OR COUNTING
    • G06V—IMAGE OR VIDEO RECOGNITION OR UNDERSTANDING
    • G06V10/00—Arrangements for image or video recognition or understanding
    • G06V10/20—Image preprocessing
    • G06V10/26—Segmentation of patterns in the image field; Cutting or merging of image elements to establish the pattern region, e.g. clustering-based techniques; Detection of occlusion
    • G—PHYSICS
    • G06—COMPUTING; CALCULATING OR COUNTING
    • G06V—IMAGE OR VIDEO RECOGNITION OR UNDERSTANDING
    • G06V10/00—Arrangements for image or video recognition or understanding
    • G06V10/20—Image preprocessing
    • G06V10/30—Noise filtering
    • G—PHYSICS
    • G06—COMPUTING; CALCULATING OR COUNTING
    • G06V—IMAGE OR VIDEO RECOGNITION OR UNDERSTANDING
    • G06V10/00—Arrangements for image or video recognition or understanding
    • G06V10/20—Image preprocessing
    • G06V10/34—Smoothing or thinning of the pattern; Morphological operations; Skeletonisation
    • G—PHYSICS
    • G06—COMPUTING; CALCULATING OR COUNTING
    • G06V—IMAGE OR VIDEO RECOGNITION OR UNDERSTANDING
    • G06V10/00—Arrangements for image or video recognition or understanding
    • G06V10/40—Extraction of image or video features
    • G06V10/44—Local feature extraction by analysis of parts of the pattern, e.g. by detecting edges, contours, loops, corners, strokes or intersections; Connectivity analysis, e.g. of connected components
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
    • Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change

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  • Engineering & Computer Science (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
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  • General Physics & Mathematics (AREA)
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  • Mycology (AREA)
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  • Biotechnology (AREA)
  • Computer Vision & Pattern Recognition (AREA)
  • Cosmetics (AREA)

Abstract

The invention discloses an oil removal shampoo and a preparation method thereof, and belongs to the technical field of cosmetics. The deoiling shampoo is prepared from mixed plant active ingredients including radix Angelicae sinensis extract, flos Rosae Rugosae extract, folium Mori extract and Pelargonium graveolens extract, and further including radix Gentianae Marcrophyllae extract, herba Swertiae Mileensis extract, radix Gentianae extract and Aloe barbadensis leaf extract. The deoiling shampoo provided by the invention has the advantages of good deoiling effect, stability and no color and pH change after long-term storage.

Description

Deoiling shampoo and preparation method thereof
Technical Field
The invention belongs to the technical field of cosmetics, and particularly relates to an oil removal shampoo and a preparation method thereof.
Background
An important function of a shampoo is to remove oil. For the selection of oily hair shampoos, degreasing is particularly important. At present, the oil removal of active ingredients of plant origin is relatively large.
CN105287273a discloses a natural plant shampoo and a preparation method thereof. The shampoo has effects of preventing alopecia, controlling oil, inhibiting white hair growth, removing dandruff, relieving itching, cleaning hair, nourishing hair root, improving thin hair, improving hair quality, dispelling pathogenic wind, dispelling cold, activating meridians, dredging collaterals, relieving dizziness and headache, and refreshing brain.
Disclosure of Invention
In the further studies of the above patent, the researchers of this patent found that the problem of color change and slight pH rise in the long-term storage (50 ℃ C., 6 months) of the deoiling shampoo made of the angelica sinensis extract, the mulberry leaf extract, the rose extract, the mulberry leaf extract and the pelargonium graveolens extract in the plant active ingredients. Researchers have unexpectedly found that altering the specific plant components therein can prevent this problem from occurring. This patent is based on this finding.
In a first aspect of the present invention, there is disclosed a deoiling shampoo, the mixed plant active ingredients comprising extract of chinese angelica root (ANGELICA POLYMORPHA SINENSIS), extract of rose (ROSA RUGOSA) flower, extract of mulberry (MORUS ALBA) leaf and extract of pelargonium graveolens (PELARGONIUM GRAVEOLENS), further comprising extract of GENTIANA macrophylla (GENTIANA MACROPHYLLA), extract of swertia japonica (SWERTIA BIMACULATA), extract of GENTIANA scana, and extract of ALOE vera (ALOE BARBADENSIS) leaf;
the mixed plant active ingredients comprise:
0.3-1 part of gentiana macrophylla extract, 3-5 parts of swertia extract, 0.3-1 part of gentian extract, 5-15 parts of angelica root extract, 5-15 parts of rose extract, 5-15 parts of mulberry leaf extract, 5-15 parts of geranium extract and 10-15 parts of aloe vera leaf extract.
The plant extracts are all commercial cosmetic raw material commodities, wherein the extraction parts of the gentiana macrophylla extract, the swertia japonica Makino extract and the pelargonium roseum extract are whole plants, and the extraction parts of the gentiana macrophylla extract are roots.
In some embodiments of the present invention, the mixed plant active ingredient comprises 0.3 parts of gentiana macrophylla extract, 3 parts of swertia extract, 3 parts of gentiana macrophylla extract, 5 parts of angelica root extract, 5 parts of rose extract, 5 parts of mulberry leaf extract, 5 parts of geranium extract, 10 parts of aloe vera leaf extract.
In some embodiments of the present invention, the mixed plant active ingredient comprises 1 part of gentiana macrophylla extract, 5 parts of swertia extract, 1 part of gentiana macrophylla extract, 15 parts of angelica root extract, 15 parts of rose extract, 15 parts of mulberry leaf extract, 15 parts of geranium extract, and 15 parts of aloe vera leaf extract.
In some embodiments of the present invention, the mixed plant active ingredient comprises 0.6 part of gentiana macrophylla extract, 3.5 parts of swertia extract, 0.6 part of gentiana macrophylla extract, 10 parts of angelica root extract, 10 parts of rose extract, 10 parts of mulberry leaf extract, 10 parts of geranium extract, 12 parts of aloe vera leaf extract.
In some embodiments of the present invention, the mixed plant active ingredient comprises 0.5 part of gentiana macrophylla extract, 4 parts of swertia extract, 0.8 parts of gentiana macrophylla extract, 8 parts of angelica root extract, 12 parts of rose extract, 10 parts of mulberry leaf extract, 12 parts of geranium extract and 12 parts of aloe vera leaf extract.
In some embodiments of the invention, foaming agents, surfactants, hair conditioning agents, astringents, preservatives, colorants, fragrances, and water are also included.
In some embodiments of the invention, the foaming agent comprises sodium laureth sulfate, sodium lauroyl sarcosinate, sodium lauroyl glutamate, sodium laureth sulfate, cocamide DEA, and glycerin.
In some embodiments of the invention, the surfactant comprises cocamidopropyl betaine, sodium chloride, and sodium benzoate.
In some embodiments of the present invention, the hair conditioning agent comprises cocamidopropyl PG-dimethyl ammonium chloride, sodium isostearyl lactoyl lactate, sodium lactate, polyquaternium-7, sodium benzoate, betaine salicylate, polyquaternium-10, phenoxyethanol, ethylhexyl glycerol, p-hydroxyacetophenone, butylene glycol, hydrolyzed yeast extract, and citric acid.
In some embodiments of the invention, the safener is methylisothiazolinone.
In some embodiments of the invention, the astringent is allantoin.
A second aspect of the present invention discloses a method for preparing the degreasing shampoo according to the first aspect, comprising the following steps:
s01, heating water, and keeping the temperature by a temperature control system;
s02, adding the foaming agent, the surfactant, the hair conditioner, the astringent and the preservative, and stirring;
s03, naturally cooling to room temperature, adding the mixed plant active ingredients, the coloring agent and the aromatic, and stirring.
In some embodiments of the invention, in S01, the water is heated to 35-50 ℃.
In some embodiments of the invention, the uniformity of the material is controlled by:
based on uniformity control of picture identification, the mixing proportion is the weight ratio of colored materials to colorless materials, and the uniformity is the distribution state of the colored materials in all materials.
The uniformity Q of the picture identification is:
A min ＝min(A i )
based on the above formula, a gravel incorporation uniformity analysis was performed.
Specifically, a high-definition camera is adopted to collect surface pictures, and crisscross segmentation of the pictures is carried out according to the same size. Based on the segmented pictures, calculating to obtain areas of the color materials by adopting an image recognition mode, wherein the method comprises the following steps of:
(1) Before edge detection is carried out on an original photo image, noise reduction and enhancement pretreatment are carried out on the image, so that the analysis quality of the image is improved;
(2) Converting the result of image preprocessing into a binary image with only black and white to obtain a clearer edge line, setting a threshold value to optimize the binary image to obtain a discrete point diagram;
(3) Discrete point expansion optimization;
(4) Adopting an imopen and an imclose operation in image recognition, closing discrete points into a color non-dependent image by combining the imopen operation and the imclose operation through a bwlabel algorithm to obtain areas ai of the color materials, and obtaining the sum A of the areas A of the color materials in each picture through superposition i ：
A i ＝∑a j
Based on the color material area A of each picture i Uniformity was calculated.
The preparation of the deoiling shampoo of the embodiment controls the uniformity of the product through picture identification, the uniformity of the product is high in detection speed, and online remote detection and control can be realized.
The invention has the beneficial effects that:
the deoiling shampoo provided by the invention adopts plant extracts with specific components in specific proportions, has a good deoiling effect, is stable, and can not change color and pH after long-term storage.
Detailed Description
Other advantages and effects of the present invention will become apparent to those skilled in the art from the following disclosure, which describes the embodiments of the present invention with reference to specific examples. The invention may be practiced or carried out in other embodiments that depart from the specific details, and the details of the present description may be modified or varied from the spirit and scope of the present invention.
The examples and comparative examples are parallel runs of the same components, component contents, preparation steps, preparation parameters, unless otherwise specified.
Example 1
A mixed plant active ingredient of a degreasing shampoo comprising:
comprises 0.3 part of gentiana macrophylla extract, 3 parts of swertia extract, 3 parts of gentian extract, 5 parts of angelica root extract, 5 parts of rose extract, 5 parts of mulberry leaf extract, 5 parts of pelargonium roseum extract and 10 parts of aloe vera leaf extract.
Example 2
A mixed plant active ingredient of a degreasing shampoo comprising:
1 part of gentiana macrophylla extract, 5 parts of swertia extract, 1 part of gentiana macrophylla extract, 15 parts of angelica root extract, 15 parts of rose extract, 15 parts of mulberry leaf extract, 15 parts of pelargonium roseum extract and 15 parts of aloe vera leaf extract.
Example 3
A mixed plant active ingredient of a degreasing shampoo comprising:
0.6 part of gentiana macrophylla extract, 3.5 parts of swertia extract, 0.6 part of gentiana macrophylla extract, 10 parts of angelica root extract, 10 parts of rose extract, 10 parts of mulberry leaf extract, 10 parts of pelargonium roseum extract and 12 parts of aloe vera leaf extract.
Example 4
A mixed plant active ingredient of a degreasing shampoo comprising:
0.5 part of gentiana macrophylla extract, 4 parts of swertia extract, 0.8 part of gentiana macrophylla extract, 8 parts of angelica root extract, 12 parts of rose extract, 10 parts of mulberry leaf extract, 12 parts of pelargonium roseum extract and 12 parts of aloe vera leaf extract.
Example 5
A mixed plant active ingredient of a degreasing shampoo comprising:
0.6 part of gentiana macrophylla extract, 3.5 parts of swertia extract, 0.8 part of gentiana macrophylla extract, 10 parts of angelica root extract, 10 parts of rose extract, 10 parts of mulberry leaf extract, 12 parts of pelargonium roseum extract and 10 parts of aloe vera leaf extract.
Comparative example 1
A mixed plant active ingredient of a degreasing shampoo comprising:
10 parts of angelica root extract, 10 parts of rose extract, 10 parts of mulberry leaf extract and 12 parts of pelargonium roseum extract.
Comparative example 2
A mixed plant active ingredient of a degreasing shampoo comprising:
comprises 5 parts of root extract, 5 parts of rose extract, 5 parts of mulberry leaf extract, 5 parts of pelargonium roseum extract and 16.3 parts of aloe vera leaf extract.
Comparative example 3
A mixed plant active ingredient of a degreasing shampoo comprising:
comprises 0.3 part of gentiana macrophylla extract, 8 parts of swertia extract, 8 parts of gentian extract, 5 parts of angelica root extract, 5 parts of rose extract, 5 parts of mulberry leaf extract and 5 parts of pelargonium roseum extract.
Example 5
An oil removing shampoo comprises the following components:
the preparation method comprises the following steps:
s01, heating water to 40 ℃, and keeping the temperature by a temperature control system;
s02, adding the components except the mixed plant active ingredients, the coloring agent and the aromatic agent, and uniformly stirring;
s03, naturally cooling to room temperature, adding the mixed plant active ingredients, the coloring agent and the aromatic, and uniformly stirring.
Comparative example 4
The difference from example 5 is that only the extracts of the root of the chinese angelica, the rose, the mulberry leaf and the geranium and the solvents thereof (i.e., components 15 to 18) are included, the extracts of the gentiana macrophylla, the swertia, the gentiana macrophylla and the aloe vera leaf and the solvents thereof (i.e., components 9 and 19) are not included, and the insufficient components are complemented with water.
Comparative example 5
The difference from example 5 is the preparation method:
s01, heating water to 60 ℃, and keeping the temperature by a temperature control system;
s02, adding the components, and stirring;
s03, naturally cooling to room temperature.
Example 6
The preparation of the degreasing shampoo differs from the preparation step of example 5 in that the uniformity of the material is controlled by the following steps:
based on uniformity control of picture identification, the mixing proportion is the weight ratio of colored materials to colorless materials, and the uniformity is the distribution state of the colored materials in all materials.
The uniformity Q of the picture identification is:
A min ＝min(A i )
based on the above formula, a gravel incorporation uniformity analysis was performed.
Specifically, a high-definition camera is adopted to collect surface pictures, and crisscross segmentation of the pictures is carried out according to the same size. Based on the segmented pictures, calculating to obtain areas of the color materials by adopting an image recognition mode, wherein the method comprises the following steps of:
(1) Before edge detection is carried out on an original photo image, noise reduction and enhancement pretreatment are carried out on the image, so that the analysis quality of the image is improved;
(2) Converting the result of image preprocessing into a binary image with only black and white to obtain a clearer edge line, setting a threshold value to optimize the binary image to obtain a discrete point diagram;
(3) Discrete point expansion optimization;
(4) Adopting an imopen and an imclose operation in image recognition, closing discrete points into a color non-dependent image by combining the imopen operation and the imclose operation through a bwlabel algorithm to obtain areas ai of the color materials, and obtaining the sum A of the areas A of the color materials in each picture through superposition i ：
A i ＝∑a j
Based on the color material area A of each picture i Uniformity was calculated.
The preparation of the deoiling shampoo of the embodiment controls the uniformity of the product through picture identification, the uniformity of the product is high in detection speed, and online remote detection and control can be realized.
In the preparation of the degreasing shampoo of this example, no significant difference in long-term storage performance was found for the product when the uniformity was above 95%. Uniformity is lower than 60%, and the long-term preservation performance of the product has obvious difference.
Experimental example performance investigation
1 Mixed plant active ingredients of deoiling shampoo
Taking the active ingredients of each of the mixed plants of examples 1-5 and comparative examples 1-3, adding deionized water to prepare a 10% by weight solution, adding 0.5% (w/v) methylisothiazolinone and 1% (w/v) ascorbic acid, storing in a sealed environment at 35 ℃ for 1 month, and observing color change and pH change. The change scores of the colors after preservation relative to the initial colors are shown in Table 1, and the preservation results are shown in Table 2.
TABLE 1 color Change scoring Table
Standard of Scoring of
No visual change in color 1
The colour change varies but is not great 3
Has obvious color change 5
TABLE 2 Properties of Mixed plant active ingredients
Color change pH change
Example 1 2.2 Slightly raise the pH to 0.1
Example 2 2.0 Slightly raise the pH to 0.1
Example 3 1.8 Unchanged
Example 4 1.2 Unchanged
Example 5 2.0 Slightly raise the pH to 0.1
Comparative example 1 5.0 The pH is obviously raised to 0.3
Comparative example 2 3.2 The pH was slightly raised, 0.2
Comparative example 3 4.6 Slightly raise the pH to 0.3
2 deoiling shampoo
The degreasing shampoo of comparative example 5 was slightly yellow brown in color and had poor sensory properties. The degreasing shampoo of example 5 and comparative example 4 was stored at room temperature for 12 months, and the color change was observed. The degreasing shampoo of example 5 was found to have no color change, and comparative example 4 had a visual change.
The degreasing shampoo of example 5 and comparative examples 4 and 5 was taken and tested for degreasing effect. The results showed no significant difference between the two.
While the preferred embodiments and examples of the present invention have been described in detail, the present invention is not limited to the above-described embodiments and examples, and various changes may be made within the knowledge of those skilled in the art without departing from the spirit of the present invention.

Claims (10)

1. The deoiling shampoo is prepared from mixed plant active ingredients including radix angelicae sinensis extract, rose extract, mulberry leaf extract and pelargonium roseum extract, and is characterized by further comprising gentiana macrophylla extract, swertia japonica extract, gentiana macrophylla extract and aloe vera leaf extract;
the mixed plant active ingredients comprise:
0.3-1 part of gentiana macrophylla extract, 3-5 parts of swertia extract, 0.3-1 part of gentian extract, 5-15 parts of angelica root extract, 5-15 parts of rose extract, 5-15 parts of mulberry leaf extract, 5-15 parts of geranium extract and 10-15 parts of aloe vera leaf extract.
2. The degreasing shampoo of claim 1, wherein the mixed plant active ingredients comprise 0.3 parts of gentiana macrophylla extract, 3 parts of swertia extract, 3 parts of gentiana macrophylla extract, 5 parts of angelica root extract, 5 parts of rose extract, 5 parts of mulberry leaf extract, 5 parts of geranium extract, and 10 parts of aloe vera leaf extract.
3. The degreasing shampoo of claim 1 or 2, wherein the mixed plant active ingredients comprise 1 part of gentiana macrophylla extract, 5 parts of swertia extract, 1 part of gentiana macrophylla extract, 15 parts of angelica root extract, 15 parts of rose extract, 15 parts of mulberry leaf extract, 15 parts of geranium extract, and 15 parts of aloe vera leaf extract.
4. A degreasing shampoo according to any of claims 1-3, wherein the mixed plant active ingredients comprise 0.6 parts of gentiana macrophylla extract, 3.5 parts of swertia extract, 0.6 parts of gentiana macrophylla extract, 10 parts of angelica root extract, 10 parts of rose extract, 10 parts of mulberry leaf extract, 10 parts of geranium extract and 12 parts of aloe vera leaf extract.
5. The degreasing shampoo of any one of claims 1-4, wherein the mixed plant active ingredients comprise 0.5 parts of gentiana macrophylla extract, 4 parts of swertia extract, 0.8 parts of gentiana macrophylla extract, 8 parts of angelica root extract, 12 parts of rose extract, 10 parts of mulberry leaf extract, 12 parts of geranium extract, and 12 parts of aloe vera leaf extract.
6. The degreasing shampoo of any of claims 1-5, further comprising foaming agents, surfactants, hair conditioning agents, astringents, preservatives, colorants, fragrances, and water.
7. The degreasing shampoo of any one of claims 1-6, wherein the foaming agent comprises sodium laureth sulfate, sodium lauroyl sarcosinate, sodium lauroyl glutamate, sodium lauroyl sulfate, cocamide DEA, and glycerin;
the surfactant comprises cocamidopropyl betaine, sodium chloride and sodium benzoate;
the hair conditioner comprises cocamidopropyl PG-dimethyl ammonium chloride, isostearyl lactoyl sodium lactate, polyquaternium-7, sodium benzoate, betaine salicylate, polyquaternium-10, phenoxyethanol, ethylhexyl glycerol, p-hydroxyacetophenone, butanediol, hydrolyzed yeast extract and citric acid;
the protective agent is methyl isothiazolinone;
the astringent is allantoin.
8. The degreasing shampoo according to any of claims 1-7, wherein the mixed plant active ingredient is present in an amount of 1-10%, preferably 3-8% by weight.
9. A method of preparing a degreasing shampoo according to any of claims 1 to 8, comprising the steps of:
s01, heating water, and keeping the temperature by a temperature control system;
s02, adding the foaming agent, the surfactant, the hair conditioner, the astringent and the preservative, and stirring;
s03, naturally cooling to room temperature, adding the mixed plant active ingredients, the coloring agent and the aromatic, and stirring.
10. The method of preparing a degreasing shampoo according to claim 9, wherein in S01, water is heated to 35-50 ℃.
CN202311080536.4A 2023-08-25 2023-08-25 Deoiling shampoo and preparation method thereof Active CN117017883B (en)

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CN114632049A (en) * 2020-12-15 2022-06-17 浙江养生堂天然药物研究所有限公司 Hair loss prevention and hair growth composition
CN114712279A (en) * 2022-04-01 2022-07-08 广州帝臣生物科技股份有限公司 Deoiling shampoo
CN115671261A (en) * 2022-10-25 2023-02-03 向小红 Mixed peptide emulsion with sleep improvement effect and preparation method thereof

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