CN115613352A - 一种透气防钻绒面料及其制备方法 - Google Patents
一种透气防钻绒面料及其制备方法 Download PDFInfo
- Publication number
- CN115613352A CN115613352A CN202211236061.9A CN202211236061A CN115613352A CN 115613352 A CN115613352 A CN 115613352A CN 202211236061 A CN202211236061 A CN 202211236061A CN 115613352 A CN115613352 A CN 115613352A
- Authority
- CN
- China
- Prior art keywords
- fabric
- proof
- mixing
- precursor
- breathable
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000004744 fabric Substances 0.000 title claims abstract description 164
- 238000002360 preparation method Methods 0.000 title claims abstract description 14
- 238000004519 manufacturing process Methods 0.000 title description 2
- 239000000835 fiber Substances 0.000 claims abstract description 64
- 229920000728 polyester Polymers 0.000 claims abstract description 36
- XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 claims abstract description 22
- 238000003490 calendering Methods 0.000 claims abstract description 18
- 230000003373 anti-fouling effect Effects 0.000 claims abstract description 13
- KWXWLBSPCCKZKO-UHFFFAOYSA-N 3-amino-5-(hydroxymethyl)phenol Chemical compound NC1=CC(O)=CC(CO)=C1 KWXWLBSPCCKZKO-UHFFFAOYSA-N 0.000 claims abstract description 12
- BRCWHGIUHLWZBK-UHFFFAOYSA-K bismuth;trifluoride Chemical compound F[Bi](F)F BRCWHGIUHLWZBK-UHFFFAOYSA-K 0.000 claims abstract description 11
- WMPIXNYJHKHSJG-UHFFFAOYSA-N ethyl 2-amino-6-hydroxybenzoate Chemical compound CCOC(=O)C1=C(N)C=CC=C1O WMPIXNYJHKHSJG-UHFFFAOYSA-N 0.000 claims abstract description 11
- 239000011787 zinc oxide Substances 0.000 claims abstract description 11
- 239000002253 acid Substances 0.000 claims abstract description 4
- 239000000758 substrate Substances 0.000 claims description 49
- 238000002156 mixing Methods 0.000 claims description 37
- 239000002243 precursor Substances 0.000 claims description 34
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 33
- WEVYAHXRMPXWCK-UHFFFAOYSA-N Acetonitrile Chemical compound CC#N WEVYAHXRMPXWCK-UHFFFAOYSA-N 0.000 claims description 24
- 239000008367 deionised water Substances 0.000 claims description 22
- 229910021641 deionized water Inorganic materials 0.000 claims description 22
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 20
- 239000001301 oxygen Substances 0.000 claims description 20
- 229910052760 oxygen Inorganic materials 0.000 claims description 20
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 16
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 claims description 16
- 239000004005 microsphere Substances 0.000 claims description 16
- 229910052710 silicon Inorganic materials 0.000 claims description 16
- 239000010703 silicon Substances 0.000 claims description 16
- 238000000034 method Methods 0.000 claims description 14
- 238000001035 drying Methods 0.000 claims description 13
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 claims description 12
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 claims description 12
- 239000012298 atmosphere Substances 0.000 claims description 12
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 claims description 11
- 239000011701 zinc Substances 0.000 claims description 11
- 229910052725 zinc Inorganic materials 0.000 claims description 11
- 239000012153 distilled water Substances 0.000 claims description 9
- XEZNGIUYQVAUSS-UHFFFAOYSA-N 18-crown-6 Chemical compound C1COCCOCCOCCOCCOCCO1 XEZNGIUYQVAUSS-UHFFFAOYSA-N 0.000 claims description 8
- UKLDJPRMSDWDSL-UHFFFAOYSA-L [dibutyl(dodecanoyloxy)stannyl] dodecanoate Chemical compound CCCCCCCCCCCC(=O)O[Sn](CCCC)(CCCC)OC(=O)CCCCCCCCCCC UKLDJPRMSDWDSL-UHFFFAOYSA-L 0.000 claims description 8
- 239000012975 dibutyltin dilaurate Substances 0.000 claims description 8
- DBMJMQXJHONAFJ-UHFFFAOYSA-M Sodium laurylsulphate Chemical compound [Na+].CCCCCCCCCCCCOS([O-])(=O)=O DBMJMQXJHONAFJ-UHFFFAOYSA-M 0.000 claims description 7
- ROTJZTYLACIJIG-UHFFFAOYSA-N pentane-1,3,5-tricarboxylic acid Chemical compound OC(=O)CCC(C(O)=O)CCC(O)=O ROTJZTYLACIJIG-UHFFFAOYSA-N 0.000 claims description 7
- 229920000747 poly(lactic acid) Polymers 0.000 claims description 7
- 239000004626 polylactic acid Substances 0.000 claims description 7
- 238000005406 washing Methods 0.000 claims description 7
- 229910052786 argon Inorganic materials 0.000 claims description 6
- 238000005530 etching Methods 0.000 claims description 6
- 229910000403 monosodium phosphate Inorganic materials 0.000 claims description 6
- 235000019799 monosodium phosphate Nutrition 0.000 claims description 6
- AJPJDKMHJJGVTQ-UHFFFAOYSA-M sodium dihydrogen phosphate Chemical compound [Na+].OP(O)([O-])=O AJPJDKMHJJGVTQ-UHFFFAOYSA-M 0.000 claims description 6
- 238000010438 heat treatment Methods 0.000 claims description 5
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims description 4
- 238000005553 drilling Methods 0.000 claims description 3
- 238000001755 magnetron sputter deposition Methods 0.000 claims description 3
- -1 (trimethoxysilyl) methyl Chemical group 0.000 claims description 2
- 229960000583 acetic acid Drugs 0.000 claims description 2
- 238000001816 cooling Methods 0.000 claims description 2
- 239000012362 glacial acetic acid Substances 0.000 claims description 2
- 229940017219 methyl propionate Drugs 0.000 claims description 2
- 238000003756 stirring Methods 0.000 claims description 2
- 238000009210 therapy by ultrasound Methods 0.000 claims description 2
- 230000035515 penetration Effects 0.000 abstract description 14
- 239000011148 porous material Substances 0.000 abstract description 13
- 230000000694 effects Effects 0.000 abstract description 12
- 230000035699 permeability Effects 0.000 abstract description 8
- 239000005543 nano-size silicon particle Substances 0.000 abstract description 7
- 230000008021 deposition Effects 0.000 abstract description 6
- 230000003405 preventing effect Effects 0.000 abstract description 6
- 238000004132 cross linking Methods 0.000 abstract description 3
- 230000002209 hydrophobic effect Effects 0.000 abstract 1
- 230000000052 comparative effect Effects 0.000 description 17
- 210000003746 feather Anatomy 0.000 description 10
- 239000012528 membrane Substances 0.000 description 9
- 238000000151 deposition Methods 0.000 description 7
- 125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 description 5
- 229910021645 metal ion Inorganic materials 0.000 description 5
- 239000004793 Polystyrene Substances 0.000 description 4
- 125000003368 amide group Chemical group 0.000 description 4
- 238000011049 filling Methods 0.000 description 4
- 239000000463 material Substances 0.000 description 4
- 239000003921 oil Substances 0.000 description 4
- 229920002223 polystyrene Polymers 0.000 description 4
- 230000002265 prevention Effects 0.000 description 4
- 241000272517 Anseriformes Species 0.000 description 3
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 3
- 238000001020 plasma etching Methods 0.000 description 3
- 238000012360 testing method Methods 0.000 description 3
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 2
- 230000009471 action Effects 0.000 description 2
- 229960001617 ethyl hydroxybenzoate Drugs 0.000 description 2
- 239000001257 hydrogen Substances 0.000 description 2
- 229910052739 hydrogen Inorganic materials 0.000 description 2
- 230000005661 hydrophobic surface Effects 0.000 description 2
- 125000004029 hydroxymethyl group Chemical group [H]OC([H])([H])* 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N phenol group Chemical group C1(=CC=CC=C1)O ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 2
- 238000009958 sewing Methods 0.000 description 2
- 230000003068 static effect Effects 0.000 description 2
- 238000009423 ventilation Methods 0.000 description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 1
- YCKRFDGAMUMZLT-UHFFFAOYSA-N Fluorine atom Chemical compound [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000005611 electricity Effects 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 229910052731 fluorine Inorganic materials 0.000 description 1
- 239000011737 fluorine Substances 0.000 description 1
- 235000015203 fruit juice Nutrition 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 239000012299 nitrogen atmosphere Substances 0.000 description 1
- 125000002924 primary amino group Chemical group [H]N([H])* 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 238000005096 rolling process Methods 0.000 description 1
- 238000000967 suction filtration Methods 0.000 description 1
- 239000013077 target material Substances 0.000 description 1
- 238000009941 weaving Methods 0.000 description 1
Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/77—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with silicon or compounds thereof
- D06M11/78—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with silicon or compounds thereof with silicon; with halides or oxyhalides of silicon; with fluorosilicates
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M10/00—Physical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. ultrasonic, corona discharge, irradiation, electric currents, or magnetic fields; Physical treatment combined with treatment with chemical compounds or elements
- D06M10/02—Physical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. ultrasonic, corona discharge, irradiation, electric currents, or magnetic fields; Physical treatment combined with treatment with chemical compounds or elements ultrasonic or sonic; Corona discharge
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M10/00—Physical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. ultrasonic, corona discharge, irradiation, electric currents, or magnetic fields; Physical treatment combined with treatment with chemical compounds or elements
- D06M10/04—Physical treatment combined with treatment with chemical compounds or elements
- D06M10/06—Inorganic compounds or elements
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M10/00—Physical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. ultrasonic, corona discharge, irradiation, electric currents, or magnetic fields; Physical treatment combined with treatment with chemical compounds or elements
- D06M10/04—Physical treatment combined with treatment with chemical compounds or elements
- D06M10/08—Organic compounds
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M10/00—Physical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. ultrasonic, corona discharge, irradiation, electric currents, or magnetic fields; Physical treatment combined with treatment with chemical compounds or elements
- D06M10/04—Physical treatment combined with treatment with chemical compounds or elements
- D06M10/08—Organic compounds
- D06M10/10—Macromolecular compounds
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/07—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with halogens; with halogen acids or salts thereof; with oxides or oxyacids of halogens or salts thereof
- D06M11/11—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with halogens; with halogen acids or salts thereof; with oxides or oxyacids of halogens or salts thereof with halogen acids or salts thereof
- D06M11/22—Halides of elements of Groups 5 or 15 of the Periodic Table
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/184—Carboxylic acids; Anhydrides, halides or salts thereof
- D06M13/192—Polycarboxylic acids; Anhydrides, halides or salts thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
- D06M13/368—Hydroxyalkylamines; Derivatives thereof, e.g. Kritchevsky bases
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/50—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with organometallic compounds; with organic compounds containing boron, silicon, selenium or tellurium atoms
- D06M13/51—Compounds with at least one carbon-metal or carbon-boron, carbon-silicon, carbon-selenium, or carbon-tellurium bond
- D06M13/513—Compounds with at least one carbon-metal or carbon-boron, carbon-silicon, carbon-selenium, or carbon-tellurium bond with at least one carbon-silicon bond
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/507—Polyesters
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/16—Synthetic fibres, other than mineral fibres
- D06M2101/30—Synthetic polymers consisting of macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M2101/32—Polyesters
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/01—Stain or soil resistance
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/10—Repellency against liquids
- D06M2200/12—Hydrophobic properties
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Physics & Mathematics (AREA)
- Plasma & Fusion (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
- Chemical Or Physical Treatment Of Fibers (AREA)
Abstract
本发明公开了一种透气防钻绒面料及其制备方法,涉及面料技术领域。本发明先对聚酯纤维进行预处理,引入极性基团,然后与1,3,5‑戊三羧酸、氧化锌、3‑氨基‑5‑(羟甲基)苯酚、2‑氨基‑6‑羟基苯甲酸乙酯反应,提高面料的抗静电效果,减少纤维间的斥力,提高面料的防钻绒效果;改性纤维编织成面料后,进行压光处理,令面料紧密的同时,使改性纤维产生交联作用,缩小面料孔隙,增益面料的防钻绒性;然后进行二次沉积处理,形成疏水的多孔纳米硅膜,与面料孔隙贯通,提高面料透气性,再后利用3‑氯三乙氧基硅烷、三氟化铋改性,增益面料的防污效果。本发明制备的透气防钻绒面料具有透气、防钻绒、防污的效果。
Description
技术领域
本发明涉及面料技术领域,具体为一种透气防钻绒面料及其制备方法。
背景技术
羽绒制品是指以养殖的鸭、鹅的毛、绒为填充料,羽绒面料为填充结构,再加以缝制的综合性实用产品。近年来,国内外对羽绒面料及其相关领域进行了深入的探究。尤其以羽绒面料钻绒的相关研究尤为突出。因为羽绒面料钻绒的直接影响羽绒面料的寿命以及使用性能,并且可能直接影响人体健康。羽绒面料的钻绒问题也是购买者长期投诉的焦点问题之一,当羽绒面料受到外界挤压时,静止空气从羽绒面料的空隙或者缝纫线的针孔中透出,羽绒随空气钻出内腔。
此外,羽绒面料为了解决防钻绒问题,常常舍弃掉透气效果,导致消费者体验感下降。且羽绒面料由于羽绒制品的特殊性,一旦水洗或机洗,极易影响羽绒填充物的质量,而人们在实际生活中,不可避免会沾染上果汁、油等油污,不仅难以清洗,影响美观,也会影响羽绒面料的寿命和质量。因此,如何发明一种防污、透气、防钻绒的面料,显得尤为重要。
发明内容
本发明的目的在于提供一种透气防钻绒面料及其制备方法,以解决现有技术中存在的问题。
为了解决上述技术问题,本发明提供如下技术方案:一种透气防钻绒面料,所述透气防钻绒面料包括面料基底和防污膜。
进一步的,所述面料基底由以下方法制得,改性纤维编织成面料后,进行压光处理;所述压光处理为热蒸汽下处理一段时间后,再于高温、一定压力下处理一段时间,再升温处理。
进一步的,所述改性纤维由聚酯纤维、1,3,5-戊三羧酸、氧化锌、3-氨基-5-(羟甲基)苯酚、2-氨基-6-羟基苯甲酸乙酯制得。
进一步的,所述防污膜由以下方法制得,将面料基底置于去离子水中,再加入聚乳酸微球、无水乙醇,静置一段时间后,加入十二烷基硫酸钠、去离子水,继续静置,取出,室温干燥后,氧等离子刻蚀得面料前体;将面料前体置于设备中,射频磁控溅射得硅膜面料;将硅膜面料、蒸馏水、无水乙醇混合,用冰醋酸调节pH,超声处理后,加入(三甲氧基硅基)丙酸甲酯,搅拌一段时间后,冷却至室温,取出,洗涤、干燥,得改性前体;将改性前体、18-冠醚-6、乙腈、三氟化铋混合,低温反应一段时间后,取出,洗涤、干燥,得透气防钻绒面料。
进一步的,一种透气防钻绒面料的制备方法,包括以下制备步骤:
(1)将预处理聚酯纤维、三羧酸锌、磷酸二氢钠、去离子水按质量比1:0.6:0.3:4~1:1.2:0.6:10混合,30kHz超声18~26min后,升温至80℃,反应33~43min后,升温至140℃,处理26~30min后,抽滤,用去离子水洗涤6~8次,60℃烘干6~9h得纤维前体;
(2)将纤维前体、3-氨基-5-(羟甲基)苯酚、2-氨基-6-羟基苯甲酸乙酯、二丁基锡二月桂酸酯按质量比1:0.3:0.3:0.001~1:0.6:0.6:0.001混合,氮气氛围下,反应1~3h后,升温至176℃,反应3~5h后,抽滤,用去离子水洗涤6~8次,60℃烘干6~9h得改性纤维;经编织成面料后,进行压光处理得面料基底;
(3)将面料基底置于面料基底质量30~38倍的去离子水,再加入面料基底质量0.1~0.3倍的聚乳酸微球、面料基底质量8~13倍的无水乙醇,静置10~20min后,加入面料基底质量0.1~0.3倍的十二烷基硫酸钠、面料基底质量1.6~3.8倍的去离子水,静置14~28min后,取出,室温干燥7~10h,置于等离子体设备中,氧气气氛下,100W刻蚀2~6min得面料前体;
(4)将面料前体置于设备中,抽真空至1.0~2.8Pa,采用硅靶材,按流量比4:1通入氩气和氧气,150W溅射15~30min得硅膜面料;将硅膜面料、蒸馏水、无水乙醇按质量比1:1:7~1:2:10混合,加入冰醋酸至溶液pH为4~5,30kHz超声28~40min,加入硅膜面料质量0.2~0.4倍的(三甲氧基硅基)丙酸甲酯,85℃、200rpm搅拌4~6h,冷却至室温后,取出,用无水乙醇洗涤6~8次,80℃干燥10~12h得改性前体;
(5)将改性前体、18-冠醚-6、乙腈、三氟化铋按质量比1:0.001:5:0.5~1:0.002:10:0.9混合,10℃反应6~10h后,取出,依次用乙腈、去离子水洗涤3~5次,40℃干燥10~12h得透气防钻绒面料。
进一步的,步骤(1)所述三羧酸锌的制备方法为:将氧化锌、1,3,5-戊三羧酸、丙酮按质量比1:1.6:8~1:2.4:16混合,36℃反应40~52min后,用去离子水洗涤6~8次,抽滤,40℃干燥6~9h。
进一步的,步骤(1)所述预处理聚酯纤维的制备方法为:将聚酯纤维置于辉光放电设备中,氧气气氛下,在5Pa、500~600V下处理150~300s。
进一步的,所述聚酯纤维的纱线线密度为50~75d。
进一步的,步骤(2)所述面料基底的经纱密度位500~600根/10cm,纬纱密度为500~600根/10cm。
进一步的,步骤(2)所述压光处理具体为:150℃蒸汽下处理1~3h,再于200℃、140T压光处理1~3h,升温至230℃,处理40~60min。
与现有技术相比,本发明所达到的有益效果是:
本发明利用改性纤维编织成面料后,经过沉积、改性处理,获得防污膜,以实现防钻绒、透气、防污的效果。
首先,本发明利用等离子体对聚酯纤维进行预处理,在聚酯纤维分子链中引入羟基、羧基等极性基团;然后利用1,3,5-戊三羧酸的羧基与氧化锌反应,形成三羧酸锌;三羧酸锌的羧基与聚酯纤维的羟基反应,金属离子附着于聚酯纤维表面,提高聚酯纤维的导电性,然后3-氨基-5-(羟甲基)苯酚、2-氨基-6-羟基苯甲酸乙酯的氨基与纤维的羧基反应,生成酰胺基团,与金属离子共同作用,提高聚酯纤维的导电性,使面料具有抗静电效果,减少纤维间的斥力,避免纤维因静电而竖立起来导致钻绒,有利于提高面料的防钻绒效果;改性纤维编织成面料后,进行压光处理,高温和垂直压力的作用下使面料紧密,增益防钻绒效果,同时高温促进改性纤维间羟甲基和酚环活泼氢反应,使改性纤维产生交联作用,缩小面料孔隙,增益面料的防钻绒性。
其次,本发明进行第一次沉积处理,利用面料基底的羟基吸附聚苯乙烯微球,再经等离子刻蚀,控制微球直径,有利于控制多孔膜孔隙;然后进行第二次沉积处理,利用射频磁控溅射,在聚苯乙烯微球微球表面沉积一层纳米硅,经超声洗涤,去除微球,在面料表面形成多孔膜,最大孔径小于羽绒材料的最小孔径,所以羽绒完全不能通过,同时还存在大量的孔隙与面料孔隙贯通,以供气体通过,提高面料透气性,此外,纳米硅膜形成疏水表面,使面料具有防污效果;然后利用3-氯三乙氧基硅烷的硅氧键接枝于表面,其氯离子与三氟化铋反应,引入氟长链,降低纳米硅膜表面能,增益面料的防污效果。
具体实施方式
下面将结合本发明实施例,对本发明实施例中的技术方案进行清楚、完整地描述,显然,所描述的实施例仅仅是本发明一部分实施例,而不是全部的实施例。基于本发明中的实施例,本领域普通技术人员在没有做出创造性劳动前提下所获得的所有其他实施例,都属于本发明保护的范围。
为了更清楚的说明本发明提供的方法通过以下实施例进行详细说明,在以下实施例中制作的透气防钻绒面料的各指标测试方法如下:
透气性:取相同厚度的实施例与对比例进行透气效果测试,采用YG461E型数字式织物透气量测定仪,在100Pa、20cm2条件下测定面料透气量。
防钻绒性:取相同大小的实施例与对比例进行钻绒效果测试,将面料缝制成33cm×20.3cm的小枕头,内填充35g、40%含量的水禽羽绒,将枕头与24个橡胶球放入机箱滚动30min,完成后根据在滚动时钻出的羽毛/羽丝数量来决定织物的防钻绒等级,等级分为1~5,5级为优秀,1级为最差。
防污性:取相同大小的实施例与对比例参照AATCC 22测试面料防水等级,等级分为0~100,100最好,0最差;参照照AATCC 118测试面料防油等级,等级分为0~8,8最好,0最差。
实施例1
(1)将线密度为50d的聚酯纤维置于辉光放电设备中,氧气气氛下,在5Pa、500V下处理150s,得预处理聚酯纤维;将氧化锌、1,3,5-戊三羧酸、丙酮按质量比1:1.6:8混合,36℃反应40min后,用去离子水洗涤6次,抽滤,40℃干燥6h得三羧酸锌;将预处理聚酯纤维、三羧酸锌、磷酸二氢钠、去离子水按质量比1:0.6:0.3:4混合,30kHz超声18min后,升温至80℃,反应33min后,升温至140℃,处理26min后,抽滤,用去离子水洗涤6次,60℃烘干6h得纤维前体;
(2)将纤维前体、3-氨基-5-(羟甲基)苯酚、2-氨基-6-羟基苯甲酸乙酯、二丁基锡二月桂酸酯按质量比1:0.3:0.3:0.001混合,氮气氛围下,反应1h后,升温至176℃,反应3h后,抽滤,用去离子水洗涤6次,60℃烘干6h得改性纤维;经编织成面料后,150℃蒸汽下处理1h,再于200℃、140T压光处理1h,升温至230℃,处理40min,得经纱密度位500根/10cm、纬纱密度为500根/10cm的面料基底;
(3)将面料基底置于面料基底质量30倍的去离子水,再加入面料基底质量0.1倍的聚乳酸微球、面料基底质量8倍的无水乙醇,静置10min后,加入面料基底质量0.1倍的十二烷基硫酸钠、面料基底质量1.6倍的去离子水,静置14min后,取出,室温干燥7h,置于等离子体设备中,氧气气氛下,100W刻蚀2min得面料前体;
(4)将面料前体置于设备中,抽真空至1.0Pa,采用硅靶材,按流量比4:1通入氩气和氧气,150W溅射15min得硅膜面料;将硅膜面料、蒸馏水、无水乙醇按质量比1:1:7混合,加入冰醋酸至溶液pH为4,30kHz超声28min,加入硅膜面料质量0.2倍的(三甲氧基硅基)丙酸甲酯,85℃、200rpm搅拌4h,冷却至室温后,取出,用无水乙醇洗涤6次,80℃干燥10h得改性前体;
(5)将改性前体、18-冠醚-6、乙腈、三氟化铋按质量比1:0.001:5:0.5混合,10℃反应6h后,取出,依次用乙腈、去离子水洗涤3次,40℃干燥10h得透气防钻绒面料。
实施例2
(1)将线密度为63d的聚酯纤维置于辉光放电设备中,氧气气氛下,在5Pa、550V下处理225s,得预处理聚酯纤维;将氧化锌、1,3,5-戊三羧酸、丙酮按质量比1:2:12混合,36℃反应46min后,用去离子水洗涤7次,抽滤,40℃干燥7.5h得三羧酸锌;将预处理聚酯纤维、三羧酸锌、磷酸二氢钠、去离子水按质量比1:0.9:0.45:7混合,30kHz超声22min后,升温至80℃,反应38min后,升温至140℃,处理28min后,抽滤,用去离子水洗涤7次,60℃烘干7.5h得纤维前体;
(2)将纤维前体、3-氨基-5-(羟甲基)苯酚、2-氨基-6-羟基苯甲酸乙酯、二丁基锡二月桂酸酯按质量比1:0.45:0.45:0.001混合,氮气氛围下,反应2h后,升温至176℃,反应4h后,抽滤,用去离子水洗涤7次,60℃烘干7.5h得改性纤维;经编织成面料后,150℃蒸汽下处理2h,再于200℃、140T压光处理2h,升温至230℃,处理50min,得经纱密度位550根/10cm、纬纱密度为550根/10cm的面料基底;
(3)将面料基底置于面料基底质量34倍的去离子水,再加入面料基底质量0.2倍的聚乳酸微球、面料基底质量10.5倍的无水乙醇,静置15min后,加入面料基底质量0.2倍的十二烷基硫酸钠、面料基底质量2.7倍的去离子水,静置21min后,取出,室温干燥8.5h,置于等离子体设备中,氧气气氛下,100W刻蚀4min得面料前体;
(4)将面料前体置于设备中,抽真空至1.9Pa,采用硅靶材,按流量比4:1通入氩气和氧气,150W溅射22min得硅膜面料;将硅膜面料、蒸馏水、无水乙醇按质量比1:1.5:8.5混合,加入冰醋酸至溶液pH为4.5,30kHz超声34min,加入硅膜面料质量0.3倍的(三甲氧基硅基)丙酸甲酯,85℃、200rpm搅拌5h,冷却至室温后,取出,用无水乙醇洗涤7次,80℃干燥11h得改性前体;
(5)将改性前体、18-冠醚-6、乙腈、三氟化铋按质量比1:0.0015:7.5:0.7混合,10℃反应8h后,取出,依次用乙腈、去离子水洗涤4次,40℃干燥11h得透气防钻绒面料。
实施例3
(1)将线密度为75d的聚酯纤维置于辉光放电设备中,氧气气氛下,在5Pa、600V下处理300s,得预处理聚酯纤维;将氧化锌、1,3,5-戊三羧酸、丙酮按质量比1:2.4:16混合,36℃反应52min后,用去离子水洗涤8次,抽滤,40℃干燥9h得三羧酸锌;将预处理聚酯纤维、三羧酸锌、磷酸二氢钠、去离子水按质量比1:1.2:0.6:10混合,30kHz超声26min后,升温至80℃,反应43min后,升温至140℃,处理30min后,抽滤,用去离子水洗涤8次,60℃烘干9h得纤维前体;
(2)将纤维前体、3-氨基-5-(羟甲基)苯酚、2-氨基-6-羟基苯甲酸乙酯、二丁基锡二月桂酸酯按质量比1:0.6:0.6:0.001混合,氮气氛围下,反应3h后,升温至176℃,反应5h后,抽滤,用去离子水洗涤8次,60℃烘干9h得改性纤维;经编织成面料后,150℃蒸汽下处理3h,再于200℃、140T压光处理3h,升温至230℃,处理60min,得经纱密度位600根/10cm、纬纱密度为600根/10cm的面料基底;
(3)将面料基底置于面料基底质量38倍的去离子水,再加入面料基底质量0.3倍的聚乳酸微球、面料基底质量13倍的无水乙醇,静置20min后,加入面料基底质量0.3倍的十二烷基硫酸钠、面料基底质量3.8倍的去离子水,静置28min后,取出,室温干燥10h,置于等离子体设备中,氧气气氛下,100W刻蚀6min得面料前体;
(4)将面料前体置于设备中,抽真空至2.8Pa,采用硅靶材,按流量比4:1通入氩气和氧气,150W溅射30min得硅膜面料;将硅膜面料、蒸馏水、无水乙醇按质量比1:2:10混合,加入冰醋酸至溶液pH为5,30kHz超声40min,加入硅膜面料质量0.4倍的(三甲氧基硅基)丙酸甲酯,85℃、200rpm搅拌6h,冷却至室温后,取出,用无水乙醇洗涤8次,80℃干燥12h得改性前体;
(5)将改性前体、18-冠醚-6、乙腈、三氟化铋按质量比1:0.002:10:0.9混合,10℃反应10h后,取出,依次用乙腈、去离子水洗涤5次,40℃干燥12h得透气防钻绒面料。
对比例1
对比例1与实施例2的区别在于步骤(1)的不同,将步骤(1)改为:将线密度为63d的聚酯纤维置于辉光放电设备中,氧气气氛下,在5Pa、550V下处理225s,得纤维前体。其余步骤同实施例2。
对比例2
对比例2与实施例2的区别在于步骤(2)的不同,将步骤(2)改为:将纤维前体、2-氨基-6-羟基苯甲酸乙酯、二丁基锡二月桂酸酯按质量比1:0.45:0.001混合,氮气氛围下,反应2h后,升温至176℃,反应4h后,抽滤,用去离子水洗涤7次,60℃烘干7.5h得改性纤维;经编织成面料后,150℃蒸汽下处理2h,再于200℃、140T压光处理2h,升温至230℃,处理50min,得经纱密度位550根/10cm、纬纱密度为550根/10cm的面料基底。其余步骤同实施例2。
对比例3
对比例3与实施例2的区别在于步骤(2)的不同,将步骤(2)改为:将纤维前体、3-氨基-5-(羟甲基)苯酚、2-氨基-6-羟基苯甲酸乙酯、二丁基锡二月桂酸酯按质量比1:0.45:0.45:0.001混合,氮气氛围下,反应2h后,升温至176℃,反应4h后,抽滤,用去离子水洗涤7次,60℃烘干7.5h得改性纤维;经编织,得经纱密度位550根/10cm、纬纱密度为550根/10cm的面料基底。其余步骤同实施例2。
对比例4
(1)将线密度为63d的聚酯纤维置于辉光放电设备中,氧气气氛下,在5Pa、550V下处理225s,得预处理聚酯纤维;将氧化锌、1,3,5-戊三羧酸、丙酮按质量比1:2:12混合,36℃反应46min后,用去离子水洗涤7次,抽滤,40℃干燥7.5h得三羧酸锌;将预处理聚酯纤维、三羧酸锌、磷酸二氢钠、去离子水按质量比1:0.9:0.45:7混合,30kHz超声22min后,升温至80℃,反应38min后,升温至140℃,处理28min后,抽滤,用去离子水洗涤7次,60℃烘干7.5h得纤维前体;
(2)将纤维前体、3-氨基-5-(羟甲基)苯酚、2-氨基-6-羟基苯甲酸乙酯、二丁基锡二月桂酸酯按质量比1:0.45:0.45:0.001混合,氮气氛围下,反应2h后,升温至176℃,反应4h后,抽滤,用去离子水洗涤7次,60℃烘干7.5h得改性纤维;经编织成面料后,150℃蒸汽下处理2h,再于200℃、140T压光处理2h,升温至230℃,处理50min,得经纱密度位550根/10cm、纬纱密度为550根/10cm的面料基底;
(3)将面料基底置于设备中,抽真空至1.9Pa,采用硅靶材,按流量比4:1通入氩气和氧气,150W溅射22min得硅膜面料;将硅膜面料、蒸馏水、无水乙醇按质量比1:1.5:8.5混合,加入冰醋酸至溶液pH为4.5,30kHz超声34min,加入硅膜面料质量0.3倍的(三甲氧基硅基)丙酸甲酯,85℃、200rpm搅拌5h,冷却至室温后,取出,用无水乙醇洗涤7次,80℃干燥11h得改性前体;
(4)将改性前体、18-冠醚-6、乙腈、三氟化铋按质量比1:0.0015:7.5:0.7混合,10℃反应8h后,取出,依次用乙腈、去离子水洗涤4次,40℃干燥11h得透气防钻绒面料。
对比例5
对比例5与实施例2的区别在于步骤(4)的不同,将步骤(4)改为:将面料前体、蒸馏水、无水乙醇按质量比1:1.5:8.5混合,加入冰醋酸至溶液pH为4.5,30kHz超声34min,加入面料前体质量0.3倍的(三甲氧基硅基)丙酸甲酯,85℃、200rpm搅拌5h,冷却至室温后,取出,用无水乙醇洗涤7次,80℃干燥11h得改性前体。其余步骤同实施例2。
对比例6
对比例6与实施例2的区别在于无步骤(5),其余步骤同实施例2。
效果例
下表1给出了采用本发明实施例1至3与对比例1至6的透气防钻绒面料的性能分析结果。
表1
从实施例与对比例的钻绒等级实验数据对比可发现,聚酯纤维经预处理后,与1,3,5-戊三羧酸、氧化锌反应,形成金属离子,附着于聚酯纤维表面,提高聚酯纤维的导电性,然后与3-氨基-5-(羟甲基)苯酚、2-氨基-6-羟基苯甲酸乙酯进一步反应,生成酰胺基团,与金属离子共同作用,提高聚酯纤维的导电性,使面料具有抗静电效果,减少纤维间的斥力,有利于提高面料的防钻绒效果;在压光处理过程中,高温和垂直压力的作用下使面料紧密,增益防钻绒效果,同时高温促进改性纤维间羟甲基和酚环活泼氢反应,使改性纤维产生交联作用,缩小面料孔隙,增益面料的防钻绒性;从实施例与对比例的透气量、防水、防油等级实验数据对比可发现,本发明进行第一次沉积处理,吸附聚苯乙烯微球,再经等离子刻蚀,控制微球直径,有利于控制多孔膜孔隙;然后进行第二次沉积处理,在聚苯乙烯微球微球表面沉积一层纳米硅,经去除,形成多孔膜,最大孔径小于羽绒材料的最小孔径,所以羽绒完全不能通过,同时还存在大量的孔隙与面料孔隙贯通,以供气体通过,提高面料透气性,此外,纳米硅膜形成疏水表面,使面料具有防污效果;然后利用3-氯三乙氧基硅烷、三氟化铋进行改性,降低纳米硅膜表面能,增益面料的防污效果。
对于本领域技术人员而言,显然本发明不限于上述示范性实施例的细节,而且在不背离本发明的精神或基本特征的情况下,能够以其他的具体形式实现本发明。因此,无论从哪一点来看,均应将实施例看作是示范性的,而且是非限制性的,本发明的范围由所附权利要求而不是上述说明限定,因此旨在将落在权利要求的等同要件的含义和范围内的所有变化囊括在本发明内。不应将权利要求中的任何标记视为限制所涉及的权利要求。
Claims (10)
1.一种透气防钻绒面料,其特征在于,所述透气防钻绒面料包括面料基底和防污膜。
2.根据权利要求1所述的一种透气防钻绒面料,其特征在于,所述面料基底由以下方法制得,改性纤维编织成面料后,进行压光处理;所述压光处理为热蒸汽下处理一段时间后,再于高温、一定压力下处理一段时间,再升温处理。
3.根据权利要求2所述的一种透气防钻绒面料,其特征在于,所述改性纤维由聚酯纤维、1,3,5-戊三羧酸、氧化锌、3-氨基-5-(羟甲基)苯酚、2-氨基-6-羟基苯甲酸乙酯制得。
4.根据权利要求1所述的一种透气防钻绒面料,其特征在于,所述防污膜由以下方法制得,将面料基底置于去离子水中,再加入聚乳酸微球、无水乙醇,静置一段时间后,加入十二烷基硫酸钠、去离子水,继续静置,取出,室温干燥后,氧等离子刻蚀得面料前体;将面料前体置于设备中,射频磁控溅射得硅膜面料;将硅膜面料、蒸馏水、无水乙醇混合,用冰醋酸调节pH,超声处理后,加入(三甲氧基硅基)丙酸甲酯,搅拌一段时间后,冷却至室温,取出,洗涤、干燥,得改性前体;将改性前体、18-冠醚-6、乙腈、三氟化铋混合,低温反应一段时间后,取出,洗涤、干燥,得透气防钻绒面料。
5.一种透气防钻绒面料的制备方法,其特征在于,包括以下制备步骤:
(1)将预处理聚酯纤维、三羧酸锌、磷酸二氢钠、去离子水按质量比1:0.6:0.3:4~1:1.2:0.6:10混合,30kHz超声18~26min后,升温至80℃,反应33~43min后,升温至140℃,处理26~30min后,抽滤,用去离子水洗涤6~8次,60℃烘干6~9h得纤维前体;
(2)将纤维前体、3-氨基-5-(羟甲基)苯酚、2-氨基-6-羟基苯甲酸乙酯、二丁基锡二月桂酸酯按质量比1:0.3:0.3:0.001~1:0.6:0.6:0.001混合,氮气氛围下,反应1~3h后,升温至176℃,反应3~5h后,抽滤,用去离子水洗涤6~8次,60℃烘干6~9h得改性纤维;经编织成面料后,进行压光处理得面料基底;
(3)将面料基底置于面料基底质量30~38倍的去离子水,再加入面料基底质量0.1~0.3倍的聚乳酸微球、面料基底质量8~13倍的无水乙醇,静置10~20min后,加入面料基底质量0.1~0.3倍的十二烷基硫酸钠、面料基底质量1.6~3.8倍的去离子水,静置14~28min后,取出,室温干燥7~10h,置于等离子体设备中,氧气气氛下,100W刻蚀2~6min得面料前体;
(4)将面料前体置于设备中,抽真空至1.0~2.8Pa,采用硅靶材,按流量比4:1通入氩气和氧气,150W溅射15~30min得硅膜面料;将硅膜面料、蒸馏水、无水乙醇按质量比1:1:7~1:2:10混合,加入冰醋酸至溶液pH为4~5,30kHz超声28~40min,加入硅膜面料质量0.2~0.4倍的(三甲氧基硅基)丙酸甲酯,85℃、200rpm搅拌4~6h,冷却至室温后,取出,用无水乙醇洗涤6~8次,80℃干燥10~12h得改性前体;
(5)将改性前体、18-冠醚-6、乙腈、三氟化铋按质量比1:0.001:5:0.5~1:0.002:10:0.9混合,10℃反应6~10h后,取出,依次用乙腈、去离子水洗涤3~5次,40℃干燥10~12h得透气防钻绒面料。
6.根据权利要求5所述的一种透气防钻绒面料的制备方法,其特征在于,步骤(1)所述三羧酸锌的制备方法为:将氧化锌、1,3,5-戊三羧酸、丙酮按质量比1:1.6:8~1:2.4:16混合,36℃反应40~52min后,用去离子水洗涤6~8次,抽滤,40℃干燥6~9h。
7.根据权利要求5所述的一种透气防钻绒面料的制备方法,其特征在于,步骤(1)所述预处理聚酯纤维的制备方法为:将聚酯纤维置于辉光放电设备中,氧气气氛下,在5Pa、500~600V下处理150~300s。
8.根据权利要求7所述的一种透气防钻绒面料的制备方法,其特征在于,所述聚酯纤维的纱线线密度为50~75d。
9.根据权利要求5所述的一种透气防钻绒面料的制备方法,其特征在于,步骤(2)所述面料基底的经纱密度位500~600根/10cm,纬纱密度为500~600根/10cm。
10.根据权利要求5所述的一种透气防钻绒面料的制备方法,其特征在于,步骤(2)所述压光处理具体为:150℃蒸汽下处理1~3h,再于200℃、140T压光处理1~3h,升温至230℃,处理40~60min。
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN202211236061.9A CN115613352A (zh) | 2022-10-10 | 2022-10-10 | 一种透气防钻绒面料及其制备方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN202211236061.9A CN115613352A (zh) | 2022-10-10 | 2022-10-10 | 一种透气防钻绒面料及其制备方法 |
Publications (1)
Publication Number | Publication Date |
---|---|
CN115613352A true CN115613352A (zh) | 2023-01-17 |
Family
ID=84863202
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN202211236061.9A Pending CN115613352A (zh) | 2022-10-10 | 2022-10-10 | 一种透气防钻绒面料及其制备方法 |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN115613352A (zh) |
Citations (13)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1414169A (zh) * | 2001-10-26 | 2003-04-30 | 青岛大学 | 一种防水透气透湿织物及其制备方法 |
CN102493180A (zh) * | 2011-12-15 | 2012-06-13 | 江南大学 | 一种拒水织物的制造方法 |
WO2017091055A1 (ko) * | 2015-11-25 | 2017-06-01 | (주)나노미래생활 | 아연 카르복실산염의 수화물의 제조 방법, 이로부터 제조된 아연 카르복실산염의 수화물 및 상기 아연 카르복실산염의 수화물을 포함한 향균 플라스틱 소재 |
CN109161979A (zh) * | 2018-08-16 | 2019-01-08 | 王泉泉 | 一种利用有机羧酸锌盐制备高透光折射率可调的聚酯纤维及其制备方法 |
CN109610183A (zh) * | 2018-11-13 | 2019-04-12 | 辽宁恒星精细化工有限公司 | 纺织品用水性聚氨酯涂层胶及面料处理方法 |
CN110055764A (zh) * | 2019-05-17 | 2019-07-26 | 康帝雅高档面料(苏州)有限公司 | 透湿防钻绒涂层面料、制造工艺及其织物 |
CN110387745A (zh) * | 2019-07-31 | 2019-10-29 | 浙江福尔普生新型材料有限公司 | 一种防水易去污羽绒服复合面料的生产工艺 |
CN111206424A (zh) * | 2020-01-11 | 2020-05-29 | 长江纺织(浙江)有限公司 | 一种涤纶纱线抗静电处理工艺 |
CN112179956A (zh) * | 2020-09-29 | 2021-01-05 | 西安交通大学 | 基于掺铝氧化锌多孔纳米薄膜的mems甲醛传感器的制备方法 |
CN112981959A (zh) * | 2020-12-17 | 2021-06-18 | 吴江精美峰实业有限公司 | 一种溶胶型导电聚酯纤维及其制备方法 |
WO2021244006A1 (zh) * | 2020-05-30 | 2021-12-09 | 周观林 | 一种抗菌抗静电易去污防羽布及其制备方法 |
CN114318264A (zh) * | 2021-12-29 | 2022-04-12 | 福建富兰光学股份有限公司 | 一种基于磁控溅射和刻蚀处理制备ito薄膜的方法 |
CN114752187A (zh) * | 2021-12-29 | 2022-07-15 | 苏州梅克兰循环科技有限公司 | 一种可循环使用的复合pet包装盒材料的制备方法 |
-
2022
- 2022-10-10 CN CN202211236061.9A patent/CN115613352A/zh active Pending
Patent Citations (13)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1414169A (zh) * | 2001-10-26 | 2003-04-30 | 青岛大学 | 一种防水透气透湿织物及其制备方法 |
CN102493180A (zh) * | 2011-12-15 | 2012-06-13 | 江南大学 | 一种拒水织物的制造方法 |
WO2017091055A1 (ko) * | 2015-11-25 | 2017-06-01 | (주)나노미래생활 | 아연 카르복실산염의 수화물의 제조 방법, 이로부터 제조된 아연 카르복실산염의 수화물 및 상기 아연 카르복실산염의 수화물을 포함한 향균 플라스틱 소재 |
CN109161979A (zh) * | 2018-08-16 | 2019-01-08 | 王泉泉 | 一种利用有机羧酸锌盐制备高透光折射率可调的聚酯纤维及其制备方法 |
CN109610183A (zh) * | 2018-11-13 | 2019-04-12 | 辽宁恒星精细化工有限公司 | 纺织品用水性聚氨酯涂层胶及面料处理方法 |
CN110055764A (zh) * | 2019-05-17 | 2019-07-26 | 康帝雅高档面料(苏州)有限公司 | 透湿防钻绒涂层面料、制造工艺及其织物 |
CN110387745A (zh) * | 2019-07-31 | 2019-10-29 | 浙江福尔普生新型材料有限公司 | 一种防水易去污羽绒服复合面料的生产工艺 |
CN111206424A (zh) * | 2020-01-11 | 2020-05-29 | 长江纺织(浙江)有限公司 | 一种涤纶纱线抗静电处理工艺 |
WO2021244006A1 (zh) * | 2020-05-30 | 2021-12-09 | 周观林 | 一种抗菌抗静电易去污防羽布及其制备方法 |
CN112179956A (zh) * | 2020-09-29 | 2021-01-05 | 西安交通大学 | 基于掺铝氧化锌多孔纳米薄膜的mems甲醛传感器的制备方法 |
CN112981959A (zh) * | 2020-12-17 | 2021-06-18 | 吴江精美峰实业有限公司 | 一种溶胶型导电聚酯纤维及其制备方法 |
CN114318264A (zh) * | 2021-12-29 | 2022-04-12 | 福建富兰光学股份有限公司 | 一种基于磁控溅射和刻蚀处理制备ito薄膜的方法 |
CN114752187A (zh) * | 2021-12-29 | 2022-07-15 | 苏州梅克兰循环科技有限公司 | 一种可循环使用的复合pet包装盒材料的制备方法 |
Non-Patent Citations (1)
Title |
---|
郑骆平等: ""无缝格状防羽绒面料一次成形生产实践", 《产业用纺织品》, vol. 37, no. 11, 25 November 2019 (2019-11-25), pages 9 - 13 * |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
JP2013530316A (ja) | 改善された羽毛の製造方法及びその改善された羽毛 | |
CN103981719A (zh) | 一种聚苯胺二氧化钛防紫外导电织物的制备方法 | |
CN115613352A (zh) | 一种透气防钻绒面料及其制备方法 | |
US8877289B2 (en) | Stainproofing method of fabric | |
CN112251919A (zh) | 一种单向导湿性织物及其制备方法 | |
Yilma et al. | Effect of plasma surface modification on comfort properties of polyester/cotton blend fabric | |
JP2006124901A (ja) | ロータス・リーフ効果を有する布帛の製造方法およびロータス・リーフ効果を有する布帛 | |
JP2011011349A (ja) | 保温性に優れた透湿防水フィルム | |
CN113910701A (zh) | 一种真空纳米防水透气面料及其应用 | |
JP2013049941A (ja) | 耐久制電撥水性ポリアミド繊維布帛及びその製造方法 | |
CN112553917B (zh) | 一种气凝胶热阻隔复合织物材料的制备方法 | |
CN112323515B (zh) | 阻汽面料及其生产方法 | |
CN114261161A (zh) | 一种羽绒服用多层复合面料及其制备方法 | |
RU2505256C2 (ru) | Способ получения электропроводящего текстильного материала | |
CN106337286A (zh) | 一种蚕丝/汉麻织物的去毛羽整理方法 | |
CN115262226B (zh) | 一种基于壳聚糖制备保暖毛织物的方法 | |
CN111826946A (zh) | 一种羊毛石墨烯混纺纱及面料的生产方法 | |
JP2019131944A (ja) | 内装織物 | |
Aileni et al. | Bivariate analysis of the hydrophobic textiles obtained by plasma treatment | |
CN115198423B (zh) | 一种抗菌阻燃涤纶面料及其制备方法 | |
CN109677094B (zh) | 一种层压防水织物的制备方法 | |
CN114737405B (zh) | 一种防水防紫外的高强度轻薄面料的制备方法 | |
CN113670005B (zh) | 人造皮肤用聚乙交酯经编支撑网的干燥方法 | |
Mekala et al. | Comparative studies on poly-β-hydroxybutyrate (PHB) with gelatin and PHB with starch as a finished fabric | |
CN113774682B (zh) | 一种耐折隔热帐篷面料涂层及所得面料 |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
PB01 | Publication | ||
PB01 | Publication | ||
SE01 | Entry into force of request for substantive examination | ||
SE01 | Entry into force of request for substantive examination |