CN116173848A - Strong-flavor powder white spirit and preparation method thereof - Google Patents

Strong-flavor powder white spirit and preparation method thereof Download PDF

Info

Publication number
CN116173848A
CN116173848A CN202310210677.7A CN202310210677A CN116173848A CN 116173848 A CN116173848 A CN 116173848A CN 202310210677 A CN202310210677 A CN 202310210677A CN 116173848 A CN116173848 A CN 116173848A
Authority
CN
China
Prior art keywords
strong aromatic
white spirit
strong
powder white
dextrin
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN202310210677.7A
Other languages
Chinese (zh)
Inventor
杨平
秦辉
蔡小波
王旭
徐志
刘波
刘利民
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Luzhou Laojiao Co Ltd
Luzhou Laojiao Brewing Co Ltd
Original Assignee
Luzhou Laojiao Co Ltd
Luzhou Laojiao Brewing Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Luzhou Laojiao Co Ltd, Luzhou Laojiao Brewing Co Ltd filed Critical Luzhou Laojiao Co Ltd
Priority to CN202310210677.7A priority Critical patent/CN116173848A/en
Publication of CN116173848A publication Critical patent/CN116173848A/en
Pending legal-status Critical Current

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J13/00Colloid chemistry, e.g. the production of colloidal materials or their solutions, not otherwise provided for; Making microcapsules or microballoons
    • B01J13/02Making microcapsules or microballoons
    • B01J13/04Making microcapsules or microballoons by physical processes, e.g. drying, spraying
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J13/00Colloid chemistry, e.g. the production of colloidal materials or their solutions, not otherwise provided for; Making microcapsules or microballoons
    • B01J13/02Making microcapsules or microballoons
    • B01J13/04Making microcapsules or microballoons by physical processes, e.g. drying, spraying
    • B01J13/043Drying and spraying
    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12HPASTEURISATION, STERILISATION, PRESERVATION, PURIFICATION, CLARIFICATION OR AGEING OF ALCOHOLIC BEVERAGES; METHODS FOR ALTERING THE ALCOHOL CONTENT OF FERMENTED SOLUTIONS OR ALCOHOLIC BEVERAGES
    • C12H1/00Pasteurisation, sterilisation, preservation, purification, clarification, or ageing of alcoholic beverages
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02ATECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A50/00TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
    • Y02A50/30Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Dispersion Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Biochemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Food Science & Technology (AREA)
  • Bioinformatics & Cheminformatics (AREA)
  • General Engineering & Computer Science (AREA)
  • General Health & Medical Sciences (AREA)
  • Genetics & Genomics (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Seasonings (AREA)
  • General Preparation And Processing Of Foods (AREA)

Abstract

The invention belongs to the field of wine products, and particularly relates to a strong aromatic powder white wine and a preparation method thereof. Aiming at the problem that the existing liquid white spirit is unfavorable for storage and transportation, the invention provides a preparation method of the strong aromatic powder white spirit on the premise of not affecting the taste and the aroma of the strong aromatic white spirit, which comprises the following steps: DP8-12 dextrin is dissolved in strong aromatic Chinese spirits to form microcapsule pre-prepared liquid, and then spray freeze drying is carried out to obtain microcapsule particles, and vacuum drying is carried out to obtain the product. According to the invention, the microcapsule wall material is dissolved, the temperature and the vacuum environment in the microcapsule particle drying process are controlled, so that the typical flavor of the strong aromatic white spirit is effectively reserved while the strong aromatic white spirit is microencapsulated, and the storage and transportation efficiency of the strong aromatic white spirit is improved.

Description

Strong-flavor powder white spirit and preparation method thereof
Technical Field
The invention belongs to the field of wine products, and particularly relates to a strong aromatic powder white wine and a preparation method thereof.
Background
White spirit is a unique alcoholic beverage formed by traditional fermentation and distillation in China, and is also called as Liuda distilled spirit in the world together with brandy, whiskey, vodka, gold spirit and rum. Because the Chinese white spirit has extremely strong social properties, the Chinese culture is inherited by the Chinese white spirit for thousands of years, the Chinese white spirit is closely combined with the Chinese social etiquette, and the high-quality Chinese white spirit even has investment value.
Because of factors such as geographical environment, climate characteristics, raw material technology and the like, the white spirit production has strong territory. Luzhou is used as the origin place of the Luzhou-flavor liquor, the production capacity of the high-quality Luzhou-flavor liquor is leading in the world, in recent years, along with the improvement of brand positioning of strategic patterns and innovation and optimization of sales channels, the regional bottleneck of the Luzhou-flavor liquor is gradually broken, the trans-regional transportation storage capacity of the Luzhou-flavor liquor is greatly improved, and due to the special attribute of the Luzhou-flavor liquor, the traditional transportation and storage mode is high in cost and easy to influence the flavor and aroma of liquor. How to improve the storage and transportation efficiency of the strong aromatic Chinese spirits and reduce the cost becomes a prospective research topic.
Disclosure of Invention
Aiming at the problem that the existing liquid white spirit is unfavorable for storage and transportation, the invention provides the strong aromatic powder white spirit which is easy to store and transport and the preparation method thereof on the premise of not affecting the taste and the aroma of the strong aromatic white spirit.
The technical scheme for solving the technical problems is as follows:
the invention provides a preparation method of strong aromatic powder white spirit, which comprises the following steps: DP8-12 dextrin is dissolved in strong aromatic Chinese spirits to form microcapsule pre-prepared liquid, and then spray freeze drying is carried out to obtain microcapsule particles, and vacuum drying is carried out to obtain the product.
Wherein the alcohol concentration of the strong aromatic Chinese spirits is 38-52%.
Wherein the mass ratio of the strong aromatic Chinese spirits to the DP8-12 dextrin is (3-4): (1-2).
Wherein the temperature of the DP8-12 dextrin dissolved in the strong aromatic Chinese spirit is 20-40 ℃. Preferably 30 ℃.
Wherein the stirring rate of the DP8-12 dextrin dissolved in the strong aromatic Chinese spirits is 800-1200 rpm.
Wherein the spray freeze drying temperature is-30 to-50 ℃.
Wherein the vacuum drying pressure is 2.7-6.7 Pa.
Wherein the vacuum drying temperature is-20 to-40 ℃.
The invention also provides the strong aromatic powder white spirit prepared by the preparation method.
Wherein the alcohol content of the strong aromatic powder white spirit is 35-58% vol.
The beneficial effects are that: the invention adopts microcapsule technology to pulverize the solid of the liquid strong aromatic Chinese liquor, so that the state is stable, reasonable microcapsule wall films are screened out, the aroma substances and other trace components of the strong aromatic Chinese liquor are fixed, and the transportation and storage efficiency can be obviously improved on the premise of ensuring the quality of the strong aromatic Chinese liquor.
The invention controls the temperature and vacuum environment in the microcapsule wall material dissolution and microcapsule particle drying process, so that the typical flavor of the strong aromatic white spirit is effectively reserved while the strong aromatic white spirit is microencapsulated, and finally the preparation of the strong aromatic powder white spirit in a real sense is realized.
Detailed Description
The specific preparation method of the strong aromatic powder white spirit comprises the following steps:
(1) 15-20 kg of strong aromatic white spirit with the alcohol concentration of 38-52% is taken, and 5-10 kg of DP8-12 dextrin is added into the strong aromatic white spirit;
(2) Heating the solution to 20-40 ℃ in a closed container by utilizing water bath, stirring at 800-1200 rpm until the DP8-12 dextrin is uniformly dissolved and filtered to form microcapsule pre-prepared liquid;
(3) Spray-freezing at-30 to-50 ℃, and vacuum-drying at-20 to-40 ℃ under the operating pressure of 2.7-6.7 Pa after the microcapsule prefabricated liquid is completely frozen to finally obtain the strong aromatic powder white spirit. Wherein the alcohol content is 35-58%.
The technical scheme of the invention is mainly innovated and improved in the following three aspects:
(1) Microencapsulated wall material
Compared with brewed wine, distilled wine such as fruit wine, flavoring wine, white wine and the like has higher alcohol content, so the wall material of the white wine microcapsule needs to have stronger alcohol binding capability. The edible microcapsule wall material has good alcohol binding degree, such as maltodextrin, cyclodextrin, and puffed dextrin.
And DP8-12 dextrin is novel dextrin, which is obtained by hydrolyzing starch by alpha-amylase and separating and removing dextrin with higher glucose polymerization degree by a proper hollow fiber ultrafilter. The main component is branched and unbranched dextrin with the polymerization degree of glucose of 8-12, has the advantages of edibility, innocuity, good water solubility, low viscosity and the like, and is suitable for microcapsule wall materials of alcohol.
The common dextrins such as white dextrins and yellow dextrins have high molecular weight, the polymerization degree of glucose is above 20, the common dextrins are difficult to be completely dissolved in water under the condition of no heating, the heating can volatilize wine components to affect the product quality, and the polymerization degree of glucose of DP8-12 dextrins is 8-12, so the common dextrins are suitable for being used as embedding agents of wine.
(2) Spray freeze drying
In the microcapsule prefabricated liquid, the boiling point of the main body aroma components of the strong aromatic Chinese liquor is low, so that the typical flavor of the strong aromatic Chinese liquor is reserved to a great extent, the microcapsule prefabricated liquid is kept in a low-temperature environment in the drying process, and a spray freeze drying technology is adopted.
Spray-freeze-drying (SFD) is a novel drying mode, combines the advantages of Spray drying and freeze drying, and can effectively maintain the original molecular structure, chemical property and biological activity of substances in the drying process.
Because the coating force and the adsorption force of the encapsulating material on the alcohol are stronger under the low-temperature condition, the spray freeze drying temperature is controlled between minus 30 ℃ and minus 50 DEG C
(3) Low temperature vacuum drying
After the microcapsule particles are formed by spray freeze drying, the microcapsule particles are sublimated from the water by maintaining the vacuum condition, and the wine body components of the strong aromatic Chinese spirits remain in the frozen microcapsule particles. The vacuum drying can remove more than 95-99% of water, and can effectively inhibit oxidation reaction of the aroma components in the strong aromatic Chinese spirits. However, the heat is required to be absorbed in the sublimation process, so that the temperature of the microencapsulated particles is further reduced to influence the sublimation speed, and therefore, proper heating is required to ensure the continuous sublimation, namely, after microcapsule particles are formed at-30 to-50 ℃, the temperature is increased to-20 to-40 ℃ for freeze drying.
In the prior art, microwave drying is adopted to prepare the powder wine, however, the microwave drying and the medium temperature kept in the prior step of microwave drying are always above 30 ℃ and even reach 55 ℃, so that alcohol molecules are volatilized and key flavor substances of the strong aromatic white wine are lost (key flavor components of the strong aromatic white wine belong to low-boiling substances) in the period, the low-temperature vacuum drying is adopted, and the temperature is controlled below-30 ℃ in the prior step of drying, so that the alcohol molecules and the flavor components can be effectively preserved.
The scheme of the present invention will be explained below with reference to examples. It will be appreciated by those skilled in the art that the following examples are illustrative of the present invention and should not be construed as limiting the scope of the invention. The examples are not to be construed as limiting the specific techniques or conditions described in the literature in this field or as per the specifications of the product. The reagents or apparatus used were conventional products commercially available without the manufacturer's attention.
Example 1
(1) Taking 20kg of strong aromatic Chinese spirit with the alcohol concentration of 52%, and adding 8kg of DP8-12 dextrin into the strong aromatic Chinese spirit;
(2) Heating the solution to 30 ℃ in a closed container by utilizing water bath, stirring the solution at a rotating speed of 1000rpm until the DP8-12 dextrin is uniformly dissolved and filtered to form microcapsule pre-prepared liquid;
(3) Spray-freezing at-45deg.C, vacuum drying at operating pressure of 5Pa and temperature of-40deg.C after microcapsule pre-preparation is completely frozen, and finally obtaining 13.28kg of Luzhou-flavor powder Chinese liquor. The content of alcohol is 58%, and the flavor of the typical strong aromatic white spirit is judged by tasting and evaluating.
Example 2
(1) Taking 20kg of strong aromatic Chinese spirit with the alcohol concentration of 52%, and adding 8kg of DP8-12 dextrin into the strong aromatic Chinese spirit;
(2) Heating the solution to 20 ℃ in a closed container by utilizing water bath, stirring the solution at a rotating speed of 1000rpm until the DP8-12 dextrin is uniformly dissolved and filtered to form microcapsule pre-prepared liquid;
(3) Spray-freezing at-45deg.C, vacuum drying at-40deg.C under 5Pa to obtain 11.36kg of Luzhou-flavor powder Chinese liquor with 36% alcohol content, and tasting to verify that the Luzhou-flavor Chinese liquor has no obvious flavor and increased sweetness.
Example 2 differs from example 1 in that the concentration of DP8-12 dextrin in the microcapsule pre-formed liquid of example 1 is higher and the content of the Luzhou-flavor powder white spirit finally formed by vacuum drying is relatively higher because the solution temperature (30 ℃ in example 1, 20 ℃ in example 2) when DP8-12 dextrin is uniformly dissolved to form the microcapsule pre-formed liquid is high, and the solubility of DP8-12 dextrin is still improved along with the rise of the temperature although the DP8-12 dextrin is easily dissolved in water.
Example 3
(1) Taking 20kg of strong aromatic Chinese spirit with the alcohol concentration of 52%, and adding 8kg of DP8-12 dextrin into the strong aromatic Chinese spirit;
(2) Heating the solution to 40 ℃ in a closed container by utilizing water bath, stirring the solution at a rotating speed of 1000rpm until the DP8-12 dextrin is uniformly dissolved and filtered to form microcapsule pre-prepared liquid;
(3) Spray-freezing at-45deg.C, vacuum drying at-40deg.C under 5Pa to obtain 13.37kg of strong aromatic powder Chinese liquor with alcohol content of 51%, and tasting and evaluating to obtain strong aromatic Chinese liquor with certain flavor.
From examples 1 to 3, the difference between the three is only that the solution temperature when DP8-12 dextrin is uniformly dissolved to form microcapsule pre-prepared liquid, although the solution can be dissolved at 20-40 ℃, the content of the prepared strong aromatic powder white spirit is relatively high and the flavor of the white spirit is better preserved when the dissolution temperature is 30 ℃.
Example 4
(1) Taking 20kg of strong aromatic Chinese spirit with the alcohol concentration of 52%, and adding 8kg of DP8-12 dextrin into the strong aromatic Chinese spirit;
(2) Heating the solution to 30 ℃ in a closed container by utilizing water bath, stirring the solution at a rotating speed of 1000rpm until the DP8-12 dextrin is uniformly dissolved and filtered to form microcapsule pre-prepared liquid;
(3) Spray-freezing at-30deg.C, vacuum drying at-40deg.C under 5Pa to obtain 13.16kg of strong aromatic powder Chinese liquor with alcohol content of 55%, and tasting and evaluating to obtain strong aromatic Chinese liquor with typical flavor.
Example 5
(1) Taking 20kg of strong aromatic Chinese spirit with the alcohol concentration of 52%, and adding 8kg of DP8-12 dextrin into the strong aromatic Chinese spirit;
(2) Heating the solution to 30 ℃ in a closed container by utilizing water bath, stirring the solution at a rotating speed of 1000rpm until the DP8-12 dextrin is uniformly dissolved and filtered to form microcapsule pre-prepared liquid;
(3) Spray-freezing at-50deg.C, vacuum drying at-40deg.C under 5Pa to obtain 13.23kg of strong aromatic powder Chinese liquor with alcohol content of 56%, and tasting and evaluating to obtain strong aromatic Chinese liquor with typical flavor.
Example 6
(1) Taking 20kg of strong aromatic Chinese spirit with the alcohol concentration of 52%, and adding 8kg of DP8-12 dextrin into the strong aromatic Chinese spirit;
(2) Heating the solution to 30 ℃ in a closed container by utilizing water bath, stirring the solution at a rotating speed of 1000rpm until the DP8-12 dextrin is uniformly dissolved and filtered to form microcapsule pre-prepared liquid;
(3) Spray-freezing at-45deg.C, vacuum drying at-20deg.C under 5Pa to obtain 13.32kg of strong aromatic powder Chinese liquor with alcohol content of 52%, and tasting and evaluating to obtain strong aromatic Chinese liquor with typical flavor.
From the above, it can be seen that the powder white spirit formed by sufficiently combining the strong aromatic white spirit with the microcapsule wall material at a proper temperature, and then freezing by spraying and vacuum drying at a proper temperature can have a higher alcohol concentration and has a typical strong aromatic white spirit style.
It is to be noted that the particular features, structures, materials, or characteristics described in this specification may be combined in any suitable manner in any one or more embodiments. Furthermore, the various embodiments described in this specification, as well as the features of the various embodiments, can be combined and combined by one skilled in the art without contradiction.

Claims (10)

1. The preparation method of the strong aromatic powder white spirit is characterized by comprising the following steps: the method comprises the following steps: DP8-12 dextrin is dissolved in strong aromatic Chinese spirits to form microcapsule pre-prepared liquid, and then spray freeze drying is carried out to obtain microcapsule particles, and vacuum drying is carried out to obtain the product.
2. The method for preparing the strong aromatic powder white spirit according to claim 1, which is characterized in that: the alcohol concentration of the strong aromatic Chinese spirits is 38-52%.
3. The method for preparing the strong aromatic powder white spirit according to claim 1 or 2, which is characterized in that: the mass ratio of the strong aromatic Chinese spirits to the DP8-12 dextrin is (3-4): (1-2).
4. The method for preparing the strong aromatic powder white spirit according to any one of claims 1 to 3, which is characterized in that: DP8-12 dextrin is dissolved in the strong aromatic Chinese spirits at 20-40 ℃; preferably 30 ℃.
5. The method for preparing the strong aromatic powder white spirit according to any one of claims 1 to 4, which is characterized in that: the stirring rate of the DP8-12 dextrin dissolved in the strong aromatic Chinese spirits is 800-1200 rpm.
6. The method for preparing the strong aromatic powder white spirit according to any one of claims 1 to 5, characterized in that: the spray freeze drying temperature is-30 to-50 ℃.
7. The method for preparing the strong aromatic powder white spirit according to any one of claims 1 to 6, characterized in that: the vacuum drying pressure is 2.7 Pa to 6.7Pa.
8. The method for preparing the strong aromatic powder white spirit according to any one of claims 1 to 7, characterized in that: the vacuum drying temperature is-20 to-40 ℃.
9. The Luzhou-flavor powder white spirit prepared by the preparation method of any one of claims 1-8.
10. The Luzhou-flavor powder white spirit according to claim 9, wherein: the alcohol content of the strong aromatic powder white spirit is 35-58% vol.
CN202310210677.7A 2023-03-07 2023-03-07 Strong-flavor powder white spirit and preparation method thereof Pending CN116173848A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202310210677.7A CN116173848A (en) 2023-03-07 2023-03-07 Strong-flavor powder white spirit and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202310210677.7A CN116173848A (en) 2023-03-07 2023-03-07 Strong-flavor powder white spirit and preparation method thereof

Publications (1)

Publication Number Publication Date
CN116173848A true CN116173848A (en) 2023-05-30

Family

ID=86450521

Family Applications (1)

Application Number Title Priority Date Filing Date
CN202310210677.7A Pending CN116173848A (en) 2023-03-07 2023-03-07 Strong-flavor powder white spirit and preparation method thereof

Country Status (1)

Country Link
CN (1) CN116173848A (en)

Citations (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2665613A1 (en) * 1990-08-13 1992-02-14 Orsan Powdered wine and strong spirit flavouring
CN1368055A (en) * 2001-02-06 2002-09-11 方晓阳 Venine product for treating rheumatic and rheumatoid arthritis
JP2007175033A (en) * 2005-12-26 2007-07-12 Sato Shokuhin Kogyo Kk Alcoholic liquor-containing solid food, and method for producing the same
CN101790325A (en) * 2007-08-28 2010-07-28 百事可乐公司 Delivery and controlled release of encapsulated water-insoluble flavorants
CN102925327A (en) * 2012-11-27 2013-02-13 邢海明 Mellow powder white spirit and preparation method thereof
CN102925328A (en) * 2012-11-27 2013-02-13 邢海明 Powder white spirit and preparation method thereof
CN103013796A (en) * 2012-11-27 2013-04-03 邢海明 Easily carried powder white wine and preparation method thereof
CN104312884A (en) * 2014-10-10 2015-01-28 江南大学 Preparation method of powdery red wine
CN104450361A (en) * 2014-11-13 2015-03-25 唐正 Powder liquor and preparation method thereof
JP2016123284A (en) * 2014-12-26 2016-07-11 アサヒビール株式会社 Method for producing powdered liquor
KR20170035164A (en) * 2015-09-22 2017-03-30 주식회사 새울 Method for production of reduction type makgeolli power entrapping alcohol
CN107338164A (en) * 2017-09-05 2017-11-10 泸州老窖集团有限责任公司 Pericarp health liquor and preparation method thereof
CN113201527A (en) * 2021-04-30 2021-08-03 齐鲁工业大学 Hop picric acid yeast microcapsule and preparation method and application thereof

Patent Citations (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2665613A1 (en) * 1990-08-13 1992-02-14 Orsan Powdered wine and strong spirit flavouring
CN1368055A (en) * 2001-02-06 2002-09-11 方晓阳 Venine product for treating rheumatic and rheumatoid arthritis
JP2007175033A (en) * 2005-12-26 2007-07-12 Sato Shokuhin Kogyo Kk Alcoholic liquor-containing solid food, and method for producing the same
CN101790325A (en) * 2007-08-28 2010-07-28 百事可乐公司 Delivery and controlled release of encapsulated water-insoluble flavorants
CN102925327A (en) * 2012-11-27 2013-02-13 邢海明 Mellow powder white spirit and preparation method thereof
CN102925328A (en) * 2012-11-27 2013-02-13 邢海明 Powder white spirit and preparation method thereof
CN103013796A (en) * 2012-11-27 2013-04-03 邢海明 Easily carried powder white wine and preparation method thereof
CN104312884A (en) * 2014-10-10 2015-01-28 江南大学 Preparation method of powdery red wine
CN104450361A (en) * 2014-11-13 2015-03-25 唐正 Powder liquor and preparation method thereof
JP2016123284A (en) * 2014-12-26 2016-07-11 アサヒビール株式会社 Method for producing powdered liquor
KR20170035164A (en) * 2015-09-22 2017-03-30 주식회사 새울 Method for production of reduction type makgeolli power entrapping alcohol
CN107338164A (en) * 2017-09-05 2017-11-10 泸州老窖集团有限责任公司 Pericarp health liquor and preparation method thereof
CN113201527A (en) * 2021-04-30 2021-08-03 齐鲁工业大学 Hop picric acid yeast microcapsule and preparation method and application thereof

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
朱秋享等: "DP(8-12)糊精的应用研究", 《福州大学学报(自然科学版)》, vol. 30, 30 November 2002 (2002-11-30), pages 733 - 736 *
黄亚东: "微胶囊技术在粉末酒生产中的应用研究", 酿酒, no. 06, 30 November 2002 (2002-11-30), pages 80 - 81 *

Similar Documents

Publication Publication Date Title
CN101531960B (en) Wine-making preparation method adopting litchi fermentation
CN103571710A (en) Cocktail and preparation method thereof
JP4542989B2 (en) Sparkling carbonated drink
AU2021101601A4 (en) Method for reducing methanol content in fruit wine and fruit wine with low methanol content
CN109234114A (en) A kind of compound small berries brandy and alcohol-free wine and preparation method thereof
CN102925328B (en) Powder white spirit and preparation method thereof
CN116173848A (en) Strong-flavor powder white spirit and preparation method thereof
CN106387182A (en) Tea flower beverage and preparation method thereof
EP2537420A1 (en) Method for the stabilisation of spheres formed by a liquid containing alcohol
CN116769555A (en) Production process of bubble yellow wine
JP6712170B2 (en) Aging enhancer for alcoholic beverages
CZ201046A3 (en) Process for preparing alcohol-free vine
JP2002034548A (en) Method for producing hawthorn wine
KR20140142105A (en) Plum sweet mirin and its manufacturing method
CN114381350A (en) Preparation method of composite flavor rum
CN106434136B (en) Production method of low-heat mild red yeast rice yellow wine
CN101555442A (en) Manufacturing method of beer flavouring agent for improving aroma
JP2007159471A (en) Foaming carbonated beverage
KR20140106305A (en) Manufacturing method of fruit jam using dried fruit
CN102138596A (en) Preparation method of instant tea powder with high scent and low bitter
CN104862204B (en) A kind of method of drinks fast-ripenin and quality optimization
TW201417726A (en) Monomeric proanthocyanidin-removed plant extract
CN114747642B (en) Method for improving quality of black tea juice by using complex enzyme
CN106387173A (en) Tea flower and black tea beverage and preparation method thereof
KR0183526B1 (en) Process for producing beer-like sparkling liquor

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination