CN116355591B - Human body static electricity eliminating spray and preparation method and application thereof - Google Patents
Human body static electricity eliminating spray and preparation method and application thereof Download PDFInfo
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- CN116355591B CN116355591B CN202310370395.3A CN202310370395A CN116355591B CN 116355591 B CN116355591 B CN 116355591B CN 202310370395 A CN202310370395 A CN 202310370395A CN 116355591 B CN116355591 B CN 116355591B
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- DVEKCXOJTLDBFE-UHFFFAOYSA-N n-dodecyl-n,n-dimethylglycinate Chemical compound CCCCCCCCCCCC[N+](C)(C)CC([O-])=O DVEKCXOJTLDBFE-UHFFFAOYSA-N 0.000 claims abstract description 26
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- 125000003277 amino group Chemical group 0.000 claims abstract 4
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- RTIXKCRFFJGDFG-UHFFFAOYSA-N Chrysin Natural products C=1C(O)=CC(O)=C(C(C=2)=O)C=1OC=2C1=CC=CC=C1 RTIXKCRFFJGDFG-UHFFFAOYSA-N 0.000 claims description 4
- FGUBFGWYEYFGRK-HNNXBMFYSA-N Pinocembrin Natural products Cc1cc(C)c2C(=O)C[C@H](Oc2c1)c3ccccc3 FGUBFGWYEYFGRK-HNNXBMFYSA-N 0.000 claims description 4
- KCFYHBSOLOXZIF-UHFFFAOYSA-N dihydrochrysin Natural products COC1=C(O)C(OC)=CC(C2OC3=CC(O)=CC(O)=C3C(=O)C2)=C1 KCFYHBSOLOXZIF-UHFFFAOYSA-N 0.000 claims description 4
- 238000000034 method Methods 0.000 claims description 4
- URFCJEUYXNAHFI-ZDUSSCGKSA-N pinocembrin Chemical compound C1([C@@H]2CC(=O)C3=C(O)C=C(C=C3O2)O)=CC=CC=C1 URFCJEUYXNAHFI-ZDUSSCGKSA-N 0.000 claims description 4
- 238000005507 spraying Methods 0.000 abstract description 36
- LZZYPRNAOMGNLH-UHFFFAOYSA-M Cetrimonium bromide Chemical compound [Br-].CCCCCCCCCCCCCCCC[N+](C)(C)C LZZYPRNAOMGNLH-UHFFFAOYSA-M 0.000 abstract description 20
- 230000000694 effects Effects 0.000 abstract description 14
- IGFHQQFPSIBGKE-UHFFFAOYSA-N Nonylphenol Natural products CCCCCCCCCC1=CC=C(O)C=C1 IGFHQQFPSIBGKE-UHFFFAOYSA-N 0.000 abstract description 11
- SNQQPOLDUKLAAF-UHFFFAOYSA-N nonylphenol Chemical compound CCCCCCCCCC1=CC=CC=C1O SNQQPOLDUKLAAF-UHFFFAOYSA-N 0.000 abstract description 11
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- 150000001412 amines Chemical group 0.000 description 15
- 238000012360 testing method Methods 0.000 description 9
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- RNMDNPCBIKJCQP-UHFFFAOYSA-N 5-nonyl-7-oxabicyclo[4.1.0]hepta-1,3,5-trien-2-ol Chemical compound C(CCCCCCCC)C1=C2C(=C(C=C1)O)O2 RNMDNPCBIKJCQP-UHFFFAOYSA-N 0.000 description 4
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- 229910001220 stainless steel Inorganic materials 0.000 description 2
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- 241000894006 Bacteria Species 0.000 description 1
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- 241000196324 Embryophyta Species 0.000 description 1
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- 235000011615 Pinus koraiensis Nutrition 0.000 description 1
- 229920002125 Sokalan® Polymers 0.000 description 1
- WGLPBDUCMAPZCE-UHFFFAOYSA-N Trioxochromium Chemical compound O=[Cr](=O)=O WGLPBDUCMAPZCE-UHFFFAOYSA-N 0.000 description 1
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- 150000008043 acidic salts Chemical class 0.000 description 1
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- 239000003242 anti bacterial agent Substances 0.000 description 1
- 239000010951 brass Substances 0.000 description 1
- 125000002091 cationic group Chemical group 0.000 description 1
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K3/00—Materials not provided for elsewhere
- C09K3/16—Anti-static materials
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
The invention provides a human body static eliminating spray and a preparation method and application thereof, and belongs to the technical field of static eliminating. The invention provides a human body static electricity eliminating spray which comprises the following components in percentage by mass: 46-56% of distilled water, 39-40% of propylene glycol, 2-12% of antistatic agent, 1-1.5% of kathon and 1-1.5% of phenytoin, wherein the antistatic agent comprises one or more of cetyltrimethylammonium bromide, cocoquaternary amine ethoxylate, nonylphenol polyoxyethylene ether and dodecyl dimethyl betaine. The static electricity eliminating spraying for human bodies can be realized in ammunition service places, and personnel can meet the standard requirement of static dangerous place operation by adopting simple measures of spraying static electricity eliminating spraying on the basis of the existing military wear, so that the static electricity eliminating spraying for human bodies has the advantages of low cost, good effect and small consumption, is convenient to carry, and is particularly suitable for preventing static electricity damage for human bodies under the condition of incomplete anti-static facilities.
Description
Technical Field
The invention relates to the technical field of static elimination, in particular to static elimination human body spray and a preparation method and application thereof.
Background
People are the subject of activities in ammunition business venues. The human body can carry static electricity of several kilovolts or even tens of thousands of volts due to the self-action and the factors of contact-separation, friction or induction with other objects. For ammunition service places, the possibility that human static electricity accidentally causes the explosive, the initiating explosive and the electrically-ignited ammunition to be ignited is one of non-negligible dangerous sources. At present, the II-type electrostatic hazard places mainly adopt the measures of making clothing, touching electrostatic balls, paving antistatic ground and the like to reduce the electrostatic hazard risk. However, when the operations such as loading, unloading, carrying, unsealing and wiping are carried out in the field, severe actions are inevitably generated, static electricity is accumulated, potential static electricity safety hazards exist, and effective and simple measures for preventing human static electricity hazard are not available at present. Therefore, research on more effective measures for preventing static electricity of human bodies and reduction of safety risks are urgently needed.
Because the existing antistatic spray on the market is mainly used for solving the problem of electrostatic shock beater when people touch metal armrests and metal door handles in winter, the surface phenomena of the electrostatic beater and the like can only be weakened in a short period, and the requirements of ammunition business places are far from being met in the aspects of reducing the surface resistivity of clothing, the effect retention time and the like. Therefore, research on static electricity eliminating spraying of human bodies suitable for ammunition service places is urgently needed, and when personnel work in the ammunition service places, standard requirements can be met by adopting simple measures of spraying the static electricity eliminating spraying on the basis of existing dressing, so that the risk of static electricity hazard is reduced.
Disclosure of Invention
Therefore, the invention aims to provide a human body static eliminating spray and a preparation method and application thereof. The static electricity eliminating spraying for human body can meet the standard requirement of static electricity dangerous place operation and reduce the static electricity hazard risk only by adopting simple measures of spraying static electricity eliminating spraying on the basis of the existing military wear.
In order to achieve the above object, the present invention provides the following technical solutions:
the invention provides a human body static electricity eliminating spray which comprises the following components in percentage by mass: 46-56% of distilled water, 39-40% of propylene glycol, 2-12% of antistatic agent, 1-1.5% of kathon and 1-1.5% of phenytoin, wherein the antistatic agent comprises one or more of cetyltrimethylammonium bromide, cocoquaternary amine ethoxylate, nonylphenol polyoxyethylene ether and dodecyl dimethyl betaine.
Preferably, the static electricity eliminating spray for eliminating human body comprises the following components in percentage by mass: 48% of distilled water, 40% of propylene glycol, 10% of antistatic agent, 1% of kathon and 1% of phenytoin.
Preferably, the antistatic agent comprises coconut alkyl quaternary amine ethoxylate and dodecyl dimethyl betaine, the mass percentage of the coconut alkyl quaternary amine ethoxylate in the static electricity eliminating spray is 1-6%, and the mass percentage of the dodecyl dimethyl betaine is 1-6%.
Preferably, the mass percentage of the coconut alkyl quaternary amine ethoxylate and the dodecyl dimethyl betaine in the static electricity eliminating spray is 5 percent.
Preferably, the antistatic agent comprises cetyl trimethyl ammonium bromide and dodecyl dimethyl betaine, and the mass percentage of the cetyl trimethyl ammonium bromide and the dodecyl dimethyl betaine in the static electricity eliminating spray is 5%.
Preferably, the antistatic agent comprises coconut alkyl quaternary amine ethoxylate and nonylphenol polyoxyethylene ether, and the mass percentage of the coconut alkyl quaternary amine ethoxylate and the nonylphenol polyoxyethylene ether in the static electricity eliminating spray is 5%.
Preferably, the antistatic agent comprises cetyl trimethyl ammonium bromide and polyoxyethylene nonylphenol ether, and the mass percentage of the cetyl trimethyl ammonium bromide and the polyoxyethylene nonylphenol ether in the static electricity eliminating spray is 5%.
The invention also provides a preparation method of the human body static eliminating spray, which comprises the following steps:
and mixing distilled water, propylene glycol, an antistatic agent, pinocembrin and phenytoin to obtain the antistatic spray for eliminating human body, wherein the antistatic agent comprises one or more of cetyl trimethyl ammonium bromide, coconut alkyl quaternary amine ethoxylate, nonylphenol polyoxyethylene ether and dodecyl dimethyl betaine.
The invention also provides application of the human body static eliminating spray in ammunition service places.
Preferably, the application is spraying on the surface of the desert camouflage fabric or jungle camouflage fabric.
The invention provides a human body static electricity eliminating spray which comprises the following components in percentage by mass: 46-56% of distilled water, 39-40% of propylene glycol, 2-12% of antistatic agent, 1-1.5% of kathon and 1-1.5% of phenytoin, wherein the antistatic agent comprises one or more of cetyltrimethylammonium bromide, cocoquaternary amine ethoxylate, nonylphenol polyoxyethylene ether and dodecyl dimethyl betaine. The static electricity eliminating spraying for human bodies can be realized in ammunition service places, and personnel can meet the standard requirement of static dangerous place operation by adopting simple measures of spraying static electricity eliminating spraying on the basis of the existing military wear, so that the static electricity eliminating spraying for human bodies has the advantages of low cost, good effect and small consumption, is convenient to carry, and is particularly suitable for preventing static electricity damage for human bodies under the condition of incomplete anti-static facilities. The data of the embodiment show that the static electricity eliminating spray for eliminating human body can reach the standard requirements of the second class of static electricity dangerous places, the effect duration is longer than 2 hours, and the static electricity eliminating spray for eliminating human body has good safety and applicability to ammunition business places and human bodies.
The antistatic agent is a main component for eliminating static electricity by spraying, belongs to a surfactant, and consists of a hydrophobic group which is uniformly and symmetrically distributed and is nonpolar and a hydrophilic group which is polar. When the antistatic agent is added into water, hydrophilic groups in antistatic agent molecules are inserted into the water, hydrophobic groups extend to the air, and after the antistatic agent is sprayed on clothes, the hydrophobic groups in the antistatic agent molecules are adsorbed on the surface of the material, a molecular layer of the antistatic agent can be formed on the surface of the antistatic agent, when the molecular layer is destroyed, the internal antistatic agent can permeate into the surface of the molecular layer, so that the surface of the clothes has a smooth antistatic molecular layer, friction can be reduced, hydrophilic groups in the antistatic agent molecules of human body static generated by friction are all arranged towards one side of the air, environmental moisture is easily absorbed, or the hydrophilic groups are combined with the moisture in the air through hydrogen bonds to form a single-molecule conducting layer, and the generated static charge is quickly leaked to achieve the antistatic purpose; the antistatic agent used by the invention has low toxicity, can not react with the fabric of military clothing, and can meet the safety requirement of antistatic spraying on the clothing; meanwhile, the antistatic agent is suitable for ammunition and packaging boxes thereof, the ammunition is basically made of metal (including iron, stainless steel and brass), a small amount of PP plastic is also made of wood (namely plant fiber) or plastic, and glass fiber reinforced plastic is also packaged, green paint is usually coated on the wooden packaging boxes, the main components of the paint are polyurethane and polyacrylic acid, the main color-developing substances of green pigment are chromium oxide, the iron and acidic salts generate mild corrosion, but the degree is not severe, the ammonium salt in the cationic antistatic agent is more acidic than the quaternary ammonium salt, and the stainless steel can generate mild corrosion, so the ammonium salt antistatic agent is not used in the antistatic agent. The antistatic agent can accelerate the leakage speed of charges and inhibit the generation of static charges by leaking static charges or reducing friction coefficient.
The propylene glycol plays a role of a softener, friction can be reduced, the friction coefficient among fibers is reduced, static electricity is not easy to generate, static electricity accumulation is not easy to form, meanwhile, the propylene glycol plays a role of a humectant, a layer of film is formed on the surface of skin, and moisture is sealed to prevent moisture evaporation.
In the invention, the pinus koraiensis plays a role of an antibacterial agent, can be compatible with cations and non-ions, and can effectively inhibit and kill bacteria and various microorganisms.
In the invention, the phenytoin plays a role of a freshener, has fresh taste, can purify air, reduce pollution and enable breath to be smooth.
The invention also provides a preparation method of the human body static eliminating spray, which is simple and easy for industrial production.
The invention also provides application of the static electricity eliminating spray for human bodies, and standard requirements of static electricity dangerous place operation can be met and static electricity hazard risks are reduced only by adopting simple measures of spraying static electricity eliminating spray on the basis of the existing military wear.
Drawings
FIG. 1 shows the variation of the surface resistivity of the jungle camouflage after spraying different human static elimination bodies in example 1;
FIG. 2 shows the variation of the surface resistivity of the desert camouflage after spraying different static electricity eliminating bodies in example 1;
FIG. 3 shows the variation of the surface resistivity of the jungle camouflage after spraying different human static elimination sprays in example 2;
FIG. 4 shows the variation of the surface resistivity of the desert camouflage after spraying different static electricity eliminating bodies in the embodiment 2;
FIG. 5 is a diagram of a verification scenario of a human body static elimination spray test;
FIG. 6 shows the variation of jungle camouflage surface resistivity in the verification of the human body static elimination spray test;
FIG. 7 shows the variation of the surface resistivity of desert camouflage in the verification of the static spray test of the human body.
Detailed Description
The invention provides a human body static electricity eliminating spray which comprises the following components in percentage by mass: 46-56% of distilled water, 39-40% of propylene glycol, 2-12% of antistatic agent, 1-1.5% of kathon and 1-1.5% of phenytoin, wherein the antistatic agent comprises one or more of Cetyl Trimethyl Ammonium Bromide (CTAB), coco alkyl quaternary amine ethoxylate (berol-561), nonylphenol polyoxyethylene ether (TX-10) and dodecyl dimethyl betaine (BS-12).
In the present invention, all materials used are commercial products in the art unless otherwise specified.
In the invention, the static electricity eliminating spray for human bodies preferably comprises the following components in percentage by mass: 48% of distilled water, 40% of propylene glycol, 10% of antistatic agent, 1% of kathon and 1% of phenytoin.
In the invention, the antistatic agent preferably comprises 1-6% of cocoalkyl quaternary amine ethoxylate by mass percent and 1-6% of dodecyl dimethyl betaine by mass percent in the antistatic agent in the human body static eliminating spray.
In the invention, the mass percentage of the coconut alkyl quaternary amine ethoxylate and the dodecyl dimethyl betaine in the static electricity eliminating spray is preferably 5 percent.
In the invention, the antistatic agent preferably comprises the hexadecyl trimethyl ammonium bromide and the dodecyl dimethyl betaine in the static electricity eliminating spray for human body, and the mass percentage of the hexadecyl trimethyl ammonium bromide and the dodecyl dimethyl betaine is preferably 5 percent.
In the invention, the antistatic agent preferably comprises coconut alkyl quaternary amine ethoxylate and nonylphenol polyoxyethylene ether, and the mass percentage of the coconut alkyl quaternary amine ethoxylate and nonylphenol polyoxyethylene ether in the static electricity eliminating spray is preferably 5%.
In the invention, the antistatic agent preferably comprises cetyl trimethyl ammonium bromide and polyoxyethylene nonylphenol ether, and the mass percentage of the cetyl trimethyl ammonium bromide and the polyoxyethylene nonylphenol ether in the static electricity eliminating spray is preferably 5%.
In the present invention, the water is preferably distilled water.
The invention also provides a preparation method of the human body static eliminating spray, which comprises the following steps:
and mixing distilled water, propylene glycol, an antistatic agent, pinocembrin and phenytoin to obtain the antistatic spray for eliminating human body, wherein the antistatic agent comprises one or more of cetyl trimethyl ammonium bromide, coconut alkyl quaternary amine ethoxylate, nonylphenol polyoxyethylene ether and dodecyl dimethyl betaine.
The specific mode of the mixing is not particularly limited, and modes known to those skilled in the art may be adopted.
The invention also provides application of the human body static eliminating spray in ammunition service places.
In the invention, the application is spraying on the surface of the desert camouflage fabric or the jungle camouflage fabric.
In the present invention, the amount of the spray coating is preferably adjusted according to the temperature and humidity, preferably 0.001mL/cm 2 。
In order to further illustrate the present invention, the following examples are provided to describe the static eliminating spray for human body and its preparation method and application in detail, but they should not be construed as limiting the scope of the invention.
Example 1
Static electricity eliminating spray shaping research
Four antistatic agents, CTAB (cetyltrimethylammonium bromide), berol-561 (cocoalkyl quaternary amine ethoxylate), TX-10 (nonylphenol polyoxyethylene ether) and BS-12 (dodecyl dimethyl betaine), were studied for their effect, and different antistatic agents having the same concentration (10 wt%) were prepared as the antistatic sprays for human body, the compositions are shown in Table 1.
TABLE 1 composition of static spray for eliminating human body (wt%)
The spray coatings were each tested by ACL800 measuring instrument (the amount of spray coating was 0.001mL/cm 2 ) After that, the change of the surface resistivity of the desert camouflage and the jungle camouflage within two hours is shown in fig. 1-2, wherein fig. 1 is the change of the surface resistivity of the jungle camouflage, fig. 2 is the change of the surface resistivity of the desert camouflage, and the experimental temperature is as follows: the relative humidity is between 19.4 and 20.3 ℃ and is as follows: 29.3% -30.4%, as can be seen from FIGS. 1-2, the effects are better for jungle camouflage, berol-561, BS-12, and for desert camouflage, CTAB, TX-10, but none of the four single components has better effect on both camouflage.
Example 2
And adopting a pairwise mixing mode to carry out experiments, namely: the four sprays were compared with each other with 5wt% CTAB+5wt% BS-12, 5wt% berol561+5wt% TX-10, 5wt% CTAB+5wt% TX-10, 5wt%berol561+5wt%BS-12, and the rest of the compositions were the same as in Table 1, as shown in FIGS. 3-4, wherein FIG. 3 is the change in the surface resistivity of the jungle camouflage, and FIG. 4 is the change in the surface resistivity of the jungle camouflage, and the experimental temperature is: the temperature is 18.1-19.6 ℃ and the relative humidity is 28.6-30.8%. By comparison, the static electricity eliminating spray of the human body with the proportion of 5 weight percent beroles 561 and 5 weight percent BS-12 has good static electricity eliminating effect on desert camouflage and jungle camouflage.
The static electricity eliminating spray test of the human body verifies that:
the composition of the static spray for eliminating human body used in the verification process of the static spray for eliminating human body is shown in table 2.
TABLE 2 composition of human body static elimination spray used in verification procedure (wt.%)
| Composition of the components | Distilled water | Propylene glycol | berol561 | BS-12 | Kathon | Fendolin |
| Content of | 48％ | 40％ | 5％ | 5％ | 1％ | 1％ |
(1) Human body electrostatic potential test verification
The previous experiments are all established on the independent spraying of the training clothes, and the actual situation is measured by the dynamic electrostatic potential tester without considering the situation of wearing activities of a human body.
The specific experimental process is as follows: personnel are in the jungle camouflage, do not spray and move on the ordinary ground mat and antistatic ground mat vigorously respectively, utilize the dynamic electrostatic potential tester to test the electrostatic potential peak value of human body and fill in the table, after spraying and spraying, move on the ordinary ground mat and antistatic ground mat vigorously respectively, record the electrostatic potential peak value of human body, the test scene is shown in figure 5, the test result is shown in table 3. As apparent from table 3, the peak value of the intense action potential of the human body on the common floor mat is very high under the condition of spraying without spraying, and the peak value of the electrostatic potential of the human body after spraying is obviously reduced, and the peak value is not much different from that on the antistatic floor mat, so that the developed effect of eliminating the electrostatic potential of the human body is verified.
TABLE 3 verification of the results of static spray test on human body elimination (temperature 23.7 ℃ C., relative humidity 32.3%)
| Peak value of human body potential | Common ground mat | Antistatic floor mat |
| Not sprayed with | 1927V | 83V |
| Spraying | 26V | 5V |
(2) Contrast verification
The effect of the product is compared with the effect of water and commercial spraying, as shown in fig. 6-7, wherein fig. 6 shows the change of the surface resistivity of jungle camouflage, and fig. 7 shows the change of the surface resistivity of desert camouflage, and as can be seen from fig. 6-7, the effect of eliminating human static electricity spraying is far better than that of water and commercial spraying.
The foregoing is merely a preferred embodiment of the present invention and is not intended to limit the present invention in any way. It should be noted that modifications and adaptations to the present invention may occur to one skilled in the art without departing from the principles of the present invention and are intended to be comprehended within the scope of the present invention.
Claims (4)
1. The human body static electricity eliminating spray is characterized by comprising the following components in percentage by mass: 48% of distilled water, 40% of propylene glycol, 10% of antistatic agent, 1% of pinocembrin and 1% of phenytoin, wherein the antistatic agent is coconut alkyl quaternary amine ethoxylate and dodecyl dimethyl betaine, and the mass percentage of the coconut alkyl quaternary amine ethoxylate and the dodecyl dimethyl betaine in the static electricity eliminating spray is 5%.
2. The method for preparing the static electricity eliminating spray for human body according to claim 1, which is characterized by comprising the following steps:
distilled water, propylene glycol, an antistatic agent, pinocembrin and phenytoin are mixed to obtain the antistatic spray for eliminating human body, wherein the antistatic agent is cocoalkyl quaternary amine ethoxylate and dodecyl dimethyl betaine.
3. Use of the static electricity eliminating spray for eliminating static electricity of human body in ammunition service place according to claim 1.
4. The use according to claim 3, characterized in that it is sprayed on the surface of a desert or jungle camouflage.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202310370395.3A CN116355591B (en) | 2023-04-10 | 2023-04-10 | Human body static electricity eliminating spray and preparation method and application thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202310370395.3A CN116355591B (en) | 2023-04-10 | 2023-04-10 | Human body static electricity eliminating spray and preparation method and application thereof |
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| CN116355591A (en) | 2023-06-30 |
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