CN115670966B - Moisturizing facial mask base cloth and preparation method thereof - Google Patents

Moisturizing facial mask base cloth and preparation method thereof Download PDF

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CN115670966B
CN115670966B CN202211400859.2A CN202211400859A CN115670966B CN 115670966 B CN115670966 B CN 115670966B CN 202211400859 A CN202211400859 A CN 202211400859A CN 115670966 B CN115670966 B CN 115670966B
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mask base
base cloth
moisturizing
porous
soaking
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CN115670966A (en
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赵孝龙
徐光洪
吴杭琪
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Yuyao Longxiang Spunlace Hot Rolling Non Woven Co ltd
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Yuyao Longxiang Spunlace Hot Rolling Non Woven Co ltd
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Abstract

The application relates to the technical field of fiber materials, and particularly discloses a preparation method of a moisturizing facial mask base fabric, which comprises the following steps: s1: soaking the porous mask base cloth in potassium lactate solution, standing for 20-30min, adding sericin solution, adjusting pH to 6-7 with hydrochloric acid solution, oscillating at constant temperature of 25-37deg.C for 5-8h, and washing with deionized water to obtain modified porous mask base cloth; s2, soaking the modified porous mask base cloth obtained in the step S1 in polyethylene glycol solution, standing for 30-45min at 25-40 ℃, washing with deionized water after the reaction is completed, drying to obtain a moisturizing mask base cloth, soaking the moisturizing mask base cloth in essence, and packaging to obtain the moisturizing mask. It has the advantage of improving the moisturizing effect of the mask base cloth.

Description

Moisturizing facial mask base cloth and preparation method thereof
Technical Field
The application relates to the technical field of fiber materials, in particular to a moisturizing facial mask base fabric and a preparation method thereof.
Background
With the improvement of society and the improvement of living standard, the beauty textile material represented by functions of beauty, health care, comfort, leisure and the like presents strong market demands, and the mask product is an important application field of modern textile materials because of the special effects of eliminating fatigue, relieving pressure, maintaining beauty, keeping young and the like, and has rapid development.
The conventional facial mask base cloth mainly comprises a filament fiber facial mask base cloth taking cotton linters as raw materials, a tencel fiber facial mask base cloth taking wood pulp cellulose as raw materials, a lyocell fiber base cloth, a cotton fiber base cloth taking cotton as raw materials, a pulp fiber facial mask base cloth and the like, and in addition, the popular black fiber non-woven fabric facial mask base cloth taking bamboo charcoal or charcoal as raw materials is also started on the market.
In view of the above-mentioned related art, the inventor believes that, in the practical application process, the moisture absorption effect of the corresponding fiber material is poor, and the mask base cloth is used as a carrier of the mask essence material, when in use, moisture in the mask essence material volatilizes along with the rise of the facial temperature of a human body, and the moisture is a carrier for conveying nutrient components in the mask essence material, so that the utilization rate of the mask essence material is reduced, and the skin care effect of the mask is reduced.
Disclosure of Invention
In order to improve the moisturizing effect of the mask base cloth, the application provides the moisturizing mask base cloth and a preparation method thereof.
The application provides a moisturizing facial mask base cloth and a preparation method thereof, which adopts the following technical scheme:
the preparation method of the moisturizing facial mask base cloth comprises the following steps:
s1: soaking the porous mask base cloth in potassium lactate solution, standing for 20-30min, adding sericin solution, adjusting pH to 6-7 with hydrochloric acid solution, oscillating at constant temperature of 25-37deg.C for 5-8 hr, and washing with deionized water to obtain modified porous mask base cloth;
s2: soaking the modified porous mask base cloth obtained in the step S1 in polyethylene glycol solution, standing for 30-45min at 25-40 ℃, washing with deionized water after the reaction is completed, drying to obtain the moisturizing mask base cloth, soaking the moisturizing mask base cloth in essence, and packaging to obtain the moisturizing mask.
According to the technical scheme, in order to improve the moisturizing performance of the mask base cloth, the porous mask base cloth with a porous and multi-gully structure is soaked in the potassium lactate solution, potassium lactate molecules are adsorbed in the porous mask base cloth, then potassium lactate is wrapped by inducing sericin self-assembly through potassium ions, and then the sericin is crosslinked with polyethylene glycol to form a layer of moisturizing film on the surface of the porous mask base cloth.
The moisturizing film formed by the potassium lactate humectant is adhered in the porous mask base cloth by utilizing the porous structure of the porous mask base cloth, so that the prepared moisturizing mask base cloth has good moisturizing capability and achieves the effects of absorbing and preserving liquid.
Optionally, the concentration of sericin is 0.1-0.5wt%.
By adopting the technical scheme, the sericin has the components and functions similar to those of the natural moisturizing factors of the skin cuticle, has the functions of moisturizing, whitening, resisting oxidation, resisting bacteria, diminishing inflammation, absorbing and inhibiting ultraviolet rays and the like on the skin, self-assembles under the induction of potassium ions of potassium lactate, wraps the potassium lactate in pores of the porous mask base cloth, and achieves the effect of high water locking and moisturizing.
Optionally, the concentration of potassium lactate is 2-5wt%.
By adopting the technical scheme, the potassium lactate can be used as a humectant, can be used as a glycerin substitute, has good hygroscopicity, can be used as a conditioner and a skin softener, and has mild effect on skin.
Optionally, the concentration of the polyethylene glycol is 0.8-1.5wt%.
By adopting the technical scheme, the polyethylene glycol can form hydrogen bonds with the sericin macromolecules, and more hydrogen bond interactions can crosslink the sericin macromolecules. The crosslinking forming of the network structure is beneficial to water locking, the polyhydroxy of the polyethylene glycol provides good hydrophilicity, and the polyethylene glycol and sericin with a moisturizing effect react on the surface of the porous mask base cloth to form a film through crosslinking, so that the liquid holding capacity is strong, and the effect of moisture holding is achieved.
Optionally, the polyethylene glycol has a molecular weight of 200-600Da.
By adopting the technical scheme, the moisture retention of the polyethylene glycol with low molecular weight is better than that of the polyethylene glycol with high molecular weight, the molecular chain movement of the polyethylene glycol with low molecular weight is relatively flexible, and the high-efficiency exchange environment of water molecules can be provided.
Optionally, the porous mask base fabric comprises the following preparation steps:
step one, twisting bamboo charcoal fiber yarns and seaweed fiber yarns into mixed fiber yarns, and braiding to form a fiber net;
soaking the fiber net in distilled water, performing ultrasonic treatment, and drying to obtain a porous fiber net;
and thirdly, overlapping and tiling 3-4 layers of porous fiber net, and extruding at constant temperature to obtain the porous mask base cloth.
By adopting the technical scheme, the bamboo charcoal fiber and the alginate fiber are woven into the porous fiber net. The prepared porous fiber net has porous and multi-gully structure, and in addition, by means of strong adsorption of bamboo charcoal, the humectant is wrapped in the pores through self-assembled sericin, and then the sericin and polyethylene glycol undergo a crosslinking reaction to form a moisturizing film, so that the high moisturizing effect of the mask base cloth is achieved, the storage capacity of liquid is improved, and the effects of absorbing and preserving liquid are achieved.
Optionally, the constant temperature extrusion reaction temperature is 30-60 ℃ and the pressure is 0.5-0.7MPa.
By adopting the technical scheme, the multi-layer mask base cloth is extruded together at a certain temperature and pressure, mutual fusion of the alginate fiber filaments and the porous bamboo charcoal fiber filaments is promoted, staggered fiber filaments are formed, dense porous gaps are achieved, and the liquid holding capacity of the mask base cloth is improved.
Optionally, the mass ratio of the alginate fiber filaments to the bamboo charcoal fiber filaments is (2-4): 1.
by adopting the technical scheme, the bamboo charcoal has a loose and porous structure, is fine and porous in molecules, hard in texture and strong in adsorption capacity, and the alginate fiber has good biocompatibility, degradability and absorbability and good moisture absorption effect, so that the bamboo charcoal fiber and the alginate fiber are combined, and the bamboo charcoal fiber has good water absorbability and moisture retention.
In summary, the application has the following beneficial effects:
1. because the application adopts the potassium lactate and the sericin, in order to soak the porous mask base cloth with porous and multi-gully structure in the potassium lactate solution, potassium lactate molecules are adsorbed in the porous mask base cloth, and the potassium lactate is wrapped by the sericin self-assembly induced by potassium ions, the moisture retention molecules are loaded in the pores of the porous mask base cloth, and the moisture retention performance of the mask base cloth is improved.
2. The application adopts sericin and polyethylene glycol, the polyhydroxy of the polyethylene glycol provides good hydrophilicity, and the surface of the porous mask base cloth is crosslinked and reacted with the sericin with moisturizing effect to form a film, so that the formed moisturizing film layer improves the capability of retaining moisture.
3. The method of the application is characterized in that bamboo charcoal fiber and alginate fiber are woven into a porous fiber net. The prepared porous fiber net has porous and multi-gully structure, and in addition, by means of strong adsorption of bamboo charcoal, the humectant is wrapped in the pores through self-assembled sericin, and then the sericin and polyethylene glycol undergo a crosslinking reaction to form a moisturizing film, so that the high moisturizing effect of the mask base cloth is achieved, the storage capacity of liquid is improved, and the effects of absorbing and preserving liquid are achieved.
Detailed Description
The present application will be described in further detail with reference to examples and comparative examples.
The following examples and comparative examples are provided as sources of raw materials: the starting materials for the examples and comparative examples are commercially available.
Examples of preparation method of moisturizing facial mask base cloth
Example 1
The preparation method of the moisturizing facial mask base fabric comprises the following steps:
step one, twisting bamboo charcoal fiber yarns and seaweed fiber yarns into mixed fiber yarns, and braiding to form a fiber net, wherein the mass ratio of the seaweed fiber yarns to the bamboo charcoal fiber yarns is 3:1;
soaking the fiber net in distilled water, performing ultrasonic treatment at room temperature for 1h with ultrasonic frequency of 30kHz, taking out, and drying at 40 ℃ to obtain a porous fiber net;
and thirdly, overlapping and tiling 3 layers of porous fiber net, and carrying out extrusion reaction for 2 hours at the temperature of 50 ℃ and the pressure of 0.6MPa to obtain the porous mask base cloth.
S1: soaking the porous mask base cloth in a potassium lactate aqueous solution, keeping the potassium lactate concentration at 4wt% and standing for 25min, then adding a sericin aqueous solution, adjusting the pH to 6 by using a 0.5mol/L hydrochloric acid solution, oscillating for 6h at a constant temperature of 30 ℃, and washing with deionized water to obtain a modified porous mask base cloth;
s2: soaking the modified porous mask base cloth obtained in the step S1 in a polyethylene glycol aqueous solution, wherein the molecular weight of the polyethylene glycol is 400Da, the concentration of the polyethylene glycol is 1wt%, reacting for 40min at 35 ℃, washing with deionized water after the reaction is finished, drying at 30 ℃ to obtain a moisturizing mask base cloth, soaking the moisturizing mask base cloth in essence, and packaging to obtain the moisturizing mask.
Example 2
The preparation method of the moisturizing facial mask base fabric comprises the following steps:
step one, twisting bamboo charcoal fiber yarns and seaweed fiber yarns into mixed fiber yarns, and braiding to form a fiber net, wherein the mass ratio of the seaweed fiber yarns to the bamboo charcoal fiber yarns is 2:1;
soaking the fiber net in distilled water, performing ultrasonic treatment at room temperature for 1h with ultrasonic frequency of 30kHz, taking out, and drying at 40 ℃ to obtain a porous fiber net;
and thirdly, overlapping and tiling 3 layers of porous fiber net, and carrying out extrusion reaction for 2 hours at the temperature of 30 ℃ and the pressure of 0.5MPa to obtain the porous mask base cloth.
S1: soaking the porous mask base cloth in a potassium lactate aqueous solution, keeping the concentration of potassium lactate at 2wt%, standing for 20min, adding a sericin aqueous solution, adjusting the pH to 6 by using a 0.5mol/L hydrochloric acid solution, oscillating for 5h at a constant temperature of 25 ℃, and washing with deionized water to obtain a modified porous mask base cloth;
s2: soaking the modified porous mask base cloth obtained in the step S1 in a polyethylene glycol aqueous solution, wherein the molecular weight of the polyethylene glycol is 200Da, the concentration of the polyethylene glycol is 0.8wt%, reacting for 30min at 25 ℃, washing with deionized water after the reaction is finished, drying at 30 ℃ to obtain a moisturizing mask base cloth, soaking the moisturizing mask base cloth in essence, and packaging to obtain the moisturizing mask.
Example 3
The preparation method of the moisturizing facial mask base fabric comprises the following steps:
step one, twisting bamboo charcoal fiber yarns and seaweed fiber yarns into mixed fiber yarns, and weaving to form a fiber net, wherein the mass ratio of the seaweed fiber yarns to the bamboo charcoal fiber yarns is 4:1;
soaking the fiber net in distilled water, performing ultrasonic treatment at room temperature for 1h with ultrasonic frequency of 30kHz, taking out, and drying at 40 ℃ to obtain a porous fiber net;
and thirdly, carrying out overlapping tiling on 4 layers of porous fiber net, and carrying out extrusion reaction for 2 hours at the temperature of 60 ℃ and the pressure of 0.7MPa to obtain the porous mask base cloth.
S1: soaking the porous mask base cloth in a potassium lactate aqueous solution, standing for 30min, adding a sericin aqueous solution, wherein the concentration of sericin is 0.5wt%, adjusting the pH value to 6 by using a 0.5mol/L hydrochloric acid solution, oscillating for 8h at a constant temperature of 37 ℃, and washing with deionized water to obtain a modified porous mask base cloth;
s2: soaking the modified porous mask base cloth obtained in the step S1 in a polyethylene glycol aqueous solution, wherein the molecular weight of the polyethylene glycol is 600Da, the concentration of the polyethylene glycol is 1.5wt%, reacting for 45min at 40 ℃, washing with deionized water after the reaction is finished, drying at 30 ℃ to obtain a moisturizing mask base cloth, soaking the moisturizing mask base cloth in essence, and packaging to obtain the moisturizing mask.
Example 4
A method for preparing a moisturizing facial mask base fabric, which is different from example 2 in that the concentration of sericin is 0.05wt%.
Example 5
A preparation method of a moisturizing facial mask base fabric is different from example 3 in that the concentration of sericin is 0.6wt%.
Example 6
A method for preparing a moisture-retaining facial mask base fabric, which is different from example 2 in that the concentration of potassium lactate is 1wt%.
Example 7
A method for preparing a moisture-retaining facial mask base fabric, which is different from example 3 in that the concentration of potassium lactate is 6wt%.
Example 8
A preparation method of a moisturizing facial mask base fabric is different from example 2 in that the concentration of polyethylene glycol is 0.6wt%.
Example 9
A method for preparing a moisturizing facial mask base fabric is different from example 3 in that the concentration of polyethylene glycol is 1.7wt%.
Example 10
A preparation method of a moisturizing facial mask base fabric is different from example 2 in that the molecular weight of polyethylene glycol is 1000Da.
Example 11
The preparation method of the moisturizing facial mask base fabric is different from that of the embodiment 2 in that the mass ratio of the alginate fiber filaments to the bamboo charcoal fiber filaments is 1:1.
Example 12
The preparation method of the moisturizing facial mask base fabric is different from that of the embodiment 3 in that the mass ratio of the alginate fiber filaments to the bamboo charcoal fiber filaments is 1:2.
Comparative example
Comparative example 1
A method for preparing a moisturizing facial mask base fabric, which is different from example 1 in that the raw material does not include potassium lactate. The preparation step of the step S1 is as follows: soaking the porous mask base cloth in sericin aqueous solution, wherein the concentration of sericin is 0.1wt%, regulating the pH value to 6 by using 0.5mol/L hydrochloric acid solution, oscillating for 5 hours at the constant temperature of 25 ℃, and washing by using deionized water to obtain the modified porous mask base cloth.
Comparative example 2
A method for preparing a moisturizing facial mask base fabric, which is different from example 1 in that the raw material does not include polyethylene glycol. The preparation step of the step S2 is as follows: and (3) dipping the modified porous mask base cloth obtained in the step (S1) into essence, and packaging to obtain the moisturizing mask.
Comparative example 3
A preparation method of a moisturizing facial mask base fabric is different from that of the embodiment 1 in that raw materials do not comprise potassium lactate, sericin and polyethylene glycol, the prepared porous facial mask base fabric is directly immersed in essence, and the moisturizing facial mask is obtained by packaging.
Performance test sample: performance test was performed using the moisturizing facial mask base fabrics without the impregnated essence prepared in examples 1 to 12 and comparative examples 1 to 3 as test samples.
The experimental method comprises the following steps: cutting 3 pieces of mask base cloth with the size of 60mm multiplied by 60mm on the same Zhang Mianmo base cloth to serve as samples, weighing the samples on a weighing balance (the accurate value is 0.0001 g), putting the weighed samples into a beaker containing water, taking out the samples after 15min for weighing, calculating the water absorption (taking the average value of three samples), putting the samples into a constant temperature and humidity box after weighing, taking out the samples after drying for 20 hours, weighing, and calculating the water retention (taking the average value of three samples).
Water absorption= (mass before water absorption of mask base cloth-mass after water absorption of mask base cloth)/mass before water absorption of mask base cloth, water retention= (mass before water absorption of mask base cloth after placing the mask base cloth in a constant temperature and humidity box for 20 hours)/mass before water absorption of mask base cloth.
TABLE 1 Performance test results
Example 1 Example 2 Example 3 Example 4 Example 5
Water absorption percentage% 620 610 600 523 516
Water retention percentage% 312 309 310 230 241
Example 6 Example 7 Example 8 Example 9 Example 10
Water absorption percentage% 403 400 451 440 479
Water retention percentage% 212 208 234 245 214
Example 11 Example 12 Comparative example 1 Comparative example 2 Comparative example 3
Water absorption percentage% 401 437 385 360 321
Water retention percentage% 347 337 187 195 130
It can be seen from the combination of examples 2-3 and examples 4-5 and the combination of table 1 that examples 2-3 are superior to examples 4-5, and sericin has potassium lactate coated in pores of the porous mask, and the reaction concentration is lower or higher than that of potassium lactate, so that the self-assembly reaction of potassium lactate and sericin is not complete, and the moisturizing effect is affected.
It can be seen from the combination of examples 2-3 and examples 6-7 and the combination of Table 1 that examples 2-3 are superior to examples 6-7 in that potassium lactate concentration is low, the amount of potassium lactate adsorbed on the surface of the porous mask base cloth is reduced, the moisturizing effect is reduced, the amount of high concentration adsorbed is increased, the pores of the mask base cloth are reduced, and the water holding capacity is affected.
It can be seen from the combination of examples 2 to 3 and examples 8 to 9 and the combination of Table 1 that examples 2 to 3 are superior to examples 8 to 9 in that polyethylene glycol and sericin form a moisturizing film with low crosslinking density at low concentration, poor water retention effect, increased crosslinking density at high concentration, blocked water molecule exchange and reduced hygroscopicity.
It can be seen from the combination of examples 2-3 and examples 11-12 and the combination of table 1 that examples 2-3 are superior to examples 11-12 in that the proportion of bamboo charcoal fibers is increased, the adsorption performance is increased, the moisture retention performance is insufficient, the fitting property of the mask base cloth is poor, the proportion of alginate fibers is increased, the moisture retention effect is increased, but the adsorption amount of the humectant is reduced.
It can be seen from the combination of example 1 and comparative examples 1 to 3 and the combination of table 1 that, compared with the common mask, potassium lactate is used as a humectant and wrapped in pores of the mask base cloth through surface treatment of the porous mask base cloth, and then sericin and polyethylene glycol are crosslinked on the surface of the porous mask base cloth to form a film, so that molecules with good moisture retention property are attached to the surface of the porous mask. Achieving the effect of deep water locking and moisture preservation.
The present embodiment is only for explanation of the present application and is not to be construed as limiting the present application, and modifications to the present embodiment, which may not creatively contribute to the present application as required by those skilled in the art after reading the present specification, are all protected by patent laws within the scope of claims of the present application.

Claims (3)

1. A preparation method of a moisturizing facial mask base fabric is characterized by comprising the following steps: the mask base cloth is porous mask base cloth, and the porous mask base cloth is subjected to the following steps:
s1: soaking the porous mask base cloth in potassium lactate solution, standing for 20-30min, adding sericin solution, adjusting pH to 6-7 with acid solution, oscillating at constant temperature of 25-37deg.C for 5-8 hr, and washing with deionized water to obtain modified porous mask base cloth;
s2: soaking the modified porous mask base cloth obtained in the step S1 in polyethylene glycol solution, standing for 30-45min at 25-40 ℃, washing with deionized water after the reaction is completed, drying to obtain a moisturizing mask base cloth, soaking the moisturizing mask base cloth in essence, and packaging to obtain a moisturizing mask;
the concentration of sericin in S1 is 0.1-0.5wt%, and the concentration of potassium lactate is 2-5wt%;
the concentration of the polyethylene glycol in the S2 is 0.8-1.5wt%;
the porous mask base cloth in the S1 is prepared by the following preparation steps:
step one, twisting bamboo charcoal fiber yarns and seaweed fiber yarns into mixed fiber yarns, and braiding to form a fiber net;
soaking the fiber net in distilled water, performing ultrasonic treatment, and drying to obtain a porous fiber net;
step three, overlapping and tiling 3-4 layers of porous fiber net, and extruding at constant temperature to obtain porous mask base cloth;
the mass ratio of the alginate fiber yarn to the bamboo charcoal fiber yarn in the first step is (2-4): 1.
2. The method for preparing the moisturizing facial mask base fabric according to claim 1, wherein the method comprises the following steps: the molecular weight of the polyethylene glycol is 200-600Da.
3. The method for preparing the moisturizing facial mask base fabric according to claim 1, wherein the method comprises the following steps: the temperature of the constant-temperature extrusion reaction in the third step is 30-60 ℃ and the pressure is 0.5-0.7MPa.
CN202211400859.2A 2022-11-09 2022-11-09 Moisturizing facial mask base cloth and preparation method thereof Active CN115670966B (en)

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Publication number Priority date Publication date Assignee Title
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CN111939085A (en) * 2020-08-19 2020-11-17 浙江大学 Preparation method of silk mask and product

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CN109431821A (en) * 2018-12-26 2019-03-08 河南工程学院 A kind of nanofiber facial mask of the shale containing opal and preparation method thereof
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