CN116084210A - Cigarette for improving sensory quality of cigarette, biological cigarette paper and preparation process - Google Patents
Cigarette for improving sensory quality of cigarette, biological cigarette paper and preparation process Download PDFInfo
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- CN116084210A CN116084210A CN202310369435.2A CN202310369435A CN116084210A CN 116084210 A CN116084210 A CN 116084210A CN 202310369435 A CN202310369435 A CN 202310369435A CN 116084210 A CN116084210 A CN 116084210A
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- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H27/00—Special paper not otherwise provided for, e.g. made by multi-step processes
- D21H27/18—Paper- or board-based structures for surface covering
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H11/00—Pulp or paper, comprising cellulose or lignocellulose fibres of natural origin only
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H17/00—Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
- D21H17/005—Microorganisms or enzymes
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H17/00—Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
- D21H17/63—Inorganic compounds
- D21H17/67—Water-insoluble compounds, e.g. fillers, pigments
- D21H17/675—Oxides, hydroxides or carbonates
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H21/00—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties
- D21H21/14—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties characterised by function or properties in or on the paper
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- Life Sciences & Earth Sciences (AREA)
- Microbiology (AREA)
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Paper (AREA)
Abstract
The invention provides a cigarette for improving the sensory quality of the cigarette, biological cigarette paper and a preparation process thereof, belonging to the technical field of material processing and cigarette production. The preparation process comprises the following steps: and respectively adding 0.1-0.3% of composite biological enzyme preparation into the needle pulp fiber slurry and the broadleaf pulp fiber slurry according to the weight percentage, carrying out biological enzyme fermentation, pulping and mixing the needle pulp fiber slurry and the broadleaf pulp fiber slurry to obtain mixed slurry, and carrying out papermaking, coating sizing and rewinding slitting processes on the mixed slurry to obtain the biological cigarette paper. By adding the composite biological enzyme preparation in a certain proportion in the cigarette paper making process, the cigarette paper is obtained and then the rolled cigarette with a certain specification is manufactured, so that the sensory quality of the cigarette can be improved, the irritation and miscellaneous gases are reduced, and the flexibility of smoke is improved.
Description
Technical Field
The invention belongs to the technical field of material processing and cigarette production, relates to a preparation process of cigarette paper, and in particular relates to biological cigarette paper and a preparation process thereof, and a cigarette for improving sensory quality of the cigarette.
Background
The cigarette paper is a sheet paper specially used for wrapping tobacco to make cigarettes. The cigarette paper mainly comprises fibers and inorganic filler, wherein the cellulose accounts for more than 70% of the total weight. Compared with other cigarette auxiliary materials such as tipping paper and forming paper, the main characteristic of the cigarette paper is that the cigarette paper participates in combustion, and in the process of the cigarette paper participating in combustion, the cigarette paper can have important influence on smoke components of cigarettes.
In the cigarette industry, more cigarette paper is used as wood pulp cigarette paper, wood pulp mainly depends on import, the price of the imported wood pulp is greatly influenced by the international market, and the price of the imported wood pulp often fluctuates greatly, so that the stability of the production cost of a cigarette paper manufacturing enterprise is influenced. The main function of the cigarette paper is to wrap tobacco shreds, and a certain amount of woody gas and pungent taste are generated in the combustion process of the cigarette so as to influence the smoking taste of the cigarette smoke, and the cigarette paper has little contribution to the richness of the smoking taste of the cigarette. Part of high-end cigarette brands use the hemp pulp cigarette paper, and the hemp pulp cigarette paper has the advantages of less irritation and miscellaneous gas caused by combustion, but higher cost.
At present, various improved cigarette papers are added with different function improvers, additives and the like. These modifiers, additives are often various synthetic fragrances or extracts, which are costly to prepare. Moreover, the different aromas produced by different additives are not acceptable to all smokers. Thus, these modified cigarette papers, while improved and advantageous in some respects, are not particularly widely used due to the cost of their manufacturing process.
Microorganisms, enzymes, often play an important role in the growth, conditioning, aging, processing and storage of tobacco leaves, improving the quality of tobacco leaves, stems and tobacco flakes, producing flavors and degrading nicotine by microorganisms or enzymes. Chinese patent CN 101775379A discloses an enzyme preparation taking nicotine dehydrogenase as an auxiliary for tobacco processing and a preparation and application method thereof, and the patent utilizes the nicotine dehydrogenase enzyme preparation in the processing process before redrying after fresh tobacco is roasted to degrade nicotine so as to achieve the effect of improving the quality of the tobacco in industrial production. However, no enzyme or microorganism has been added to the cigarette paper to improve the cigarette paper performance.
In recent years, with the improvement of living standard, consumers have pursued higher sensory quality of cigarettes. The cigarette paper is an important part affecting the sensory quality of cigarettes, how to adjust and improve the performance of the cigarette paper, reduce or utilize the smell generated by other substances to cover the wooden gas generated by the combustion of common cigarette paper, improve the sensory quality of cigarettes and reduce the production cost of the cigarette paper, which is the key point of developing and improving the production of the cigarette paper.
Disclosure of Invention
Aiming at the defects in the prior art, the invention provides a cigarette for improving the sensory quality of the cigarette, biological cigarette paper and a preparation process thereof. By adding a certain proportion of the compound biological enzyme preparation, the sensory quality of the cigarette paper can be improved, the irritation and miscellaneous gases are reduced, the flexibility of smoke is improved, and the production cost is reduced.
In order to solve the above problems, an aspect of the present invention provides a preparation process of biological cigarette paper, the preparation process comprising the steps of: adding 0.1-0.3% of composite biological enzyme preparation into needle pulp fiber slurry and broadleaf pulp fiber slurry respectively, performing biological enzyme fermentation, pulping the needle pulp fiber slurry and the broadleaf pulp fiber slurry respectively, mixing to obtain mixed pulp, and papermaking by using the mixed pulp to obtain biological cigarette paper. In addition, the preparation process can further carry out coating sizing and rewinding slitting treatment on the biological cigarette paper so as to obtain the cigarette paper which can be directly used for wrapping cut tobacco.
The invention also provides biological cigarette paper which is prepared by the preparation method. The biological cigarette paper is composed of, by weight, 10-35 parts of needle pulp fibers, 20-70 parts of broadleaf pulp fibers, 20-40 parts of calcium carbonate and 3-6 parts of water.
In yet another aspect, the invention provides a cigarette for improving the sensory quality of the cigarette, said cigarette comprising a biological cigarette paper and cut filler composition as described in any of the above.
The beneficial effects of the invention include at least one of the following:
1. according to the preparation process of the biological cigarette paper, in the papermaking process of the cigarette paper, the sensory quality of the cigarette paper can be improved, the irritation and miscellaneous gases are reduced, and the flexibility of smoke is improved by adding a certain proportion of the compound biological enzyme preparation;
2. the wood pulp raw material is processed by the biotechnology to prepare the biological cigarette paper, so that the problems of irritation, miscellaneous gases and the like caused by the combustion of the cigarette paper can be effectively reduced after the cigarette is rolled, the sensory quality of the cigarette is improved, and the sensory quality is superior to that of the wood pulp cigarette paper;
3. the biological cigarette paper of the application is used for replacing cigarettes made of wood pulp cigarette paper, so that the sensory quality of the cigarettes can be improved, and the production cost of the cigarettes is greatly reduced.
Detailed Description
In order to more clearly illustrate the general inventive concept, a detailed description is given below by way of example.
In the following description, numerous specific details are set forth in order to provide a thorough understanding of the present invention, however, the present invention may be practiced in other ways than those described herein, and therefore the scope of the present invention is not limited to the specific embodiments disclosed below.
In the present invention, unless expressly stated or limited otherwise, a first feature "up" or "down" a second feature may be the first and second features in direct contact, or the first and second features in indirect contact via an intervening medium. In the description of the present specification, a description referring to terms "one embodiment," "some embodiments," "examples," "specific examples," or "some examples," etc., means that a particular feature, structure, material, or characteristic described in connection with the embodiment or example is included in at least one embodiment or example of the present invention. In this specification, schematic representations of the above terms are not necessarily directed to the same embodiment or example. Furthermore, the particular features, structures, materials, or characteristics described may be combined in any suitable manner in any one or more embodiments or examples.
In one exemplary embodiment of the present invention, the process of preparing the bio-cigarette paper may be accomplished by the following steps.
(1) Biological enzyme fermentation
The compound biological enzyme preparation is prepared by mixing lignin-reducing enzyme systems and pectase systems according to the mass ratio of (1-9) to (1-9). The wood pulp has high lignin and pectin content, and the lignin is pyrolyzed to generate catechol, phenol and alkyl catechol, which can generate astringent taste, and the woody smell has cancer promotion activity, and the pectin is pyrolyzed to harmful substances such as methanol carbonyl and the like, so that the cigarette is choked and stimulated. The chemical components can influence the sensory quality of cigarettes, and the lignin and pectin content in the cigarette paper pulp can be effectively reduced by using a lignin-reducing enzyme system and a pectin-reducing enzyme system, so that the irritation and miscellaneous gases caused by the combustion of the cigarette paper are reduced, the purity of smoke is improved, and the sensory quality of cigarettes is improved.
Wherein the lignin reducing enzyme system comprises any one or more of cellulase, lignin catalase, wood flour softening enzyme, xylanase, laccase and lignin enzyme I, however, the invention is not limited to the above. The components of the pectase-reducing enzyme system are any one or more of pentosanase, glucanase, pectinesterase, polygalacturonase and pectin lyase, however, the invention is not limited to the above. The enzymes in the lignin-lowering enzyme system and the pectin-lowering enzyme system are extracted from animals, plants and microorganisms, however, the present invention is not limited thereto.
The enzyme activity of the composite biological enzyme preparation is 50000-200000 u/g, the enzyme activity refers to the ability of the enzyme to catalyze a certain specific reaction under certain conditions, namely the enzyme activity, and the enzyme activity is a characteristic exclusive index for expressing enzyme preparation products.
And (3) respectively adding the composite biological enzyme preparation with the weight percentage of 0.1-0.3% into the needle pulp fiber slurry and the broadleaf pulp fiber slurry for biological enzyme fermentation. The fermentation time of the biological enzyme is 1-5 h, and the fermentation temperature is 30-70 ℃; preferably, the fermentation time of the biological enzyme is 1-3 hours, and the fermentation temperature is 35-60 ℃. Experiments prove that the temperature is in a temperature range of 35-60 ℃ which is the optimal temperature range of the activity of the selected composite biological enzyme preparation, the fermentation time can reach the target fermentation effect after 1 hour, and the sensory quality can be negatively influenced after more than 5 hours.
(2) Preparation of mixed pulp
Pulping the needle pulp fiber slurry for 2-4 times; preferably, the needle pulp fiber slurry is pulped for 2-3 times. Pulping the broadleaf pulp fiber slurry for 1-2 times; preferably, the broadleaf pulp fiber slurry is pulped 1 time. And then, mixing 10-35 parts of needle pulp fibers, 20-70 parts of broadleaf pulp fibers, 20-40 parts of calcium carbonate and 3-6 parts of water by weight to obtain mixed paper pulp. The calcium carbonate is added mainly for improving the air permeability of the cigarette paper, and adjusting the combustion speed and the combustion uniformity of the cigarette paper to adapt to the combustion of tobacco.
(3) Papermaking forming process
And (3) carrying out papermaking, sizing coating and rewinding slitting processes on the mixed paper pulp to obtain the biological cigarette paper.
The papermaking forming process specifically comprises pulping, pulp mixing, filler adding, net part pressing, drying cylinder, sizing, drying cylinder, roll paper, rewinding, slitting and packaging.
The biological cigarette paper and the tobacco shred are used for preparing the cigarette. Wherein the cut tobacco can be prepared from tobacco leaf fermented by adding biological enzyme preparation. The biological enzyme preparation is any one or more of cellulase, protease, alpha-amylase, glucanase and flavonoid synthase, however, the present invention is not limited thereto. The dosage of the biological enzyme preparation is 1-6% of the weight of the tobacco leaf. The fermentation environment is as follows: and (3) standing and fermenting for 24-72 h under the environment of 40-50 ℃ and 60-80% of humidity. The circumference diameter of the cigarette is 15-30 mm; preferably, the diameter of the circumference of the cigarette is 17-27 mm.
Example 1
The biological cigarette paper samples No. 1-No. 9 are prepared by the method.
Sample 1#
(1) Biological enzyme fermentation
The compound biological enzyme preparation is prepared by mixing cellulase and pentosanase according to a mass ratio of 4:1. The enzyme activity of the composite biological enzyme preparation is 100000 u/g. The composite biological enzyme preparation with the weight percentage of 0.3 percent is respectively added into the needle pulp fiber slurry and the broadleaf pulp fiber slurry for biological enzyme fermentation. The bio-enzyme fermentation time is 3 h and the temperature is 45 ℃.
(2) Preparation of mixed pulp
Pulping needle pulp fiber slurry for 2 times, and pulping broad leaf pulp fiber slurry for 1 time. Subsequently, 15 parts by weight of needle pulp fiber slurry, 45 parts by weight of broadleaf pulp fiber slurry, 35 parts by weight of calcium carbonate, and 5 parts by weight of water were mixed to obtain mixed pulp.
(3) Papermaking forming process
And (3) carrying out papermaking, sizing coating and rewinding slitting processes on the mixed paper pulp to obtain a biological cigarette paper sample No. 1.
Sample 2 #)
(1) Biological enzyme fermentation
The compound biological enzyme preparation lignin enzyme I, cellulase and pectin esterase and pectin lyase are mixed according to the mass ratio of 5:1. The enzyme activity of the composite biological enzyme preparation is 100000 u/g. The composite biological enzyme preparation with the weight percentage of 0.3 percent is respectively added into the needle pulp fiber slurry and the broadleaf pulp fiber slurry for biological enzyme fermentation. The bio-enzyme fermentation time is 3 h and the temperature is 45 ℃.
(2) Preparation of mixed pulp
Pulping needle pulp fiber slurry for 2 times, and pulping broad leaf pulp fiber slurry for 1 time. Subsequently, 15 parts by weight of needle pulp fiber slurry, 45 parts by weight of broadleaf pulp fiber slurry, 35 parts by weight of calcium carbonate, and 5 parts by weight of water were mixed to obtain mixed pulp.
(3) Papermaking forming process
And (3) carrying out papermaking, sizing coating and rewinding slitting processes on the mixed paper pulp to obtain a biological cigarette paper sample No. 2.
Sample 3 #)
(1) Biological enzyme fermentation
The compound biological enzyme preparation is prepared by mixing wood flour softening enzyme and pectin esterase according to a mass ratio of 6:1. The enzyme activity of the composite biological enzyme preparation is 100000 u/g. The composite biological enzyme preparation with the weight percentage of 0.3 percent is respectively added into the needle pulp fiber slurry and the broadleaf pulp fiber slurry for biological enzyme fermentation. The bio-enzyme fermentation time is 3 h and the temperature is 45 ℃.
(2) Preparation of mixed pulp
Pulping needle pulp fiber slurry for 2 times, and pulping broad leaf pulp fiber slurry for 1 time. Subsequently, 15 parts by weight of needle pulp fiber slurry, 45 parts by weight of broadleaf pulp fiber slurry, 35 parts by weight of calcium carbonate, and 5 parts by weight of water were mixed to obtain mixed pulp.
(3) Papermaking forming process
And (3) carrying out papermaking, sizing coating and rewinding slitting processes on the mixed paper pulp to obtain a biological cigarette paper sample No. 3.
Sample 4 #)
(1) Biological enzyme fermentation
The compound biological enzyme preparation is prepared by mixing lignin enzyme I and pectin esterase according to a mass ratio of 6:1. The enzyme activity of the composite biological enzyme preparation is 100000 u/g. The composite biological enzyme preparation with the weight percentage of 0.2 percent is respectively added into the needle pulp fiber slurry and the broadleaf pulp fiber slurry for biological enzyme fermentation. The bio-enzyme fermentation time is 3 h and the temperature is 45 ℃.
(2) Preparation of mixed pulp
Pulping needle pulp fiber slurry for 2 times, and pulping broad leaf pulp fiber slurry for 1 time. Subsequently, 15 parts by weight of needle pulp fiber slurry, 45 parts by weight of broadleaf pulp fiber slurry, 35 parts by weight of calcium carbonate, and 5 parts by weight of water were mixed to obtain mixed pulp.
(3) Papermaking forming process
And (3) carrying out papermaking, sizing coating and rewinding slitting processes on the mixed paper pulp to obtain a biological cigarette paper sample No. 4.
Sample 5 #)
(1) Biological enzyme fermentation
The compound biological enzyme preparation is prepared by mixing laccase, lignin enzyme I, pentosanase and glucanase according to a mass ratio of 5:1. The enzyme activity of the composite biological enzyme preparation is 100000 u/g. The composite biological enzyme preparation with the weight percentage of 0.1 percent is respectively added into the needle pulp fiber slurry and the broadleaf pulp fiber slurry for biological enzyme fermentation. The bio-enzyme fermentation time is 3 h and the temperature is 45 ℃.
(2) Preparation of mixed pulp
Pulping needle pulp fiber slurry for 2 times, and pulping broad leaf pulp fiber slurry for 1 time. Subsequently, 15 parts by weight of needle pulp fiber slurry, 45 parts by weight of broadleaf pulp fiber slurry, 35 parts by weight of calcium carbonate, and 5 parts by weight of water were mixed to obtain mixed pulp.
(3) Papermaking forming process
And (3) carrying out papermaking, sizing coating and rewinding slitting processes on the mixed paper pulp to obtain a biological cigarette paper sample No. 5.
Sample 6#
(1) Biological enzyme fermentation
The compound biological enzyme preparation is prepared by mixing cellulase, lignin catalase, wood flour softening enzyme and pectin lyase according to a mass ratio of 6:1. The enzyme activity of the composite biological enzyme preparation is 100000 u/g. The composite biological enzyme preparation with the weight percentage of 0.1 percent is respectively added into the needle pulp fiber slurry and the broadleaf pulp fiber slurry for biological enzyme fermentation. The bio-enzyme fermentation time is 3 h and the temperature is 45 ℃.
(2) Preparation of mixed pulp
Pulping needle pulp fiber slurry for 2 times, and pulping broad leaf pulp fiber slurry for 1 time. Subsequently, 15 parts by weight of needle pulp fiber slurry, 45 parts by weight of broadleaf pulp fiber slurry, 35 parts by weight of calcium carbonate, and 5 parts by weight of water were mixed to obtain mixed pulp.
(3) Papermaking forming process
And (3) carrying out papermaking, sizing coating and rewinding slitting processes on the mixed paper pulp to obtain a biological cigarette paper sample No. 6.
Sample 7 #)
(1) Biological enzyme fermentation
The compound biological enzyme preparation is prepared by mixing laccase and pectase and polygalacturonase according to a mass ratio of 5:1. The enzyme activity of the composite biological enzyme preparation is 100000 u/g. The composite biological enzyme preparation with the weight percentage of 0.1 percent is respectively added into the needle pulp fiber slurry and the broadleaf pulp fiber slurry for biological enzyme fermentation. The bio-enzyme fermentation time is 3 h and the temperature is 45 ℃.
(2) Preparation of mixed pulp
Pulping needle pulp fiber slurry for 2 times, and pulping broad leaf pulp fiber slurry for 1 time. Subsequently, 20 parts by weight of needle pulp fiber slurry, 40 parts by weight of broadleaf pulp fiber slurry, 35 parts by weight of calcium carbonate, and 5 parts by weight of water were mixed to obtain mixed pulp.
(3) Papermaking forming process
And (3) carrying out papermaking, sizing coating and rewinding slitting processes on the mixed paper pulp to obtain a biological cigarette paper sample No. 7.
Sample 8 #)
(1) Biological enzyme fermentation
The compound biological enzyme preparation is prepared by mixing wood flour softening enzyme, xylanase, glucanase, pectin lyase and polygalacturonase according to a mass ratio of 6:1. The enzyme activity of the composite biological enzyme preparation is 100000 u/g. The composite biological enzyme preparation with the weight percentage of 0.1 percent is respectively added into the needle pulp fiber slurry and the broadleaf pulp fiber slurry for biological enzyme fermentation. The bio-enzyme fermentation time is 3 h and the temperature is 45 ℃.
(2) Preparation of mixed pulp
Pulping needle pulp fiber slurry for 2 times, and pulping broad leaf pulp fiber slurry for 1 time. Subsequently, 20 parts by weight of needle pulp fiber slurry, 40 parts by weight of broadleaf pulp fiber slurry, 35 parts by weight of calcium carbonate, and 5 parts by weight of water were mixed to obtain mixed pulp.
(3) Papermaking forming process
And (3) carrying out papermaking, sizing coating and rewinding slitting processes on the mixed paper pulp to obtain a biological cigarette paper sample No. 8.
Sample 9 #)
(1) Biological enzyme fermentation
The compound biological enzyme preparation is prepared by mixing xylanase, lignin catalase and polygalacturonase according to a mass ratio of 5:1. The enzyme activity of the composite biological enzyme preparation is 100000 u/g. The composite biological enzyme preparation with the weight percentage of 0.1 percent is respectively added into the needle pulp fiber slurry and the broadleaf pulp fiber slurry for biological enzyme fermentation. The bio-enzyme fermentation time is 3 h and the temperature is 45 ℃.
(2) Preparation of mixed pulp
Pulping needle pulp fiber slurry for 2 times, and pulping broad leaf pulp fiber slurry for 1 time. Subsequently, 25 parts by weight of needle pulp fiber slurry, 35 parts by weight of broadleaf pulp fiber slurry, 35 parts by weight of calcium carbonate, and 5 parts by weight of water were mixed to obtain mixed pulp.
(3) Papermaking forming process
And (3) carrying out papermaking, sizing coating and rewinding slitting processes on the mixed paper pulp to obtain a biological cigarette paper sample No. 9.
Contrast cigarette paper D1#
The wood pulp type cigarette paper on the market is selected as the contrast cigarette paper D1#.
Example 2
The biological cigarette papers 1# to 9# and the comparison cigarette papers D1# in the example 1 are processed and prepared together with tobacco shreds by using a cigarette making machine with the model ZJ17 provided by Changde tobacco machinery Limited company, and cigarettes 10# to 18# and comparison cigarettes D2# with the circumference diameter of 20 mm are sequentially and correspondingly obtained, wherein the tobacco shreds are prepared from tobacco leaves fermented by adding a biological enzyme. The biological enzyme preparation comprises cellulase, protease, alpha-amylase, glucanase and flavonoid synthetase, the dosage of the biological enzyme preparation is 3% of the weight of tobacco leaves, and the fermentation environment is: and (3) standing and fermenting for 36h at the temperature of 45 ℃ and the humidity of 70%.
Test 1 physicochemical Property detection
Physical and chemical property detection is carried out on biological cigarette paper 1# to 9# and comparison cigarette paper D1# prepared in the example 1, and a cigarette paper index statistical table and a cigarette paper chemical composition index statistical table shown in the table 1 are obtained.
Table 1 cigarette paper index statistics table
Table 2 statistical table of chemical composition index of cigarette paper
As shown in Table 1, the indexes of the biological cigarette paper No. 1-9 are smaller in numerical difference compared with the comparative cigarette paper D1, even some indexes are better than D1, and the energy absorption of No. 1-9 is higher than D1 in energy absorption indexes. The biological cigarette paper obtained by the preparation method of the application has stable indexes and reaches the standard of cigarette paper on the market.
As shown in Table 2, compared with the comparative cigarette paper D1#, the chemical components of the biological cigarette paper 1# -9# are smaller than the lignin and pectin content of D1#, which means that the biological cigarette paper prepared by the preparation method reduces the lignin and pectin content of wood pulp, for example, the lignin and pectin content of wood pulp can be correspondingly controlled to 65-86% and 50-74% of the original content respectively, so that the influence of woody gas and tingling and hot feeling in the cigarette paper on the smoke taste of cigarettes is reduced.
Test 2 sensory quality evaluation
17 professional sensory evaluation workers are randomly selected, and sensory quality evaluation is carried out on cigarettes 10# to 18# and comparison cigarettes D2# prepared in example 2. The sensory quality of the cigarette disclosed by the invention is referred to in GB 5606.4-2005 part 4: the cigarette sensory quality judgment standard in the sensory technology requirements comprises the following steps: the gloss, fragrance, harmony, miscellaneous odor, irritation and aftertaste, and specific evaluation criteria are shown in Table 3.
Table 3 criteria for judging the sensory quality of cigarettes
And scoring the sensory quality of cigarettes 10# to 18# and the sensory quality of comparison cigarettes D2# by a professional sensory evaluator according to the sensory quality evaluation criteria of cigarettes in Table 3, and calculating an average value as a final comprehensive score to obtain a cigarette sensory quality evaluation table as shown in Table 4.
Table 4 sensory quality evaluation table of cigarettes
As shown in Table 4, compared with the comparative cigarette D2#, the scores of the three evaluation criteria of 10# -18 # aroma, miscellaneous gas and irritation are all higher than D2#, and the combined score of 10# -18 # is also higher than D2#, and is all over 91.
The cigarette made of the biological cigarette paper can effectively reduce the problems of irritation, miscellaneous gases and the like caused by the combustion of the cigarette paper, improve the sensory quality of the cigarette, and has better sensory quality than wood pulp cigarette paper.
Test 3 flue gas index test
And (3) carrying out smoke index detection on cigarettes 10# to 18# and comparison cigarettes D2# prepared in the embodiment 2, and obtaining a cigarette smoke index statistical table shown in Table 5.
Table 5 statistics of cigarette smoke index
As shown in Table 5, compared with the D2# smoke of the comparison cigarettes, the tar, nicotine, carbon monoxide and water in the 10# to 18# smoke of the cigarettes have smaller numerical differences, which indicates that the cigarette smoke prepared by the biological cigarette paper has stable indexes and reaches the standards of the cigarette paper on the market.
The foregoing is merely exemplary of the present invention and is not intended to limit the present invention. Various modifications and variations of the present invention will be apparent to those skilled in the art. Any modification, equivalent replacement, improvement, etc. which come within the spirit and principles of the invention are to be included in the scope of the claims of the present invention.
Claims (10)
1. A preparation process of biological cigarette paper, which is characterized by comprising the following steps:
adding 0.1-0.3% of composite biological enzyme preparation into needle pulp fiber slurry and broadleaf pulp fiber slurry respectively, performing biological enzyme fermentation, pulping the needle pulp fiber slurry and the broadleaf pulp fiber slurry respectively, mixing to obtain mixed pulp, and papermaking by using the mixed pulp to obtain biological cigarette paper.
2. The process for preparing biological cigarette paper according to claim 1, wherein the enzyme activity of the composite biological enzyme preparation is 50000-200000 u/g; the compound biological enzyme preparation is formed by mixing a lignin-reducing enzyme system and a pectin-reducing enzyme system according to the mass ratio of (1-9) to (1-9).
3. The process for preparing biological cigarette paper according to claim 2, wherein the lignin reducing enzyme system comprises one or more of cellulase, lignin catalase, wood flour softening enzyme, xylanase, laccase and lignin enzyme I; the pectase-reducing enzyme system comprises one or more of pentosanase, glucanase, pectase, polygalacturonase and pectolytic enzyme.
4. The process for preparing biological cigarette paper according to claim 1, wherein the fermentation time of the biological enzyme is 1-5 h, and the fermentation temperature is 30-70 ℃.
5. The process for preparing biological cigarette paper according to claim 1, wherein the beating times of the needle pulp fiber slurry are 2-4 times, and the beating times of the broadleaf pulp fiber slurry are 1-2 times.
6. A biological cigarette paper, characterized in that the biological cigarette paper is prepared by the preparation method according to any one of claims 1-5.
7. The biological cigarette paper of claim 6, wherein the biological cigarette paper is composed of 10-35 parts by weight of needle pulp fibers after biological fermentation, 20-70 parts by weight of broadleaf pulp fibers after biological fermentation, 20-40 parts by weight of calcium carbonate, and 3-6 parts by weight of water.
8. A cigarette for improving the sensory quality of the cigarette, which is characterized by comprising the biological cigarette paper and tobacco shreds according to any one of claims 6-7.
9. The cigarette of claim 8, wherein the tobacco cut filler is made from tobacco leaf fermented with a biological enzyme preparation.
10. The cigarette of claim 8, wherein the cigarette has a circumferential diameter of 15-30 mm.
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| Application Number | Priority Date | Filing Date | Title |
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| CN202310369435.2A CN116084210A (en) | 2023-04-10 | 2023-04-10 | Cigarette for improving sensory quality of cigarette, biological cigarette paper and preparation process |
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| CN202310369435.2A CN116084210A (en) | 2023-04-10 | 2023-04-10 | Cigarette for improving sensory quality of cigarette, biological cigarette paper and preparation process |
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Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101775379A (en) * | 2010-01-20 | 2010-07-14 | 云南万芳生物技术有限公司 | Enzyme preparation using nicotine dehydrogenase to assist tobacco processing, and preparation and use methods |
| CN103726410A (en) * | 2013-12-28 | 2014-04-16 | 蚌埠卷烟材料厂 | Application of corn wrapping in filter rod grooved paper |
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