CN116536130A - Wine aging accelerating storage system and wine aging accelerating storage method - Google Patents
Wine aging accelerating storage system and wine aging accelerating storage method Download PDFInfo
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- CN116536130A CN116536130A CN202210085169.6A CN202210085169A CN116536130A CN 116536130 A CN116536130 A CN 116536130A CN 202210085169 A CN202210085169 A CN 202210085169A CN 116536130 A CN116536130 A CN 116536130A
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12H—PASTEURISATION, STERILISATION, PRESERVATION, PURIFICATION, CLARIFICATION OR AGEING OF ALCOHOLIC BEVERAGES; METHODS FOR ALTERING THE ALCOHOL CONTENT OF FERMENTED SOLUTIONS OR ALCOHOLIC BEVERAGES
- C12H1/00—Pasteurisation, sterilisation, preservation, purification, clarification, or ageing of alcoholic beverages
- C12H1/22—Ageing or ripening by storing, e.g. lagering of beer
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
- Y02W90/00—Enabling technologies or technologies with a potential or indirect contribution to greenhouse gas [GHG] emissions mitigation
- Y02W90/10—Bio-packaging, e.g. packing containers made from renewable resources or bio-plastics
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Bioinformatics & Cheminformatics (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- Health & Medical Sciences (AREA)
- General Engineering & Computer Science (AREA)
- General Health & Medical Sciences (AREA)
- Genetics & Genomics (AREA)
- Food Science & Technology (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Distillation Of Fermentation Liquor, Processing Of Alcohols, Vinegar And Beer (AREA)
Abstract
The invention relates to a wine aging accelerating storage system and a wine aging accelerating storage method, comprising a plurality of wine storage tanks, wherein a wine external circulation body is arranged outside the wine storage tanks; a filling frame is arranged in the wine external circulation body, and unglazed ceramic bodies are filled in the filling frame. The method comprises the steps of installing a wine external circulation body outside a plurality of wine storage tanks, installing a filling frame on the wine external circulation body, and filling unglazed ceramic bodies on the filling frame; a wine liquid circulation pipeline, a wine liquid circulation pump, a one-way valve, an air pump and an air inlet pipe are connected between the wine storage tank and the wine liquid external circulation body; adding brewed wine into a wine storage tank; the wine circulating pump and the air pump are started, so that the wine and the air start to continuously flow in the wine storage tank and the wine external circulating body respectively.
Description
Technical Field
The invention relates to the technical field of wine liquid storage, in particular to a wine liquid aging accelerating storage system and a wine liquid aging accelerating storage method.
Background
The white spirit is the traditional distilled durian spirit in China, has long history, is popular, has vivid national characteristics, and is unique in wine products in terms of unique color, aroma and taste. However, the newly brewed white spirit has strong irritation, pungency and difficult feeling of swallowing, and various components of the wine can be balanced through ageing, so that the wine quality is mellow and harmonious.
The Chinese white spirit is produced with grains as main material and through solid fermentation, steaming, and several tens of production steps, and through the steps of producing valuable non-matter cultural heritage, the intelligent and inventive steps of the laborers are condensed. The alcohol content is up to about 70% vol in the steaming process, and a large amount of free alcohol molecules move rapidly, so that low-boiling-point substances are emitted, and the feeling of pungency, rushing and difficult swallowing is formed. In order to reduce the irritation and make the wine molecule change from 'polar positive' to 'polar negative' so as to attain the goal of making wine quality soft, smooth and pleasant in fragrance, the crude oil must be stored, and the industry called natural ageing so as to obtain the invented finished product. The quality and flavor of the white spirit are closely related to storage aging, and the traditional process is to store the white spirit in a pottery jar, and the storage period is generally more than 3 years, so that the white spirit has mellow, soft and soft feeling.
The length of the ageing period directly determines the market share of the wine products and the economic benefits of manufacturers. With the continuous deep understanding of the physical change and chemical change mechanism in the aging process, many wineries try to age by adopting an artificial aging technology.
The existing artificial ageing method mainly comprises a physical method, a chemical method, a biological method, a microbiological method and the like, and has certain success. The high energy aging method comprises ultraviolet light irradiation method, ray irradiation method, ultrasonic treatment method, laser irradiation method, high frequency electric field method, microwave treatment method, etc., for example Fu Benli, etc., when the freshly brewed wine is irradiated with laser, the wine taste can be removed after short-term storage, however, the flavor and the products of the aging process of the aging method are difficult to control; the low-energy ageing method includes stirring, powerful oscillation, heating, infrared irradiation, superhigh pressure jet, freezing, magnetic field treatment, etc. and may be used in treating wine for about one week to shorten ageing period, but the ageing method has low energy, unstable simple hydrogen bond association and re-showing hot and dry feeling after some period of time to result in easy ageing Chen Xiaoguo. Microwave ripening, ultrasonic ripening, magnetic ripening, high-pressure ripening, X-ray ripening, etc. Oxidation (ozone ripening, oxygen ripening, potassium permanganate oxidation), catalysis (acid catalysis, catalyst catalysis), and the like. Biological method: YS-II, yellow serofluid and the like. The difficulty of the biological microorganism aging accelerating technology is high, and further development and research are still needed.
The natural aging stage of the white spirit plays a vital role in improving the quality of the wine body, and the aging can make the wine body 'flavor-enhancing', 'Ping Lie', 'cover riot' and 'impurity-removing', so that the white spirit is a necessary path of the finished white spirit. However, the traditional natural aging for several years not only causes the volatilization loss of the wine body, but also requires a great deal of investment of resources such as people, wealth, things and the like, and increases the production cost of enterprises. Therefore, the artificial ripening technology for enabling the new wine to reach the quality of the old wine in a short time is a research hotspot in the white wine industry.
Although many of the existing aging methods are mostly of empirical nature and small scale, there is no perfect aging technology and theoretical system corresponding to the technology. The ageing period can greatly influence the production cost of the white spirit. The longer the ageing time is, the larger the enterprise investment is, and the loss of sprinkling is increased, so that the production efficiency and the production scale of the enterprise are greatly influenced.
The method has a certain ageing effect on the white spirit to different degrees, but has some problems, mainly including that firstly, due components in the non-traditional white spirit are easy to generate a large number, and secondly, the aging effect is unstable and durable, the polymerized and associated parts are easy to depolymerize and disperse, and the hot explosion characteristic of the new white spirit is restored again, so that the aging phenomenon is serious. Thus, to date, there is no method that can completely simulate the natural aging process of white spirit.
Chinese patent application (CN 105907589 a) discloses a method for storage aging of white spirit, which includes three stages of pre-storage aging, mid-storage aging, and post-storage aging. The earlier stage storage is aged: pumping the raw wine to be treated into an outdoor open-air stainless steel wine tank, and heating by sun-exposure in summer and autumn and artificial steam in winter and spring, and controlling the wine temperature to be 35-40 ℃; wherein the stirring is carried out for 30-35min every day for the first 6-8 days, and clean air is introduced during stirring; stirring for 50-60min every 10-12 days, and introducing clean air during stirring; when the stainless steel wine tank is aerated and stirred, an inlet hole of the stainless steel wine tank is opened for exhausting, and the inlet hole is closed at ordinary times and is exhausted by a breather valve; the pre-storage aging time is 3-4 months;
the medium-term storage aging: sub-packaging the primary wine subjected to primary storage and aging in a pottery jar, and sealing and storing in a natural forest for 3-4 months; then adding water into the original wine according to the required alcohol degree to reduce the alcohol degree, pumping the original wine into a stainless steel wine tank in a room, and adding aged ceramic altar slices with the mass ratio of 3-5% and granular medical stone with the mass ratio of 1-3% into the stainless steel wine tank in the room; stirring every 15-17 days for 50-60min, introducing clean air during stirring, and storing for aging for 6-8 months;
The later-stage storage and aging are carried out: and subpackaging the aged white spirit stored in the middle stage in a pottery jar, placing the pottery jar in an underground cellar, and statically storing the liquor in the jar for 24-26 months at the temperature of 26-28 ℃ and the humidity of 65-75% to obtain the required white spirit. The aging method of the white spirit takes 33-38 months. The aging period is still longer, the operation procedure is complex, the consumption of manpower and material resources is large, the wine damage in the aging process is large, the effect of wine aging is not obvious, and the method is only applicable to a single wine storage tank.
Chinese patent application (CN 112126576 a) discloses a method for promoting aging of white spirit, wherein during aging of white spirit, ceramic powder is added into white spirit to accelerate aging of white spirit; the particle size of the ceramic powder is 10-80 meshes. The method has low cost, quick action and easy usage, and increases specific surface area, adsorption performance and metal dissolution, accelerates oxidation, hydrogen bond association and esterification of Chinese liquor, shortens aging time of Chinese liquor, and reduces production cost of Chinese liquor. However, in the method for promoting the aging of the white spirit, the pottery jar is crushed into the pottery powder and then the pottery powder is directly added into the white spirit, the pottery powder is immersed in the white spirit in a static state at the bottom of the white spirit, the effective contact area of the pottery powder and the white spirit is greatly limited, although the contact specific surface area of the pottery powder with the white spirit is theoretically increased compared with that of the ceramic container, the effective contact area of the pottery powder with the white spirit is only the pottery powder accumulated on the surface layer in the wine storage container, and the rest of the pottery powder covered on the surface layer is not in effective contact with the white spirit. In addition, as the granularity of the ceramic powder is finer, a large amount of ceramic powder is carried out along with the stirring or pouring of wine in the process, that is, people drink the ceramic powder into the human body together while drinking wine, which is liable to cause harm to the body of a drinker, and the method is only applicable to a single wine storage tank.
Chinese patent application (CN 212174927U) discloses a ageing device for promoting quality improvement of white spirit, comprising: the device comprises a tank body, a ceramic column, a stirring device, a wine inlet pipe and a wine outlet pipe; the ceramic column is arranged in the tank body, the ceramic column is of a hollow structure, and the hollow part of the ceramic column is communicated with the tank body; the stirring device stretches into the tank body; the wine inlet pipe is communicated with the tank body; the wine outlet pipe is also communicated with the tank body. The device is simple to operate and high in practicality. Compared with natural aging, the wine body is magnetically stirred regularly, so that the dynamic balance between ethanol molecules and water molecules is continuously broken, brownian motion is accelerated, and the wine has a good promotion effect on aging of new wine. The ceramic columns in the tank body have oxidation and adsorption effects, and a unique micro-oxygen environment and a unique breathing effect of wine in the tank are formed among the ceramic columns, so that the ageing of the white wine in the storage process can be accelerated, and the ageing time of the white wine is effectively shortened. The ageing accelerating device for promoting the quality improvement of the white spirit is only provided with the ceramic column and the stirring device in the tank body for storing the white spirit, and the contact area of the white spirit and the ceramic is not obviously increased. And after the ceramic column and the stirring device are arranged in the wine storage tank body, the loading and unloading of wine liquid can be affected, the quality of the wine liquid is reduced, the processing and manufacturing cost of the tank body can be greatly improved, and the device can be only suitable for a single wine storage tank.
Chinese patent application (CN 110317705A) discloses a method for accelerating aging of white spirit. The method comprises the steps of connecting new wine into an outdoor storage container, connecting old wine, placing an adsorption column, introducing oxygen, leading the white wine which is aged for a period of time into an indoor storage container from the outdoor storage container, and controlling the indoor temperature. Compared with the traditional natural aging technology, the method can accelerate the aging of the new wine for 1 year, thereby achieving the effect of natural aging for 9-10 years; and the peculiar smell and the miscellaneous taste of the aged white spirit are obviously disappeared, the taste is mellow, sweet and soft, the aftertaste is long, and the aged white spirit has prominent taste. The method for accelerating aging of the white spirit adopts a blending method of new and old wine and uses the old wine to trigger the new wine to accelerate the aging process of the new wine, however, according to the technical scheme disclosed in the patent application document, the aging process of the new wine can be influenced by seasons and environmental temperature, the aging period is very long, and the method is only applicable to a single wine storage tank.
Chinese patent application (CN 106479849A) discloses a process method for rapidly promoting ageing of white spirit and a wine storage container, wherein the method comprises the following steps: firstly, selecting a large wine storage container with the capacity of more than 30 tons, and arranging a ceramic medium in the container; secondly, filling the white spirit to be aged into a wine storage container, and blending with the flavoring wine after the white spirit is in an alcohol concentration range; thirdly, stirring the white wine in the wine storage container in the morning and afternoon respectively, wherein the stirring time is 40 minutes each time, and the stirring lasts for 3 days; fourth, sealing the tank of the white spirit which is successfully prepared, storing for 6 months and filling. By utilizing the advantages of small occupied area, accurate measurement and the like of the stainless steel large tank, the ceramic chip treatment medium and other auxiliary methods are added into the large tank according to the chemical reaction and physical change mechanism in the storage process of the ceramic tank, so that the oxidation, hydrogen bonding and acetification reactions of the white wine are accelerated, and the purposes of saving space, shortening the storage period and reducing cost are achieved. The technological process for fast promoting ageing of white spirit and the wine container have the advantages that only ceramic medium is placed into a large wine container for regular stirring, meanwhile, flavoring wine is added for blending, the technological process is complex in operation, long in ageing period, the structural complexity of the large wine container is increased, the ceramic medium placed in the large wine container is not easy to replace and is in a static state for a long time, the effect of increasing the specific surface area of the ceramic medium is not obvious, and the method and the wine container are only applicable to a single wine storage tank.
Chinese patent application (CN 106047623 a) discloses a method and apparatus for aging a new wine mineralized with a glaze, in which the new wine to be aged is stored in contact with a glaze particle, the glaze particle is micropores of a conventional container made of the glaze, and the glaze particle is rich in metal ions for promoting aging of the wine, and mainly includes iron, manganese, copper, chromium and cadmium. The invention can adsorb low boiling point small molecules and other miscellaneous flavors when storing new wine; the glaze contains a trace amount of metal ions, so that the reaction speed is increased, such as esterification reaction, and the ageing of the wine quality is promoted; the contact area of the wine liquid and the glaze particles is increased to the greatest extent, and the method is economical and practical, has small investment and does not need equipment and energy. However, the method and the device for accelerating aging of the new wine mineralized by the glaze also put the glaze particles into a stainless steel container, the wall of the stainless steel container is provided with a plurality of micropores with the pore diameter smaller than the particle diameter of the glaze particles, and then the stainless steel column is put into a wine pool. The stainless steel container and the glaze particles in the stainless steel container in the device are in a static state in the wine pool, so that the contact and ion exchange process of wine liquid and the glaze particles cannot be accelerated, and the method and the device can only be applied to a single wine storage tank.
Disclosure of Invention
The invention aims to overcome the defects in the prior art, and provides the accelerated wine aging storage system which has the advantages of simple structure, high wine aging efficiency, short aging process period, high degree of automation, small occupied area and low manufacturing cost, can increase the comparison area of the wine contacted with the ceramic body by hundreds of times on the basis of keeping the existing stainless steel wine storage tank, and can simultaneously age and catalyze the wine in a plurality of wine storage tanks.
In order to achieve the above purpose, the technical scheme of the invention is to provide a storage system for accelerating aging of wine, the system comprises a plurality of wine storage tanks, at least one wine external circulation body is arranged outside the plurality of wine storage tanks, a wine circulation pipeline is connected between the plurality of wine storage tanks and the at least one wine external circulation body, a wine circulation pump and a valve are connected in series on the wine circulation pipeline, an air inlet pipe is further arranged on the at least one wine external circulation body, an air pump is connected on the air inlet pipe, and exhaust ports are respectively arranged on the plurality of wine storage tanks; at least one wine external circulation body is internally provided with a filling frame, and unglazed ceramic bodies are filled in the filling frame.
In order to facilitate processing and manufacturing of the wine liquid external circulation body and facilitate installation and use of the wine liquid external circulation body, and facilitate installation and replacement of the wine liquid external circulation body, the wine liquid external circulation body is arranged in an aging workshop or a control room, the wine liquid external circulation body is of a tower structure, the wine liquid external circulation body of the tower structure comprises a shell of an integral structure or a split structure, the packing frame is arranged in the shell, the packing frame comprises a frame of the integral structure or the split structure which is matched with the internal structure of the shell, a plurality of layers of trays or net drums are arranged on the frame, or the frame and the trays or net drums of the layers form the integral structure, the trays are provided with meshes, and the unglazed ceramic body is arranged on the trays or in the net drums. The internal volume of the tower-type structure wine liquid external circulation body is 1% -15% of the sum of the internal volumes of the plurality of wine storage tanks.
In order to facilitate the improvement of the structural strength of the frame and the tray, the service life of the frame and the tray is prolonged, the craftsman manufacture of the frame and the tray is facilitated, and the wine is not polluted, further preferred technical scheme is that the frame and the tray or the net barrel comprises a metal frame and a metal tray or a metal net barrel, or comprises an unglazed ceramic frame and an unglazed ceramic tray or an unglazed net barrel.
In order to increase the specific surface area of contact between the wine and the unglazed ceramic body as much as possible, and to facilitate the processing and manufacturing of the unglazed ceramic body without polluting the wine, the further preferred technical scheme is that the unglazed ceramic body comprises any one or any combination of unglazed ceramic sheets, unglazed ceramic particles, unglazed ceramic balls, unglazed ceramic honeycomb blocks.
In order to facilitate the connection between the plurality of wine storage tanks and at least one wine external circulation body, and to reduce the energy consumption of the wine circulation pump as much as possible in the wine circulation process of the plurality of connected wine storage tanks and at least one wine external circulation body, reduce the volume of the wine circulation pump, avoid the countercurrent and leakage of wine, facilitate the control of the inlet and outlet of wine and gas in each wine storage tank independently, the further preferred technical scheme is that a wine outlet pipe is arranged at the bottom or the lower part of the shell, a wine inlet pipe is arranged at the top or the upper part of the shell, the wine outlet pipe at the bottom or the lower part of the shell is connected with one end of a tower outlet collecting pipeline through a tower outlet circulating pump connected in series, the other end of the tower outlet collecting pipeline is respectively connected with one end of a plurality of tower outlet wine circulation pipelines, and the other end of the tower outlet wine circulation pipeline is respectively connected with a tower outlet check valve and a tower outlet control valve in series; the top or upper portion of the shell body is connected with one end of a tower return wine circulating pump in series, the other end of the tower return collecting pipeline is respectively connected with one ends of a plurality of tower return wine circulating pipelines, the other ends of the tower return wine circulating pipelines are respectively connected with a plurality of wine storage tank bottoms or lower wine discharge pipes, and a tower return check valve and a tower return control valve are respectively connected in series on the tower return wine circulating pipelines.
In order to enable the gas to be in full mixing contact with the wine in each of the plurality of wine storage tanks, and avoid the wine to flow into the air inlet pipe and the air pump, the air inlet state in each of the plurality of wine storage tanks is conveniently controlled, the further preferred technical scheme is that the bottom or the lower part of the shell is provided with an air inlet pipe communicated with the inside of the shell, the top or the upper part of the shell is provided with an air conveying pipe communicated with the inside of the shell, the air inlet pipe is connected with an air outlet of the air pump, the air conveying pipe is respectively connected with one ends of a plurality of air conveying branch pipes through an air conveying collecting pipe, the other ends of the plurality of air conveying branch pipes are respectively connected with an air conveying one-way valve and an air inlet of the bottom or the lower part of the plurality of wine storage tanks in series, the air outlet on the plurality of wine storage tanks is respectively arranged at the top or the upper part of each wine storage tank, and a valve cap is respectively arranged on each air outlet.
In order to ensure that the wine in each of the plurality of wine storage tanks is uniformly conveyed into at least one wine external circulation body through a wine circulation pipe, and the gas is uniformly conveyed into each of the plurality of wine storage tanks, further preferably, the technical scheme is that a plurality of wine discharge pipes are uniformly distributed at the bottom or the lower part of each of the plurality of wine storage tanks, at least one wine return pipe is respectively arranged at the top or the upper part of each of the plurality of wine storage tanks, a plurality of air inlets are respectively distributed at the bottom or the lower part of each of the plurality of wine storage tanks, at least one air outlet is respectively arranged at the top or the upper part of each of the plurality of wine storage tanks, the wine flows into at least one tower liquid circulation body through a tower outlet circulation pipe, a tower outlet wine circulation pump, a tower outlet one-way valve and a tower return one-way valve from top to bottom, and the gas flows into at least one of the plurality of wine storage tanks from top to bottom through an air pump, an air inlet pipe, an air delivery collecting pipe, an air delivery pipe, an air outlet, an air delivery one-way valve and a plurality of air delivery pipe from top to bottom to top or from top to bottom in each of the plurality of wine storage tanks; the stirrer is arranged in the wine storage tanks, the stirrer comprises a stirring shaft arranged in the wine storage tanks, stirring blades are arranged on the stirring shaft, one end of the stirring shaft extends out of the wine storage tanks and is connected with a driving motor arranged outside the wine storage tanks, or a vibrating rod or an ultrasonic vibrator is arranged in the wine storage tanks.
In order to accelerate the aging process of the wine and promote the oxidation-reduction reaction between the wine and more beneficial metal elements, the content of harmful metal elements in the clay for manufacturing the pottery is strictly limited, and further preferably, the unglazed ceramic contains at least 1.1-1.3 wt% of copper oxide, 1.3-1.8 wt% of ferric oxide, 0.1-0.2 wt% of magnesium oxide, 0.01-0.02 wt% of sodium oxide, 0.01-0.02 wt% of potassium oxide, 0.005-0.008 wt% of aluminum trioxide, 0.001-0.003 wt% of titanium, 0.003-0.005 wt% of manganese, 0.001-0.002 wt% of nickel, 0.001-0.002 wt% of chromium and 0.001-0.002 wt% of lead in the clay for manufacturing the pottery, wherein the content of copper metal and the iron metal is blended with the copper powder and the clay.
The invention also aims to overcome the defects existing in the prior art, and provides a method for accelerating the aging and storing of the wine by adopting an accelerating wine aging and storing device, which has the advantages of simple structure, high wine aging efficiency, short aging process period, high degree of automation, small occupied area and low manufacturing cost, can increase the comparison area of the wine contacted with the ceramic body by hundreds of times on the basis of keeping the existing stainless steel wine storing tank, and can simultaneously perform aging and catalysis on the wine in a plurality of wine storing tanks.
The method for accelerating the aging storage of the wine by adopting the accelerating aging storage system of the wine comprises the following steps:
s1, at least one wine external circulation body is arranged outside a plurality of wine storage tanks, a filling frame is arranged in at least one wine external circulation body, and unglazed ceramic bodies are filled on the filling frame;
s2, connecting a tower outlet wine circulation pipeline, a tower return wine circulation pipeline, a tower outlet wine circulation pump, a tower return wine circulation pump and a tower outlet one-way valve between a plurality of wine storage tanks and at least one wine external circulation body, wherein the tower return one-way valve, the tower outlet control valve, the tower return control valve, the air pump, the air inlet pipe, the air transmission collecting pipe, the air transmission branch pipe and the air transmission one-way valve;
s3, adding brewed wine into a plurality of wine storage tanks respectively;
s4, starting a tower outlet wine circulating pump, a tower return wine circulating pump and an air pump, so that wine starts to continuously circulate from top to bottom in a plurality of wine storage tanks and at least one wine external circulating body respectively, and simultaneously, gas continuously flows from bottom to top or from bottom to top in a plurality of wine storage tanks and at least one wine external circulating body respectively, and the gas flowing into the plurality of wine storage tanks is discharged from an exhaust port arranged at the top or upper part of the plurality of wine storage tanks respectively;
S5, regularly detecting the aging state of the liquor in each of a plurality of liquor storage tanks, closing a tower outlet control valve and a tower return control valve which are connected with the corresponding liquor storage tank after the liquor in a certain liquor storage tank reaches a set aging index, and closing a tower outlet liquor circulating pump, a tower return liquor circulating pump and an air pump or respectively closing a tower outlet control valve and a tower return control valve which are connected in series on a tower outlet liquor circulating pipeline and a tower return liquor circulating pipeline after the liquor in all the liquor storage tanks reaches the set aging index;
s6, taking out the unglazed ceramic body filled on the filling frame periodically, and repeatedly using the unglazed ceramic body after high-temperature treatment at 500-650 ℃.
In order to monitor and control the aging process of the wine, the wine which is aged to a specific index is timely led out from the wine storage tanks, then new wine is added again to improve the production efficiency and improve the economic benefit, the preferred technical scheme is that the tower outlet wine circulating pump, the tower return wine circulating pump, the air pump, the tower outlet control valve and the tower return control valve are respectively connected with the controller, the circulating flow rate of the wine between a plurality of wine storage tanks and at least one wine external circulating body and the flow rate of gas in a plurality of wine storage tanks and at least one wine external circulating body are controlled by the controller, and unglazed ceramic bodies filled on the filling frames in the at least one wine external circulating body are replaced according to the detection result of the metal ion content of the wine in the plurality of wine storage tanks.
The invention has the advantages and beneficial effects that: the accelerated wine aging storage system has the advantages of simple structure, high wine aging efficiency, short period of aging process and high degree of automation, can be used for keeping the existing stainless steel wine storage tank, has small occupied area and low cost, can ensure that the transition metal of an unsaturated electronic layer in the wine is obviously increased, and can continuously or intermittently, uniformly and thoroughly and slowly circulate between the wine storage tank and the wine external circulation body, so that the comparison area of the wine and the ceramic body can be increased by hundreds of times, and even thousands of times. The filling materials added in the wine liquid external circulation body can be taken out and replaced periodically, the taken-out filling materials can be repeatedly used after being treated at high temperature, adsorbates on the unglazed ceramic body can be evaporated and carbonized after being heated at high temperature, and the oxidation activity of metal oxides in the unglazed ceramic body can be recovered after being treated at high temperature, and the characteristics of simultaneously aging and catalyzing the wine liquid in a plurality of wine storage tanks can be continued.
According to the accelerated wine aging storage system, at least one wine external circulation body is arranged outside a plurality of wine storage tanks, so that wine forms internal and external circulation of the wine through a wine circulation pipeline and a wine circulation pump, and dynamic contact between the wine and the ceramic body is formed by repeated contact of the wine with circulation of unglazed ceramic body filler in the wine external circulation body in the internal and external circulation process. The characteristic that the unglazed ceramic filler has large specific surface area is utilized, the number of times of dynamic contact exchange between the wine liquid and the metal in the unglazed ceramic body is greatly increased, so that the metal in the unglazed ceramic body enters the wine body in an ionic state, meanwhile, the gas in the external circulation of the wine liquid can be introduced by the air pump, the oxidation of the metal ions in the unglazed ceramic body is increased, the wine liquid can be further promoted to be converted into sol as soon as possible, and the sol tends to be perfect and stable after the wine liquid is stored for a certain time, so that a certain perfect wine body is formed.
The unglazed ceramic body has a plurality of pores, the surface is not blocked by the glaze layer, and the wine can also permeate into the unglazed ceramic body to be contacted with metal elements in the unglazed ceramic body, so that various metal elements enter the wine body in the form of metal ions. Thereby promoting the formation of sol in the wine body.
Colloidal particles in the wine are obviously formed by molecular or ionic coalescence. The particles in the sol are composed of a gel core, colloidal particles and a micelle. How the trace components in the wine body form sol, the key is the formation of gum nuclei. The white spirit is colloid, its colloid core is made up of mixture of ethyl palmitate, ethyl oleate and ethyl linoleate, and the formation of colloidal particles in white spirit is not simple mutual accumulation of molecules, and is related to metal elements in the spirit body, especially to transition elements with unsaturated electronic layers. Namely, the A ion (or atom) of the metal element is combined with a plurality of B ions (or molecules) or a plurality of A ions and B ions (or molecules) in a coordination bond mode to form complex chemical particles with certain characteristics so as to form a gel core in the wine body. Such complex chemical particles of complexing composition are generally referred to as complex ions or complexing molecules.
The types and the contents of the metal elements in the wine body are different, so that the rubber cores and the rubber particles formed in the wine body are inevitably different, and the style of the wine body is quite different. The ceramic filler is mainly used for adding Fe, cu, si, pb, mn, al, ca, mg, cr, ce, cd, ni and other elements, and the stainless steel tank has fewer types of elements for storing wine, so that the ceramic tank fragments can be crushed and added into the wine external circulation body, the solid-liquid contact interface is increased, the content of metal elements is increased, and the types of the metal elements are increased. Thus, the gum cores in the wine body can be diversified.
Drawings
FIG. 1 is a schematic diagram of a system for accelerating aging of wine in accordance with the present invention;
FIG. 2 is a schematic diagram of a cross-sectional structure of a wine storage tank in the accelerated aging storage system of the invention;
FIG. 3 is a schematic diagram of the cross-sectional structure of the external circulation body of the liquor in the accelerated liquor aging storage system of the invention; .
In the figure: 1. a wine storage tank; 2. an external circulation body of wine liquid; 2.1, a filling frame; 2.2, unglazed ceramic body; 2.3, a shell; 2.4, a tray; 2.5, mesh openings; 3. a wine circulation pipeline; 3.1, a tower outlet liquor circulation pipeline; 3.2, returning to the tower liquor circulation pipeline; 4. a liquor circulating pump; 4.1, a tower outlet liquor circulating pump; 4.2, a tower returning liquor circulating pump; 5. a control valve; 6. an air inlet pipe; 7. An air pump; 8. an exhaust port; 9. a wine liquid discharge pipe; 10. a wine liquid input pipe; 11. discharging the tower from the collecting pipeline; 12. a tower outlet pipe one-way valve; 13. a tower outlet control valve; 14. a liquor return pipe; 15. a tower returning collecting pipeline; 16. a wine liquid discharge pipe; 17. a tower returning one-way valve; 18. a tower returning control valve; 19. a gas pipe; 20. a gas transfer header; 21. the gas transmission is divided into pipes; 22. a gas transmission one-way valve; 23. a gas transmission control valve; 24. an air inlet; 25. and a valve cap.
Detailed Description
The following describes the embodiments of the present invention further with reference to the drawings and examples. The following examples are only for more clearly illustrating the technical aspects of the present invention, and are not intended to limit the scope of the present invention.
Example 1
As shown in fig. 1-3, the invention is an accelerated wine aging storage system, the system comprises a plurality of wine storage tanks 1, at least one wine external circulation body 2 is arranged outside the plurality of wine storage tanks 1, a wine circulation pipeline 3 is connected between the plurality of wine storage tanks 1 and the at least one wine external circulation body 2, a wine circulation pump 4 and a control valve 5 are connected in series on the wine circulation pipeline 3, an air inlet pipe 6 is also arranged on the at least one wine external circulation body 2, an air pump 7 is connected on the air inlet pipe 6, and exhaust ports 8 are respectively arranged on the plurality of wine storage tanks 1; at least one wine external circulation body 2 is internally provided with a filling frame 2.1, and unglazed ceramic bodies 2.2 are filled in the filling frame 2.1. Wherein a plurality of wine storage tanks 1 can all adopt stainless steel wine storage tanks, and at least one wine external circulation body 2 can be arranged beside a plurality of wine storage tanks 1, also can be arranged on the upper part beside a plurality of wine storage tanks 1, and a wine circulation pipeline 3 can also be a stainless steel pipe, and a wine circulation pump 4 can also be a stainless steel pump body.
Example 2
On the basis of the embodiment 1, in order to facilitate the processing and manufacturing of at least one wine external circulation body 2 and the installation and use of at least one wine external circulation body 2, and facilitate the installation and replacement of a filling frame 2.1 and an unglazed ceramic body 2.2 inside the wine external circulation body 2, the preferred embodiment of the invention is that the at least one wine external circulation body is arranged in an aging workshop or a control room, the at least one wine external circulation body 2 is in a tower structure, the wine external circulation body 2 in the tower structure comprises a shell 2.3 in an integral structure, the filling frame 2.1 is arranged in the shell 2.3, the filling frame 2.1 comprises a frame in the integral structure matched with the internal structure of the shell 2.3, a plurality of layers of trays 2.4 are arranged on the frame, meshes 2.5 are arranged on the trays 2.4, and the unglazed ceramic body 2.2 is arranged on the trays 2.4. The internal volume of the tower-structured wine external circulation body 2 is 1% of the sum of the internal volumes of the plurality of wine storage tanks 1, and the rest of the structure is the same as that in embodiment 1.
Example 3
On the basis of embodiment 2, at least one wine external circulation body 2 is tower structure, tower structure's wine external circulation body 2 includes split structure's casing 2.3, packing frame 2.1 sets up in casing 2.3, and packing frame 2.1 includes the frame of split structure with casing 2.3 internal structure looks adaptation, is provided with a plurality of layers of net section of thick bamboo on the frame, unglazed ceramic body 2.2 sets up on the net section of thick bamboo. The internal volume of the tower-structured wine external circulation body 2 is 7.5% of the sum of the internal volumes of the plurality of wine storage tanks 1, the rest of the structure is the same as that of the embodiment 2, and the rest of the structure is the same as that of the embodiment 2.
Example 4
On the basis of the embodiment 2, the at least one wine liquid external circulation body 2 is in a tower structure, the wine liquid external circulation body 2 of the tower structure comprises a shell 2.3 of an integral structure, the filling frame 2.1 is arranged in the shell 2.3, the filling frame 2.1 comprises a frame of the integral structure which is matched with the internal structure of the shell 2.3, the frame and a plurality of layers of net drums form the integral structure, and the unglazed ceramic body 2.2 is arranged on the net drums. The internal volume of the tower-structured wine external circulation body 2 is 15% of the sum of the internal volumes of the plurality of wine storage tanks 1, and the rest of the structure is the same as that in embodiment 2.
Example 5
On the basis of the embodiment 2, in order to facilitate the improvement of the structural strength of the frame and the tray 2.4 and the improvement of the service life of the frame and the tray 2.4, and simultaneously facilitate the manufacture of the frame and the tray 2.4 by technicians without polluting wine, a further preferred embodiment of the invention is that the frame and the tray 2.4 comprise a metal frame and a metal tray, and the rest of the structures are the same as those in the embodiment 2.
Example 6
On the basis of example 5, in order to further increase the contact specific surface area of the liquor and the unglazed ceramic body 2.2, and at the same time, the volume of the liquor external circulation body 2 can be further reduced, and the unglazed ceramic frame and unglazed ceramic tray 2.4 can be adopted, and the rest of the structure is the same as that in example 5.
Example 7
In order to achieve the specific surface area of contact between the liquor and the unglazed ceramic body 2.2 as much as possible on the basis of the example 6, and simultaneously facilitate the processing and manufacturing of the unglazed ceramic body 2.2 without polluting the liquor, a further preferred embodiment of the present invention is that unglazed ceramic body 2.2 is selected from unglazed ceramic sheets, and the rest of the structure is the same as the structure in the example 6.
Example 8
On the basis of the embodiment 6, unglazed ceramic particles can also be selected as unglazed ceramic bodies 2.2, and the rest of the structure is the same as that of the embodiment 6.
Example 9
On the basis of the embodiment 6, the unglazed ceramic body 2.2 can also be unglazed ceramic balls, and the rest structure is the same as that in the embodiment 6
Example 10
The unglazed ceramic body 2.2 can also be unglazed ceramic honeycomb blocks based on the embodiment 6, and the other structures are the same as those in the embodiment 6.
Example 11
On the basis of the embodiment 6, the unglazed ceramic body 2.2 may be a combination of unglazed ceramic sheets and unglazed ceramic particles and unglazed ceramic balls and unglazed ceramic honeycomb blocks, and the other structures are the same as those in the embodiment 6.
Example 12
On the basis of examples 6-11, in order to facilitate the connection between a plurality of wine storage tanks 1 and at least one wine external circulation body 2, and in order to reduce the energy consumption of the wine circulation pump 4 as much as possible in the wine circulation process of the connected plurality of wine storage tanks 1 and at least one wine external circulation body 2, the volume of the wine circulation pump 4 is reduced, and the reflux and leakage of the wine are avoided, the bottom of the shell 2.3 is provided with a wine outlet pipe 9, the top of the shell 2.3 is provided with a wine inlet pipe 10, the wine outlet pipe 9 at the bottom of the shell 2.3 is connected with one end of a tower outlet collection pipeline 11 through a tower outlet circulation pump 4.1 connected in series, the other end of the tower outlet collection pipeline 11 is respectively connected with one end of a plurality of tower outlet wine circulation pipelines 3.1, the other ends of the plurality of tower outlet wine circulation pipelines 3.1 are respectively connected with a tower outlet pipe one-way valve 12 and a tower outlet control valve 13 in series, and the other ends of the plurality of tower outlet wine circulation pipelines 3.1 are respectively connected with a plurality of reflux pipes 14; the wine liquid input pipe 10 at the top of the shell 2.3 is connected with one end of a tower return collecting pipeline 15 through a tower return wine liquid circulating pump 4.2 connected in series, the other end of the tower return collecting pipeline 15 is respectively connected with one ends of a plurality of tower return wine liquid circulating pipelines 3.2, the other ends of the tower return wine liquid circulating pipelines 3.2 are respectively connected with a plurality of wine liquid discharge pipes 16 at the bottom of the wine storage tank 1, and a tower return check valve 17 and a tower return control valve 18 are respectively connected in series on the tower return wine liquid circulating pipelines 3.2, and the rest of the structure is the same as that in the embodiments 6-11.
Example 13
On the basis of the embodiments 6-11, a wine outlet pipe 9 is arranged at the lower part of the shell 2.3, a wine inlet pipe 10 is arranged at the upper part of the shell 2.3, the wine outlet pipe 9 at the lower part of the shell 2.3 is connected with one end of a tower outlet collecting pipeline 11 through a tower outlet wine circulating pump 4.1 connected in series, the other end of the tower outlet collecting pipeline 11 is respectively connected with one ends of a plurality of tower outlet wine circulating pipelines 3.1, a tower outlet check valve 12 and a tower outlet control valve 13 are respectively connected on the plurality of tower outlet wine circulating pipelines 3.1 in series, and the other ends of the plurality of tower outlet wine circulating pipelines 3.1 are respectively connected with a plurality of wine return pipes 14 at the upper part of the wine storage tanks 1; the wine liquid input pipe 10 at the upper part of the shell 2.3 is connected with one end of a tower return collecting pipeline 15 through a tower return wine liquid circulating pump 4.2 connected in series, the other end of the tower return collecting pipeline 15 is respectively connected with one ends of a plurality of tower return wine liquid circulating pipelines 3.2, the other ends of the tower return wine liquid circulating pipelines 3.2 are respectively connected with a plurality of wine liquid discharge pipes 16 at the lower part of the wine storage tank 1, and a tower return check valve 17 and a tower return control valve 18 are respectively connected in series on the tower return wine liquid circulating pipelines 3.2, and the rest of the structures are the same as those in the embodiments 6-11.
Example 14
In order to enable the fully mixed contact between the gas and the wine and avoid the wine flowing into the air inlet pipe 6 and the air pump 7 and simultaneously facilitate the control of the air inlet state in each of the plurality of wine storage tanks 1, further preferred embodiments of the present invention are that the air inlet pipe 6 communicated with the interior of the casing 2.3 is arranged at the bottom of the casing 2.3, the air inlet pipe 19 communicated with the interior of the casing 2.3 is arranged at the top of the casing 2.3, the air inlet pipe 6 is connected with the air outlet of the air pump 7, the air inlet pipe 19 is respectively connected with one end of the plurality of air distribution pipes 21 through the air collecting pipe 20, and the air distribution check valve 22 and the air distribution control valve 23 are respectively connected in series with the plurality of air distribution pipes 21, the other end of the plurality of air distribution pipes 21 is respectively connected with the air inlet 24 at the bottom of the plurality of wine storage tanks 1, the air outlet 8 on the plurality of wine storage tanks 1 is respectively arranged at the top of each wine storage tank 1, and the air outlet 8 is respectively arranged at the top of each air outlet 8, and the rest of the structure is the same as that of the valve cap structure of the valve cap 12 or 13 in the embodiment.
Example 15
On the basis of embodiment 13, the lower part of the shell 2.3 is provided with an air inlet pipe 6 communicated with the interior of the shell 2.3, the upper part of the shell 2.3 is provided with an air pipe 19 communicated with the interior of the shell 2.3, the air inlet pipe 6 is connected with an air outlet of the air pump 7, the air pipe 19 is respectively connected with one ends of a plurality of air branch pipes 21 through an air delivery collecting pipe 20, the air delivery branch pipes 21 are respectively connected with an air delivery one-way valve 22 and an air delivery control valve 23 in series, the other ends of the air branch pipes 21 are respectively connected with air inlets 24 at the lower parts of a plurality of wine storage tanks 1, the air outlets 8 on the plurality of wine storage tanks 1 are respectively arranged at the upper part of each wine storage tank 1, and each air outlet 8 is respectively provided with a valve cap 25, and the rest structures are the same as those in embodiment 12 or 13.
Example 16
In order to enable the wine in each of the plurality of wine storage tanks to be uniformly conveyed into at least one wine external circulation body through the wine circulation pipeline and the gas to be uniformly conveyed into each of the plurality of wine storage tanks on the basis of examples 14 or 15, a further preferred embodiment of the present invention is that a plurality of wine discharge pipes 16 are uniformly distributed at the bottoms of the plurality of wine storage tanks 1 respectively, at least one wine return pipe 14 is arranged at the tops of the plurality of wine storage tanks 1 respectively, a plurality of air inlets 24 are uniformly distributed at the bottoms of the plurality of wine storage tanks 1 respectively, at least one air outlet 8 is arranged at the tops of the plurality of wine storage tanks 1 respectively, the wine flows from top to bottom in the plurality of wine storage tanks 1 and at least one wine external circulation body 2 through a tower outlet liquid circulation pipeline 3.1, a tower return wine circulation pipeline 3.2, a tower outlet wine circulation pump 4.1, a tower return wine circulation pump 4.2, a tower outlet one-way valve 12 and a tower return one-way valve 17, and gas flows from bottom to top through an air pump 7, an air inlet pipe 6, an air pipe 19, an air pipe collecting pipe 20, an air pipe branch 21, an air pipe one-way valve 22 and an air outlet 8, flows from bottom to top or from top to bottom in the plurality of wine storage tanks 1 and at least one wine external circulation body 2, and a stirrer is respectively arranged in the plurality of wine storage tanks, and comprises a stirring shaft arranged in the wine storage tanks, a stirring blade is arranged on the stirring shaft, one end of the stirring shaft extends out of the wine storage tanks and is connected with a driving motor arranged outside the wine storage tanks (not shown), or vibration bars or ultrasonic vibrators (not shown in the drawing) are respectively arranged in the plurality of wine storage tanks. The remaining structure is the same as that in embodiment 14 or 15.
Example 17
On the basis of the embodiment 14 or 15, a plurality of liquor discharge pipes 16 are respectively and uniformly distributed at the lower part of the plurality of liquor storage tanks 1, at least one liquor return pipe 14 is respectively arranged at the upper part of the plurality of liquor storage tanks 6, a plurality of air inlets 24 are respectively and uniformly distributed at the lower part of the plurality of liquor storage tanks 1, at least one air outlet 8 is respectively arranged at the upper part of the plurality of liquor storage tanks 1, liquor flows from top to bottom or from bottom to top in the plurality of liquor storage tanks 1 and at least one liquor external circulation body 2 through a liquor outlet circulation pipeline 3.1, a liquor return circulation pipeline 3.2, a liquor outlet circulation pump 4.1, a liquor return circulation pump 4.2, a liquor outlet check valve 12 and a liquor return check valve 17, the gas flows from bottom to top in the wine storage tanks 1 and the at least one wine external circulation body 2 through the air pump 7, the air inlet pipe 6, the air pipe 19, the air collecting pipe 20, the air distribution branch pipe 21, the air distribution check valve 22 and the air outlet 8, the stirrer is arranged in the wine storage tanks, the stirrer comprises a stirring shaft arranged in the wine storage tanks, stirring blades are arranged on the stirring shaft, one end of the stirring shaft extends out of the wine storage tanks and is connected with a driving motor arranged outside the wine storage tanks, or a vibrating rod or an ultrasonic vibrator is arranged in the wine storage tanks, and the rest of the structure is the same as that in the embodiment 14 or 15.
Example 18
Further preferred embodiments of the present invention, in order to accelerate the progress of aging of the liquor and promote the oxidation-reduction reaction between the liquor and more beneficial metal elements, strictly limit the content of harmful metal elements in the clay for manufacturing the ceramic, further preferred embodiments of the present invention, the unglazed ceramic contains at least 1.1wt% of copper oxide, 1.8wt% of ferric oxide, 0.1wt% of magnesium oxide, 0.08wt% of zinc oxide, 0.01wt% of sodium oxide, 0.02wt% of potassium oxide, 0.005wt-% of aluminum trioxide, 0.002wt% of titanium, 0.003wt% of manganese, 0.001wt% of nickel, 0wt% of chromium, 0wt% of lead in the clay for manufacturing the ceramic, respectively, by adding copper powder and iron powder to the clay, the remaining structure is the same as the structure in example 16 or 17.
Example 19
Based on the embodiment 16 or 17, the unglazed ceramic body contains at least 1.2wt% of copper oxide, 1.55wt% of iron oxide, 0.15wt% of magnesium oxide, 0.065wt% of zinc oxide, 0.015wt% of sodium oxide, 0.015wt% of potassium oxide, 0.0065 wt% of aluminum oxide, 0.0015wt% of titanium, 0.004wt% of manganese, 0 to 0.0005wt% of nickel, 0 to 0.0005wt% of chromium, 0 to 0.0005wt% of lead in the pug for manufacturing the ceramic, respectively, wherein the contents of copper metal and iron metal are formulated by adding copper powder and iron powder to the pug, and the rest of the structure is the same as the structure in the embodiment 16 or 17.
Example 20
Based on example 16 or 17, the unglazed ceramic body contains at least 1.3wt% of copper, 1.8wt% of iron, 0.2wt% of magnesium, 0.05wt% of zinc, 0.02wt% of sodium, 0.01wt% of potassium, 0.008 wt% of aluminum, 0.001wt% of titanium, 0.005wt% of manganese, 0wt% of nickel, 0.001wt% of chromium, 0.001wt% of lead in the pug for manufacturing the ceramic, respectively, wherein the contents of copper metal and iron metal are formulated by adding copper powder and iron powder to the pug, and the rest of the structure is the same as the structure in example 16 or 17.
The invention also aims to overcome the defects existing in the prior art, and provides a method for accelerating the aging and storing of the wine by adopting an accelerating wine aging and storing device, which has the advantages of simple structure, high wine aging efficiency, short aging process period, high degree of automation, small occupied area and low manufacturing cost, can increase the comparison area of the wine contacted with the ceramic body by hundreds of times on the basis of keeping the existing stainless steel wine storing tank, and can simultaneously perform aging and catalysis on the wine in a plurality of wine storing tanks.
Example 21
The method for accelerating the aging storage of the wine by adopting the accelerating aging storage system of the wine comprises the following steps:
S1, at least one wine external circulation body 2 is arranged outside a plurality of wine storage tanks 1, a filling frame 2.1 is arranged in at least one wine external circulation body 2, and unglazed ceramic bodies 2.2 are filled in the filling frame 2.1;
s2, connecting a tower outlet wine circulation pipeline 3.1, a tower return wine circulation pipeline 3.2, a tower outlet wine circulation pump 4.1, a tower return wine circulation pump 4.2, a tower outlet check valve 12, a tower return check valve 17, a tower outlet control valve 13, a tower return control valve 18, an air pump 7, an air inlet pipe 6, an air transmission collecting pipe 20, an air transmission branch pipe 21 and an air transmission check valve 22 between the plurality of wine storage tanks 1 and at least one wine external circulation body 2;
s3, adding brewed wine into a plurality of wine storage tanks 1;
s4, starting a tower outlet wine circulating pump 4.1, a tower return wine circulating pump 4.2 and an air pump 7, so that wine starts to continuously circulate from top to bottom in a plurality of wine storage tanks 1 and at least one wine outer circulating body 2, and simultaneously, gas continuously flows from bottom to top or from top to bottom in a plurality of wine storage tanks 1 and at least one wine outer circulating body 2 along with the wine, and the gas flowing into the plurality of wine storage tanks 1 is discharged from an exhaust port 8 arranged at the top or upper part of the plurality of wine storage tanks 1;
S5, regularly detecting the aging state of each wine in each wine storage tank 1 in a plurality of wine storage tanks 1, closing a tower outlet control valve 13 and a tower return control valve 18 which are connected with the corresponding wine storage tank 1 after the wine in a certain wine storage tank 1 reaches a set aging index, and closing a tower outlet wine circulation pump 4.1, a tower return wine circulation pump 4.2 and an air pump 7 or respectively closing the tower outlet control valve 13 and the tower return control valve 18 which are connected on the tower outlet wine circulation pipeline 3.1 and the tower return wine circulation pipeline 3.2 after the wine in all the wine storage tanks 1 reaches the set aging index;
s6, taking out the unglazed ceramic body filled on the filling frame periodically, and repeatedly using the unglazed ceramic body after high-temperature treatment at 500 ℃ or 650 ℃.
Example 22
Based on the embodiment 21, in order to monitor and control the aging process of the liquor, the liquor which has been aged to a specific index is timely led out from the liquor storage tanks, then new liquor is added again to improve the production efficiency and economic benefit, and the preferred embodiment of the invention is that the liquor outlet circulating pump 4.1, the liquor return circulating pump 4.2, the air pump 7, the liquor outlet control valve 13 and the liquor return control valve 14 are respectively connected with a controller (not shown in the figure), the circulating flow rate of the liquor between each liquor storage tank 1 of a plurality of liquor storage tanks 1 and at least one liquor external circulating body 2 is controlled by the controller, and the flow rate of gas in each liquor storage tank 1 of the plurality of liquor storage tanks 1 and at least one liquor external circulating body 2 is controlled by the controller, and the non-ceramic body 2.2 filled in the packing frame 2.1 of the at least one liquor external circulating body 2 is replaced according to the detection result of the metal ion content of the liquor in the plurality of liquor storage tanks 1 at regular intervals, and the rest of the method is the same as that in the embodiment 21.
The wine circulating body device is arranged outside the wine storage tank to store wine, so that the wine storage tank is convenient to use, good in wine storage effect and capable of being used throughout the year. The longer the equipment is used for storing the wine, the better the taste of the wine. The comparison result of the wine stored by the device and the wine stored by other wine storage containers for a period of time with the wine with the same wine flavor type is as follows:
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the foregoing is merely a preferred embodiment of the present invention, and it should be noted that it will be apparent to those skilled in the art that several modifications and variations can be made without departing from the technical principle of the present invention, and these modifications and variations should also be regarded as the scope of the invention.
Claims (10)
1. The system is characterized by comprising a plurality of wine storage tanks, wherein at least one wine external circulation body is arranged outside the plurality of wine storage tanks, a wine circulation pipeline is connected between the plurality of wine storage tanks and the at least one wine external circulation body, a wine circulation pump and a valve are connected in series on the wine circulation pipeline, an air inlet pipe is further arranged on the at least one wine external circulation body, an air pump is connected on the air inlet pipe, and exhaust ports are respectively arranged on the plurality of wine storage tanks; at least one wine external circulation body is internally provided with a filling frame, and unglazed ceramic bodies are filled in the filling frame.
2. The accelerated wine aging storage system of claim 1, wherein the at least one wine external circulation body is arranged in an aging workshop or a control room, the wine external circulation body of the tower structure is of a tower structure, the wine external circulation body of the tower structure comprises a shell of an integral structure or a split structure, the packing frame is arranged in the shell, the packing frame comprises a frame of the integral structure or the split structure which is matched with the internal structure of the shell, a plurality of layers of trays or net drums are arranged on the frame, or the frame and the plurality of layers of trays or net drums form the integral structure, the trays are provided with meshes, and the unglazed ceramic body is arranged on the tray or in the net drum.
3. The accelerated liquor aging storage system of claim 2 wherein the frame and tray or mesh drum comprises a metal frame and metal tray or metal mesh drum or an unglazed ceramic frame and unglazed ceramic tray or unglazed mesh drum.
4. The accelerated liquor aging storage system of claim 3 wherein the unglazed ceramic body comprises any one of unglazed ceramic flakes, unglazed ceramic particles, unglazed ceramic balls, unglazed ceramic honeycomb blocks, or any combination thereof.
5. The accelerated wine aging storage system of claim 4, wherein a wine discharge pipe is arranged at the bottom or the lower part of the shell, a wine input pipe is arranged at the top or the upper part of the shell, the wine discharge pipe at the bottom or the lower part of the shell is connected with one end of a tower outlet collecting pipeline through a tower outlet wine circulating pump connected in series, the other end of the tower outlet collecting pipeline is respectively connected with one ends of a plurality of tower outlet wine circulating pipelines, a tower outlet check valve and a tower outlet control valve are respectively connected in series on the tower outlet wine circulating pipelines, and the other ends of the tower outlet wine circulating pipelines are respectively connected with wine return pipes at the top or the upper part of a plurality of wine storage tanks; the top or upper portion of the shell body is connected with one end of a tower return wine circulating pump in series, the other end of the tower return collecting pipeline is respectively connected with one ends of a plurality of tower return wine circulating pipelines, the other ends of the tower return wine circulating pipelines are respectively connected with a plurality of wine storage tank bottoms or lower wine discharge pipes, and a tower return check valve and a tower return control valve are respectively connected in series on the tower return wine circulating pipelines.
6. The accelerated wine aging storage system of claim 5, wherein an air inlet pipe communicated with the inside of the shell is arranged at the bottom or the lower part of the shell, an air pipe communicated with the inside of the shell is arranged at the top or the upper part of the shell, the air inlet pipe is connected with an air outlet of the air pump, the air pipe is respectively connected with one ends of a plurality of air branch pipes through an air delivery collecting pipe, an air delivery check valve and an air delivery control valve are respectively connected in series with the plurality of air branch pipes, the other ends of the plurality of air branch pipes are respectively connected with air inlets at the bottom or the lower part of a plurality of wine storage tanks, the air outlets on the plurality of wine storage tanks are respectively arranged at the top or the upper part of each wine storage tank, and a valve cap is respectively arranged on each air outlet.
7. The accelerated liquor aging storage system of claim 6, wherein a plurality of liquor discharge pipes are respectively and uniformly distributed at the bottom or the lower part of the plurality of liquor storage tanks, at least one liquor return pipe is respectively and uniformly distributed at the top or the upper part of the plurality of liquor storage tanks, a plurality of air inlets are respectively and uniformly distributed at the bottom or the lower part of the plurality of liquor storage tanks, at least one air outlet is respectively formed at the top or the upper part of the plurality of liquor storage tanks, liquor flows from top to bottom or from top to top in the plurality of liquor storage tanks and at least one liquor external circulation body through a liquor outlet circulation pipeline, a liquor return circulation pipeline, a liquor outlet circulation pump, a liquor return circulation pump, a liquor outlet check valve and a return check valve in the plurality of liquor storage tanks, and gas flows from bottom to top in the at least one liquor external circulation body through an air pump, an air inlet pipe, a gas delivery collection pipe, a gas delivery check valve and an air outlet; the stirrer is arranged in the wine storage tanks, the stirrer comprises a stirring shaft arranged in the wine storage tanks, stirring blades are arranged on the stirring shaft, one end of the stirring shaft extends out of the wine storage tanks and is connected with a driving motor arranged outside the wine storage tanks, or a vibrating rod or an ultrasonic vibrator is arranged in the wine storage tanks.
8. The accelerated liquor aging storage system of claim 4 wherein the unglazed ceramic body comprises at least 1.1 to 1.3wt% copper oxide, 1.3 to 1.8wt% ferric oxide, 0.1 to 0.2wt% magnesium oxide, 0.01 to 0.02wt% sodium oxide, 0.01 to 0.02wt% potassium oxide, 0.005 to 0.008 wt% aluminum oxide, 0.001 to 0.003wt% titanium, 0.003 to 0.005wt% manganese, 0.001 to 0.002wt% nickel, 0.001 to 0.002wt% chromium, 0.001 to 0.002wt% lead, respectively, in the pug of the manufacturing pottery, wherein the contents of copper metal and iron metal are formulated by adding copper powder and iron powder to the pug.
9. A method for accelerating the aging of wine using the system for accelerating the aging of wine according to any one of claims 1 to 8, comprising the steps of:
s1, at least one wine external circulation body is arranged outside a plurality of wine storage tanks, a filling frame is arranged in at least one wine external circulation body, and unglazed ceramic bodies are filled on the filling frame;
s2, connecting a tower outlet wine circulation pipeline, a tower return wine circulation pipeline, a tower outlet wine circulation pump, a tower return wine circulation pump and a tower outlet one-way valve between a plurality of wine storage tanks and at least one wine external circulation body, wherein the tower return one-way valve, the tower outlet control valve, the tower return control valve, the air pump, the air inlet pipe, the air transmission collecting pipe, the air transmission branch pipe and the air transmission one-way valve;
S3, respectively adding brewed wine into a plurality of wine storage tanks;
s4, starting a tower outlet wine circulating pump, a tower return wine circulating pump and an air pump, so that wine starts to continuously circulate from top to bottom or from bottom to top in a plurality of wine storage tanks and at least one wine external circulating body, and simultaneously, accompanying with the continuous flow of gas from bottom to top in a plurality of wine storage tanks and at least one wine external circulating body, the gas flowing into a plurality of wine storage tanks is discharged from an exhaust port arranged at the top or upper part of the plurality of wine storage tanks;
s5, regularly detecting the aging state of the liquor in each of a plurality of liquor storage tanks, closing a tower outlet control valve and a tower return control valve which are connected with the corresponding liquor storage tank after the liquor in a certain liquor storage tank reaches a set aging index, and closing a tower outlet liquor circulating pump, a tower return liquor circulating pump and an air pump or respectively closing a tower outlet control valve and a tower return control valve which are connected in series on a tower outlet liquor circulating pipeline and a tower return liquor circulating pipeline after the liquor in all the liquor storage tanks reaches the set aging index;
s6, taking out the unglazed ceramic body filled on the filling frame periodically, and repeatedly using the unglazed ceramic body after high-temperature treatment at 500-650 ℃.
10. The accelerated aging storage method of wine according to claim 9, wherein the tower outlet wine circulation pump, the tower return wine circulation pump, the air pump, the tower outlet control valve and the tower return control valve are respectively connected with a controller, circulation flow rates of wine between a plurality of wine storage tanks and at least one wine external circulation body and flow rates of gas in a plurality of wine storage tanks and at least one wine external circulation body are controlled by the controller, and unglazed ceramic bodies filled on a filling frame in the at least one wine external circulation body are replaced according to detection results of the content of metal ions of the wine in the plurality of wine storage tanks.
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| CN114940936A (en) * | 2022-05-17 | 2022-08-26 | 胥伟 | Wine jar capable of accelerating aging of wine and manufacturing method thereof |
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