CN116236401A - Nanofiber mask with anti-acne effect and preparation method thereof - Google Patents

Nanofiber mask with anti-acne effect and preparation method thereof Download PDF

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Publication number
CN116236401A
CN116236401A CN202310074487.7A CN202310074487A CN116236401A CN 116236401 A CN116236401 A CN 116236401A CN 202310074487 A CN202310074487 A CN 202310074487A CN 116236401 A CN116236401 A CN 116236401A
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CN
China
Prior art keywords
nanofiber
mask
component
essential oil
acne
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN202310074487.7A
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Chinese (zh)
Inventor
刘媛媛
刘华振
张毅
崔建祥
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Wuxi Micro Control Medical Technology Co ltd
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Wuxi Micro Control Medical Technology Co ltd
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Publication date
Application filed by Wuxi Micro Control Medical Technology Co ltd filed Critical Wuxi Micro Control Medical Technology Co ltd
Priority to CN202310074487.7A priority Critical patent/CN116236401A/en
Publication of CN116236401A publication Critical patent/CN116236401A/en
Pending legal-status Critical Current

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Classifications

    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
    • A61K8/0212—Face masks
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/67—Vitamins
    • A61K8/673—Vitamin B group
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A61K8/86—Polyethers
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P17/00—Drugs for dermatological disorders
    • A61P17/10—Anti-acne agents
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • D—TEXTILES; PAPER
    • D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01D—MECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
    • D01D5/00—Formation of filaments, threads, or the like
    • D01D5/0007—Electro-spinning
    • D01D5/0015—Electro-spinning characterised by the initial state of the material
    • D01D5/003—Electro-spinning characterised by the initial state of the material the material being a polymer solution or dispersion
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
    • Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change

Abstract

The invention belongs to the field of cosmetics, and discloses a nanofiber facial mask with an anti-acne effect and a preparation method thereof. The invention is prepared from the following raw materials in percentage by mass: and (3) a component A: 5-15% of polyethylene glycol and 59-91.4% of water; and B1: 1-10% of tea tree essential oil; and a component B2: jojoba oil 0.1-1%; and B3, a component: 1% -5% of juniper essential oil, and component C: 50.5-5% of provitamin B; and D, a component: 1-5% of natural essential oil emulsifier. In addition, the tea tree essential oil, the jojoba oil and the juniper essential oil are combined to be used, and the anti-acne effect of the obtained facial mask is better than that of a single essential oil through the synergistic effect of the tea tree essential oil, the jojoba oil and the juniper essential oil. The nanofiber facial mask obtained by the invention has excellent anti-acne effect, whitening and moisturizing functions, and meanwhile, the product does not need to be matched with essence, so that the nanofiber facial mask is easier to package and store. The whole preparation process flow is short, the operation is simple, and the prepared nanofiber mask has high acne-inhibiting effect and high production value.

Description

Nanofiber mask with anti-acne effect and preparation method thereof
Technical Field
The invention belongs to the technical field of masks, and particularly relates to a nanofiber mask with an anti-acne effect and a preparation method thereof.
Background
With the improvement of the living standard of modern people, people pay attention to the health and beauty of the face increasingly. Acne is a chronic inflammatory skin disease of the pilosebaceous glands, which is well developed on the face and commonly known as acne. 80-90% of people have the disease, and most patients do not adopt proper medicines and skin care products for nursing when growing acne, but squeeze by hands to discharge pus blood, but the method can leave scars and affect the appearance.
The nanofiber mask is a nano composite fiber which is prepared by mixing a high polymer solution and an active ingredient and directly spinning, does not need mask cloth, can be directly dissolved and attached to skin after being applied to the face, can be better absorbed by the skin, reduces the adsorption force of the mask cloth, does not have the phenomenon of reverse water absorption by the mask cloth, can effectively reduce the use amount of the active ingredient, and improves the bioavailability of the active ingredient, and is a novel mask. In the cosmetic field, cosmetic masks based on nanofibers make percutaneous absorption of the pharmaceutical and cosmetic active ingredients superior to other mask carriers. The medicine and the cosmetic active ingredients exist in the polymer nano fiber in the form of tiny particles, and the dissolution or release efficiency is higher. The nanofiber is used as a carrier for drug delivery, has extremely large specific surface area and porous structure, extremely strong interpenetration with other substances, extremely facilitates the diffusion and dissolution of the drug, improves the percutaneous penetration quantity of the drug and improves the percutaneous absorption of the drug.
Disclosure of Invention
The invention aims to: the nanofiber mask with the anti-acne effect and the preparation method thereof are provided, and the problems in the prior art are solved.
The technical scheme is as follows: the nanofiber mask with the anti-acne effect is prepared from the following raw materials in percentage by mass:
and (3) a component A: 5-15% of polyethylene glycol and 59-91.4% of water;
and B1: 1-10% of tea tree essential oil;
and a component B2: jojoba oil 0.1-1%;
and B3, a component: 1-5% of juniper essential oil.
And C, component: 50.5-5% of provitamin B;
and D, a component: 1-5% of natural essential oil emulsifier.
In a further embodiment, the material is prepared from the following raw materials in percentage by mass:
and (3) a component A: polyethylene glycol 10%, water 77.5%;
and B1: tea tree essential oil 5%;
and a component B2: jojoba oil 0.5%;
and B3, a component: juniper essential oil 2%.
And C, component: vitamin B53%;
and D, a component: 2% of natural essential oil emulsifier.
In a further embodiment, the active component with anti-acne effect is at least one of tea tree essential oil, jojoba oil and juniper essential oil.
In a further embodiment, the natural essential oil emulsifier is composed of one or more of lecithin, lanolin alcohol, lanolin acid, and beeswax.
In a further embodiment, the polyethylene glycol has a molecular weight average molecular weight of 30000 to 40000.
In a further embodiment, a method for preparing a nanofiber facial mask with anti-acne efficacy comprises the following steps:
(1) Mixing polyethylene glycol powder in the component A with water at room temperature, and stirring uniformly to obtain polyethylene glycol aqueous solution at room temperature for later use;
(2) Uniformly mixing the component B and the component D, and then adding the mixed solution into the polyethylene glycol aqueous solution obtained in the step (1), uniformly stirring, and standing at normal temperature for later use;
(3) Adding the component C into the mixed solution obtained in the step (2), and uniformly stirring to obtain an electrostatic spinning solution;
(4) Adding the mixed solution obtained in the step (3) into an electrostatic spinning machine for electrostatic spinning, and preparing the nanofiber mask with the anti-acne effect;
(5) Or the spinning solution obtained in the step (3) is referred to in situ on the face to prepare a nanofiber mask through portable electrostatic spinning equipment;
(6) Cutting the nanofiber obtained in the step (4) and the non-woven base cloth together by using a die, and processing to obtain the nanofiber facial mask conforming to the facial shape.
In a further embodiment, a method of preparing a nanofiber facial mask having anti-acne efficacy,
the electrostatic spinning parameters in the step (4) (5): the electrostatic spinning has the applied voltage of 8-15KV, the receiving distance of 10-25cm and the injection speed of 0.5-2mL/h; preferably, it is: the injection speed is 0.8-1.2mL/h, the receiving distance is 15-20cm, and the spinning voltage is 9-11kV.
In a further embodiment, a method for preparing a nanofiber facial mask with anti-acne efficacy, the operating conditions in steps (1) - (5) are: the ambient temperature is 20-30 ℃ and the humidity is 30-50% RH; preferably, it is: : the ambient temperature was 28℃and humidity 40% RH.
In a further embodiment, a method of using a nanofiber facial mask with anti-acne efficacy comprises the steps of: after washing the face, wetting the facial skin with purified water or spray, then applying the cut nanofiber mask with anti-acne efficacy, supplementing water to wet the face, completely dissolving the mask after a few seconds, applying the mask on the skin, and massaging and absorbing.
In a further embodiment, a method of using a nanofiber facial mask with anti-acne efficacy comprises the steps of: after washing the face, wetting the facial skin with purified water or spray, then preparing a nanofiber mask on the face in situ by using a portable electrostatic spinning device, after the mask is prepared, completely dissolving and applying the mask on the skin after a few seconds, and massaging and absorbing the mask
Compared with the prior art, the invention has the following advantages:
(1) The nanofiber preparation process is simple to operate and has no harsh requirements on equipment and treatment environment;
(2) The nanofiber facial mask provided by the invention has excellent anti-acne curative effect through loading bioactive substances on nanofibers, has whitening, moisturizing and repairing functions, and is beneficial to skin;
(3) According to the invention, tea tree essential oil, jojoba oil and juniper berry essential oil are combined, and the anti-wrinkle effect of the obtained facial mask is better than that of a single essential oil through the synergistic effect of the tea tree essential oil, jojoba oil and juniper berry essential oil.
(4) The nanofiber facial mask obtained by the invention has excellent anti-acne effect, simultaneously has whitening and moisturizing functions by adding vitamin B5, and simultaneously does not need to be matched with essence, so that the nanofiber facial mask is easier to package and store.
(5) The nanofiber mask prepared in situ by using the portable electrostatic spinning device can be more adhered to human skin, is easy to penetrate through the stratum corneum of the skin to reach the deep layer of the skin, enhances the anti-acne effect, and is safe and free of stimulation. According to different parts, zonal or local nursing can be realized, and accurate anti-acne skin care can be realized.
Detailed Description
In the following description, numerous specific details are set forth in order to provide a more thorough understanding of the present invention. It will be apparent, however, to one skilled in the art that embodiments of the invention may be practiced without one or more of these details. . In other instances, well-known features have not been described in detail in order to avoid obscuring the embodiments of the invention.
In the description of the present invention, it should be understood that the terms "upper," "lower," "front," "rear," "left," "right," "top," "bottom," "inner," "outer," and the like indicate orientations or positional relationships based on the orientations or positional relationships, merely to facilitate description of the present invention and to simplify the description, and do not indicate or imply that the devices or elements being referred to must have a particular orientation, be configured and operated in a particular orientation, and thus should not be construed as limiting the present invention.
The following description of the embodiments of the present invention will be made clearly and completely, and it is apparent that the described embodiments are only some embodiments of the present invention, but not all embodiments. All other embodiments, which can be made by those skilled in the art based on the embodiments of the invention without making any inventive effort, are intended to be within the scope of the invention.
Example 1
(1) Adding 10g of polyethylene glycol into 77.5g of water, stirring and dissolving at room temperature to obtain a polyethylene glycol solution;
(2) Uniformly mixing 5g of tea tree essential oil, 0.5g of jojoba oil, 2g of juniper essential oil and 2g of lecithin, and then adding the mixed solution into the polyethylene glycol aqueous solution in the step (1), uniformly stirring, and standing at normal temperature for later use;
(3) Adding 3g of vitamin B5 component into the mixed solution in the step (2), and uniformly stirring to obtain an electrostatic spinning solution;
(4) Adding the mixed solution obtained in the step (3) into an electrostatic spinning machine for electrostatic spinning, wherein the spinning conditions are as follows: the spinning voltage was 15KV, the receiving distance was 15cm, the solution flow rate was 1ml/h, the ambient temperature was 30℃and the relative humidity was 30%. The nanofiber mask with the anti-acne effect is prepared.
(5) Cutting the nanofiber obtained in the step (4) and the non-woven base cloth together by using a die, and processing to obtain the nanofiber facial mask conforming to the facial shape.
(6) After washing the face, wetting the facial skin with purified water or spray, then applying the cut nanofiber mask with anti-acne efficacy, supplementing water to wet the face, completely dissolving the mask after a few seconds, applying the mask on the skin, and massaging and absorbing.
Example 2
(1) Adding 15g of polyethylene glycol into 70g of water, stirring and dissolving at room temperature to obtain a polyethylene glycol solution;
(2) Uniformly mixing 5g of tea tree essential oil, 2g of jojoba oil, 2g of juniper essential oil and 3g of lecithin, and then adding the mixed solution into the polyethylene glycol aqueous solution in the step (1), uniformly stirring, and standing at normal temperature for later use;
(3) Adding 3g of vitamin B5 component into the mixed solution in the step (2), and uniformly stirring to obtain an electrostatic spinning solution;
(4) Adding the mixed solution obtained in the step (3) into a portable electrostatic spinning device for electrostatic spinning, washing the face, wetting the facial skin with purified water or spray, and preparing the nanofiber mask with the anti-acne effect on the face in situ. Spinning conditions: the spinning voltage was 10KV, the receiving distance was 20cm, the solution flow rate was 0.8ml/h, the ambient temperature was 25℃and the relative humidity was 40%. The nanofiber mask with the anti-acne effect is prepared in situ on the face.
(5) After the preparation of the facial mask is finished, the facial mask is completely dissolved and applied on the skin after a few seconds, and the facial mask can be massaged and absorbed.
As a preferable case, the polyethylene glycol in the formula not only can be used as a spinning aid and can load essential oil to form the nanofiber facial mask, but also has good moisturizing effect. The tea tree essential oil is pure natural plant essential oil extracted from Melaleuca alternifolia leaf of Myrtaceae in a distillation mode. The tea tree essential oil has excellent antibacterial, anti-inflammatory and mite-killing effects; has excellent purifying effect, has strong permeability for the skin of human body, and can well play the roles of diminishing inflammation, relieving itching and promoting wound healing. Improving suppuration of wound and acne skin infection. Can dredge sebaceous glands, regulate skin water oil balance state, and remove vaccinia and dirty parts caused by varicella and herpes zoster. Has good therapeutic effect on acne, and can be used for treating acne.
The juniper berry essential oil is an essential oil obtained by extracting fresh mature juniper fruit. Juniper berry essential oil or pale yellow or pale green. Has astringent, antibacterial and toxic materials removing effects, is very suitable for treating acne and eczema, can be used for assisting in treating acne and skin inflammation, and also can be used for astringing pores, regulating oil secretion and making skin warm and moist without dryness.
The jojoba oil is oil in seeds of jojoba, has strong permeability, is easily absorbed by skin, can diminish inflammation and sterilize, and has the characteristics of anti-inflammation and healing promotion; jojoba oil also contains abundant vitamin D and protein, and has effects in supplementing water, keeping moisture, preventing skin water loss, balancing skin pH, regulating sebaceous gland secretion function, increasing skin elasticity, delaying aging, and improving acne, xerosis cutis, fine wrinkles, and enlarged pores. The skin-care oil is matched with other essential oils, can improve the absorbability of skin, and is a good base oil.
The vitamin B5 has effects of promoting keratosis of skin, moisturizing, and relieving pain and itching of skin.
The natural essential oil emulsifier is used in the formula, so that oily essential oil can be converted into aqueous essential oil, and the aqueous essential oil is uniformly dispersed in the electrostatic spinning solution, so that layering phenomenon is avoided, and the essential oil can be ensured to be uniformly distributed in the nanofiber solution after electrostatic spinning.
In addition, the specific features described in the above embodiments may be combined in any suitable manner without contradiction. The various possible combinations of the invention are not described in detail in order to avoid unnecessary repetition.

Claims (10)

1. The nanofiber mask with the anti-acne effect is characterized by being prepared from the following raw materials in percentage by mass:
and (3) a component A: 5-15% of polyethylene glycol and 59-91.4% of water;
and B1: 1-10% of tea tree essential oil;
and a component B2: jojoba oil 0.1-1%;
and B3, a component: 1-5% of juniper essential oil.
And C, component: 50.5-5% of provitamin B;
and D, a component: 1-5% of natural essential oil emulsifier.
2. The nanofiber facial mask with anti-acne effect according to claim 1, which is characterized by being prepared from the following raw materials in percentage by mass:
and (3) a component A: polyethylene glycol 10%, water 77.5%;
and B1: tea tree essential oil 5%;
and a component B2: jojoba oil 0.5%;
and B3, a component: juniper essential oil 2%.
And C, component: vitamin B53%;
and D, a component: 2% of natural essential oil emulsifier.
3. The nanofiber facial mask with anti-acne efficacy according to claim 2, wherein the nanofiber facial mask is characterized by comprising the following components in parts by weight: the anti-acne active ingredients are more than one of tea tree essential oil, jojoba oil and juniper berry essential oil.
4. The nanofiber facial mask with anti-acne efficacy according to claim 2, wherein the nanofiber facial mask is characterized by comprising the following components in parts by weight: the natural essential oil emulsifier is composed of one or more of lecithin, lanolin alcohol, lanolin acid and beeswax.
5. The nanofiber facial mask with anti-acne efficacy according to claim 2, wherein the nanofiber facial mask is characterized by comprising the following components in parts by weight: the average molecular weight of the polyethylene glycol is 30000-40000.
6. The method for preparing a nanofiber facial mask with anti-acne efficacy according to claim 1,
the method is characterized by comprising the following steps of:
(1) Mixing polyethylene glycol powder in the component A with water at room temperature, and stirring uniformly to obtain polyethylene glycol aqueous solution at room temperature for later use;
(2) Uniformly mixing the component B and the component D, and then adding the mixed solution into the polyethylene glycol aqueous solution obtained in the step (1), uniformly stirring, and standing at normal temperature for later use;
(3) Adding the component C into the mixed solution obtained in the step (2), and uniformly stirring to obtain an electrostatic spinning solution;
(4) Adding the mixed solution obtained in the step (3) into an electrostatic spinning machine for electrostatic spinning, and preparing the nanofiber mask with the anti-acne effect;
(5) Or the spinning solution obtained in the step (3) is referred to in situ on the face to prepare a nanofiber mask through portable electrostatic spinning equipment;
(6) Cutting the nanofiber obtained in the step (4) and the non-woven base cloth together by using a die, and processing to obtain the nanofiber facial mask conforming to the facial shape.
7. The method for preparing the nanofiber facial mask with anti-acne effect according to claim 6, wherein the method comprises the following steps of: the electrostatic spinning parameters in the step (4) (5): the electrostatic spinning has the applied voltage of 8-15KV, the receiving distance of 10-25cm and the injection speed of 0.5-2mL/h.
8. The method for preparing the nanofiber facial mask with anti-acne effect according to claim 6, wherein the method comprises the following steps of: the conditions of the operations in steps (1) - (5) are: the ambient temperature is 20-30 ℃, and the humidity is 30-50% RH: preferably, it is: the ambient temperature was 28℃and humidity 40% RH.
9. The method of using a nanofiber facial mask with anti-acne efficacy according to any one of claim 6, comprising the following steps: after washing the face, wetting the facial skin with purified water or spray, then applying the cut nanofiber mask with anti-acne efficacy, supplementing water to wet the face, completely dissolving the mask after a few seconds, applying the mask on the skin, and massaging and absorbing.
10. The method of using a nanofiber facial mask with anti-acne efficacy according to any one of claim 6, comprising the following steps: after washing the face, wetting the facial skin with purified water or spray, then preparing a nanofiber mask on the face in situ by using a portable electrostatic spinning device, and after the mask is prepared, completely dissolving and applying the mask on the skin after a few seconds, and massaging and absorbing.
CN202310074487.7A 2023-02-07 2023-02-07 Nanofiber mask with anti-acne effect and preparation method thereof Pending CN116236401A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202310074487.7A CN116236401A (en) 2023-02-07 2023-02-07 Nanofiber mask with anti-acne effect and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202310074487.7A CN116236401A (en) 2023-02-07 2023-02-07 Nanofiber mask with anti-acne effect and preparation method thereof

Publications (1)

Publication Number Publication Date
CN116236401A true CN116236401A (en) 2023-06-09

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ID=86634374

Family Applications (1)

Application Number Title Priority Date Filing Date
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Country Status (1)

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