CN116158502A - 一种环保防腐剂及其制备方法 - Google Patents

一种环保防腐剂及其制备方法 Download PDF

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CN116158502A
CN116158502A CN202210855019.9A CN202210855019A CN116158502A CN 116158502 A CN116158502 A CN 116158502A CN 202210855019 A CN202210855019 A CN 202210855019A CN 116158502 A CN116158502 A CN 116158502A
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冯绍健
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    • A—HUMAN NECESSITIES
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    • B01F27/80—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis
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    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
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    • B01F27/90—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis with paddles or arms 
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    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
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    • B01F27/96—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis with openwork frames or cages
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Abstract

本发明属于防腐剂加工技术领域，具体而言，是一种环保防腐剂制备方法以及通过该方法制备的环保防腐剂；环保防腐剂制备方法，包括以下步骤：步骤一：添加原料；步骤二：向漏盘内缓慢注入溶剂物料，并对蜂胶原料进行搅动，使其分散溶解；步骤三：将粘覆在处理容器内壁的物料刮下，减少蜂胶等物料残留在容器内壁的情况；步骤五：物料粘稠度合格后排出收集，涂覆在食品表面进行防腐处理；所制备的环保防腐剂的组成包括：蜂胶、食用酒精和山梨酸钾；所述蜂胶分散设备包括支座、混合罐、盖、漏盘、搅拌器和加热器；其中，混合罐和搅拌器构成处理容器；在保证对物料的充分搅动处理的基础上，提高设备对于物料的搅动性能和设备自身的清洗性能。

Description

一种环保防腐剂及其制备方法
技术领域
本发明属于防腐剂加工技术领域，具体而言，是一种环保防腐剂制备方法以及通过该方法制备的环保防腐剂。
背景技术
油脂氧化是食品变质的主要原因之一；油脂氧化反应不仅降低了食品的营养价值，并且有些氧化产物还具有毒副作用，影响了食品的质量和安全，而且部分油脂经高温诱导会加速氧化酸败；
蜂胶作为天然抗氧化剂，可直接或间接作用于食品、果蔬以及肉类、禽蛋和豆腐等副食品的防腐保鲜中；
蜂胶具有脂溶性，本身不溶于水，部分是溶于酒精的，因此在制备以蜂胶为原料的环保防腐剂过程中，为增强蜂胶可溶性部分的溶解分散需要，在保持对团状蜂胶原料进行溶解和过滤处理的情况下，对其进行充分搅动；
现有专利号为CN201410042456.4的一种交联壳聚糖食品防腐剂及其制备方法和应用，该专利文献中，公开了一种通过对物料进行高速机械搅拌，使物料充分溶解并进行乳化处理的方案；但是该专利文献中未提到的是，对于产品质量要求较高的防腐剂产品在制备过程中，其容器需要在准备期间进行充分清洗，从而避免产品质量收到影响。
发明内容
为了实现在保证对物料的充分搅动处理的基础上，提高设备对于物料的搅动性能和设备自身的清洗性能的目的，本发明采用以下技术方案：
本申请提供的环保防腐剂制备方法，包括以下步骤：
步骤一：将蜂胶原料投入至处理容器内的漏盘中；
步骤二：向漏盘内缓慢注入溶剂物料，并对蜂胶原料进行搅动，使其分散溶解；
步骤三：利用安装在处理容器外侧的加热器，提供处理容器内的物料易于溶解所需的温度；
步骤四：将粘覆在处理容器内壁的物料刮下，减少蜂胶等物料残留在容器内壁的情况，增加环保防腐剂的配料精准度和后续的清理维护效果；
步骤五：物料粘稠度合格后排出收集，涂覆在食品表面进行防腐处理。
通过环保防腐剂制备方法制备的环保防腐剂的组成包括：按照质量份数取蜂胶5～10份、食用酒精20～50份、山梨酸钾0.8～2.3份、对羟基苯甲酸丙酯1.2～1.8份和对羟基苯甲酸乙酯2～5份。
本申请中提供的环保防腐剂制备方法中对于蜂胶等原料在溶剂中分散和残留物在内壁上的刮动处理步骤是通过蜂胶分散设备来进行的，通过在容器内对蜂胶原料进行过滤和搅动，加快原料的分散效果，并通过插接配合的杆体结构，增加搅拌器的搅拌稳定性，同时能使装置整体易于拆离清洗。
所述蜂胶分散设备包括支座、混合罐、盖、漏盘和搅拌器；
其中，混合罐和搅拌器构成处理容器。
支座上固定连接有混合罐，混合罐上安装有盖，盖上转动连接有搅拌器，搅拌器的下端与平衡器插接配合，平衡器转动连接在混合罐的底部；
搅拌器的下端固定连接有多边形柱，平衡器上设置有插孔，多边形柱与插孔之间插接配合，从而使设备整体的拆卸性能提高。
盖上设有灌料管，混合罐底部设有排料管。
漏盘安装在盖的下侧，搅拌器贯穿漏盘，搅拌器在漏盘的上下两侧分别安装有搅拌棒和U型臂，平衡器上固定连接有L型臂。
通过控制搅拌器以自身的轴线为轴进行转动，从而使U型臂、搅拌棒和L型臂对物料进行充分搅动，使蜂胶原料在揉压过程中，与向漏盘中缓慢注入的食用酒精等溶剂物料充分接触，增加蜂胶原料的分散和溶解性能，进而在保持对团状蜂胶原料进行溶解和过滤处理的情况下，对其进行充分搅动。
附图说明
以下附图仅旨在于对本发明做示意性说明和解释，其中：
图1为本发明的环保防腐剂制备方法的流程图；
图2为本发明的蜂胶分散设备整体的结构示意图；
图3为本发明的混合罐、加热器和搅拌器的结构示意图；
图4为本发明的混合罐、排料管和搅拌器的结构示意图；
图5为本发明的T型塞的结构示意图；
图6为本发明的漏盘、搅拌器和U型臂的结构示意图；
图7为本发明的平衡器、L型臂、控制盘和升降座的结构示意图；
图8为本发明的内壁刮板、铰接杆和底部刮动臂的结构示意图；
图9为本发明的搅拌器、U型臂和搅拌棒的结构示意图；
图10为本发明的平衡器、L型臂和控制盘的结构示意图；
图11为本发明的控制盘、固定套筒和插杆的结构示意图；
图12为本发明的固定环和定位环的结构示意图；
图13为本发明的漏盘、橡胶环和按压器的结构示意图；
图14为本发明的连接座和按压器的结构示意图。
图中：支座11；混合罐12；盖13；灌料管14；排料管15；T型塞16；限位沿17；加热器18；漏盘21；橡胶环22；搅拌器31；U型臂32；搅拌棒33；安装座34；平衡器41；L型臂42；控制盘43；升降座44；伸缩驱动器45；内壁刮板51；铰接杆52；底部刮动臂53；刮板54；固定套筒61；固定环62；定位环63；插杆64；连接座71；按压器72。
具体实施方式
本申请提供的环保防腐剂制备方法，包括以下步骤：
步骤一：将蜂胶原料投入至处理容器内的漏盘21中；
步骤二：向漏盘21内缓慢注入溶剂物料，并对蜂胶原料进行搅动，使其分散溶解；
步骤三：利用安装在处理容器外侧的加热器18，提供处理容器内的物料易于溶解所需的温度；
步骤四：将粘覆在处理容器内壁的物料刮下，减少蜂胶等物料残留在容器内壁的情况，增加环保防腐剂的配料精准度和后续的清理维护效果；
步骤五：物料粘稠度合格后排出收集，涂覆在食品表面进行防腐处理。
通过环保防腐剂制备方法制备的环保防腐剂的组成包括：按照质量份数取蜂胶5～10份、食用酒精20～350份、山梨酸钾0.8～2.3份、对羟基苯甲酸丙酯1.2～1.8份和对羟基苯甲酸乙酯2～5份。
食用酒精在添加到处理容器内后，将蜂胶原料进行溶解，通过加热器18将调整至适合蜂胶原料的适合的溶解温度，并利用加热器18将食用酒精部分蒸干，调整半成品物料的粘稠度。
参照图2-4、图6和图9-10所示，说明本发明提供的环保防腐剂制备方法中对于蜂胶等原料在溶剂中分散和残留物在内壁上的刮动处理步骤中使用到的蜂胶分散设备，利用搅拌器31对蜂胶原料进行充分揉压，使蜂胶原料在溶剂中分散和溶解的实施例：
混合罐12通过支座11安装在地面上，混合罐12的顶部可拆卸固定连接有盖13，盖13上转动连接有搅拌器31；
搅拌器31通过自身上的H型结构卡在盖13上，搅拌器31的侧部固定连接有用于对物料进行搅动的U型臂32和搅拌棒33；
盖13的上侧安装有安装座34，安装座34上通过支架安装有用于驱动搅拌器31以自身的轴线为轴进行转动的转动驱动器；
盖13的下侧安装有漏盘21，搅拌器31贯穿漏盘21，混合罐12底部转动连接有平衡器41，搅拌器31的下端固定连接有多边形柱，平衡器41上设置有插孔，多边形柱与插孔之间插接配合；
从而使平衡器41和搅拌器31之间能够同步转动，并且平衡器41上安装有多个L型臂42；
可将搅拌器31和盖13一同从混合罐12上拆离，进行搅拌器31的工作状态和清洗状态的切换，对容器内壁进行充分清洗。
盖13上设置有灌料管14，混合罐12的底部设置有排料管15，通过搅拌器31对漏盘21内的团状蜂胶原料和混合罐12的溶剂物料进行搅动；
启动转动驱动器，通过控制搅拌器31以自身的轴线为轴进行转动，从而使U型臂32、搅拌棒33和L型臂42对漏盘21和混合罐12内的物料进行充分搅动，使蜂胶原料在揉压过程中，与向漏盘21中缓慢注入的食用酒精等溶剂物料充分接触，增加蜂胶原料的分散和溶解性能，进而在保持对团状蜂胶原料进行溶解和过滤处理的情况下，对其进行充分搅动；
本申请中的转动驱动器可选用步进电机或伺服电机。
加热器18通过环形支架固定连接在混合罐12外侧，且均匀分布设置有多个，通过多个加热器18提供处理容器内的物料易于溶解所需的温度。
参照图3-4、图7-8和图10-12所示，说明本发明提供的环保防腐剂制备方法中对于蜂胶等原料在溶剂中分散和残留物在内壁上的刮动处理步骤中使用到的蜂胶分散设备，对混合罐12内侧的底面进行物料刮除，增加物料防粘连的清理效果的实施例：
平衡器41上滑动连接有控制盘43，控制盘43上安装有底部刮动臂53，底部刮动臂53通过扭簧组件转动连接在控制盘43上；
其中，扭簧组件包括固定套筒61、固定环62、定位环63和插杆64；
底部刮动臂53与固定套筒61固定连接，固定套筒61上固定连接有固定环62，固定环62通过扭簧固定连接有定位环63，定位环63端部设有方型柱，控制盘43上设有供方型柱插接的方孔，控制盘43上横向插入安装有插杆64，插杆64贯穿固定套筒61和固定环62后，将定位环63上的方型柱顶紧在方孔内，插杆64与控制盘43之间通过紧固件固定连接；
在扭簧的作用下，底部刮动臂53的下端始终与混合罐12的底部相抵接，从而在控制控制盘43在平衡器41上进行滑动的过程中，带动底部刮动臂53对混合罐12的底部粘覆的物料进行刮动；
混合罐12的下侧安装有伸缩驱动器45，伸缩驱动器45的活动端上安装有横板，横板上转动连接有升降座44，升降座44滑动连接在平衡器41内，并与控制盘43固定连接；
通过启动伸缩驱动器45，带动控制盘43竖向移动，从而在刮板54与混合罐12内侧的底面作用下，带动底部刮动臂53进行转动，对混合罐12内侧的底面进行物料刮除，增加物料防粘连的清理效果；
本申请中的伸缩驱动器可选用电动伸缩杆或液压缸。
进一步地，在底部刮动臂53上安装刮板54，能够进一步提高底部刮动臂53的清理效果。
参照图3-5所示，说明本发明提供的环保防腐剂制备方法中对于蜂胶等原料在溶剂中分散和残留物在内壁上的刮动处理步骤中使用到的蜂胶分散设备，通过对排料管15的结构进行改进，增加对粘覆的物料刮除性能的实施例：
排料管15内滑动连接有T型塞16，T型塞16顶部橡胶柱与排料管15内壁相贴合，T型塞16主体竖柱的下端的侧部固定连接有横柱，横柱滑动连接在排料管15上的竖槽内，便于手动控制其位置；
排料管15侧部还设置有支管，手动控制T型塞16下移，之后通过紧固件将T型塞16在排料管15内进行位置固定，使支管与混合罐12之间连通，进行排料操作；
手动控制T型塞16上移，能使T型塞16顶部与混合罐12内侧的底部抵接，从而使刮板54与混合罐12内侧的底部贴合效果提高，将粘覆的物料刮除处理，进一步减少蜂胶等物料残留在容器内壁的情况，增加环保防腐剂的配料精准度和后续的清理维护效果；
参照图7-13所示，说明本发明提供的环保防腐剂制备方法中对于蜂胶等原料在溶剂中分散和残留物在内壁上的刮动处理步骤中使用到的蜂胶分散设备，对容器内壁进行刮动的实施例：
L型臂42上横向滑动连接有内壁刮板51，底部刮动臂53端部铰接连接有铰接杆52，该铰接杆52与内壁刮板51滑动连接。
通过启动伸缩驱动器45，带动控制盘43竖向移动，从而在刮板54与混合罐12内侧的底面作用下，带动底部刮动臂53进行转动，对混合罐12内侧的底面进行物料刮除，同时通过铰接杆52带动内壁刮板51对混合罐12内壁进行物料刮除，增加物料防粘连的清理效果，进一步减少蜂胶等物料残留在容器内壁的情况。
参照图6-13所示，说明本发明提供的环保防腐剂制备方法中对于蜂胶等原料在溶剂中分散和残留物在内壁上的刮动处理步骤中使用到的蜂胶分散设备，利用按压器72对漏盘21进行扭动处理，增加蜂胶原料的分散效果和溶解效果的实施例：
漏盘21通过限位沿17连接在盖13的下侧，限位沿17用于限制漏盘21的竖向移动，限位沿17的内侧与漏盘21外侧之间留有间隙；
漏盘21能够在限位沿17内水平窜动移动，并且漏盘21侧部还安装有缓冲碰撞冲击的橡胶环22；
搅拌器31上固定连接有两个圆盘，搅拌器31贯穿漏盘21后，形成穿孔，该穿孔的内侧与搅拌器31主体转轴的外侧之间留有漏盘21横向窜动的间隙，两个圆盘分别位于穿孔的上下两侧，在漏盘21横向窜动过程中，圆盘将穿孔进行封堵；
其中一个内壁刮板51上固定连接有连接座71，连接座71上滑动连接有按压器72，连接座71和按压器72之间固定连接有弹簧；
弹簧带动按压器72对漏盘21进行推动，在搅拌器31以自身的轴线为轴进行转动的过程中，按压器72对漏盘21进行扭动处理，使漏盘21内的物料与搅拌棒33之间充分接触，增加蜂胶原料的分散效果和溶解效果。
参照图13-14所示，说明本发明提供的环保防腐剂制备方法中对于蜂胶等原料在溶剂中分散和残留物在内壁上的刮动处理步骤中使用到的蜂胶分散设备，增加原料在漏盘21内的抖落性能的实施例：
按压器72上设置有球形凸起，球形凸起与漏盘21周侧的漏孔抵接配合，在按压器72对漏盘21进行扭动处理过程中，起到对漏盘21震动处理的作用，增加漏盘21内的物料漏下效果。

Claims (10)

1.一种环保防腐剂制备方法，其特征在于：包括以下步骤：
步骤一：将蜂胶原料投入至处理容器内的漏盘(21)中；
步骤二：向漏盘(21)内缓慢注入溶剂物料，并对蜂胶原料进行搅动，使其分散溶解；
步骤三：利用安装在处理容器外侧的加热器(18)，提供处理容器内的物料易于溶解所需的温度；
步骤四：将粘覆在处理容器内壁的物料刮下；
步骤五：物料粘稠度合格后排出收集，涂覆在食品表面进行防腐处理。
2.根据权利要求1所述的环保防腐剂制备方法，其特征在于：所述处理容器包括混合罐(12)，混合罐(12)顶部设置的盖(13)上转动连接有搅拌器(31)，盖(13)的下侧安装有漏盘(21)，搅拌器(31)贯穿漏盘(21)，混合罐(12)底部转动连接有平衡器(41)，平衡器(41)与搅拌器(31)的端部插接配合，使平衡器(41)和搅拌器(31)之间能够同步转动，将搅拌器(31)和盖(13)一同从混合罐(12)上拆离，进行搅拌器(31)的工作状态和清洗状态的切换。
3.根据权利要求2所述的环保防腐剂制备方法，其特征在于：所述搅拌器(31)通过自身上的H型结构卡在盖(13)上，搅拌器(31)的侧部固定连接有用于对物料进行搅动的U型臂(32)和搅拌棒(33)。
4.根据权利要求2所述的环保防腐剂制备方法，其特征在于：所述搅拌器(31)的下端固定连接有多边形柱，平衡器(41)上设置有插孔，多边形柱与插孔之间插接配合。
5.根据权利要求2所述的环保防腐剂制备方法，其特征在于：所述加热器(18)通过环形支架固定连接在混合罐(12)外侧，且均匀分布设置有多个。
6.根据权利要求2所述的环保防腐剂制备方法，其特征在于：所述平衡器(41)上安装有多个L型臂(42)。
7.根据权利要求6所述的环保防腐剂制备方法，其特征在于：所述L型臂(42)上横向滑动连接有内壁刮板(51)。
8.根据权利要求2所述的环保防腐剂制备方法，其特征在于：所述平衡器(41)上滑动连接有控制盘(43)，控制盘(43)上安装有底部刮动臂(53)，底部刮动臂(53)通过扭簧组件转动连接在控制盘(43)上，底部刮动臂(53)的侧部与混合罐(12)底部抵接连接。
9.根据权利要求8所述的环保防腐剂制备方法，其特征在于：所述底部刮动臂(53)端部铰接连接有铰接杆(52)，铰接杆(52)与内壁刮板(51)滑动连接。
10.利用权利要求2所述的环保防腐剂制备方法所制备出的环保防腐剂，其特征在于：该环保防腐剂的组成包括：按照质量份数取蜂胶5～10份、食用酒精20～50份、山梨酸钾0.8～2.3份、对羟基苯甲酸丙酯1.2～1.8份和对羟基苯甲酸乙酯2～5份。
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CN117816010B (zh) * 2024-03-05 2024-05-07 天津星宇医药科技有限公司 一种适用于航天员的食品配料罐及制备方法

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