CN115678695A - Hair-care and brain-strengthening shampoo soap and preparation method thereof - Google Patents
Hair-care and brain-strengthening shampoo soap and preparation method thereof Download PDFInfo
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- CN115678695A CN115678695A CN202211144487.1A CN202211144487A CN115678695A CN 115678695 A CN115678695 A CN 115678695A CN 202211144487 A CN202211144487 A CN 202211144487A CN 115678695 A CN115678695 A CN 115678695A
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Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
Landscapes
- Cosmetics (AREA)
Abstract
The invention discloses a hair care and brain strengthening shampoo soap and a preparation method thereof. The shampoo soap is mainly prepared from natural extracts, is natural and non-irritant, has good cleaning effect, has good hair blackening and hair increasing effects, and has certain brain strengthening effect.
Description
Technical Field
The invention relates to a shampoo soap, in particular to a hair-care and brain-strengthening shampoo soap and a preparation method thereof. Belongs to the technical field of washing and protecting articles.
Background
The shampoo soap is a hair cleaning product, and is used for pre-washing with clear water to wash off sweat and dirt on hair, and then is used for quickly washing hair by using a proper amount of the shampoo soap. Shampoo soaps have the following problems:
1. most shampoo soaps are derived from fatty soaps and tend to deposit on the hair and scalp, exhibit poor lathering, readily form insoluble materials, and exhibit poor cleansing performance.
2. The existing shampoo soap is weak in alkalinity, so that scales of hair can be opened, and the hair is easy to damage, so that the hair washing needs to be rapid and accurate. The long-term use of the shampoo soap inevitably causes the hair to be dry and poor.
3. Shampoo soaps contain many chemical additives and are harmful to the skin and human body.
4. At present, like products in the market have no effects of blackening hair, increasing hair, strengthening brain and the like. However, modern people have irregular daily work and rest, insufficient long-term sleep, serious fatigue problem, reduced overall physical quality, dry and easy-to-break hair, serious split phenomenon and poor hair quality. And the air pollution is more and more serious, and the ultraviolet rays in the sunlight damage hair, and the hair is further damaged by hair dyeing, perm and electric hair dryers, so the hair quality is worse. In addition, the existing shampoo soap mostly adopts chemical raw materials, has strong irritation to scalp, is sensitized and damaged, and can affect brain memory cells and influence the brain after long-term use. Therefore, higher requirements are put forward on the hair care and brain strengthening effects of the shampoo soap.
Patent CN107603789B discloses a conditioning solid laundry soap, which contains the following components besides the common components of a shampoo soap: A. the natural soap base accounts for 70 to 85 percent of the weight percentage of the shampoo soap; B. synthetic detergent surfactant in 5-25 wt% of the shampoo soap; C. the hair conditioner accounts for 0.25 to 3.5 weight percent of the shampoo soap, and the balance is deionized water. The patent technology mainly improves soap base, obviously improves foaming performance, but has general hair care effect, basically has no hair blackening and hair increasing effects, and also has no brain strengthening effect.
Patent application CN109419638A discloses an anti-dandruff shampoo soap comprising: 20-30 parts of main surfactant, 10-17 parts of cosurfactant, 1-3 parts of thickening agent, 3-5 parts of cosolvent, 1-6 parts of ethylene glycol monostearate, 1-5 parts of cyclopentylsiloxane/dimethiconol, 0.1-1 part of anti-dandruff agent, 0.3-0.8 part of iodopropynyl butyl carbamate, 3-6 parts of citric acid and 1-3 parts of plant essential oil. The patent application has good foaming effect and good anti-dandruff effect, but has the problems of high chemical raw material content and basically no hair care and brain strengthening effects.
Disclosure of Invention
The invention aims to overcome the defects of the prior art and provides the hair care and brain strengthening shampoo soap and the preparation method thereof, and the hair care and brain strengthening shampoo soap has good hair blackening and hair strengthening effects and a certain brain strengthening effect.
In order to realize the purpose, the invention adopts the following technical scheme:
a hair care and brain tonic shampoo soap is prepared by mixing the following components in parts by weight: 0.5 to 5 parts of gallnut extract, 0.5 to 5 parts of fleece-flower root extract, 0.3 to 3 parts of black wolfberry extract, 1 to 15 parts of acer truncatum seed extract, 0.5 to 5 parts of logwood extract, 0.3 to 3 parts of ginger extract, 0.3 to 3 parts of mulberry seed extract, 0.5 to 5 parts of Chinese honeylocust fruit extract, 0.5 to 5 parts of pine needle extract, 0.5 to 5 parts of citric acid, 0.5 to 5 parts of honey, 8 to 10 parts of lemon oil, 4 to 5 parts of sodium hydroxide and 10 to 15 parts of water.
Preferably, the preparation method of the gallnut extract comprises the following steps: washing and drying nutgall, crushing the nutgall into 80-100 meshes to obtain nutgall powder, adding the nutgall powder into an ethanol aqueous solution with the volume concentration of 70-80% and the weight of 7-9 times of the nutgall powder, soaking the nutgall powder for 6-8 hours at room temperature, carrying out ultrasonic oscillation treatment on the nutgall powder for 45-55 minutes at the temperature of 55-65 ℃, centrifuging the nutgall powder, taking supernatant, and concentrating the supernatant under reduced pressure to obtain an extract with the relative density of 1.10-1.20.
Preferably, the preparation method of the polygonum multiflorum extract comprises the following steps: firstly, cleaning and drying polygonum multiflorum, then crushing the polygonum multiflorum into 80-100 meshes to obtain polygonum multiflorum powder, then adding the polygonum multiflorum powder into an ethanol water solution with volume concentration of 75-85% and weight which is 7-9 times of the polygonum multiflorum powder, soaking the polygonum multiflorum powder for 6-8 hours at room temperature, then carrying out ultrasonic oscillation treatment on the polygonum multiflorum powder for 40-50 minutes at the temperature of 50-60 ℃, centrifuging the polygonum multiflorum powder to obtain a supernatant, and concentrating the supernatant under reduced pressure to obtain an extract with the relative density of 1.15-1.25.
Preferably, the preparation method of the lycium ruthenicum extract comprises the following steps: firstly, cleaning fresh lycium ruthenicum, transferring the cleaned fresh lycium ruthenicum to a flash extractor, and carrying out flash extraction by using distilled water, wherein the mass ratio of the lycium ruthenicum to the distilled water is 1: 15-20, the extraction power is 80-100W, the extraction temperature is 50-55 ℃, the extraction times are 2-3, each time extraction is 1-2 minutes, the extraction products are combined, the supernatant is obtained by centrifugation, and freeze drying is carried out, thus obtaining the product.
Preferably, the preparation method of the acer truncatum seed extract comprises the following steps: firstly, acer truncatum seeds are cleaned, dried and crushed to 80-100 meshes to obtain acer truncatum seed powder, then the acer truncatum seed powder is added into 80-85% ethanol water solution with volume concentration of 7-9 times of the weight of the acer truncatum seed powder, then microwave extraction is carried out for 5-7 minutes by 400-500W, supernatant is obtained by centrifugation, and the supernatant is decompressed and concentrated to extract with relative density of 1.20-1.25, thus obtaining the acer truncatum seed extract.
Preferably, the preparation method of the logwood extract comprises the following steps: firstly, washing and drying the bark of logwood, then crushing the logwood to 80-100 meshes to obtain logwood powder, then adding the logwood powder into a methanol aqueous solution with volume concentration of 50-60% and weight of 7-9 times of the logwood powder, soaking the logwood powder for 8-10 hours at room temperature, then carrying out ultrasonic oscillation treatment on the logwood powder for 40-50 minutes at 50-60 ℃, centrifuging the logwood powder, taking the supernatant, and concentrating the supernatant under reduced pressure to obtain an extract with relative density of 1.20-1.30.
Preferably, the preparation method of the ginger extract comprises the following steps: cleaning fresh ginger, slicing and drying, crushing to 80-100 meshes to obtain ginger powder, adding the ginger powder into water, adding papain and ferrous sulfate while stirring, stirring and heating at 55-60 ℃ for 6-8 hours, naturally cooling to room temperature, centrifuging to obtain supernatant, and spray-drying to obtain the ginger powder; wherein the mass ratio of the ginger powder to the water to the papain to the ferrous sulfate is 1:7 to 9:3 to 4:1 to 1.5.
Preferably, the preparation method of the mulberry seed extract comprises the following steps: firstly, cleaning fresh mulberry seeds, transferring the cleaned fresh mulberry seeds to a flash extractor, and carrying out flash extraction by using distilled water, wherein the mass ratio of the mulberry seeds to the distilled water is 1: 15-20, the extraction power is 80-100W, the extraction temperature is 45-50 ℃, the extraction times are 2-3, each time of extraction lasts for 1-2 minutes, the extraction products are combined, the supernatant is obtained by centrifugation, and the freeze drying is carried out, thus obtaining the product.
Preferably, the preparation method of the saponin extract is as follows: cleaning and drying the saponin, crushing the saponin to 80-100 meshes to obtain saponin powder, then placing the saponin powder into a supercritical carbon dioxide extraction kettle, adding 70-80% ethanol aqueous solution with volume concentration of 0.4-0.5 times of the weight of the saponin powder, introducing carbon dioxide at the flow rate of 8-10L/h, extracting at the temperature of 55-65 ℃, the extraction pressure of 18-22 MPa and the extraction time of 120-130 minutes to obtain an extract, finally adding the extract into a separation kettle, and controlling the pressure in the separation kettle to be 18-22 MPa and the temperature to be 55-65 ℃ to obtain the saponin powder.
Preferably, the preparation method of the pine needle extract comprises the following steps: pine needles are cleaned and dried, and then crushed into 80-100 meshes to obtain pine needle powder, the pine needle powder is added into an 80-90% ethanol water solution with volume concentration of 7-9 times of the weight of the pine needle powder, then microwave extraction is carried out for 8-10 minutes by using 500-600W, supernatant is obtained by centrifugation, and the extract is concentrated under reduced pressure to obtain the pine needle extract with the relative density of 1.25-1.30.
The preparation method of the hair care and brain strengthening shampoo soap comprises the following specific steps:
(1) Firstly, stirring and dissolving sodium hydroxide with a formula amount in water with a formula amount to obtain a sodium hydroxide solution, then adding lemon oil and citric acid with a formula amount into the sodium hydroxide solution preheated to 65-75 ℃, keeping the temperature, stirring and reacting for 45-55 minutes, and drying to obtain a soap base;
(2) Then heating the soap base to 65-75 ℃, and stirring for 20-30 minutes under the condition of heat preservation to obtain soap base molten liquid;
(3) And then adding the formula amount of Chinese honeylocust fruit extract into the soap base molten liquid, stirring and uniformly mixing, then continuously adding the formula amount of Chinese gall extract, polygonum multiflorum extract, lycium ruthenicum extract, acer truncatum seed extract, logwood extract, ginger extract, mulberry seed extract, pine needle extract and honey, stirring and uniformly mixing, pouring into a mould, naturally cooling and solidifying, demoulding, and naturally air-drying to obtain the shampoo soap.
Preferably, in the step (3), the gallnut extract, the polygonum multiflorum extract, the lycium ruthenicum extract, the acer truncatum seed extract, the logwood extract, the ginger extract, the mulberry seed extract, the pine needle extract and the honey are mixed uniformly at 26-30 ℃ in advance and then fed, the feeding is carried out slowly at a constant speed for 15-20 minutes, and the uniform mixing is realized after the feeding is finished and the stirring is carried out for 20-30 minutes.
The invention has the beneficial effects that:
the shampoo soap is prepared from a Chinese gall extract, a polygonum multiflorum extract, a black wolfberry extract, a acer truncatum seed extract, a logwood extract, a ginger extract, a mulberry seed extract, a pine needle extract, honey, citric acid, lemon oil, sodium hydroxide, water and the like serving as raw materials. The shampoo soap is mainly prepared from natural extracts, is natural, has no stimulation, has good cleaning effect, has good hair blackening and hair increasing effects, and has a certain brain strengthening effect. The invention has the following advantages:
1. the hair cleansing cream is weak in acidity (pH = 6.0-6.5), can effectively remove greasy feeling of scalp, and has good cleansing effect.
2. The invention belongs to the synthesis of various pure natural plant extracts, has no chemical additive, is natural and has no stimulation.
3. The extract of Acer Truncatum Bunge seed contains nervonic acid (tetracosan-cis-15-olefine acid) as main component, has the functions of repairing skin cells, repairing brain cells by rapid absorption through hair roots, repairing brain cells and skin tissues by rapid absorption through pores of skin, preventing and improving cardiovascular and cerebrovascular diseases, and strengthening brain.
4. The Galla chinensis extract contains tannic acid, polygoni Multiflori radix contains emodin and stilbene glucoside, fructus Lycii contains anthocyanidin, folium lignum sappan contains fatty acid, flavonoids, tannin, etc., rhizoma Zingiberis recens extract contains zingiberene, etc., mori fructus seed extract contains unsaturated fatty acid, linoleic acid, and folium Pini extract contains pinene, etc. The components have synergistic effect, and can increase melanin in hair follicle, blacken hair, promote hair follicle repair, increase hair, repair brain cells, and strengthen brain.
5. The natural extract component of the invention can rapidly penetrate through scalp, realize rapid absorption and improve the use effect of the shampoo soap. The shampoo soap disclosed by the invention is tried by thousands of people, and the effect is obvious after the shampoo soap is used.
Detailed Description
The present invention will be further illustrated by the following examples, which are intended to be merely illustrative and not limitative.
Example 1:
a hair care and brain strengthening shampoo soap is prepared by mixing the following components: 0.5kg of Chinese gall extract, 0.5kg of polygonum multiflorum extract, 0.3kg of lycium ruthenicum extract, 1kg of acer truncatum seed extract, 0.5kg of logwood extract, 0.3kg of ginger extract, 0.3kg of mulberry seed extract, 0.5kg of Chinese honeylocust fruit extract, 0.5kg of pine needle extract, 0.5kg of citric acid, 0.5kg of honey, 8kg of lemon oil, 4kg of sodium hydroxide and 10kg of water.
The preparation method of the gallnut extract comprises the following steps: cleaning nutgall, drying, crushing to 80 meshes to obtain nutgall powder, adding the nutgall powder into a 7-time volume concentration 70% ethanol aqueous solution, soaking at room temperature for 6 hours, carrying out 30kHz ultrasonic oscillation treatment at 55 ℃ for 45 minutes, centrifuging, taking supernatant, and concentrating under reduced pressure to obtain an extract with the relative density of 1.10.
The preparation method of the polygonum multiflorum extract comprises the following steps: firstly, cleaning and drying polygonum multiflorum, then crushing the polygonum multiflorum into 80 meshes to obtain polygonum multiflorum powder, then adding the polygonum multiflorum powder into a 7-time ethanol water solution with volume concentration of 75% by weight, soaking the polygonum multiflorum powder for 6 hours at room temperature, then carrying out ultrasonic oscillation treatment for 40 minutes at 35kHz at 50 ℃, centrifuging the polygonum multiflorum powder, taking supernatant, and concentrating the supernatant under reduced pressure to obtain an extract with the relative density of 1.15.
The preparation method of the lycium ruthenicum extract comprises the following steps: firstly, cleaning fresh lycium ruthenicum, then transferring the cleaned fresh lycium ruthenicum to a flash extractor, and carrying out flash extraction by using distilled water, wherein the mass ratio of the lycium ruthenicum to the distilled water is 1:15, extracting at the extraction power of 80W and the extraction temperature of 50 ℃ for 2 times, extracting for 1 minute each time, combining the extracted products, centrifuging, taking the supernatant, and freeze-drying to obtain the product.
The preparation method of the acer truncatum seed extract comprises the following steps: firstly, washing acer truncatum seeds, drying, and then crushing to 80 meshes to obtain acer truncatum seed powder, then adding the acer truncatum seed powder into 80% ethanol aqueous solution with volume concentration 7 times of the weight of the acer truncatum seed powder, then carrying out microwave extraction for 5 minutes by 400W, centrifuging to obtain supernatant, and carrying out reduced pressure concentration to obtain extract with relative density of 1.20.
The preparation method of the logwood extract comprises the following steps: cleaning bark of folium lignum sappan, drying, pulverizing to 80 mesh to obtain folium lignum sappan powder, adding folium lignum sappan powder into 7 times of 50% methanol water solution, soaking at room temperature for 8 hr, treating with 40kHz ultrasonic oscillation at 50 deg.C for 40 min, centrifuging to obtain supernatant, and concentrating under reduced pressure to obtain extract with relative density of 1.20.
The preparation method of the ginger extract comprises the following steps: cleaning fresh ginger, slicing, drying, pulverizing to 80 mesh to obtain ginger powder, adding into water, adding papain and ferrous sulfate under stirring, heating at 55 deg.C under stirring for 6 hr, naturally cooling to room temperature, centrifuging to obtain supernatant, and spray drying; wherein the mass ratio of the ginger powder to the water to the papain to the ferrous sulfate is 1:7:3:1.
the preparation method of the mulberry seed extract comprises the following steps: firstly, cleaning fresh mulberry seeds, transferring the cleaned fresh mulberry seeds to a flash extractor, and carrying out flash extraction by using distilled water, wherein the mass ratio of the mulberry seeds to the distilled water is 1:15, extracting at the extraction power of 80W and the extraction temperature of 45 ℃ for 2 times, extracting for 1 minute each time, combining the extracted products, centrifuging, taking the supernatant, and freeze-drying to obtain the product.
The preparation method of the saponin extract comprises the following steps: cleaning and drying the Chinese honeylocust, crushing the Chinese honeylocust to 80 meshes to obtain Chinese honeylocust powder, then placing the Chinese honeylocust powder in a supercritical carbon dioxide extraction kettle, adding 70% ethanol aqueous solution with volume concentration of 0.4 time of the weight of the Chinese honeylocust powder, introducing carbon dioxide at the flow rate of 8L/h, extracting at the temperature of 55 ℃, the extraction pressure of 18MPa and the extraction time of 120 minutes to obtain an extract, finally adding the extract into a separation kettle, and controlling the pressure in the separation kettle to be 18MPa and the temperature to be 55 ℃ to obtain the Chinese honeylocust extract.
The preparation method of the pine needle extract comprises the following steps: the preparation method comprises the steps of cleaning pine needles, drying, crushing to 80 meshes to obtain pine needle powder, adding the pine needle powder into an 80% ethanol aqueous solution with volume concentration of 7 times of the pine needle powder, performing microwave extraction for 8 minutes by using 500W, centrifuging to obtain supernatant, and performing reduced pressure concentration to obtain an extract with the relative density of 1.25.
The preparation method of the hair care and brain strengthening shampoo soap comprises the following specific steps:
(1) Firstly stirring and dissolving the sodium hydroxide with the formula amount in the water with the formula amount to obtain a sodium hydroxide solution, then adding the lemon oil and the citric acid with the formula amount into the sodium hydroxide solution preheated to 65 ℃, keeping the temperature, stirring and reacting for 45 minutes, and drying to obtain a soap base;
(2) Then heating the soap base to 65 ℃, and stirring for 20 minutes under the condition of heat preservation to obtain soap base melt;
(3) And then adding the formula amount of the Chinese honeylocust fruit extract into the soap base molten liquid, stirring and uniformly mixing, then continuously adding the formula amount of the Chinese gall extract, the polygonum multiflorum extract, the black wolfberry fruit extract, the acer truncatum seed extract, the logwood extract, the ginger extract, the mulberry seed extract, the pine needle extract and the honey, stirring and uniformly mixing, pouring into a mould, naturally cooling and solidifying, demoulding, and naturally air drying to obtain the shampoo soap.
In the step (3), the gallnut extract, the polygonum multiflorum extract, the lycium ruthenicum extract, the acer truncatum seed extract, the logwood extract, the ginger extract, the mulberry seed extract, the pine needle extract and the honey are mixed uniformly at 26 ℃ in advance and then fed, the feeding is carried out at a constant speed and slowly for 15 minutes, and the uniform mixing is realized after the feeding is finished and the stirring is carried out for 20 minutes.
Example 2:
a hair care and brain tonic shampoo soap is prepared by mixing the following components: 5kg of Chinese gall extract, 5kg of polygonum multiflorum extract, 3kg of lycium ruthenicum extract, 15kg of acer truncatum seed extract, 5kg of logwood extract, 3kg of ginger extract, 3kg of mulberry seed extract, 5kg of saponin extract, 5kg of pine needle extract, 5kg of citric acid, 5kg of honey, 10kg of lemon oil, 5kg of sodium hydroxide and 15kg of water.
The preparation method of the galla chinensis extract comprises the following steps: cleaning and drying nutgall, and crushing to 100 meshes to obtain nutgall powder, adding the nutgall powder into an 80% ethanol water solution with volume concentration 9 times of the nutgall powder, soaking for 8 hours at room temperature, then carrying out ultrasonic oscillation treatment for 55 minutes at 40kHz under the condition of 65 ℃, centrifuging, taking supernatant, and concentrating under reduced pressure to obtain an extract with the relative density of 1.20.
The preparation method of the polygonum multiflorum extract comprises the following steps: cleaning and drying polygonum multiflorum, crushing to 100 meshes to obtain polygonum multiflorum powder, adding the polygonum multiflorum powder into a 9-time volume concentration 85% ethanol aqueous solution, soaking at room temperature for 8 hours, carrying out ultrasonic oscillation treatment at 60 ℃ and 45kHz for 50 minutes, centrifuging, taking supernatant, and concentrating under reduced pressure to obtain an extract with the relative density of 1.25.
The preparation method of the lycium ruthenicum extract comprises the following steps: firstly, cleaning fresh lycium ruthenicum, transferring the cleaned fresh lycium ruthenicum to a flash extractor, and carrying out flash extraction by using distilled water, wherein the mass ratio of the lycium ruthenicum to the distilled water is 1:20, extracting at the extraction power of 100W and the extraction temperature of 55 ℃ for 3 times, extracting for 2 minutes each time, combining the extracted products, centrifuging to obtain a supernatant, and freeze-drying to obtain the traditional Chinese medicine composition.
The preparation method of the acer truncatum seed extract comprises the following steps: firstly, washing acer truncatum seeds, drying, then crushing to 100 meshes to obtain acer truncatum seed powder, then adding the acer truncatum seed powder into ethanol aqueous solution with the volume concentration of 85% and the weight 9 times that of the acer truncatum seed powder, then carrying out microwave extraction for 7 minutes by using 500W, centrifuging to obtain supernatant, and carrying out reduced pressure concentration to obtain extract with the relative density of 1.25.
The preparation method of the logwood extract comprises the following steps: cleaning bark of logwood, drying, pulverizing to 100 mesh to obtain logwood powder, adding logwood powder into 9 times of 60% methanol aqueous solution, soaking at room temperature for 10 hr, performing ultrasonic vibration treatment at 60 deg.C and 50kHz for 50 min, centrifuging to obtain supernatant, and concentrating under reduced pressure to obtain extract with relative density of 1.30.
The preparation method of the ginger extract comprises the following steps: cleaning fresh ginger, slicing, drying, pulverizing to 100 mesh to obtain ginger powder, adding into water, adding papain and ferrous sulfate under stirring, heating at 60 deg.C under stirring for 8 hr, naturally cooling to room temperature, centrifuging to obtain supernatant, and spray drying; wherein the mass ratio of the ginger powder to the water to the papain to the ferrous sulfate is 1:9:4:1.5.
the preparation method of the mulberry seed extract comprises the following steps: firstly, cleaning fresh mulberry seeds, transferring the cleaned fresh mulberry seeds to a flash extractor, and carrying out flash extraction by using distilled water, wherein the mass ratio of the mulberry seeds to the distilled water is 1:20, the extraction power is 100W, the extraction temperature is 50 ℃, the extraction times are 3 times, each time is 2 minutes, the extraction products are combined, the supernatant is obtained by centrifugation, and the freeze drying is carried out, thus obtaining the compound.
The preparation method of the saponin extract comprises the following steps: cleaning and drying the Chinese honeylocust fruit, crushing the Chinese honeylocust fruit into 100 meshes to obtain Chinese honeylocust fruit powder, then placing the Chinese honeylocust fruit powder into a supercritical carbon dioxide extraction kettle, adding 80% ethanol aqueous solution with volume concentration of 0.5 time of the weight of the Chinese honeylocust fruit powder, introducing carbon dioxide at the flow rate of 10L/h, extracting at the temperature of 65 ℃, the extraction pressure of 22MPa and the extraction time of 130 minutes to obtain an extract, finally adding the extract into a separation kettle, and controlling the pressure in the separation kettle at the temperature of 65 ℃ to obtain the Chinese honeylocust fruit extract.
The preparation method of the pine needle extract comprises the following steps: the preparation method comprises the steps of cleaning and drying pine needles, then crushing the pine needles to 100 meshes to obtain pine needle powder, then adding the pine needle powder into 90% ethanol aqueous solution with the volume concentration being 9 times of the weight of the pine needle powder, then extracting the pine needle powder for 10 minutes by using 600W microwaves, centrifuging the extract to obtain supernatant, and concentrating the supernatant under reduced pressure to obtain extract with the relative density of 1.30.
The preparation method of the hair-care brain-strengthening shampoo soap comprises the following specific steps:
(1) Firstly stirring and dissolving the formula amount of sodium hydroxide in the formula amount of water to obtain a sodium hydroxide solution, then adding the formula amount of lemon oil and citric acid into the sodium hydroxide solution preheated to 75 ℃, keeping the temperature, stirring and reacting for 55 minutes, and drying to obtain a soap base;
(2) Then heating the soap base to 75 ℃, and stirring for 30 minutes under the condition of heat preservation to obtain soap base melt;
(3) And then adding the formula amount of the Chinese honeylocust fruit extract into the soap base molten liquid, stirring and uniformly mixing, then continuously adding the formula amount of the Chinese gall extract, the polygonum multiflorum extract, the black wolfberry fruit extract, the acer truncatum seed extract, the logwood extract, the ginger extract, the mulberry seed extract, the pine needle extract and the honey, stirring and uniformly mixing, pouring into a mould, naturally cooling and solidifying, demoulding, and naturally air drying to obtain the shampoo soap.
In the step (3), the Chinese gall extract, the polygonum multiflorum extract, the lycium ruthenicum extract, the acer truncatum seed extract, the logwood extract, the ginger extract, the mulberry seed extract, the pine needle extract and the honey are mixed uniformly at 30 ℃ in advance and then fed, the feeding is carried out slowly at a constant speed for 20 minutes, and the uniform mixing is realized by stirring for 30 minutes after the feeding is finished.
Example 3:
a hair care and brain tonic shampoo soap is prepared by mixing the following components: 5kg of nutgall extract, 0.5kg of polygonum multiflorum extract, 3kg of lycium ruthenicum extract, 1kg of acer truncatum seed extract, 5kg of logwood extract, 0.3kg of ginger extract, 3kg of mulberry seed extract, 0.5kg of saponin extract, 5kg of pine needle extract, 0.5kg of citric acid, 5kg of honey, 8kg of lemon oil, 5kg of sodium hydroxide and 10kg of water.
The preparation method of the gallnut extract comprises the following steps: cleaning and drying nutgall, and crushing to 100 meshes to obtain nutgall powder, adding the nutgall powder into an 80% ethanol water solution with volume concentration of 7 times of the nutgall powder, soaking for 6 hours at room temperature, then carrying out ultrasonic oscillation treatment for 55 minutes at 30kHz at 65 ℃, centrifuging, taking supernatant, and concentrating under reduced pressure to obtain an extract with the relative density of 1.10.
The preparation method of the polygonum multiflorum extract comprises the following steps: firstly, cleaning and drying polygonum multiflorum, then crushing the polygonum multiflorum to 100 meshes to obtain polygonum multiflorum powder, then adding the polygonum multiflorum powder into a 7-time ethanol water solution with volume concentration of 85% by weight, soaking the polygonum multiflorum powder for 6 hours at room temperature, then carrying out ultrasonic oscillation treatment for 50 minutes at 35kHz at the temperature of 60 ℃, centrifuging the polygonum multiflorum powder, taking supernatant, and concentrating the supernatant under reduced pressure to obtain an extract with the relative density of 1.15.
The preparation method of the lycium ruthenicum extract comprises the following steps: firstly, cleaning fresh lycium ruthenicum, transferring the cleaned fresh lycium ruthenicum to a flash extractor, and carrying out flash extraction by using distilled water, wherein the mass ratio of the lycium ruthenicum to the distilled water is 1:20, extracting at the extraction power of 80W and the extraction temperature of 55 ℃ for 2 times, extracting for 2 minutes each time, combining the extracted products, centrifuging, taking the supernatant, and freeze-drying to obtain the traditional Chinese medicine composition.
The preparation method of the acer truncatum seed extract comprises the following steps: firstly, washing acer truncatum seeds, drying, and then crushing to 80 meshes to obtain acer truncatum seed powder, then adding the acer truncatum seed powder into an 80% ethanol aqueous solution with the volume concentration of 9 times the weight of the acer truncatum seed powder, then extracting for 5 minutes by using 500W microwaves, centrifuging to obtain a supernatant, and concentrating under reduced pressure to obtain an extract with the relative density of 1.25.
The preparation method of the logwood extract comprises the following steps: cleaning bark of folium lignum sappan, drying, pulverizing to 80 mesh to obtain folium lignum sappan powder, adding folium lignum sappan powder into 9 times of 50% methanol water solution, soaking at room temperature for 10 hr, performing ultrasonic vibration at 50kHz for 40 min at 50 deg.C, centrifuging to obtain supernatant, and concentrating under reduced pressure to obtain extract with relative density of 1.30.
The preparation method of the ginger extract comprises the following steps: cleaning fresh ginger, slicing, drying, pulverizing to 80 mesh to obtain ginger powder, adding the ginger powder into water, adding papain and ferrous sulfate while stirring, stirring and heating at 60 deg.C for 6 hr, naturally cooling to room temperature, centrifuging to obtain supernatant, and spray drying; wherein the mass ratio of the ginger powder to the water to the papain to the ferrous sulfate is 1:9:3:1.5.
the preparation method of the mulberry seed extract comprises the following steps: firstly, cleaning fresh mulberry seeds, transferring the cleaned fresh mulberry seeds to a flash extractor, and carrying out flash extraction by using distilled water, wherein the mass ratio of the mulberry seeds to the distilled water is 1:15, extracting at the extraction power of 100W and the extraction temperature of 45 ℃ for 3 times, extracting for 1 minute each time, combining the extracted products, centrifuging, taking the supernatant, and freeze-drying to obtain the product.
The preparation method of the saponin extract comprises the following steps: cleaning and drying the Chinese honeylocust, crushing the Chinese honeylocust to 100 meshes to obtain Chinese honeylocust powder, then placing the Chinese honeylocust powder in a supercritical carbon dioxide extraction kettle, adding 80% ethanol water solution with volume concentration of 0.4 time of the weight of the Chinese honeylocust powder, introducing carbon dioxide at the flow rate of 8L/h, extracting at the temperature of 65 ℃, the extraction pressure of 18MPa and the extraction time of 130 minutes to obtain an extract, finally adding the extract into a separation kettle, and controlling the pressure in the separation kettle to be 18MPa and the temperature to be 65 ℃ to obtain the Chinese honeylocust extract.
The preparation method of the pine needle extract comprises the following steps: the preparation method comprises the steps of cleaning and drying pine needles, then crushing the pine needles to 80 meshes to obtain pine needle powder, then adding the pine needle powder into 9 times of 80% ethanol water solution by weight, then extracting for 8 minutes by using 600W microwaves, centrifuging to obtain supernatant, and concentrating under reduced pressure to obtain extract with the relative density of 1.30.
The preparation method of the hair-care brain-strengthening shampoo soap comprises the following specific steps:
(1) Firstly, stirring and dissolving sodium hydroxide with a formula amount in water with a formula amount to obtain a sodium hydroxide solution, then adding lemon oil and citric acid with a formula amount into the sodium hydroxide solution preheated to 65 ℃, preserving heat, stirring and reacting for 55 minutes, and drying to obtain a soap base;
(2) Then heating the soap base to 65 ℃, and stirring for 30 minutes under the condition of heat preservation to obtain soap base melt;
(3) And then adding the formula amount of the Chinese honeylocust fruit extract into the soap base molten liquid, stirring and uniformly mixing, then continuously adding the formula amount of the Chinese gall extract, the polygonum multiflorum extract, the black wolfberry fruit extract, the acer truncatum seed extract, the logwood extract, the ginger extract, the mulberry seed extract, the pine needle extract and the honey, stirring and uniformly mixing, pouring into a mould, naturally cooling and solidifying, demoulding, and naturally air drying to obtain the shampoo soap.
In the step (3), the gallnut extract, the polygonum multiflorum extract, the lycium ruthenicum extract, the acer truncatum seed extract, the logwood extract, the ginger extract, the mulberry seed extract, the pine needle extract and the honey are mixed uniformly at 26 ℃ in advance and then fed, the feeding is carried out slowly at a constant speed for 20 minutes, and the uniform mixing is realized after the feeding is finished and the stirring is carried out for 20 minutes.
Example 4:
a hair care and brain strengthening shampoo soap is prepared by mixing the following components: 3kg of nutgall extract, 3kg of polygonum multiflorum extract, 2kg of lycium ruthenicum extract, 8kg of acer truncatum seed extract, 3kg of logwood extract, 2kg of ginger extract, 2kg of mulberry seed extract, 4kg of saponin extract, 3kg of pine needle extract, 4kg of citric acid, 4kg of honey, 9kg of lemon oil, 4.5kg of sodium hydroxide and 12kg of water.
The preparation method of the gallnut extract comprises the following steps: cleaning nutgall, drying, crushing to 90 meshes to obtain nutgall powder, adding the nutgall powder into 8 times of ethanol aqueous solution with volume concentration of 75% by weight, soaking at room temperature for 7 hours, carrying out 35kHz ultrasonic oscillation treatment for 50 minutes at 60 ℃, centrifuging, taking supernatant, and concentrating under reduced pressure to obtain an extract with the relative density of 1.15.
The preparation method of the polygonum multiflorum extract comprises the following steps: firstly, cleaning and drying polygonum multiflorum, then crushing the polygonum multiflorum to 100 meshes to obtain polygonum multiflorum powder, then adding the polygonum multiflorum powder into an ethanol water solution with volume concentration of 80 percent and 8 times of the weight of the polygonum multiflorum powder, soaking the polygonum multiflorum powder for 7 hours at room temperature, then carrying out ultrasonic oscillation treatment for 45 minutes at 40kHz under the condition of 55 ℃, centrifuging the polygonum multiflorum powder, taking supernatant, and concentrating the supernatant under reduced pressure to obtain an extract with the relative density of 1.20.
The preparation method of the lycium ruthenicum extract comprises the following steps: firstly, cleaning fresh lycium ruthenicum, transferring the cleaned fresh lycium ruthenicum to a flash extractor, and carrying out flash extraction by using distilled water, wherein the mass ratio of the lycium ruthenicum to the distilled water is 1:18, extracting at the extraction power of 90W and the extraction temperature of 53 ℃ for 3 times, extracting for 2 minutes each time, combining the extracted products, centrifuging, taking the supernatant, and freeze-drying to obtain the product.
The preparation method of the acer truncatum seed extract comprises the following steps: firstly, washing acer truncatum seeds, drying, then crushing to 100 meshes to obtain acer truncatum seed powder, then adding the acer truncatum seed powder into 8-time volume concentration 83% ethanol aqueous solution, then performing microwave extraction for 6 minutes by using 500W, centrifuging to obtain supernatant, and performing reduced pressure concentration to obtain extract with the relative density of 1.25.
The preparation method of the logwood extract comprises the following steps: cleaning bark of logwood, drying, pulverizing to 90 mesh to obtain logwood powder, adding logwood powder into 55% methanol aqueous solution with volume concentration of 8 times of the logwood powder, soaking at room temperature for 9 hr, performing ultrasonic oscillation treatment at 55 deg.C and 45kHz for 45 min, centrifuging to obtain supernatant, and concentrating under reduced pressure to obtain extract with relative density of 1.25.
The preparation method of the ginger extract comprises the following steps: cleaning fresh ginger, slicing, drying, pulverizing to 100 mesh to obtain ginger powder, adding the ginger powder into water, adding papain and ferrous sulfate while stirring, stirring and heating at 58 deg.C for 7 hr, naturally cooling to room temperature, centrifuging to obtain supernatant, and spray drying; wherein the mass ratio of the ginger powder to the water to the papain to the ferrous sulfate is 1:8:3.5:1.2.
the preparation method of the mulberry seed extract comprises the following steps: firstly, cleaning fresh mulberry seeds, transferring the cleaned fresh mulberry seeds to a flash extractor, and carrying out flash extraction by using distilled water, wherein the mass ratio of the mulberry seeds to the distilled water is 1:18, the extraction power is 100W, the extraction temperature is 48 ℃, the extraction times are 3 times, each time is 2 minutes, the extraction products are combined, the supernatant is obtained by centrifugation, and the freeze drying is carried out, thus obtaining the compound.
The preparation method of the saponin extract comprises the following steps: cleaning and drying gleditsia sinensis, crushing to 100 meshes to obtain gleditsia sinensis powder, then placing the gleditsia sinensis powder in a supercritical carbon dioxide extraction kettle, adding 75% ethanol aqueous solution with volume concentration being 0.5 times of the weight of the gleditsia sinensis powder, introducing carbon dioxide at the flow rate of 9L/h, wherein the extraction temperature is 60 ℃, the extraction pressure is 20MPa, and the extraction time is 125 minutes to obtain an extract, finally adding the extract into a separation kettle, and controlling the pressure in the separation kettle to be 20MPa and the temperature to be 60 ℃ to obtain the gleditsia sinensis extract.
The preparation method of the pine needle extract comprises the following steps: the preparation method comprises the steps of cleaning and drying pine needles, then crushing the pine needles to 90 meshes to obtain pine needle powder, then adding the pine needle powder into an ethanol aqueous solution with the volume concentration of 85% and the weight 8 times that of the pine needle powder, then extracting the pine needle powder for 9 minutes by using 600W microwaves, centrifuging the extract to obtain supernatant, and concentrating the supernatant under reduced pressure to obtain an extract with the relative density of 1.30.
The preparation method of the hair-care brain-strengthening shampoo soap comprises the following specific steps:
(1) Firstly stirring and dissolving the formula amount of sodium hydroxide in the formula amount of water to obtain a sodium hydroxide solution, then adding the formula amount of lemon oil and citric acid into the sodium hydroxide solution preheated to 70 ℃, keeping the temperature, stirring and reacting for 50 minutes, and drying to obtain a soap base;
(2) Then heating the soap base to 70 ℃, and stirring for 25 minutes under the condition of heat preservation to obtain soap base melt;
(3) And then adding the formula amount of the Chinese honeylocust fruit extract into the soap base molten liquid, stirring and uniformly mixing, then continuously adding the formula amount of the Chinese gall extract, the polygonum multiflorum extract, the black wolfberry fruit extract, the acer truncatum seed extract, the logwood extract, the ginger extract, the mulberry seed extract, the pine needle extract and the honey, stirring and uniformly mixing, pouring into a mould, naturally cooling and solidifying, demoulding, and naturally air drying to obtain the shampoo soap.
In the step (3), the gallnut extract, the polygonum multiflorum extract, the lycium ruthenicum extract, the acer truncatum seed extract, the logwood extract, the ginger extract, the mulberry seed extract, the pine needle extract and the honey are mixed uniformly at 28 ℃ in advance and then fed, the feeding is carried out at a constant speed and slowly for 18 minutes, and the uniform mixing is realized by stirring for 25 minutes after the feeding is finished.
Comparative example 1
A hair care and brain strengthening shampoo soap is prepared by mixing the following components: 0.5kg of nutgall extract, 0.5kg of polygonum multiflorum extract, 0.3kg of lycium ruthenicum extract, 0.5kg of logwood extract, 0.3kg of ginger extract, 0.3kg of mulberry seed extract, 0.5kg of Chinese honeylocust fruit extract, 0.5kg of pine needle extract, 0.5kg of citric acid, 0.5kg of honey, 8kg of lemon oil, 4kg of sodium hydroxide and 10kg of water.
The preparation method of the gallnut extract comprises the following steps: cleaning and drying nutgall, and crushing to 80 meshes to obtain nutgall powder, adding the nutgall powder into a 7-time-by-weight ethanol aqueous solution with the volume concentration of 70%, soaking for 6 hours at room temperature, then carrying out ultrasonic oscillation treatment for 45 minutes at 30kHz under the condition of 55 ℃, centrifuging, taking supernatant, and concentrating under reduced pressure to obtain an extract with the relative density of 1.10.
The preparation method of the polygonum multiflorum extract comprises the following steps: firstly, cleaning and drying polygonum multiflorum, then crushing the polygonum multiflorum into 80 meshes to obtain polygonum multiflorum powder, then adding the polygonum multiflorum powder into a 7-time ethanol water solution with volume concentration of 75% by weight, soaking the polygonum multiflorum powder for 6 hours at room temperature, then carrying out ultrasonic oscillation treatment for 40 minutes at 35kHz at 50 ℃, centrifuging the polygonum multiflorum powder, taking supernatant, and concentrating the supernatant under reduced pressure to obtain an extract with the relative density of 1.15.
The preparation method of the lycium ruthenicum extract comprises the following steps: firstly, cleaning fresh lycium ruthenicum, transferring the cleaned fresh lycium ruthenicum to a flash extractor, and carrying out flash extraction by using distilled water, wherein the mass ratio of the lycium ruthenicum to the distilled water is 1:15, extracting at the extraction power of 80W and the extraction temperature of 50 ℃ for 2 times, extracting for 1 minute each time, combining the extracted products, centrifuging, taking the supernatant, and freeze-drying to obtain the product.
The preparation method of the logwood extract comprises the following steps: cleaning bark of logwood, drying, pulverizing into 80 mesh to obtain logwood powder, adding logwood powder into 7 times of methanol water solution with volume concentration of 50%, soaking at room temperature for 8 hr, performing ultrasonic oscillation treatment at 50 deg.C and 40kHz for 40 min, centrifuging to obtain supernatant, and concentrating under reduced pressure to obtain extract with relative density of 1.20.
The preparation method of the ginger extract comprises the following steps: cleaning fresh ginger, slicing, drying, pulverizing to 80 mesh to obtain ginger powder, adding the ginger powder into water, adding papain and ferrous sulfate while stirring, stirring and heating at 55 deg.C for 6 hr, naturally cooling to room temperature, centrifuging to obtain supernatant, and spray drying; wherein the mass ratio of the ginger powder to the water to the papain to the ferrous sulfate is 1:7:3:1.
the preparation method of the mulberry seed extract comprises the following steps: firstly, cleaning fresh mulberry seeds, transferring the cleaned fresh mulberry seeds to a flash extractor, and carrying out flash extraction by using distilled water, wherein the mass ratio of the mulberry seeds to the distilled water is 1:15, extracting at the extraction power of 80W and the extraction temperature of 45 ℃ for 2 times, extracting for 1 minute each time, combining the extracted products, centrifuging, taking the supernatant, and freeze-drying to obtain the traditional Chinese medicine composition.
The preparation method of the saponin extract comprises the following steps: cleaning and drying the Chinese honeylocust fruit, crushing the Chinese honeylocust fruit into 80 meshes to obtain Chinese honeylocust fruit powder, then placing the Chinese honeylocust fruit powder into a supercritical carbon dioxide extraction kettle, adding 70% ethanol aqueous solution with the volume concentration being 0.4 time of the weight of the Chinese honeylocust fruit powder, introducing carbon dioxide at the flow rate of 8L/h, extracting at the temperature of 55 ℃, the extraction pressure of 18MPa and the extraction time of 120 minutes to obtain an extract, finally adding the extract into a separation kettle, and controlling the pressure in the separation kettle to be 18MPa and the temperature to be 55 ℃ to obtain the Chinese honeylocust fruit extract.
The preparation method of the pine needle extract comprises the following steps: the preparation method comprises the steps of cleaning pine needles, drying, crushing to 80 meshes to obtain pine needle powder, adding the pine needle powder into an 80% ethanol aqueous solution with volume concentration of 7 times of the pine needle powder, performing microwave extraction for 8 minutes by using 500W, centrifuging to obtain supernatant, and performing reduced pressure concentration to obtain an extract with the relative density of 1.25.
The preparation method of the hair care and brain strengthening shampoo soap comprises the following specific steps:
(1) Firstly stirring and dissolving the sodium hydroxide with the formula amount in the water with the formula amount to obtain a sodium hydroxide solution, then adding the lemon oil and the citric acid with the formula amount into the sodium hydroxide solution preheated to 65 ℃, keeping the temperature, stirring and reacting for 45 minutes, and drying to obtain a soap base;
(2) Then heating the soap base to 65 ℃, and stirring for 20 minutes under the condition of heat preservation to obtain soap base melt;
(3) And then adding the formula amount of Chinese honeylocust fruit extract into the soap base molten liquid, stirring and mixing uniformly, then continuously adding the formula amount of Chinese gall extract, polygonum multiflorum extract, lycium ruthenicum extract, logwood extract, ginger extract, mulberry seed extract, pine needle extract and honey, stirring and mixing uniformly, pouring into a mould, naturally cooling and solidifying, demoulding, and naturally air-drying to obtain the shampoo soap.
In the step (3), the gallnut extract, the polygonum multiflorum extract, the lycium ruthenicum extract, the acer truncatum seed extract, the logwood extract, the ginger extract, the mulberry seed extract, the pine needle extract and the honey are mixed uniformly at 26 ℃ in advance and then fed, the feeding is carried out at a constant speed and slowly for 15 minutes, and the uniform mixing is realized after the feeding is finished and the stirring is carried out for 20 minutes.
Comparative example 2
A hair care and brain tonic shampoo soap is prepared by mixing the following components: 0.5kg of Chinese gall extract, 0.5kg of polygonum multiflorum extract, 0.3kg of lycium ruthenicum extract, 1kg of acer truncatum seed extract, 0.5kg of logwood extract, 0.3kg of ginger extract, 0.3kg of mulberry seed extract, 0.5kg of Chinese honeylocust fruit extract, 0.5kg of pine needle extract, 0.5kg of citric acid, 0.5kg of honey, 8kg of lemon oil, 4kg of sodium hydroxide and 10kg of water.
The preparation method of the galla chinensis extract comprises the following steps: cleaning and drying nutgall, and crushing to 80 meshes to obtain nutgall powder, adding the nutgall powder into a 7-time-by-weight ethanol aqueous solution with the volume concentration of 70%, soaking for 6 hours at room temperature, then carrying out ultrasonic oscillation treatment for 45 minutes at 30kHz under the condition of 55 ℃, centrifuging, taking supernatant, and concentrating under reduced pressure to obtain an extract with the relative density of 1.10.
The preparation method of the polygonum multiflorum extract comprises the following steps: cleaning and drying polygonum multiflorum, crushing to 80 meshes to obtain polygonum multiflorum powder, adding the polygonum multiflorum powder into a 75% ethanol aqueous solution with volume concentration 7 times the weight of the polygonum multiflorum powder, soaking for 6 hours at room temperature, carrying out 35kHz ultrasonic oscillation treatment for 40 minutes at 50 ℃, centrifuging, taking supernatant, and concentrating under reduced pressure to obtain an extract with the relative density of 1.15.
The preparation method of the lycium ruthenicum extract comprises the following steps: firstly, cleaning fresh lycium ruthenicum, transferring the cleaned fresh lycium ruthenicum to a flash extractor, and carrying out flash extraction by using distilled water, wherein the mass ratio of the lycium ruthenicum to the distilled water is 1:15, extracting at 50 ℃ for 2 times for 1 minute at the extraction power of 80W, combining the extracted products, centrifuging to obtain supernatant, and freeze-drying to obtain the product.
The preparation method of the acer truncatum seed extract comprises the following steps: firstly, washing acer truncatum seeds, drying, and then crushing to 80 meshes to obtain acer truncatum seed powder, then adding the acer truncatum seed powder into 80% ethanol aqueous solution with volume concentration 7 times of the weight of the acer truncatum seed powder, then carrying out microwave extraction for 5 minutes by 400W, centrifuging to obtain supernatant, and carrying out reduced pressure concentration to obtain extract with relative density of 1.20.
The preparation method of the logwood extract comprises the following steps: cleaning bark of logwood, drying, pulverizing into 80 mesh to obtain logwood powder, adding logwood powder into 7 times of methanol water solution with volume concentration of 50%, soaking at room temperature for 8 hr, performing ultrasonic oscillation treatment at 50 deg.C and 40kHz for 40 min, centrifuging to obtain supernatant, and concentrating under reduced pressure to obtain extract with relative density of 1.20.
The preparation method of the ginger extract comprises the following steps: cleaning fresh ginger, slicing, drying, pulverizing to 80 mesh to obtain ginger powder, adding the ginger powder into water, adding papain and ferrous sulfate while stirring, stirring and heating at 55 deg.C for 6 hr, naturally cooling to room temperature, centrifuging to obtain supernatant, and spray drying; wherein the mass ratio of the ginger powder to the water to the papain to the ferrous sulfate is 1:7:3:1.
the preparation method of the mulberry seed extract comprises the following steps: firstly, cleaning fresh mulberry seeds, transferring the cleaned fresh mulberry seeds to a flash extractor, and carrying out flash extraction by using distilled water, wherein the mass ratio of the mulberry seeds to the distilled water is 1:15, extracting at the extraction power of 80W and the extraction temperature of 45 ℃ for 2 times, extracting for 1 minute each time, combining the extracted products, centrifuging, taking the supernatant, and freeze-drying to obtain the traditional Chinese medicine composition.
The preparation method of the saponin extract comprises the following steps: cleaning and drying the Chinese honeylocust, crushing the Chinese honeylocust to 80 meshes to obtain Chinese honeylocust powder, then placing the Chinese honeylocust powder in a supercritical carbon dioxide extraction kettle, adding 70% ethanol aqueous solution with volume concentration of 0.4 time of the weight of the Chinese honeylocust powder, introducing carbon dioxide at the flow rate of 8L/h, extracting at the temperature of 55 ℃, the extraction pressure of 18MPa and the extraction time of 120 minutes to obtain an extract, finally adding the extract into a separation kettle, and controlling the pressure in the separation kettle to be 18MPa and the temperature to be 55 ℃ to obtain the Chinese honeylocust extract.
The preparation method of the pine needle extract comprises the following steps: the preparation method comprises the steps of cleaning pine needles, drying, crushing to 80 meshes to obtain pine needle powder, adding the pine needle powder into an 80% ethanol aqueous solution with volume concentration of 7 times of the pine needle powder, performing microwave extraction for 8 minutes by using 500W, centrifuging to obtain supernatant, and performing reduced pressure concentration to obtain an extract with the relative density of 1.25.
The preparation method of the hair care and brain strengthening shampoo soap comprises the following specific steps:
(1) Firstly, stirring and dissolving sodium hydroxide with a formula amount in water with a formula amount to obtain a sodium hydroxide solution, then adding lemon oil and citric acid with a formula amount into the sodium hydroxide solution preheated to 65 ℃, preserving heat, stirring and reacting for 45 minutes, and drying to obtain a soap base;
(2) Then heating the soap base to 65 ℃, and stirring for 20 minutes under the condition of heat preservation to obtain soap base melt;
(3) And then adding the formula amount of the Chinese honeylocust fruit extract into the soap base molten liquid, stirring and uniformly mixing, then sequentially adding the formula amount of the Chinese gall extract, the polygonum multiflorum extract, the black wolfberry extract, the acer truncatum seed extract, the logwood extract, the ginger extract, the mulberry seed extract, the pine needle extract and the honey, stirring and mixing for 20 minutes, pouring into a mold, naturally cooling and solidifying, demolding, and naturally air drying to obtain the shampoo soap.
1200 patients with senile dementia caused by white hair combined with degenerative brain injury, the age of 50-70 years old and half of men and women, which are randomly and averagely divided into 6 groups, are aged 50-70 years old and half of men and women, and half of men and women in each group (200 persons), respectively use the shampoo soaps of examples 1-4 and comparative examples 1 and 2, the hair and the scalp are fully wetted once a day, the shampoo soaps are rubbed and foamed in the palm and then fully contacted with the scalp for 1 minute, the shampoo soaps are washed clean and then absorb excessive water by a dry towel, and the hair state is examined after the shampoo towels are continuously used for one year, and the results are shown in table 1.
And (3) comparing with the white hair condition before use, and inspecting the black hair effect, wherein the specific standards are as follows:
1. and (3) healing: the white hair is completely blackened;
2. the effect is shown: over 80% (including 80%) of white hairs turn black;
3. the method has the following advantages: 30-80% (including 30%, not including 80%) of white hair turns black;
4. and (4) invalidation: the white hair turned black at 30% or less (not including 30%).
The hair growth effect examination standard is as follows:
1. the hair growth is obvious: the hairline is obviously moved forward, and the hair is visible to the naked eye;
2. hair growth is generally increased: the hairline slightly moves forward, and the hair is thicker;
3. no hair increasing effect: the hairline is unchanged and even continuously moves backwards, and the hair is not thicker than before use.
TABLE 1 Hair Condition examination before and after shampoo application
The intelligent change of the patient is evaluated by adopting an Alzheimer disease rating scale-cognition part, so that the brain strengthening effect investigation is carried out:
efficacy index = (pre-treatment integral-post-treatment integral)/post-treatment integral × 100%;
the specific measurement criteria are:
1. the effect is shown: the curative effect index is more than or equal to 20 percent;
2. the improvement is as follows: 20 percent more than the curative effect index more than or equal to 10 percent
3. No step back: more than 10% and more than or equal to 0% of curative effect index
4. And (4) invalidation: less than 0%.
TABLE 2 examination of brain tonic Effect
| Display effect (human) | Progress (human)) | No back step (human) | Invalid (human) | |
| Example 1 | 196 | 4 | 0 | 0 |
| Example 2 | 196 | 4 | 0 | 0 |
| Example 3 | 198 | 2 | 0 | 0 |
| Example 4 | 200 | 0 | 0 | 0 |
| Comparative example 1 | 183 | 15 | 2 | 0 |
| Comparative example 2 | 190 | 10 | 0 | 0 |
As can be seen from tables 1 and 2, the hair soaps of examples 1 to 4 have good hair blackening and hair growth promoting effects, and have certain brain strengthening effects.
The acer truncatum seed extract is omitted in the comparative example 1, the gallnut extract, the polygonum multiflorum extract, the lycium ruthenicum extract, the acer truncatum seed extract, the logwood extract, the ginger extract, the mulberry seed extract, the pine needle extract and the honey are directly fed at one time in the comparative example 2, the hair blackening effect, the hair increasing effect and the brain strengthening effect of the shampoo soap are obviously poor, the synergistic effect of the components is illustrated, and the use performance of the shampoo soap is directly influenced by the feeding control in the preparation process.
Although the present invention has been described with reference to the specific embodiments, it is not intended to limit the scope of the present invention, and various modifications and variations can be made by those skilled in the art without inventive changes based on the technical solution of the present invention.
Claims (10)
1. The hair care and brain strengthening shampoo soap is characterized by being prepared by mixing the following components in parts by weight: 0.5-5 parts of gallnut extract, 0.5-5 parts of fleece-flower root extract, 0.3-3 parts of black wolfberry extract, 1-15 parts of acer truncatum seed extract, 0.5-5 parts of logwood extract, 0.3-3 parts of ginger extract, 0.3-3 parts of mulberry seed extract, 0.5-5 parts of Chinese honeylocust fruit extract, 0.5-5 parts of pine needle extract, 0.5-5 parts of citric acid, 0.5-5 parts of honey, 8-10 parts of lemon oil, 4-5 parts of sodium hydroxide and 10-15 parts of water.
2. The hair care and brain tonic shampoo soap according to claim 1, wherein the gallnut extract is prepared by the following steps: washing and drying nutgall, and crushing the nutgall into 80-100 meshes to obtain nutgall powder, adding the nutgall powder into an ethanol water solution with volume concentration of 70-80% and 7-9 times of the weight of the nutgall powder, soaking the nutgall powder for 6-8 hours at room temperature, then carrying out ultrasonic oscillation treatment on the nutgall powder for 45-55 minutes at the temperature of 55-65 ℃, centrifuging the nutgall powder to obtain a supernatant, and concentrating the supernatant under reduced pressure to obtain an extract with the relative density of 1.10-1.20.
3. The hair care and brain tonic shampoo soap of claim 1, wherein the polygonum multiflorum extract is prepared by the following method: firstly, cleaning and drying polygonum multiflorum, then crushing the polygonum multiflorum into 80-100 meshes to obtain polygonum multiflorum powder, then adding the polygonum multiflorum powder into an ethanol water solution with volume concentration of 75-85% and weight which is 7-9 times of the polygonum multiflorum powder, soaking the polygonum multiflorum powder for 6-8 hours at room temperature, then carrying out ultrasonic oscillation treatment on the polygonum multiflorum powder for 40-50 minutes at the temperature of 50-60 ℃, centrifuging the polygonum multiflorum powder to obtain a supernatant, and concentrating the supernatant under reduced pressure to obtain an extract with the relative density of 1.15-1.25.
4. The hair care and brain strengthening shampoo soap according to claim 1, wherein the lycium ruthenicum extract is prepared by the following method: firstly, cleaning fresh lycium ruthenicum, transferring the cleaned fresh lycium ruthenicum to a flash extractor, and carrying out flash extraction by using distilled water, wherein the mass ratio of the lycium ruthenicum to the distilled water is 1: 15-20, the extraction power is 80-100W, the extraction temperature is 50-55 ℃, the extraction times are 2-3, each time for 1-2 minutes, the extraction products are combined, the supernatant is obtained by centrifugation, and the freeze drying is carried out, thus obtaining the product.
5. The hair care and brain strengthening shampoo soap according to claim 1, wherein the acer truncatum seed extract is prepared by the following method: firstly, washing and drying acer truncatum seeds, then crushing the acer truncatum seeds into 80-100 meshes to obtain acer truncatum seed powder, then adding the acer truncatum seed powder into 80-85% ethanol aqueous solution with volume concentration of 7-9 times of the weight of the acer truncatum seed powder, then performing microwave extraction for 5-7 minutes by using 400-500W, centrifuging to obtain supernatant, and performing reduced pressure concentration to obtain extract with relative density of 1.20-1.25.
6. The hair care and brain tonic shampoo soap according to claim 1, wherein the logwood extract is prepared by the following method: firstly, bark of logwood is cleaned, dried and crushed to 80-100 meshes to obtain logwood powder, then the logwood powder is added into methanol water solution with volume concentration of 50-60% and 7-9 times of the logwood powder, the logwood powder is soaked for 8-10 hours at room temperature, then the logwood powder is treated by ultrasonic oscillation for 40-50 minutes at 50-60 ℃, and the logwood powder is centrifuged to take supernatant, and is decompressed and concentrated to extract with relative density of 1.20-1.30, thus obtaining the logwood powder.
7. The hair care and brain tonic shampoo soap according to claim 1, wherein the ginger extract is prepared by the following method: cleaning fresh ginger, slicing and drying, then crushing to 80-100 meshes to obtain ginger powder, then adding the ginger powder into water, adding papain and ferrous sulfate while stirring, stirring and heating at 55-60 ℃ for 6-8 hours, naturally cooling to room temperature, centrifuging to take supernatant, and spray-drying to obtain the ginger powder; wherein the mass ratio of the ginger powder to the water to the papain to the ferrous sulfate is 1:7 to 9:3 to 4:1 to 1.5.
8. The hair care and brain tonic shampoo soap according to claim 1, wherein the mulberry seed extract is prepared by the following method: firstly, cleaning fresh mulberry seeds, transferring the cleaned fresh mulberry seeds to a flash extractor, and carrying out flash extraction by using distilled water, wherein the mass ratio of the mulberry seeds to the distilled water is 1: 15-20, the extraction power is 80-100W, the extraction temperature is 45-50 ℃, the extraction times are 2-3, each time extraction is 1-2 minutes, the extraction products are combined, the supernatant is obtained by centrifugation, and freeze drying is carried out, thus obtaining the product.
9. The hair care and brain tonic shampoo soap according to claim 1, wherein the saponin extract is prepared by the following method: cleaning and drying gleditsia sinensis, crushing to 80-100 meshes to obtain gleditsia sinensis powder, then placing the gleditsia sinensis powder in a supercritical carbon dioxide extraction kettle, adding 70-80% ethanol aqueous solution with volume concentration of 0.4-0.5 times of the weight of the gleditsia sinensis powder, introducing carbon dioxide at the flow rate of 8-10L/h, wherein the extraction temperature is 55-65 ℃, the extraction pressure is 18-22 MPa, and the extraction time is 120-130 minutes to obtain an extract, finally adding the extract into a separation kettle, and controlling the pressure in the separation kettle to be 18-22 MPa and the temperature to be 55-65 ℃ to obtain the gleditsia sinensis extract.
10. The method for preparing the hair care and brain strengthening shampoo soap according to any one of claims 1 to 9, which is characterized by comprising the following specific steps:
(1) Firstly stirring and dissolving the sodium hydroxide with the formula amount in the water with the formula amount to obtain a sodium hydroxide solution, then adding the lemon oil and the citric acid with the formula amount into the sodium hydroxide solution preheated to 65-75 ℃, keeping the temperature, stirring and reacting for 45-55 minutes, and drying to obtain a soap base;
(2) Then heating the soap base to 65-75 ℃, and stirring for 20-30 minutes under the condition of heat preservation to obtain soap base molten liquid;
(3) And then adding the formula amount of Chinese honeylocust fruit extract into the soap base molten liquid, stirring and uniformly mixing, then continuously adding the formula amount of Chinese gall extract, polygonum multiflorum extract, lycium ruthenicum extract, acer truncatum seed extract, logwood extract, ginger extract, mulberry seed extract, pine needle extract and honey, stirring and uniformly mixing, pouring into a mould, naturally cooling and solidifying, demoulding, and naturally air-drying to obtain the shampoo soap.
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