CN115725203A - Orange printing ink and preparation method thereof - Google Patents
Orange printing ink and preparation method thereof Download PDFInfo
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- CN115725203A CN115725203A CN202111010229.XA CN202111010229A CN115725203A CN 115725203 A CN115725203 A CN 115725203A CN 202111010229 A CN202111010229 A CN 202111010229A CN 115725203 A CN115725203 A CN 115725203A
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- 238000002360 preparation method Methods 0.000 title abstract description 6
- 239000003921 oil Substances 0.000 claims abstract description 33
- 235000019198 oils Nutrition 0.000 claims abstract description 33
- 239000002002 slurry Substances 0.000 claims abstract description 13
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 claims abstract description 12
- 229910052791 calcium Inorganic materials 0.000 claims abstract description 12
- 239000011575 calcium Substances 0.000 claims abstract description 12
- 239000004698 Polyethylene Substances 0.000 claims abstract description 11
- 239000001053 orange pigment Substances 0.000 claims abstract description 11
- -1 polyethylene Polymers 0.000 claims abstract description 11
- 229920000573 polyethylene Polymers 0.000 claims abstract description 11
- 239000011347 resin Substances 0.000 claims abstract description 11
- 229920005989 resin Polymers 0.000 claims abstract description 11
- 235000012424 soybean oil Nutrition 0.000 claims abstract description 11
- 239000003549 soybean oil Substances 0.000 claims abstract description 11
- 239000001052 yellow pigment Substances 0.000 claims abstract description 11
- 239000002994 raw material Substances 0.000 claims abstract description 9
- 239000000049 pigment Substances 0.000 claims description 23
- 238000003756 stirring Methods 0.000 claims description 13
- 238000000034 method Methods 0.000 claims description 10
- 229910017052 cobalt Inorganic materials 0.000 claims description 7
- 239000010941 cobalt Substances 0.000 claims description 7
- GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt atom Chemical compound [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 claims description 7
- 238000000227 grinding Methods 0.000 claims description 7
- XOFYZVNMUHMLCC-ZPOLXVRWSA-N prednisone Chemical compound O=C1C=C[C@]2(C)[C@H]3C(=O)C[C@](C)([C@@](CC4)(O)C(=O)CO)[C@@H]4[C@@H]3CCC2=C1 XOFYZVNMUHMLCC-ZPOLXVRWSA-N 0.000 claims description 7
- PWHULOQIROXLJO-UHFFFAOYSA-N Manganese Chemical compound [Mn] PWHULOQIROXLJO-UHFFFAOYSA-N 0.000 claims description 6
- 229910052748 manganese Inorganic materials 0.000 claims description 6
- 239000011572 manganese Substances 0.000 claims description 6
- 238000002156 mixing Methods 0.000 claims description 3
- 239000000758 substrate Substances 0.000 claims description 3
- 235000005206 Hibiscus Nutrition 0.000 description 19
- 241000218033 Hibiscus Species 0.000 description 19
- 235000007185 Hibiscus lunariifolius Nutrition 0.000 description 19
- GTRGJJDVSJFNTE-UHFFFAOYSA-N chembl2009633 Chemical compound OC1=CC=C2C=C(S(O)(=O)=O)C=CC2=C1N=NC1=CC=CC=C1 GTRGJJDVSJFNTE-UHFFFAOYSA-N 0.000 description 19
- 238000005259 measurement Methods 0.000 description 4
- 239000000463 material Substances 0.000 description 3
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 description 2
- 239000003086 colorant Substances 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 238000001035 drying Methods 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 244000130592 Hibiscus syriacus Species 0.000 description 1
- 235000018081 Hibiscus syriacus Nutrition 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 239000012752 auxiliary agent Substances 0.000 description 1
- 229910000019 calcium carbonate Inorganic materials 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000001459 lithography Methods 0.000 description 1
- WPBNNNQJVZRUHP-UHFFFAOYSA-L manganese(2+);methyl n-[[2-(methoxycarbonylcarbamothioylamino)phenyl]carbamothioyl]carbamate;n-[2-(sulfidocarbothioylamino)ethyl]carbamodithioate Chemical compound [Mn+2].[S-]C(=S)NCCNC([S-])=S.COC(=O)NC(=S)NC1=CC=CC=C1NC(=S)NC(=O)OC WPBNNNQJVZRUHP-UHFFFAOYSA-L 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000004806 packaging method and process Methods 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 239000011265 semifinished product Substances 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 238000003325 tomography Methods 0.000 description 1
Images
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- Inks, Pencil-Leads, Or Crayons (AREA)
Abstract
The invention provides orange printing ink and a preparation method thereof. The orange printing ink comprises the following raw materials in percentage by weight: 29 to 35 percent of resin oil, 1 to 2 percent of nano calcium, 8 to 9 percent of medium yellow pigment, 3.4 to 4 percent of orange pigment, 1.5 to 2.5 percent of polyethylene wax, 12 to 14 percent of soybean oil, 20 to 22 percent of gloss oil, 3 to 4 percent of light oil, 13 to 15 percent of fluorescent slurry and 1.5 to 2.5 percent of drier. The orange printing ink provided by the invention has the advantages of high color vividness, high brightness and high chroma.
Description
Technical Field
The application relates to the technical field of printing ink, in particular to orange printing ink and a preparation method thereof.
Background
The color target of spot color ink in the offset lithography industry is mainly according to Pantone, DIC, TOYO, HKS, DIN and other color rulers. However, the colors of these color rulers are all specific, and cannot meet all the requirements of printed products in actual production.
The statements in the background section are merely prior art as they are known to the inventors and do not, of course, represent prior art in the field.
Disclosure of Invention
The invention aims to provide a novel Orange ink (called special color ink of hibiscus brilliant Orange) and a preparation method thereof.
The orange printing ink provided by the invention comprises the following raw materials in percentage by weight:
29 to 35 percent of resin oil, 1 to 2 percent of nano calcium, 8 to 9 percent of medium yellow pigment, 3.4 to 4 percent of orange pigment, 1.5 to 2.5 percent of polyethylene wax, 12 to 14 percent of soybean oil, 20 to 22 percent of gloss oil, 3 to 4 percent of light oil, 13 to 15 percent of fluorescent slurry and 1.5 to 2.5 percent of drier.
In some embodiments of the invention, the drier comprises manganese, a type a-drier and cobalt, a type B-drier.
In some embodiments of the invention, the type a drier manganese is present in the orange ink in an amount of 1 to 1.5% and the type B drier cobalt is present in the orange ink in an amount of 0.5 to 1%.
In some embodiments of the present invention, the orange ink comprises the following raw materials in weight percent: 30 to 32 percent of resin oil, 1 to 1.5 percent of nano calcium, 8.3 to 8.6 percent of medium yellow pigment, 3.5 to 3.8 percent of orange pigment, 1.9 to 2.1 percent of polyethylene wax, 12 to 13 percent of soybean oil, 20 to 21 percent of gloss oil, 3 to 3.5 percent of light oil, 14 to 15 percent of fluorescent slurry and 1.5 to 2.5 percent of drier.
In some embodiments of the invention, when the substrate is white double-sided offset paper, the color value of the orange ink after printing is 75.2 degrees, 48.3 degrees, 67.9 degrees, 83.4 degrees and 54.6 degrees; color difference range: the color difference value delta E is less than 1.
The invention provides a preparation method of orange printing ink, which comprises the following steps:
s1: mixing and stirring 29-35% of resin oil, 1-2% of nano calcium, 8-9% of medium yellow pigment, 3.4-4% of orange pigment, 1.5-2.5% of polyethylene wax, 12-14% of soybean oil, 20-22% of gloss oil, 3-4% of light oil and 13-15% of fluorescent slurry until the color is uniform;
s2: after the pigment obtained in the step S1 is fully wetted, grinding the pigment to a required fineness;
s3: and (3) adding 1.5-2.5% of drier into the pigment obtained in the step (S2), and uniformly stirring.
In some embodiments of the invention, in step S2, the pigment is ground to a fineness <10 μm.
In some embodiments of the invention, step S2 comprises: the pigment obtained in step S1 was left for 4 hours or more to sufficiently wet the pigment.
In some embodiments of the invention, the time for stirring in step S1 and step S3 is 30 to 50min.
The special color ink of the hibiscus brilliant orange provided by the invention is high in color brightness, brightness and chroma.
Additional aspects and advantages of the invention will be set forth in part in the description which follows and, in part, will be obvious from the description, or may be learned by practice of the invention.
Drawings
The accompanying drawings, which are included to provide a further understanding of the disclosure, illustrate embodiments of the disclosure and together with the description serve to explain the disclosure and are not to limit the disclosure. In the drawings:
fig. 1 is a schematic process flow diagram of preparing a specialty color ink of hibiscus brilliant orange according to an embodiment of the present invention.
Fig. 2 is a schematic color diagram of the specialty color ink of hibiscus brilliant orange according to an embodiment of the invention.
Fig. 3 is a color schematic of Pantone 2018U.
FIG. 4 (a) is a target orange pattern, and (b) and (c) are schematic illustrations of swatches prepared with the Brilliant orange spot color ink of the present invention and Pantone 2018U, respectively.
Detailed Description
In the following, only certain exemplary embodiments are briefly described. As those skilled in the art will recognize, the described embodiments may be modified in various different ways, all without departing from the spirit or scope of the present invention. Accordingly, the drawings and description are to be regarded as illustrative in nature, and not as restrictive.
The following disclosure provides many different embodiments or examples for implementing different features of the invention. To simplify the disclosure of the present invention, the components and arrangements of specific examples are described below. Of course, they are merely examples and are not intended to limit the present invention. Furthermore, the present invention may repeat reference numerals and/or letters in the various examples, such repetition is for the purpose of simplicity and clarity and does not in itself dictate a relationship between the various embodiments and/or configurations discussed. In addition, the present invention provides examples of various specific processes and materials, but one of ordinary skill in the art may recognize applications of other processes and/or uses of other materials.
The embodiments of the present invention will be described in more detail below with reference to the drawings and examples, so that the aspects of the present invention and the advantages of its various aspects can be better understood. However, the specific embodiments and examples described below are for illustrative purposes only and are not limiting of the invention.
The invention provides a special color ink of hibiscus brilliant orange, which comprises the following raw materials in percentage by weight: 29 to 35 percent of resin oil, 1 to 2 percent of nano calcium, 8 to 9 percent of medium yellow pigment, 3.4 to 4 percent of orange pigment, 1.5 to 2.5 percent of polyethylene wax, 12 to 14 percent of soybean oil, 20 to 22 percent of gloss oil, 3 to 4 percent of light oil, 13 to 15 percent of fluorescent slurry and 1.5 to 2.5 percent of drier.
The nano calcium in the invention refers to nano calcium carbonate; the fluorescent slurry is a slurry liquid prepared by taking fluorescent powder as a main raw material and including other additives, and has a fluorescent effect after being dried.
Wherein the drier may comprise manganese type A drier and cobalt type B drier. Optionally, the content of the type A drier manganese in the special color ink of the hibiscus color orange is 1-1.5%, and the content of the type B drier cobalt in the special color ink of the hibiscus color orange is 0.5-1%.
The preferred formula of the special color ink of the hibiscus brilliant orange provided by the invention is as follows: 30 to 32 percent of resin oil, 1 to 1.5 percent of nano calcium, 8.3 to 8.6 percent of medium yellow pigment, 3.5 to 3.8 percent of orange pigment, 1.9 to 2.1 percent of polyethylene wax, 12 to 13 percent of soybean oil, 20 to 21 percent of gloss oil, 3 to 3.5 percent of light oil, 14 to 15 percent of fluorescent slurry and 1.5 to 2.5 percent of drier.
The printing stock that brilliant orange spot color printing ink of shrubalthea that this application provided was suitable for is white two-sided offset paper. The color value of the special color ink of the hibiscus brilliant orange after printing is 75.2 degrees, 48.3 degrees for a, 67.9 degrees for b and 54.6 degrees for C, 83.4H; color difference range: the color difference value delta E is less than 1; measurement setup: measurement mode M1, illuminant/viewing angle D50/2 DEG, delta E mode CIE Delta 2000. There may be slight variations in substrate color values depending on the batch produced, but the color values of the hibiscus brilliant orange spot color ink of the present application after printing are within the above ranges.
As shown in figure 1, the invention provides a method for preparing the special color ink of hibiscus brilliant orange, which comprises the following steps of S1-S3:
s1: mixing and stirring resin oil, nano calcium, medium yellow pigment, orange pigment, polyethylene wax, soybean oil, gloss oil, light oil and fluorescent slurry until the color is uniform.
Optionally, the above pigments are stirred for 30-50 min by using a planetary stirrer until the color is uniform.
S2: and (3) after the pigment obtained in the step (S1) is fully wetted, grinding the pigment to the required fineness.
Optionally, the mixed pigment is left for more than 4h to thoroughly wet the pigment obtained in step S1.
The special color ink is prepared by adopting a semi-finished product or a finished product base ink, and the special color ink of the hibiscus brilliant orange is prepared by adopting the pigment, and can meet the printability requirement only by grinding the special color ink to a certain fineness. The pigment can be ground to a fineness of <10 μm using a three-roll mill. Usually, the required requirements are achieved by grinding 2 times.
S3: and (3) adding a drier into the pigment obtained in the step (S2), and uniformly stirring to obtain the pigment.
Similar to the step S1, the stirring time is generally 30-50 min, and the mixture can be uniformly stirred.
After the ink is prepared, removing bubbles generated during ink stirring through a three-roller grinding machine, and packaging.
The present invention will be described below with reference to specific examples. The values of the process conditions taken in the following examples are exemplary and ranges of values are provided as indicated in the foregoing summary, and reference may be made to conventional techniques for process parameters not specifically noted. The following examples are all tests which are conventional in the art, except where otherwise specified. Unless otherwise indicated, the reagents and instruments used in the technical scheme provided by the invention can be purchased from conventional channels or on the market.
Examples
In this example, a hibiscus brilliant orange spot color ink is prepared, and the raw materials are shown in table 1, and the specific steps are as follows:
first, the following materials were charged into an ink stirring tank in the proportions shown in table 1: resin oil, nano calcium, medium yellow pigment, orange pigment, polyethylene wax, soybean oil, gloss oil, light oil and fluorescent slurry. Then stirring the above pigment for 30min by using a planetary stirrer until the color is uniform, and standing for 4h to fully wet the pigment. And then setting the pressure of a three-roller grinder according to the fineness requirement, and grinding for 2 times by adopting the three-roller grinder. Thirdly, adding the following auxiliary agents in proportion and stirring for 30min until the mixture is uniform: manganese as a type-drier and cobalt as a type-drier.
TABLE 1 raw materials used in the examples
0.06 Cubic Centimeter (CC) of uniformly stirred special color ink of the hibiscus brilliant orange is measured by using an IGT (ultraviolet fluorescence tomography) quantifier, the uniform color ink is added on a uniform ink roller of a color bang CB225A color developing instrument, the uniform ink is started for 70-90 seconds, and the ink is uniformly rolled and then is developed. The sample is detected by using X-rite eXact, the target value of the hibiscus brilliant orange spot color ink is set as L:75.2, a:48.3, b:67.9, C:83.4 and H:54.6 degrees, and the color difference value is set as qualified when delta E is less than 1. Measurement setup: measurement mode M1, illuminant/viewing angle D50/2 DEG, delta E mode CIE Delta 2000. The color and printability of the ink are determined, the color is shown in FIG. 2, and the color value detection result is shown in Table 2. And simultaneously, a fineness plate, a viscosity meter and a fluidity meter are used for measuring the fineness, viscosity and fluidity of the ink. Finally, the drying property of the ink is determined through a drying experiment. The results are shown in Table 2.
TABLE 2 example ink Performance parameters
As can be seen from the table 2, the special color ink of the hibiscus brilliant orange provided by the invention has excellent printing performance, high brightness and high chroma.
Fig. 4 (a) shows a target orange pattern having color values of L:75.2, a:48.3, b:67.9, C:83.4, H: 54.6. For the target orange pattern shown in fig. 4 (a), a swatch printed using the hibiscus brilliant orange spot color ink of the present invention is shown in fig. 4 (b). The printing stock is white double-sided offset paper. It can be seen that the swatch color shown in fig. 4 (b) is very close to the color of the target orange pattern shown in fig. 4 (a).
The Pantone 2018U is an orange spot color in Pantone colors, and the Pantone 2018U color value is as follows: l:70.0, a:41.7, b:58.3, C:71.7, H:54.4 degrees. See figure 3 for its color. Which is the universal color in the existing universal color rule that is closest to the target orange pattern color shown in fig. 4 (a).
For the target orange pattern shown in fig. 4 (a), the preview proof using Pantone 2018U color output by the image processing software is shown in fig. 4 (c). It can be seen that there is a large difference (Δ E = 8.2) between the sample color shown in fig. 4 (c) and the color of the target orange pattern shown in fig. 4 (a).
Therefore, in this embodiment, for the orange pattern shown in fig. 4 (a), the printing requirement cannot be satisfied by using the existing Pantone 2018U spot color, but the target can be achieved by using the hibiscus brilliant orange spot color ink of the present invention.
As can be seen from FIGS. 2-4, the specialty color ink of hibiscus brilliant orange of the present invention has high color vividness, high brightness and high chroma compared to Pantone 2018U.
Finally, it should be noted that: although the present invention has been described in detail with reference to the foregoing embodiments, it will be apparent to those skilled in the art that changes may be made in the embodiments and/or equivalents thereof without departing from the spirit and scope of the invention. Any modification, equivalent replacement, or improvement made within the spirit and principle of the present invention should be included in the protection scope of the present invention.
Claims (9)
1. The orange printing ink is characterized by comprising the following raw materials in percentage by weight:
29 to 35 percent of resin oil, 1 to 2 percent of nano calcium, 8 to 9 percent of medium yellow pigment, 3.4 to 4 percent of orange pigment, 1.5 to 2.5 percent of polyethylene wax, 12 to 14 percent of soybean oil, 20 to 22 percent of gloss oil, 3 to 4 percent of light oil, 13 to 15 percent of fluorescent slurry and 1.5 to 2.5 percent of drier.
2. The orange ink according to claim 1, wherein the drier comprises manganese type a-drier and cobalt type B-drier.
3. The orange ink according to claim 2, wherein the content of manganese type a-drier in the orange ink is 1 to 1.5%, and the content of cobalt type B-drier in the orange ink is 0.5 to 1%.
4. The orange ink according to claim 1, characterized in that it comprises the following raw materials in percentage by weight: 30 to 32 percent of resin oil, 1 to 1.5 percent of nano calcium, 8.3 to 8.6 percent of medium yellow pigment, 3.5 to 3.8 percent of orange pigment, 1.9 to 2.1 percent of polyethylene wax, 12 to 13 percent of soybean oil, 20 to 21 percent of gloss oil, 3 to 3.5 percent of light oil, 14 to 15 percent of fluorescent slurry and 1.5 to 2.5 percent of drier.
5. The orange ink according to claim 1, wherein the orange ink has a color value after printing of L75.2, a 48.3, b 67.9, C83.4, H54.6 ° when the substrate is a white offset double-sided offset paper; color difference range: the color difference value delta E is less than 1.
6. A method for preparing orange printing ink is characterized by comprising the following steps:
s1: mixing and stirring 29-35% of resin oil, 1-2% of nano calcium, 8-9% of medium yellow pigment, 3.4-4% of orange pigment, 1.5-2.5% of polyethylene wax, 12-14% of soybean oil, 20-22% of gloss oil, 3-4% of light oil and 13-15% of fluorescent slurry until the color is uniform;
s2: after the pigment obtained in the step S1 is fully wetted, grinding the pigment to a required fineness;
s3: and (3) adding 1.5-2.5% of drier into the pigment obtained in the step (S2), and uniformly stirring.
7. The method according to claim 6, wherein in step S2, the pigment is ground to a fineness of <10 μm.
8. The method according to claim 6, wherein step S2 includes: the pigment obtained in step S1 was left for 4 hours or more to sufficiently wet the pigment.
9. The method of claim 6, wherein the stirring time in step S1 and step S3 is 30 to 50min.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202111010229.XA CN115725203B (en) | 2021-08-31 | 2021-08-31 | Orange ink and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202111010229.XA CN115725203B (en) | 2021-08-31 | 2021-08-31 | Orange ink and preparation method thereof |
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| CN115725203B CN115725203B (en) | 2024-04-12 |
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| Publication number | Publication date |
|---|---|
| CN115725203B (en) | 2024-04-12 |
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