CN115554177A - Two-component cleansing lotion and preparation method thereof - Google Patents
Two-component cleansing lotion and preparation method thereof Download PDFInfo
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- CN115554177A CN115554177A CN202211156752.8A CN202211156752A CN115554177A CN 115554177 A CN115554177 A CN 115554177A CN 202211156752 A CN202211156752 A CN 202211156752A CN 115554177 A CN115554177 A CN 115554177A
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- 238000002360 preparation method Methods 0.000 title claims abstract description 15
- 239000006210 lotion Substances 0.000 title description 2
- 239000000284 extract Substances 0.000 claims abstract description 60
- 239000003755 preservative agent Substances 0.000 claims abstract description 38
- 230000002335 preservative effect Effects 0.000 claims abstract description 38
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 34
- 239000003995 emulsifying agent Substances 0.000 claims abstract description 30
- 239000004094 surface-active agent Substances 0.000 claims abstract description 30
- 239000002480 mineral oil Substances 0.000 claims abstract description 29
- 235000010446 mineral oil Nutrition 0.000 claims abstract description 29
- 241001506047 Tremella Species 0.000 claims abstract description 25
- 150000004676 glycans Chemical class 0.000 claims abstract description 24
- 229920001282 polysaccharide Polymers 0.000 claims abstract description 24
- 239000005017 polysaccharide Substances 0.000 claims abstract description 24
- 239000003906 humectant Substances 0.000 claims abstract description 23
- 244000178870 Lavandula angustifolia Species 0.000 claims abstract description 20
- 235000010663 Lavandula angustifolia Nutrition 0.000 claims abstract description 20
- 239000001102 lavandula vera Substances 0.000 claims abstract description 20
- 235000018219 lavender Nutrition 0.000 claims abstract description 20
- 235000013399 edible fruits Nutrition 0.000 claims abstract description 18
- 241000972673 Phellodendron amurense Species 0.000 claims abstract description 15
- 230000001815 facial effect Effects 0.000 claims abstract description 13
- 240000001972 Gardenia jasminoides Species 0.000 claims abstract 3
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims description 51
- TXFPEBPIARQUIG-UHFFFAOYSA-N 4'-hydroxyacetophenone Chemical compound CC(=O)C1=CC=C(O)C=C1 TXFPEBPIARQUIG-UHFFFAOYSA-N 0.000 claims description 34
- PRAKJMSDJKAYCZ-UHFFFAOYSA-N squalane Chemical compound CC(C)CCCC(C)CCCC(C)CCCCC(C)CCCC(C)CCCC(C)C PRAKJMSDJKAYCZ-UHFFFAOYSA-N 0.000 claims description 34
- 239000002738 chelating agent Substances 0.000 claims description 30
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 30
- 239000002994 raw material Substances 0.000 claims description 26
- 238000012360 testing method Methods 0.000 claims description 26
- 239000007788 liquid Substances 0.000 claims description 22
- 238000007599 discharging Methods 0.000 claims description 20
- 238000011049 filling Methods 0.000 claims description 20
- 239000011734 sodium Substances 0.000 claims description 20
- 229910052708 sodium Inorganic materials 0.000 claims description 20
- 238000003756 stirring Methods 0.000 claims description 20
- 239000004088 foaming agent Substances 0.000 claims description 19
- HVUMOYIDDBPOLL-XWVZOOPGSA-N Sorbitan monostearate Chemical compound CCCCCCCCCCCCCCCCCC(=O)OC[C@@H](O)[C@H]1OC[C@H](O)[C@H]1O HVUMOYIDDBPOLL-XWVZOOPGSA-N 0.000 claims description 17
- OWBTYPJTUOEWEK-UHFFFAOYSA-N butane-2,3-diol Chemical compound CC(O)C(C)O OWBTYPJTUOEWEK-UHFFFAOYSA-N 0.000 claims description 17
- 229940087068 glyceryl caprylate Drugs 0.000 claims description 17
- 229940105132 myristate Drugs 0.000 claims description 17
- JXTPJDDICSTXJX-UHFFFAOYSA-N n-Triacontane Natural products CCCCCCCCCCCCCCCCCCCCCCCCCCCCCC JXTPJDDICSTXJX-UHFFFAOYSA-N 0.000 claims description 17
- GHBFNMLVSPCDGN-UHFFFAOYSA-N rac-1-monooctanoylglycerol Chemical compound CCCCCCCC(=O)OCC(O)CO GHBFNMLVSPCDGN-UHFFFAOYSA-N 0.000 claims description 17
- 229950011392 sorbitan stearate Drugs 0.000 claims description 17
- 229940032094 squalane Drugs 0.000 claims description 17
- TUNFSRHWOTWDNC-UHFFFAOYSA-N tetradecanoic acid Chemical compound CCCCCCCCCCCCCC(O)=O TUNFSRHWOTWDNC-UHFFFAOYSA-N 0.000 claims description 17
- SNPLKNRPJHDVJA-ZETCQYMHSA-N D-panthenol Chemical compound OCC(C)(C)[C@@H](O)C(=O)NCCCO SNPLKNRPJHDVJA-ZETCQYMHSA-N 0.000 claims description 16
- 239000002253 acid Substances 0.000 claims description 16
- 229940101267 panthenol Drugs 0.000 claims description 16
- 235000020957 pantothenol Nutrition 0.000 claims description 16
- 239000011619 pantothenol Substances 0.000 claims description 16
- 125000002801 octanoyl group Chemical group C(CCCCCCC)(=O)* 0.000 claims description 15
- 239000000463 material Substances 0.000 claims description 11
- 239000003109 Disodium ethylene diamine tetraacetate Substances 0.000 claims description 10
- ZGTMUACCHSMWAC-UHFFFAOYSA-L EDTA disodium salt (anhydrous) Chemical compound [Na+].[Na+].OC(=O)CN(CC([O-])=O)CCN(CC(O)=O)CC([O-])=O ZGTMUACCHSMWAC-UHFFFAOYSA-L 0.000 claims description 10
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 10
- MRUAUOIMASANKQ-UHFFFAOYSA-O carboxymethyl-[3-(dodecanoylamino)propyl]-dimethylazanium Chemical compound CCCCCCCCCCCC(=O)NCCC[N+](C)(C)CC(O)=O MRUAUOIMASANKQ-UHFFFAOYSA-O 0.000 claims description 10
- 238000001816 cooling Methods 0.000 claims description 10
- 235000019301 disodium ethylene diamine tetraacetate Nutrition 0.000 claims description 10
- 238000010438 heat treatment Methods 0.000 claims description 10
- 229940075468 lauramidopropyl betaine Drugs 0.000 claims description 10
- 229940049920 malate Drugs 0.000 claims description 10
- BJEPYKJPYRNKOW-UHFFFAOYSA-N malic acid Chemical compound OC(=O)C(O)CC(O)=O BJEPYKJPYRNKOW-UHFFFAOYSA-N 0.000 claims description 10
- 238000000034 method Methods 0.000 claims description 10
- 229940057950 sodium laureth sulfate Drugs 0.000 claims description 10
- SXHLENDCVBIJFO-UHFFFAOYSA-M sodium;2-[2-(2-dodecoxyethoxy)ethoxy]ethyl sulfate Chemical compound [Na+].CCCCCCCCCCCCOCCOCCOCCOS([O-])(=O)=O SXHLENDCVBIJFO-UHFFFAOYSA-M 0.000 claims description 10
- 239000000049 pigment Substances 0.000 claims description 9
- 239000003795 chemical substances by application Substances 0.000 claims description 8
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims description 6
- 238000000265 homogenisation Methods 0.000 claims description 6
- 239000002562 thickening agent Substances 0.000 claims description 6
- 240000001548 Camellia japonica Species 0.000 claims description 5
- 235000018597 common camellia Nutrition 0.000 claims description 5
- 235000015112 vegetable and seed oil Nutrition 0.000 claims description 5
- 230000003750 conditioning effect Effects 0.000 claims description 4
- PUPZLCDOIYMWBV-UHFFFAOYSA-N (+/-)-1,3-Butanediol Chemical compound CC(O)CCO PUPZLCDOIYMWBV-UHFFFAOYSA-N 0.000 claims description 3
- DGSZGZSCHSQXFV-UHFFFAOYSA-N 2,3-bis(2-ethylhexanoyloxy)propyl 2-ethylhexanoate Chemical compound CCCCC(CC)C(=O)OCC(OC(=O)C(CC)CCCC)COC(=O)C(CC)CCCC DGSZGZSCHSQXFV-UHFFFAOYSA-N 0.000 claims description 3
- QCDWFXQBSFUVSP-UHFFFAOYSA-N 2-phenoxyethanol Chemical compound OCCOC1=CC=CC=C1 QCDWFXQBSFUVSP-UHFFFAOYSA-N 0.000 claims description 3
- ANZUDYZHSVGBRF-UHFFFAOYSA-N 3-ethylnonane-1,2,3-triol Chemical compound CCCCCCC(O)(CC)C(O)CO ANZUDYZHSVGBRF-UHFFFAOYSA-N 0.000 claims description 3
- 229920001214 Polysorbate 60 Polymers 0.000 claims description 3
- 230000003020 moisturizing effect Effects 0.000 claims description 3
- 229960005323 phenoxyethanol Drugs 0.000 claims description 3
- 239000001818 polyoxyethylene sorbitan monostearate Substances 0.000 claims description 3
- 235000010989 polyoxyethylene sorbitan monostearate Nutrition 0.000 claims description 3
- 229940113124 polysorbate 60 Drugs 0.000 claims description 3
- WXMKPNITSTVMEF-UHFFFAOYSA-M sodium benzoate Chemical compound [Na+].[O-]C(=O)C1=CC=CC=C1 WXMKPNITSTVMEF-UHFFFAOYSA-M 0.000 claims description 3
- 235000010234 sodium benzoate Nutrition 0.000 claims description 3
- 239000004299 sodium benzoate Substances 0.000 claims description 3
- 239000011780 sodium chloride Substances 0.000 claims description 3
- 229940061605 tetrasodium glutamate diacetate Drugs 0.000 claims description 3
- UZVUJVFQFNHRSY-OUTKXMMCSA-J tetrasodium;(2s)-2-[bis(carboxylatomethyl)amino]pentanedioate Chemical compound [Na+].[Na+].[Na+].[Na+].[O-]C(=O)CC[C@@H](C([O-])=O)N(CC([O-])=O)CC([O-])=O UZVUJVFQFNHRSY-OUTKXMMCSA-J 0.000 claims description 3
- 230000009977 dual effect Effects 0.000 claims 1
- 239000000047 product Substances 0.000 abstract description 35
- 239000003921 oil Substances 0.000 abstract description 18
- 230000007794 irritation Effects 0.000 abstract description 5
- 239000012467 final product Substances 0.000 abstract description 3
- 230000036555 skin type Effects 0.000 abstract description 2
- 230000000052 comparative effect Effects 0.000 description 48
- 239000006260 foam Substances 0.000 description 20
- 239000000203 mixture Substances 0.000 description 17
- 235000019198 oils Nutrition 0.000 description 16
- 241000157835 Gardenia Species 0.000 description 15
- CDQSJQSWAWPGKG-UHFFFAOYSA-N butane-1,1-diol Chemical compound CCCC(O)O CDQSJQSWAWPGKG-UHFFFAOYSA-N 0.000 description 14
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- 239000012085 test solution Substances 0.000 description 9
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- 230000014759 maintenance of location Effects 0.000 description 7
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- 238000005187 foaming Methods 0.000 description 6
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- 230000003078 antioxidant effect Effects 0.000 description 3
- 239000006071 cream Substances 0.000 description 3
- UWKAYLJWKGQEPM-UHFFFAOYSA-N linalool acetate Natural products CC(C)=CCCC(C)(C=C)OC(C)=O UWKAYLJWKGQEPM-UHFFFAOYSA-N 0.000 description 3
- 235000011929 mousse Nutrition 0.000 description 3
- 230000007935 neutral effect Effects 0.000 description 3
- 239000000419 plant extract Substances 0.000 description 3
- GLZPCOQZEFWAFX-UHFFFAOYSA-N Geraniol Chemical compound CC(C)=CCCC(C)=CCO GLZPCOQZEFWAFX-UHFFFAOYSA-N 0.000 description 2
- 206010061218 Inflammation Diseases 0.000 description 2
- 239000004909 Moisturizer Substances 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 2
- 238000013329 compounding Methods 0.000 description 2
- ZYGHJZDHTFUPRJ-UHFFFAOYSA-N coumarin Chemical compound C1=CC=C2OC(=O)C=CC2=C1 ZYGHJZDHTFUPRJ-UHFFFAOYSA-N 0.000 description 2
- 238000002474 experimental method Methods 0.000 description 2
- UWKAYLJWKGQEPM-LBPRGKRZSA-N linalyl acetate Chemical compound CC(C)=CCC[C@](C)(C=C)OC(C)=O UWKAYLJWKGQEPM-LBPRGKRZSA-N 0.000 description 2
- 230000001333 moisturizer Effects 0.000 description 2
- RGUVUPQQFXCJFC-UHFFFAOYSA-N n-hydroxyoctanamide Chemical compound CCCCCCCC(=O)NO RGUVUPQQFXCJFC-UHFFFAOYSA-N 0.000 description 2
- 238000011056 performance test Methods 0.000 description 2
- 230000008569 process Effects 0.000 description 2
- 238000013112 stability test Methods 0.000 description 2
- INYYVPJSBIVGPH-UHFFFAOYSA-N 14-episinomenine Natural products C1CN(C)C2CC3=CC=C(OC)C(O)=C3C31C2C=C(OC)C(=O)C3 INYYVPJSBIVGPH-UHFFFAOYSA-N 0.000 description 1
- 102000008186 Collagen Human genes 0.000 description 1
- 108010035532 Collagen Proteins 0.000 description 1
- AQASRZOCERRGBL-UHFFFAOYSA-N Dauricine Natural products CN1CCC2=CC(OC)=C(OC)C=C2C1CC1=CC=C(O)C(OC2=CC=C(C=C2)CC2N(C)CCC=3C=C(C(=CC=32)OC)OC)=C1 AQASRZOCERRGBL-UHFFFAOYSA-N 0.000 description 1
- 239000005792 Geraniol Substances 0.000 description 1
- GLZPCOQZEFWAFX-YFHOEESVSA-N Geraniol Natural products CC(C)=CCC\C(C)=C/CO GLZPCOQZEFWAFX-YFHOEESVSA-N 0.000 description 1
- 244000062245 Hedychium flavescens Species 0.000 description 1
- 206010020751 Hypersensitivity Diseases 0.000 description 1
- 208000002193 Pain Diseases 0.000 description 1
- PTPHDVKWAYIFRX-UHFFFAOYSA-N Palmatine Natural products C1C2=C(OC)C(OC)=CC=C2C=C2N1CCC1=C2C=C(OC)C(OC)=C1 PTPHDVKWAYIFRX-UHFFFAOYSA-N 0.000 description 1
- RBBVPNQTBKHOEQ-KKSFZXQISA-O Phellodendrine Chemical compound C1CC2=CC(OC)=C(O)C=C2[C@H]2[N@+]1(C)CC(C=C(C(=C1)O)OC)=C1C2 RBBVPNQTBKHOEQ-KKSFZXQISA-O 0.000 description 1
- INYYVPJSBIVGPH-QHRIQVFBSA-N Sinomenine Chemical compound C([C@@H]1N(CC2)C)C3=CC=C(OC)C(O)=C3[C@@]32[C@@H]1C=C(OC)C(=O)C3 INYYVPJSBIVGPH-QHRIQVFBSA-N 0.000 description 1
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- 230000009471 action Effects 0.000 description 1
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- 208000026935 allergic disease Diseases 0.000 description 1
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- 230000003064 anti-oxidating effect Effects 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 230000003385 bacteriostatic effect Effects 0.000 description 1
- 230000004888 barrier function Effects 0.000 description 1
- YBHILYKTIRIUTE-UHFFFAOYSA-N berberine Chemical compound C1=C2CC[N+]3=CC4=C(OC)C(OC)=CC=C4C=C3C2=CC2=C1OCO2 YBHILYKTIRIUTE-UHFFFAOYSA-N 0.000 description 1
- 229940093265 berberine Drugs 0.000 description 1
- QISXPYZVZJBNDM-UHFFFAOYSA-N berberine Natural products COc1ccc2C=C3N(Cc2c1OC)C=Cc4cc5OCOc5cc34 QISXPYZVZJBNDM-UHFFFAOYSA-N 0.000 description 1
- RARWEROUOQPTCJ-RBUKOAKNSA-N cepharamine Natural products C1CC2=CC=C(OC)C(O)=C2[C@@]2(CCN3C)[C@]13C=C(OC)C(=O)C2 RARWEROUOQPTCJ-RBUKOAKNSA-N 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 229930002875 chlorophyll Natural products 0.000 description 1
- 235000019804 chlorophyll Nutrition 0.000 description 1
- ATNHDLDRLWWWCB-AENOIHSZSA-M chlorophyll a Chemical compound C1([C@@H](C(=O)OC)C(=O)C2=C3C)=C2N2C3=CC(C(CC)=C3C)=[N+]4C3=CC3=C(C=C)C(C)=C5N3[Mg-2]42[N+]2=C1[C@@H](CCC(=O)OC\C=C(/C)CCC[C@H](C)CCC[C@H](C)CCCC(C)C)[C@H](C)C2=C5 ATNHDLDRLWWWCB-AENOIHSZSA-M 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 229920001436 collagen Polymers 0.000 description 1
- 230000001276 controlling effect Effects 0.000 description 1
- 229960000956 coumarin Drugs 0.000 description 1
- 235000001671 coumarin Nutrition 0.000 description 1
- AQASRZOCERRGBL-ROJLCIKYSA-N dauricine Chemical compound CN1CCC2=CC(OC)=C(OC)C=C2[C@H]1CC1=CC=C(O)C(OC2=CC=C(C=C2)C[C@H]2N(C)CCC=3C=C(C(=CC=32)OC)OC)=C1 AQASRZOCERRGBL-ROJLCIKYSA-N 0.000 description 1
- 239000008367 deionised water Substances 0.000 description 1
- 229910021641 deionized water Inorganic materials 0.000 description 1
- 230000003467 diminishing effect Effects 0.000 description 1
- FPVGTPBMTFTMRT-UHFFFAOYSA-L disodium;2-amino-5-[(4-sulfonatophenyl)diazenyl]benzenesulfonate Chemical compound [Na+].[Na+].C1=C(S([O-])(=O)=O)C(N)=CC=C1N=NC1=CC=C(S([O-])(=O)=O)C=C1 FPVGTPBMTFTMRT-UHFFFAOYSA-L 0.000 description 1
- 239000012153 distilled water Substances 0.000 description 1
- 235000019233 fast yellow AB Nutrition 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 210000000245 forearm Anatomy 0.000 description 1
- 229940113087 geraniol Drugs 0.000 description 1
- -1 glycerol tri (ethyl hexanoate) ester Chemical class 0.000 description 1
- 230000004054 inflammatory process Effects 0.000 description 1
- 230000005764 inhibitory process Effects 0.000 description 1
- 230000002045 lasting effect Effects 0.000 description 1
- 239000001656 lutein Substances 0.000 description 1
- 235000012680 lutein Nutrition 0.000 description 1
- 229960005375 lutein Drugs 0.000 description 1
- KBPHJBAIARWVSC-RGZFRNHPSA-N lutein Chemical compound C([C@H](O)CC=1C)C(C)(C)C=1\C=C\C(\C)=C\C=C\C(\C)=C\C=C\C=C(/C)\C=C\C=C(/C)\C=C\[C@H]1C(C)=C[C@H](O)CC1(C)C KBPHJBAIARWVSC-RGZFRNHPSA-N 0.000 description 1
- ORAKUVXRZWMARG-WZLJTJAWSA-N lutein Natural products CC(=C/C=C/C=C(C)/C=C/C=C(C)/C=C/C1=C(C)CCCC1(C)C)C=CC=C(/C)C=CC2C(=CC(O)CC2(C)C)C ORAKUVXRZWMARG-WZLJTJAWSA-N 0.000 description 1
- 238000012423 maintenance Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- QUCQEUCGKKTEBI-UHFFFAOYSA-N palmatine Chemical compound COC1=CC=C2C=C(C3=C(C=C(C(=C3)OC)OC)CC3)[N+]3=CC2=C1OC QUCQEUCGKKTEBI-UHFFFAOYSA-N 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 230000008439 repair process Effects 0.000 description 1
- 230000003252 repetitive effect Effects 0.000 description 1
- 229930002966 sinomenine Natural products 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 230000000087 stabilizing effect Effects 0.000 description 1
- 230000001954 sterilising effect Effects 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- KBPHJBAIARWVSC-XQIHNALSSA-N trans-lutein Natural products CC(=C/C=C/C=C(C)/C=C/C=C(C)/C=C/C1=C(C)CC(O)CC1(C)C)C=CC=C(/C)C=CC2C(=CC(O)CC2(C)C)C KBPHJBAIARWVSC-XQIHNALSSA-N 0.000 description 1
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- 238000005303 weighing Methods 0.000 description 1
- FJHBOVDFOQMZRV-XQIHNALSSA-N xanthophyll Natural products CC(=C/C=C/C=C(C)/C=C/C=C(C)/C=C/C1=C(C)CC(O)CC1(C)C)C=CC=C(/C)C=CC2C=C(C)C(O)CC2(C)C FJHBOVDFOQMZRV-XQIHNALSSA-N 0.000 description 1
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Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/31—Hydrocarbons
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/03—Liquid compositions with two or more distinct layers
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/14—Preparations for removing make-up
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Engineering & Computer Science (AREA)
- Biotechnology (AREA)
- Botany (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Gerontology & Geriatric Medicine (AREA)
- Dermatology (AREA)
- Cosmetics (AREA)
Abstract
The embodiment of the application discloses a bi-component cleansing facial cleanser and a preparation method thereof, and the bi-component cleansing facial cleanser comprises a component A and a component B, wherein the component A comprises the following components in parts by weight: 30-85 parts of water, 1-10 parts of mineral oil, 10-40 parts of surfactant, 0.02-0.8 part of tremella polysaccharide, 0.5-5 parts of emulsifier, 1-30 parts of humectant and 0.01-0.5 part of preservative; the component B comprises the following components in parts by weight: 8-75 parts of mineral oil, 0.01-0.6 part of amur corktree bark extract, 0.01-0.6 part of lavender flower extract, 0.01-0.6 part of gardenia fruit extract and 0.01-0.5 part of preservative; the mass ratio of the component A to the component B is 20; according to the technical scheme, the mass ratio of the component A to the component B in the product is controlled, the user can adjust the using amount of the component B according to the skin condition of the user when the product is used, the oil-water ratio of the final product is further adjusted, so that the product can be suitable for crowds with different skin types, is fresh and cool after being used, is not pulled dry, is low in irritation, reduces the oil film feeling after being used, and is high in interestingness.
Description
Technical Field
The application relates to the field of daily chemicals, in particular to a bi-component cleansing facial cleanser and a preparation method thereof.
Background
The makeup removing products are various at present, and comprise makeup removing oil, makeup removing cream and the like. However, the cleansing oil is greasy after use, is not suitable for oily skin, has poor cleansing effect, and although the cleansing cream has strong plot strength, needs to be cleaned for the second time after use, and is tedious to use.
As a novel makeup removing product, the makeup removing mousse can be comprehensively attached to skin due to fine hand feeling and is convenient to use. The conventional makeup removing mousse generally adopts an aqueous solution as an inner material, foams by the action of a foam pump, generally increases the oil-water ratio in order to enhance the cleaning effect, but the makeup removing product with high water-oil ratio is not suitable for oily skin, so that a makeup removing product capable of adjusting the oil-water ratio aiming at users with different skin types is needed.
Disclosure of Invention
The embodiment of the application provides a bi-component cleansing facial cleanser and a manufacturing method thereof, which can effectively enhance the stability of cleansing mousse, make foam more lasting and ensure that the comfort of skin of a user is not pulled dry after the user uses the cleansing facial cleanser.
The embodiment of the application provides a bi-component cleansing liquid, which comprises a component A and a component B, wherein the component A comprises the following components in parts by weight: 30-85 parts of water, 1-10 parts of mineral oil, 10-40 parts of surfactant, 0.02-0.8 part of tremella polysaccharide, 0.5-5 parts of emulsifier, 1-30 parts of humectant and 0.01-0.5 part of preservative;
the component B comprises the following components in parts by weight: 8-75 parts of mineral oil, 0.01-0.6 part of phellodendron bark extract, 0.01-0.6 part of lavender flower extract, 0.01-0.6 part of gardenia fruit extract and 0.01-0.5 part of preservative;
the mass ratio of the component A to the component B is 20.
Preferably, the component A comprises the following raw materials in parts by weight: 30-55 parts of water, 2-4 parts of mineral oil, 10-20 parts of surfactant, 0.02-0.06 part of tremella polysaccharide, 0.5-3 parts of emulsifier, 1-20 parts of humectant and 0.01-0.05 part of preservative;
the component B comprises the following raw materials in parts by weight: 16-52 parts of mineral oil, 0.01-0.1 part of amur corktree bark extract, 0.01-0.1 part of lavender flower extract, 0.01-0.1 part of gardenia fruit extract and 0.01-0.05 part of preservative;
the mass ratio of the component A to the component B is 20.
Preferably, the component A also comprises 0.1 to 0.5 part of foaming agent, 0.01 to 0.1 part of chelating agent, 0.01 to 0.05 part of pH regulator or 0.01 to 0.1 part of thickening agent in parts by weight;
the component B also comprises 0.5 to 1.1 parts of conditioner, 0.01 to 0.08 part of chelating agent or 0.001 to 0.03 part of pigment in parts by weight.
Preferably, the foaming agent comprises sodium cocoyl malate; the chelating agent comprises at least one of disodium EDTA and tetrasodium glutamate diacetate; the pH regulator comprises citric acid and the thickener comprises sodium chloride.
Preferably, the conditioning agent comprises at least one of panthenol, squalane, camellia seed oil, and glycerol tri (ethyl hexanoate).
Preferably, the surfactant comprises at least one of sodium laureth sulfate, sodium cocamidopropionate or lauramidopropyl betaine.
Preferably, the emulsifier comprises at least two of polyglyceryl-10 myristate, sorbitan stearate, polysorbate-60.
Preferably, the moisturizer comprises: at least one of butylene glycol, ethylene glycol, methyl propylene glycol, or ethyl hexyl glycerol; the preservative comprises: at least one of glyceryl caprylate, caprylyl hydroximic acid, phenoxyethanol, p-hydroxyacetophenone and sodium benzoate.
The application also provides a preparation method of the bi-component cleansing facial cleanser, which comprises the following steps:
sequentially adding the raw materials in the component A in parts by weight into a clean batching pot, starting stirring at the rotating speed of 30-50 revolutions/min, stirring and heating to 65 ℃, cooling to room temperature, testing, discharging and filling;
and (3) sequentially adding the raw materials in the component B in parts by weight into a clean batching pot at room temperature, starting homogenization at the speed of 1000-1500 rpm for 1-2 minutes until the materials are uniformly mixed, testing, discharging and filling.
The application also provides a using method of the two-component cleansing facial cleanser, wherein the component A and the component B are mixed according to the proportion of 20 to 3 to 9 and are used after being shaken up.
The beneficial effects of the invention at least comprise:
the invention provides a bi-component cleansing facial cleanser, which comprises a component A and a component B, wherein the component A is matched with a proper surfactant and an emulsifier on the basis of a conventional water phase component, and tremella polysaccharide is adopted to replace a polyol component in a part of moisturizing agent, so that the cleansing facial cleanser has high stability after foaming, and the component B is an oil phase and is matched with a plant extract, so that the skin maintenance in the cleansing process is effectively ensured, the antioxidant effect is realized, and the damage of the cleansing product to the skin is reduced; when the product is used, a user can adjust the using amount of the component B according to the skin condition of the user, so that the state of the final product is adjusted, the product can be suitable for people with different skins, the product is fresh and cool after being used, the skin is not pulled dry, the irritation is low, and the interestingness is increased by the manual DIY of the user.
Detailed Description
The technical solutions in the embodiments of the present application are clearly and completely described below, and it is obvious that the described embodiments are only a part of the embodiments of the present application, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present application.
The embodiment of the application provides a two-component cleansing facial cleanser and a preparation method thereof. The following are detailed below. It should be noted that the following description of the embodiments is not intended to limit the preferred order of the embodiments. In addition, in the description of the present application, the term "including" means "including but not limited to". The terms first, second, third and the like are used merely as labels, and do not impose numerical requirements or an established order. Various embodiments of the invention may exist in a range of versions; it should be understood that the description in range format is merely for convenience and brevity and should not be construed as an inflexible limitation on the scope of the invention; accordingly, the described range descriptions should be considered to have specifically disclosed all the possible sub-ranges as well as individual numerical values within that range. For example, it is contemplated that the description of a range from 1 to 6 has specifically disclosed sub-ranges such as, for example, from 1 to 3, from 1 to 4, from 1 to 5, from 2 to 4, from 2 to 6, from 3 to 6, etc., as well as individual numbers within a range such as, for example, 1, 2, 3, 4, 5, and 6, as applicable regardless of the range. In addition, whenever a numerical range is indicated herein, it is meant to include any number (fractional or integer) recited within the indicated range.
The application provides a two-component cleansing facial cleanser, which comprises a component A and a component B, wherein the component A comprises the following components in parts by weight: 30-85 parts of water, 1-10 parts of mineral oil, 10-40 parts of surfactant, 0.02-0.8 part of tremella polysaccharide, 0.5-5 parts of emulsifier, 1-30 parts of humectant and 0.01-0.5 part of preservative;
the component B comprises the following components in parts by weight: 8-75 parts of mineral oil, 0.01-0.6 part of amur corktree bark extract, 0.01-0.6 part of lavender flower extract, 0.01-0.6 part of gardenia fruit extract and 0.01-0.5 part of preservative;
the mass ratio of the component A to the component B is 20-20.
Further, the component A comprises the following raw materials in parts by weight: 30-55 parts of water, 2-4 parts of mineral oil, 10-20 parts of surfactant, 0.02-0.06 part of tremella polysaccharide, 0.5-3 parts of emulsifier, 1-20 parts of humectant and 0.01-0.05 part of preservative; the component B comprises the following raw materials in parts by weight: 16-52 parts of mineral oil, 0.01-0.1 part of amur corktree bark extract, 0.01-0.1 part of lavender flower extract, 0.01-0.1 part of gardenia fruit extract and 0.01-0.05 part of preservative;
the mass ratio of the component A to the component B is 20.
Further, the component A also comprises at least one of 0.1 to 0.5 part of foaming agent, 0.01 to 0.1 part of chelating agent, 0.01 to 0.05 part of pH regulator or 0.01 to 0.1 part of thickening agent in parts by weight;
the component B also comprises at least one of a conditioning agent of 0.5 to 1.1 parts, a chelating agent of 0.01 to 0.08 part or a pigment of 0.001 to 0.03 part by weight.
Specifically, the sudsing agent comprises sodium cocoyl malate.
Specifically, the chelating agent comprises at least one of disodium EDTA and tetrasodium glutamate diacetate.
Specifically, the PH adjuster includes citric acid and the thickener includes sodium chloride.
Specifically, the conditioning agent comprises at least one of panthenol, squalane, camellia seed oil and glycerol tri (ethyl hexanoate).
Specifically, the surfactant comprises at least one of sodium laureth sulfate, sodium cocamidopropionate, or lauramidopropyl betaine.
Specifically, the emulsifier comprises a hydrophilic emulsifier and a lipophilic emulsifier, and specifically can be at least two of polyglycerol-10 myristate, sorbitan stearate and polysorbate-60, and preferably comprises the hydrophilic emulsifier and the lipophilic emulsifier simultaneously.
Specifically, the moisturizer comprises: at least one of butylene glycol, ethylene glycol, methyl propylene glycol or ethyl hexyl glycerol;
specifically, the preservative comprises: at least one of glyceryl caprylate, caprylyl hydroximic acid, phenoxyethanol, p-hydroxyacetophenone and sodium benzoate.
Specifically, the water is deionized water.
Specifically, the pigment is an oil-soluble pigment, including but not limited to oil-soluble chlorophyll, oil-soluble B-carotene, food blue, acid red, acid yellow ginger yellow pigment, lutein.
The application also provides a preparation method of the bi-component cleansing liquid, which comprises the following steps:
sequentially adding the raw materials in the component A in parts by weight into a clean batching pot, starting stirring at the rotating speed of 30-50 revolutions/min, stirring and heating to 65 ℃, cooling to room temperature, testing, discharging and filling;
and (3) sequentially adding the raw materials in the component B in parts by weight into a clean batching pot at room temperature, starting homogenization at the speed of 1000-1500 rpm for 1-2 minutes until the materials are uniformly mixed, testing, discharging and filling.
The application also provides a using method of the bi-component cleansing liquid, wherein the component A and the component B are mixed according to the proportion of 20.
It can be appreciated that the present invention provides a two-component cleansing liquid which has the following beneficial effects:
the cleansing product is high in stability after foaming by arranging the component A to be matched with a proper surfactant and an emulsifier on the basis of a conventional water-phase component and adopting tremella polysaccharide to replace a part of polyol component in the humectant, and the cleansing product is effectively guaranteed to be maintained on the skin in the cleansing process by arranging the component B to be an oil phase and matching with a plant extract, so that an anti-oxidation effect is realized, and the damage of the cleansing product to the skin is reduced; when the skin care product is used, the usage amount of the component B can be adjusted by a user according to the skin condition of the user, so that the oil-water ratio in the final product is adjusted, the product can be suitable for people with different skin conditions, is fresh and cool after being used, is not pulled dry, reduces the oil film feeling after being used, and is strong in interestingness and attractive in appearance.
The cortex phellodendri bark extract, the lavender flower extract and the gardenia fruit extract are adopted as the curing components in the component B, and the skin can be cured by compounding the cortex phellodendri bark extract, the lavender flower extract and the gardenia fruit extract, so that the antioxidant effect is realized, and the damage of makeup removing products to the skin is reduced.
The conditioner adopts high-efficiency moisture-retaining components such as squalane, camellia seed oil and the like as the conditioner, helps to improve moisture balance and repair barriers, and ensures the mildness of the formula.
The lavender flower extract is selected to replace the traditional essence components, the extract contains linalyl acetate, linalool acetate, geraniol, coumarin and other components, the bacteriostatic effect is good, the extract has a color, and the aesthetic degree of a two-phase product is improved.
The cortex phellodendri extract is selected, and mainly contains berberine, and contains palmatine, phellodendrine, dauricine, sinomenine, cortex phellodendri chinensis and the like, can promote the generation of collagen, can slow down aging and inhibit the growth of hair by combining the inoxidizability of the extract, and has the functions of anti-inflammation and odor inhibition.
The gardenia fruit extract can be matched with the phellodendron bark extract and the lavender flower extract to play the roles of relieving and resisting allergy, improving the resistance of the skin, sterilizing and diminishing inflammation.
The following description is given by way of specific examples.
It should be noted that the plant extracts and the related auxiliary reagents in the examples of the present application are commercially available from Daihuang, perfection (China) Inc., hangzhou Lin Biotech, inc., hangzhou Lizhuang Makeup Biotech, inc.
Example 1
The two-component cleansing liquid comprises a component A and a component B, wherein the component A comprises the following components in parts by weight: 55 parts of water, 2 parts of mineral oil, 35 parts of surfactant, 0.02 part of tremella polysaccharide, 0.5 part of emulsifier, 2 parts of humectant, 0.01 part of preservative, 0.1 part of foaming agent, 0.01 part of pH regulator and 0.01 part of chelating agent;
the component B comprises the following components in parts by weight: 18 parts of mineral oil, 0.01 part of amur corktree bark extract, 0.01 part of lavender flower extract, 0.01 part of gardenia fruit extract, 0.5 part of conditioner, 0.01 part of preservative and 0.01 part of chelating agent;
the mass ratio of the component A to the component B is 20.
Wherein the surfactant is sodium laureth sulfate, sodium cocamidopropionate or lauramidopropyl betaine, and the mass ratio of the surfactant to the surfactant is 3:1:1.
the emulsifier is polyglycerol-10 myristate and sorbitan stearate, and the weight ratio of the polyglycerol-10 myristate to the sorbitan stearate is 1.15:1.
the humectant is a mixture of butanediol, ethylene glycol and methyl propylene glycol, and the weight ratio of the butanediol to the ethylene glycol to the methyl propylene glycol is (1.2).
The preservative is a mixture of p-hydroxyacetophenone, glyceryl caprylate and caprylyl hydroximic acid, and the weight ratio of the p-hydroxyacetophenone to the glyceryl caprylate to the caprylyl hydroximic acid is 1.
The foaming agent is sodium cocoyl malate.
The chelating agent is disodium EDTA.
The pH regulator is citric acid.
The conditioner comprises panthenol and squalane, wherein the weight ratio of the panthenol to the squalane is 1:0.1.
the preparation method comprises the following steps:
sequentially adding the raw materials in the component A in parts by weight into a clean batching pot, starting stirring at the rotating speed of 30-50 revolutions/min, stirring and heating to 65 ℃, cooling to room temperature, testing, discharging and filling;
and (3) sequentially adding the raw materials in the component B in parts by weight into a clean batching pot at room temperature, starting homogenization at the speed of 1000-1500 rpm for 1-2 minutes until the materials are uniformly mixed, testing, discharging and filling.
Example 2
The two-component cleansing liquid comprises a component A and a component B, wherein the component A comprises the following components in parts by weight: 55 parts of water, 2 parts of mineral oil, 35 parts of surfactant, 0.3 part of tremella polysaccharide, 0.5 part of emulsifier, 16 parts of humectant, 0.01 part of preservative, 0.1 part of foaming agent, 0.01 part of pH regulator and 0.01 part of chelating agent;
the component B comprises the following components in parts by weight: 18 parts of mineral oil, 0.01 part of amur corktree bark extract, 0.01 part of lavender flower extract, 0.01 part of gardenia fruit extract, 0.5 part of conditioner, 0.01 part of preservative and 0.01 part of chelating agent;
the mass ratio of the component A to the component B is 20.
Wherein the surfactant is sodium laureth sulfate, sodium cocamidopropionate or lauramidopropyl betaine in a mass ratio of 3:1:1.
the emulsifier is polyglycerol-10 myristate and sorbitan stearate, and the weight ratio of the polyglycerol-10 myristate to the sorbitan stearate is 1.15:1.
the humectant is a mixture of butanediol, ethylene glycol and methyl propylene glycol, and the weight ratio of the butanediol to the ethylene glycol to the methyl propylene glycol is (1.2).
The preservative is a mixture of p-hydroxyacetophenone, glyceryl caprylate and caprylyl hydroximic acid, and the weight ratio of the p-hydroxyacetophenone to the glyceryl caprylate to the caprylyl hydroximic acid is 1.
The foaming agent is sodium cocoyl malate.
The chelating agent is disodium EDTA.
The pH regulator is citric acid.
The conditioner comprises panthenol and squalane, wherein the weight ratio of the panthenol to the squalane is 1:0.1.
the preparation method comprises the following steps:
sequentially adding the raw materials in the component A in parts by weight into a clean batching pot, starting stirring at the rotating speed of 30-50 revolutions/min, stirring and heating to 65 ℃, cooling to room temperature, testing, discharging and filling;
at room temperature, sequentially adding the raw materials in the component B in parts by weight into a clean batching pot, starting homogenizing at the speed of 1000-1500 rpm of a homogenizer, homogenizing and dispersing for 1-2 minutes until the materials are uniformly mixed, testing, discharging and filling.
Example 3
The two-component cleansing liquid comprises a component A and a component B, wherein the component A comprises the following components in parts by weight: 55 parts of water, 2 parts of mineral oil, 35 parts of surfactant, 0.6 part of tremella polysaccharide, 0.5 part of emulsifier, 20 parts of humectant, 0.01 part of preservative, 0.1 part of foaming agent, 0.01 part of pH regulator and 0.01 part of chelating agent;
the component B comprises the following components in parts by weight: 18 parts of mineral oil, 0.01 part of amur corktree bark extract, 0.01 part of lavender flower extract, 0.01 part of gardenia fruit extract, 0.5 part of conditioner, 0.01 part of preservative and 0.01 part of chelating agent;
the mass ratio of the component A to the component B is 20.
Wherein the surfactant is sodium laureth sulfate, sodium cocamidopropionate or lauramidopropyl betaine, and the mass ratio of the surfactant to the surfactant is 3:1:1.
the emulsifier is polyglycerol-10 myristate and sorbitan stearate, and the weight ratio of the polyglycerol-10 myristate to the sorbitan stearate is 1.15:1.
the humectant is a mixture of butanediol, ethylene glycol and methyl propylene glycol, and the weight ratio of the butanediol to the ethylene glycol to the methyl propylene glycol is 1.2.
The preservative is a mixture of p-hydroxyacetophenone, glyceryl caprylate and caprylyl hydroximic acid, and the weight ratio of the p-hydroxyacetophenone to the glyceryl caprylate to the caprylyl hydroximic acid is 1.
The foaming agent is sodium cocoyl malate.
The chelating agent is disodium EDTA.
The pH regulator is citric acid.
The conditioner comprises panthenol and squalane, wherein the weight ratio of the panthenol to the squalane is 1:0.1.
the preparation method comprises the following steps:
sequentially adding the raw materials in the component A in parts by weight into a clean batching pot, starting stirring at the rotating speed of 30-50 revolutions/min, stirring and heating to 65 ℃, cooling to room temperature, testing, discharging and filling;
and (3) sequentially adding the raw materials in the component B in parts by weight into a clean batching pot at room temperature, starting homogenization at the speed of 1000-1500 rpm for 1-2 minutes until the materials are uniformly mixed, testing, discharging and filling.
Example 4
The two-component cleansing liquid comprises a component A and a component B, wherein the component A comprises the following components in parts by weight: 55 parts of water, 2 parts of mineral oil, 35 parts of surfactant, 0.3 part of tremella polysaccharide, 0.5 part of emulsifier, 16 parts of humectant, 0.01 part of preservative, 0.1 part of foaming agent, 0.01 part of pH regulator and 0.01 part of chelating agent;
the component B comprises the following components in parts by weight: 18 parts of mineral oil, 0.01 part of amur corktree bark extract, 0.01 part of lavender flower extract, 0.01 part of gardenia fruit extract, 0.5 part of conditioner, 0.01 part of preservative and 0.01 part of chelating agent;
the mass ratio of the component A to the component B is 20.
Wherein the surfactant is sodium laureth sulfate, sodium cocamidopropionate or lauramidopropyl betaine in a mass ratio of 3:1:1.
the emulsifier is polyglycerol-10 myristate and sorbitan stearate, and the weight ratio of the polyglycerol-10 myristate to the sorbitan stearate is 1.15:1.
the humectant is a mixture of butanediol, ethylene glycol and methyl propylene glycol, and the weight ratio of the butanediol to the ethylene glycol to the methyl propylene glycol is 1.2.
The preservative is a mixture of p-hydroxyacetophenone, glyceryl caprylate and caprylyl hydroximic acid, and the weight ratio of the p-hydroxyacetophenone to the glyceryl caprylate to the caprylyl hydroximic acid is 1.
The foaming agent is sodium cocoyl malate.
The chelating agent is disodium EDTA.
The pH regulator is citric acid.
The conditioner is a mixture of panthenol, squalane, camellia seed oil and glycerol tri (ethyl hexanoate) ester, and the weight ratio of the conditioner to the oil is 1:0.1:0.02:1.
the preparation method comprises the following steps:
sequentially adding the raw materials in the component A in parts by weight into a clean batching pot, starting stirring at the rotating speed of 30-50 revolutions/min, stirring and heating to 65 ℃, cooling to room temperature, testing, discharging and filling;
at room temperature, sequentially adding the raw materials in the component B in parts by weight into a clean batching pot, starting homogenizing at the speed of 1000-1500 rpm of a homogenizer, homogenizing and dispersing for 1-2 minutes until the materials are uniformly mixed, testing, discharging and filling.
Example 5
The two-component cleansing liquid comprises a component A and a component B, wherein the component A comprises the following components in parts by weight: 55 parts of water, 2 parts of mineral oil, 35 parts of surfactant, 0.3 part of tremella polysaccharide, 0.5 part of emulsifier, 16 parts of humectant, 0.01 part of preservative, 0.1 part of foaming agent, 0.01 part of pH regulator and 0.01 part of chelating agent;
the component B comprises the following components in parts by weight: 18 parts of mineral oil, 0.01 part of amur corktree bark extract, 0.01 part of lavender flower extract, 0.01 part of gardenia fruit extract, 0.5 part of conditioner, 0.01 part of preservative, 0.01 part of chelating agent and 0.001 part of pigment; the mass ratio of the component A to the component B is 20.
Wherein the surfactant is sodium laureth sulfate, sodium cocamidopropionate or lauramidopropyl betaine in a mass ratio of 3:1:1.
the emulsifier is polyglycerol-10 myristate and sorbitan stearate, and the weight ratio of the polyglycerol-10 myristate to the sorbitan stearate is 1.15:1.
the humectant is a mixture of butanediol, ethylene glycol and methyl propylene glycol, and the weight ratio of the butanediol to the ethylene glycol to the methyl propylene glycol is 1.2.
The preservative is a mixture of p-hydroxyacetophenone, glyceryl caprylate and caprylhydroxamic acid, wherein the weight ratio of the p-hydroxyacetophenone to the glyceryl caprylate to the caprylhydroxamic acid is 1.
The foaming agent is sodium cocoyl malate.
The chelating agent is disodium EDTA.
The pH regulator is citric acid.
The conditioner comprises panthenol and squalane, wherein the weight ratio of the panthenol to the squalane is 1:0.1.
the pigment is oil-soluble B-carotene.
The preparation method comprises the following steps:
sequentially adding the raw materials in the component A in parts by weight into a clean batching pot, starting stirring at the rotating speed of 30-50 revolutions/min, stirring and heating to 65 ℃, cooling to room temperature, testing, discharging and filling;
and (3) sequentially adding the raw materials in the component B in parts by weight into a clean batching pot at room temperature, starting homogenization at the speed of 1000-1500 rpm for 1-2 minutes until the materials are uniformly mixed, testing, discharging and filling.
Example 6
The two-component cleansing liquid comprises a component A and a component B, wherein the component A comprises the following components in parts by weight: 55 parts of water, 2 parts of mineral oil, 35 parts of surfactant, 0.3 part of tremella polysaccharide, 0.5 part of emulsifier, 16 parts of humectant, 0.01 part of preservative, 0.1 part of foaming agent, 0.01 part of pH regulator and 0.01 part of chelating agent;
the component B comprises the following components in parts by weight: 18 parts of mineral oil, 0.01 part of amur corktree bark extract, 0.01 part of lavender flower extract, 0.01 part of gardenia fruit extract, 0.5 part of conditioner, 0.01 part of preservative and 0.01 part of chelating agent;
the mass ratio of the component A to the component B is 20.
Wherein the surfactant is sodium laureth sulfate, sodium cocamidopropionate or lauramidopropyl betaine in a mass ratio of 3:1:1.
the emulsifier is polyglycerol-10 myristate and sorbitan stearate, and the weight ratio of the polyglycerol-10 myristate to the sorbitan stearate is 1.15:1.
the humectant is a mixture of butanediol, ethylene glycol and methyl propylene glycol, and the weight ratio of the butanediol to the ethylene glycol to the methyl propylene glycol is 1.2.
The preservative is a mixture of p-hydroxyacetophenone, glyceryl caprylate and caprylyl hydroximic acid, and the weight ratio of the p-hydroxyacetophenone to the glyceryl caprylate to the caprylyl hydroximic acid is 1.
The foaming agent is sodium cocoyl malate.
The chelating agent is disodium EDTA.
The pH regulator is citric acid.
The conditioner comprises panthenol and squalane, wherein the weight ratio of the panthenol to the squalane is 1:0.1.
the preparation method comprises the following steps:
sequentially adding the raw materials in the component A in parts by weight into a clean batching pot, starting stirring at the rotating speed of 30-50 revolutions/min, stirring and heating to 65 ℃, cooling to room temperature, testing, discharging and filling;
at room temperature, sequentially adding the raw materials in the component B in parts by weight into a clean batching pot, starting homogenizing at the speed of 1000-1500 rpm of a homogenizer, homogenizing and dispersing for 1-2 minutes until the materials are uniformly mixed, testing, discharging and filling.
Example 7
The two-component cleansing liquid comprises a component A and a component B, wherein the component A comprises the following components in parts by weight: 55 parts of water, 2 parts of mineral oil, 35 parts of surfactant, 0.3 part of tremella polysaccharide, 0.5 part of emulsifier, 16 parts of humectant, 0.01 part of preservative, 0.1 part of foaming agent, 0.01 part of pH regulator and 0.01 part of chelating agent;
the component B comprises the following components in parts by weight: 18 parts of mineral oil, 0.01 part of amur corktree bark extract, 0.01 part of lavender flower extract, 0.01 part of gardenia fruit extract, 0.5 part of conditioner, 0.01 part of preservative and 0.01 part of chelating agent;
the mass ratio of the component A to the component B is 20.
Wherein the surfactant is sodium laureth sulfate, sodium cocamidopropionate or lauramidopropyl betaine in a mass ratio of 3:1:1.
the emulsifier is polyglycerol-10 myristate and sorbitan stearate, and the weight ratio of the polyglycerol-10 myristate to the sorbitan stearate is 1.15:1.
the humectant is a mixture of butanediol, ethylene glycol and methyl propylene glycol, and the weight ratio of the butanediol to the ethylene glycol to the methyl propylene glycol is 1.2.
The preservative is a mixture of p-hydroxyacetophenone, glyceryl caprylate and caprylyl hydroximic acid, and the weight ratio of the p-hydroxyacetophenone to the glyceryl caprylate to the caprylyl hydroximic acid is 1.
The foaming agent is sodium cocoyl malate.
The chelating agent is disodium EDTA.
The pH regulator is citric acid.
The conditioner comprises panthenol and squalane, wherein the weight ratio of the panthenol to the squalane is 1:0.1.
the preparation method comprises the following steps:
sequentially adding the raw materials in the component A in parts by weight into a clean batching pot, starting stirring at the rotating speed of 30-50 revolutions/min, stirring and heating to 65 ℃, cooling to room temperature, testing, discharging and filling;
at room temperature, sequentially adding the raw materials in the component B in parts by weight into a clean batching pot, starting homogenizing at the speed of 1000-1500 rpm of a homogenizer, homogenizing and dispersing for 1-2 minutes until the materials are uniformly mixed, testing, discharging and filling.
Comparative example 1
The components are the same as in example 2, except that the mass ratio of the component A to the component B is 20.
Comparative example 2
The components are the same as in example 2, except that the mass ratio of the component A to the component B is 20.
Comparative example 3
The components are the same as those in example 2, except that no tremella polysaccharide is added, and the fraction of the humectant is increased to 15.4 parts.
Comparative example 4
The composition was the same as in example 2, except that no cork tree bark extract, lavender flower extract and gardenia fruit extract were added to the B composition, and the mineral oil fraction was increased to 18.03 parts.
Comparative examples 1 to 4 were prepared in the same manner as in example 2 above.
Performance testing
The portions of examples 1 to 5 and comparative examples 1 to 4 were subjected to a foam stability test, a makeup removal performance test and a human sensory evaluation test.
Experiment-foam stability test
The specific method comprises the following steps:
samples of examples 1-3, comparative example 1, comparative example 2 and comparative example 4 were taken and the foaming properties of the products were tested using a Roche foam tester, with the following steps:
preparing a test solution: weighing 3g of each sample into a 1000mL volumetric flask (which is dissolved in a small beaker and then transferred), adding distilled water to the scale, and shaking up.
Operation of the roche foam meter: preheating the super thermostat to 40 +/-1 ℃ and keeping the temperature of the Roche foam instrument at 40 +/-1 ℃. Sucking part of the test solution by using a 200mL quantitative funnel, washing along a wall tube of the foam meter, taking the test solution, putting the test solution into the bottom of the foam meter to 50mL by aligning with a standard scale, sucking 200mL of the test solution by using the 200mL quantitative funnel, fixing the central position of the funnel to ensure that the test solution is vertical to the section of the graduated tube, ensuring that the test solution drips along the central line of the graduated tube, and arranging an outlet of the bulb tube on a 900mL scale mark.
And opening the bulb piston to enable the test solution to flow down, starting a stopwatch immediately when the test solution in the bulb runs out, recording the foam height as the foaming height, and recording the foam height as the foam stabilizing height after recording for 5 min. Taking the average of two results within the allowable error range (the absolute difference between two independent test results obtained under the repetitive conditions is not more than 5 mm) as the final result, and keeping the result to be integer number, wherein the specific test results are shown in the table 1:
TABLE 1
As can be seen from the data in table 1, in comparative example 1, example 2, example 3 and comparative example 3, it can be seen that by controlling the amount of tremella polysaccharide added with tremella polysaccharide, part of polyol is replaced by tremella polysaccharide, and the proportion of part of polyol is reduced, so that the foam of the obtained foaming type facial cleanser is more stable, and the more the proportion of tremella polysaccharide is, the better the stability is;
comparing comparative example 1, comparative example 2 and example 2, it can be seen that the product oil-water ratio in comparative example 1 is lower, the product oil-water ratio in comparative example 2 is high, and the stability of the foamed foam can also be improved by reasonably regulating the ratio of the oil phase to the water phase.
Secondly, comparing comparative example 1, comparative example 2 and comparative example 4, it can be seen that the mass of the component B is reduced, the mass proportion of the corresponding natural component is also small, the mass proportion of the component B of comparative example 2 is larger than that of comparative example 1, a part of the natural component is added, although the foaming height is increased after the natural component is added, the natural component has a certain influence on the stability of the foam, the natural component is reduced, and the stability of the foam is possibly improved.
Experiment two the makeup removal performance test method specifically: the appropriate amount of lipstick, foundation, mascara, and eyeliner were applied evenly to the forearm, respectively, and waited for 2 hours until completely dry.
The makeup remover cleansers of examples 1-4, comparative example 1 and comparative example 2 were then squeezed out by a foam pump about 1g onto makeup, gently rubbed for 30s, and then rinsed out, and the makeup removing effect was recorded and compared, as shown in table 2.
0-clear residue 1-small residue 2-slight residue 3-no residue
TABLE 2
Example 1 | Example 2 | Example 3 | Example 4 | Comparative example 1 | Comparative example 2 | |
Lipstick | 3 | 3 | 2 | 3 | 0 | 3 |
Foundation make-up | 2 | 3 | 3 | 3 | 1 | 3 |
Mascara cream | 3 | 3 | 3 | 3 | 3 | 3 |
Eye line | 3 | 3 | 3 | 3 | 3 | 2 |
From the test results, in comparative examples 1-4, comparative example 1 and comparative example 2, it can be seen that the component a and the component B of the present application have a suitable oil-water ratio after being mixed, and can effectively improve the makeup removing ability of the makeup, so that the product has high cleansing ability for both the makeup with water-based components such as mascara, eyeliner, and the liquid or paste makeup with oil-based components such as lipstick and foundation, etc., the product with comparative example 1 is a product with a water-based phase, the oil phase and the water phase of comparative example 2 are close, and the ratio of the oil phase to the water phase is close to 1:1, the two show that the cleansing power of the makeup is different for the oily component and the makeup and the aqueous component, and it is noted that although the cleansing effect of comparative example 2 is also good, the generated foam is easily defoamed due to the excessive oil phase, and the oil film feeling after use is obvious.
Experiment three specific methods for human body sensory evaluation test: 60 Asian yellow female human species including 20 oily skin female, 20 dry skin female and 20 neutral skin female were collected, and whether oil film feeling (strong oil film feeling of 1 point, no oil film feeling of 5 points), irritation (no irritation feeling of 1 point, obvious stinging feeling of 5 points) and moisturizing effect (no tightness of 5 points, obvious tightness of 1 point) were produced or not was scored using the cleansing liquid prepared in example 2, example 5, example 6, example 7 and comparative examples 1 to 4, and the statistical result of the average value was shown in Table 3;
TABLE 3
As can be seen from table 3:
in the sensory evaluation on whether the oily film feeling is generated in comparative example 2, example 5 and example 6, the female with dry skin can better tolerate the product with high content of the component B, relatively moisten and care the skin, have less oily film feeling, and the female with oily skin can reduce the content of the component B so as to achieve the purpose of reducing the oily film feeling, the product is suitable for the female with the neutral skin within the range of the compounding ratio of the component A and the component B, is more obvious compared with comparative example 1 and comparative example 2, the component B content of the comparative example 1 is less, most of the product is the water phase component, the water phase component and the oil phase component in the comparative example 2 are basically 1, the female with oily skin has obvious oily film feeling, and the results of the comparative example 3 and the comparative example 4 are not much different from those of the example 2.
Comparing the sensory evaluation on whether skin is irritated or not in comparative example 1, comparative example 2, example 5 and example 6, it can be seen that the formula of the product is mild, the higher the content of the component B is for women with dry skin, the lower the corresponding irritation, and the comparative example 4 shows that the effect of better skin protection can not be achieved without adding natural components, therefore, the added plant-extracted natural components can achieve the effects of caring skin, achieving an antioxidant effect and reducing the damage of makeup removing products to skin.
Compared with the sensory evaluation on the moisture retention in comparative example 1, comparative example 2, example 5 and example 6, it can be seen that the product has a better moisture retention effect on women with oily skin, neutral skin and dry skin when the mass ratio of the component A to the component B is within the range of 20-3-9, and the moisture retention effect on women with oily skin and dry skin is affected by the higher water phase or oil-water ratio of the product compared with comparative example 1 and comparative example 2, and the moisture retention effect is slightly affected by the addition of the tremella polysaccharide compared with the stability of foam when the tremella polysaccharide is added or not compared with comparative example 3 and comparative example 4, but the moisture retention effect is slightly affected by the absence of the addition of the natural tremella polysaccharide, so that the moisture retention effect of the product is achieved by the moisture retention agent, and the natural tremella component plays a role in maintaining.
Comparing example 2, example 5, example 6 and example 7 with the comparative example, it can be seen that the product without added pigment is that the product has a bluish blue/transparent double phase due to the added lavender flower extract, and a bright orange/transparent double phase after added pigment, so that the product has a more novel appearance and meets the market demand.
The above-mentioned embodiments of the present application provide a two-component cleansing liquid and a method for making the same, which are described in detail, and the specific examples are applied herein to explain the principles and embodiments of the present application, and the description of the above-mentioned embodiments is only used to help understanding the method and the core concept of the present application; meanwhile, for those skilled in the art, according to the idea of the present application, there may be variations in the specific embodiments and the application scope, and in summary, the content of the present specification should not be construed as a limitation to the present application.
Claims (10)
1. The bi-component cleansing liquid is characterized by comprising a component A and a component B, wherein the component A comprises the following components in parts by weight: 30-85 parts of water, 1-10 parts of mineral oil, 10-40 parts of surfactant, 0.02-0.8 part of tremella polysaccharide, 0.5-5 parts of emulsifier, 1-30 parts of humectant and 0.01-0.5 part of preservative;
the component B comprises the following components in parts by weight: 8-75 parts of mineral oil, 0.01-0.6 part of amur corktree bark extract, 0.01-0.6 part of lavender flower extract, 0.01-0.6 part of gardenia fruit extract and 0.01-0.5 part of preservative;
the mass ratio of the component A to the component B is 20.
2. The two-component cleansing liquid according to claim 1, wherein the component a comprises the following raw materials in parts by weight: 30-55 parts of water, 2-4 parts of mineral oil, 10-20 parts of surfactant, 0.02-0.06 part of tremella polysaccharide, 0.5-3 parts of emulsifier, 1-20 parts of humectant and 0.01-0.05 part of preservative;
the component B comprises the following raw materials in parts by weight: 16-52 parts of mineral oil, 0.01-0.1 part of amur corktree bark extract, 0.01-0.1 part of lavender flower extract, 0.01-0.1 part of gardenia fruit extract and 0.01-0.05 part of preservative;
the mass ratio of the component A to the component B is 20-20.
3. The two-component cleansing liquid according to claim 1, wherein said a-component further comprises, by weight, 0.1 to 0.5 parts of a foaming agent, 0.01 to 0.1 parts of a chelating agent, 0.01 to 0.05 parts of a PH adjuster, or 0.01 to 0.1 parts of a thickener;
the component B also comprises 0.5 to 1.1 parts of conditioner, 0.01 to 0.08 part of chelating agent or 0.001 to 0.03 part of pigment in parts by weight.
4. The dual component cleansing cleanser of claim 3, wherein the foaming agent comprises sodium cocoyl malate; the chelating agent comprises at least one of disodium EDTA and tetrasodium glutamate diacetate; the pH regulator comprises citric acid and the thickener comprises sodium chloride.
5. The two-component cleansing liquid according to claim 3, wherein said conditioning agent comprises at least one of panthenol, squalane, camellia seed oil, and glycerol tri (ethyl hexanoate).
6. The two-component cleansing liquid according to claim 1 wherein said surfactant comprises at least one of sodium laureth sulfate, sodium cocamidopropionate, or lauramidopropyl betaine.
7. The two-component cleansing liquid according to claim 1, wherein said emulsifier comprises at least two of polyglyceryl-10 myristate, sorbitan stearate, polysorbate-60.
8. The two-component cleansing liquid according to claim 1 wherein said moisturizing agent comprises: at least one of butylene glycol, ethylene glycol, methyl propylene glycol or ethyl hexyl glycerol; the preservative comprises: at least one of glyceryl caprylate, caprylyl hydroximic acid, phenoxyethanol, p-hydroxyacetophenone and sodium benzoate.
9. The preparation method of the bi-component cleansing facial cleanser is characterized by comprising the following steps:
sequentially adding the raw materials in the component A in parts by weight into a clean batching pot, starting stirring at the rotating speed of 30-50 revolutions per minute, stirring and heating to 65 ℃, cooling to room temperature, testing, discharging and filling;
and (3) sequentially adding the raw materials in the component B in parts by weight into a clean batching pot at room temperature, starting homogenization at the speed of 1000-1500 rpm for 1-2 minutes until the materials are uniformly mixed, testing, discharging and filling.
10. A using method of a two-component makeup removing cleansing liquid is characterized in that a component A and a component B are mixed according to a ratio of 20 to 3 to 9 and are used after being shaken up.
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US20050075265A1 (en) * | 2003-09-12 | 2005-04-07 | L'oreal | Two-phase compositions and uses thereof |
CN110420152A (en) * | 2019-08-20 | 2019-11-08 | 中山中研化妆品有限公司 | A kind of salubrious mild double-deck make up remover and preparation method thereof |
CN112675048A (en) * | 2020-12-31 | 2021-04-20 | 彭氏(惠州)实业发展有限公司 | Double-layer makeup removing mousse and preparation method thereof |
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US20050075265A1 (en) * | 2003-09-12 | 2005-04-07 | L'oreal | Two-phase compositions and uses thereof |
CN110420152A (en) * | 2019-08-20 | 2019-11-08 | 中山中研化妆品有限公司 | A kind of salubrious mild double-deck make up remover and preparation method thereof |
CN112675048A (en) * | 2020-12-31 | 2021-04-20 | 彭氏(惠州)实业发展有限公司 | Double-layer makeup removing mousse and preparation method thereof |
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