JPH09131393A - Deodorant, deodorizing composition, and deodorizing cosmetic - Google Patents
Deodorant, deodorizing composition, and deodorizing cosmeticInfo
- Publication number
- JPH09131393A JPH09131393A JP7317239A JP31723995A JPH09131393A JP H09131393 A JPH09131393 A JP H09131393A JP 7317239 A JP7317239 A JP 7317239A JP 31723995 A JP31723995 A JP 31723995A JP H09131393 A JPH09131393 A JP H09131393A
- Authority
- JP
- Japan
- Prior art keywords
- extract
- deodorant
- aqueous solution
- composition
- plant
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
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- 108090000623 proteins and genes Proteins 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 230000002797 proteolythic effect Effects 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 230000001953 sensory effect Effects 0.000 description 1
- 229920002545 silicone oil Polymers 0.000 description 1
- 229920002050 silicone resin Polymers 0.000 description 1
- 229910000030 sodium bicarbonate Inorganic materials 0.000 description 1
- 235000017557 sodium bicarbonate Nutrition 0.000 description 1
- 229910000029 sodium carbonate Inorganic materials 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 230000003381 solubilizing effect Effects 0.000 description 1
- 238000001179 sorption measurement Methods 0.000 description 1
- 229940001941 soy protein Drugs 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 230000003068 static effect Effects 0.000 description 1
- 229960004274 stearic acid Drugs 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000004094 surface-active agent Substances 0.000 description 1
- 235000007586 terpenes Nutrition 0.000 description 1
- 239000002562 thickening agent Substances 0.000 description 1
- 238000012546 transfer Methods 0.000 description 1
- 229940099259 vaseline Drugs 0.000 description 1
- 239000013585 weight reducing agent Substances 0.000 description 1
- 229940119569 wormwood extract Drugs 0.000 description 1
Landscapes
- Cosmetics (AREA)
- Disinfection, Sterilisation Or Deodorisation Of Air (AREA)
Abstract
Description
【0001】[0001]
【発明の属する技術分野】本発明は消臭剤、消臭組成物
および消臭化粧料に関し、特にタバコ臭等の不快な臭い
に対して良好な消臭効果を有する消臭剤、消臭組成物及
び消臭化粧料に関する。TECHNICAL FIELD The present invention relates to a deodorant, a deodorant composition and a deodorant cosmetic, and in particular, a deodorant and a deodorant composition having a good deodorant effect against unpleasant odors such as tobacco odor. Items and deodorant cosmetics.
【0002】[0002]
【従来の技術】タバコ等の不快な臭いは、髪の毛や衣服
等に付着しやすく、また一度付着するとその臭いが持続
するので多くの人に不快感を与えている。特に最近、若
い女性は清潔指向を反映して、髪にタバコ等の不快な臭
いがつくのを極端に嫌うようになっている。2. Description of the Related Art The unpleasant odor of cigarettes or the like easily attaches to hair, clothes, etc., and once attached, the odor persists, causing many people to feel unpleasant. Particularly recently, young women have become extremely reluctant to have an unpleasant odor such as cigarettes in their hair, reflecting their cleanliness.
【0003】従来、タバコ臭等の消臭方法としては、香
料成分を利用して臭いをマスキングする方法、植物抽出
液を利用して消臭する方法、種々の化学反応を利用して
消臭する方法、物質の吸着、包接作用を利用して消臭す
る方法等が知られている。中でも、化粧料の分野におい
ては、香料成分を利用して臭いをマスキングする方法及
び植物抽出液を利用して消臭する方法が汎用されてい
る。しかしながら、香料成分を利用して臭いをマスキン
グする方法では、各消費者に香りの好みがあり、すべて
の消費者に受け入れられない等の問題がある。Conventionally, as a method of deodorizing tobacco odor, a method of masking the odor using a fragrance component, a method of deodorizing using a plant extract, and a method of deodorizing various chemical reactions are used. A method, a method of deodorizing by utilizing a substance adsorption, an inclusion action, and the like are known. Among them, in the field of cosmetics, a method of masking odor by using a fragrance component and a method of deodorizing by using a plant extract are widely used. However, the method of masking the odor by using the fragrance component has a problem that each consumer has a scent preference and cannot be accepted by all consumers.
【0004】[0004]
【発明の解決しようとする課題】一方で、植物抽出液を
利用して消臭する方法は、さまざまな種類の植物抽出液
でその効果があるとうたわれ、例えば、特開昭64−6
8264号公報、特開昭64−68265号公報、特開
平1−242066号公報、特開平3−294215号
公報、特開平5−255059号公報、特開平5−27
9690号公報、特開平6−219928号公報などが
報告されている。On the other hand, the method of deodorizing using a plant extract is said to be effective for various kinds of plant extracts, and is disclosed in, for example, JP-A-64-6.
No. 8264, No. 64-68265, No. 1-242066, No. 3-294215, No. 5-255059, No. 5-27.
Japanese Patent No. 9690, Japanese Unexamined Patent Publication No. 6-219928 and the like have been reported.
【0005】しかし、消臭組成物にこれらを利用する場
合、前記各文献において報告されるごとく、各植物抽出
物を単独で用いたのではその消臭効果は不十分であっ
た。本発明は前記従来技術の課題に鑑みなされたもので
あり、その目的は、さらに消臭効果の改善された消臭
剤、消臭組成物及び消臭化粧料を提供することをにあ
る。However, when these are used in the deodorant composition, as reported in the above-mentioned documents, the deodorant effect is insufficient when each plant extract is used alone. The present invention has been made in view of the above problems of the prior art, and an object thereof is to provide a deodorant, a deodorant composition, and a deodorant cosmetic having an improved deodorant effect.
【0006】[0006]
【課題を解決するための手段】前記従来技術の課題に鑑
み本発明者らが鋭意研究を重ねた結果、ニンジン、アロ
エ、ヨモギ、チャ、ビワ、シソ、ゲンノショウコの7種
の植物群より選択される2種以上の植物抽出液を含む消
臭剤が優れた不快臭、特にタバコ臭の消臭効果を有する
ことを見出し、本発明の完成に至った。As a result of intensive studies conducted by the present inventors in view of the above-mentioned problems of the prior art, they were selected from seven plant groups of carrot, aloe, mugwort, tea, loquat, perilla, and ginger ginger. It was found that a deodorant containing two or more kinds of plant extracts having the above-mentioned effect has an excellent deodorizing effect on unpleasant odors, particularly tobacco odor, and has completed the present invention.
【0007】すなわち、本発明の消臭剤は、ニンジン、
アロエ、ヨモギ、チャ、ビワ、シソ、ゲンノショウコの
7種の植物群より選ばれる2種以上の植物抽出液を含む
ことを特徴とする。なお、本発明の消臭組成物において
は、本発明の消臭剤を含むことが好ましく、特に植物抽
出液の総配合量が、組成物全量中の0.0001〜10
重量%であることが好ましい。That is, the deodorant of the present invention is carrot,
It is characterized in that it contains two or more kinds of plant extract liquids selected from seven kinds of plant groups of aloe, mugwort, tea, loquat, perilla, and ginkgo biloba. In the deodorant composition of the present invention, it is preferable to include the deodorant of the present invention, and particularly, the total amount of the plant extract solution is 0.0001 to 10 in the total amount of the composition.
% By weight.
【0008】また、本発明の消臭組成物は、特にタバコ
臭の消臭効果を有するものであることを特徴とする。ま
た、本発明の消臭化粧料は、本発明の消臭組成物を含む
ことを特徴とする。なお、本発明の消臭化粧料は、毛髪
用として用いることが好ましい。また、本発明の消臭化
粧料は、皮膚用として用いることが好ましい。また、本
発明の消臭化粧料は、メーキャップ用として用いること
が好ましい。また、本発明の消臭組成物は、室内用とし
て用いることが好ましい。Further, the deodorant composition of the present invention is characterized by having a deodorizing effect on tobacco odor. The deodorant cosmetic composition of the present invention is characterized by containing the deodorant composition of the present invention. The deodorant cosmetic composition of the present invention is preferably used for hair. The deodorant cosmetic composition of the present invention is preferably used for skin. The deodorant cosmetic composition of the present invention is preferably used for makeup. Further, the deodorant composition of the present invention is preferably used for indoor use.
【0009】[0009]
【発明の実施の形態】以下、本発明の実施形態に基づ
き、本発明をさらに詳細に説明する。本発明は、ニンジ
ン、アロエ、ヨモギ、チャ、ビワ、シソ、ゲンノショウ
コの7種の植物群より選ばれる2種以上の植物抽出液を
含むことを特徴とする。本発明において、上記7種の植
物抽出液を含む場合に、各抽出液の配合量比は、2種の
抽出液の比が、例えば、以下の数値となるように調整す
ることが好ましい。BEST MODE FOR CARRYING OUT THE INVENTION The present invention will now be described in more detail based on the embodiments of the present invention. The present invention is characterized by containing two or more kinds of plant extract liquids selected from seven kinds of plant groups of carrot, aloe, mugwort, tea, loquat, perilla and ginger ginger. In the present invention, when the above 7 kinds of plant extracts are contained, the blending ratio of each extract is preferably adjusted so that the ratio of the 2 kinds of extract is, for example, the following numerical value.
【0010】ニンジン:アロエ=1:1〜1:5 ニンジン:ヨモギ=1:1〜1:5 ニンジン:チャ=1:1〜1:7 ニンジン:ビワ=1:1〜1:5 ニンジン:シソ=5:2〜1:1 ニンジン:ゲンノショウコ=1:1〜1:5 アロエ:ヨモギ=2:1〜1:2 アロエ:チャ=1:1〜1:5 アロエ:ビワ=2:1〜1:2 アロエ:シソ=5:2〜1:1 アロエ:ゲンノショウコ=2:1〜1:2 ヨモギ:チャ=1:1〜1:5 ヨモギ:ビワ=2:1〜1:2 ヨモギ:シソ=5:2〜1:1 ヨモギ:ゲンノショウコ=2:1〜1:2 チャ:ビワ=5:1〜1:1 チャ:シソ=7:1〜1:1 チャ:ゲンノショウコ=2:1〜1:2 ビワ:シソ=5:2〜1:1 ビワ:ゲンノショウコ=2:1〜1:2 シソ:ゲンノショウコ=5:2〜1:1Carrot: Aloe = 1: 1 to 1: 5 Carrot: Mugwort = 1: 1 to 1: 5 Carrot: Cha = 1: 1 to 1: 7 Carrot: Loquat = 1: 1 to 1: 5 Carrot: Perilla = 5: 2 to 1: 1 Carrot: Genshokuko = 1: 1 to 1: 5 Aloe: Mugwort = 2: 1 to 1: 2 Aloe: Cha = 1: 1 to 1: 5 Aloe: Loquat = 2: 1 to 1 : 2 Aloe: Perilla = 5: 2 to 1: 1 Aloe: Genshosho = 2: 1 to 1: 2 Wormwood: Cha = 1: 1 to 1: 5 Wormwood: Loquat = 2: 1 to 1: 2 Wormwood: Perilla = 5: 2 to 1: 1 Mugwort: Genosho = 2: 1 to 1: 2 Cha: Loquat = 5: 1 to 1: 1 Cha: Perilla = 7: 1 to 1: 1 Cha: Genosho = 2: 1 to 1: 2 Loquat: Perilla = 5: 2-1: 1 Loquat: Genso-shoko = 2: 1 to 1: 2 Perilla: Geno-shoko = : 2 to 1: 1
【0011】また、本発明の消臭化粧料に3種以上の抽
出液を組み合わせて用いる場合には、これらの配合量比
を組み合わせて例えば、ニンジンとアロエとビワを組み
合わせる場合には、ニンジン:アロエ、ニンジン:ビワ
及びアロエ:ビワが上記各数値を満たすように調整する
ことが好ましい。本発明に用いられる植物抽出液は、そ
の抽出溶媒として水、無機酸水溶液、無機アルカリ水溶
液、有機溶媒の一種又は二種以上の混合溶媒を用いて抽
出する。When the deodorant cosmetic composition of the present invention is used in combination with three or more kinds of extract liquids, for example, when carrot, aloe and loquat are combined by combining the blending ratios thereof, carrot: It is preferable to adjust aloe, carrot: loquat, and aloe: loquat so as to satisfy the above numerical values. The plant extract used in the present invention is extracted using water, an inorganic acid aqueous solution, an inorganic alkaline aqueous solution, or a mixed solvent of two or more kinds of organic solvents as the extraction solvent.
【0012】無機酸水溶液は、例えば、塩酸水溶液、硫
酸水溶液、硝酸水溶液、酢酸水溶液、クエン酸水溶液等
が挙げられ、好ましいpHは2〜6である。無機アルカ
リ水溶液は、例えば重炭酸ナトリウム水溶液、炭酸ナト
リウム水溶液、水酸化ナトリウム水溶液、クエン酸ナト
リウム水溶液、炭酸カリウム水溶液、炭酸水素カリウム
水溶液、水酸化カリウム水溶液クエン酸カリウム水溶液
等が挙げられ、好ましいpHは、8〜12である。また
上記無機酸水溶液と上記無機アルカリ水溶液の混合緩衝
液での抽出も行うことができる。Examples of the inorganic acid aqueous solution include hydrochloric acid aqueous solution, sulfuric acid aqueous solution, nitric acid aqueous solution, acetic acid aqueous solution, citric acid aqueous solution, and the like, and the preferable pH is 2-6. Examples of the inorganic alkaline aqueous solution include sodium bicarbonate aqueous solution, sodium carbonate aqueous solution, sodium hydroxide aqueous solution, sodium citrate aqueous solution, potassium carbonate aqueous solution, potassium hydrogen carbonate aqueous solution, potassium hydroxide aqueous solution and potassium citrate aqueous solution. , 8-12. Further, extraction with a mixed buffer solution of the above inorganic acid aqueous solution and the above inorganic alkaline aqueous solution can also be performed.
【0013】有機溶媒としては、種々の溶媒、エーテ
ル、ケトン、アルコール等が挙げられ、特に、炭素数が
1〜3の低級アルコール、グリセリン、プロピレングリ
コール、1,3−ブチレングリコール、ポリエチレング
リコール、及びそれらの水溶液を用いることが好適であ
る。本発明に用いられる植物抽出液は、各植物の葉、地
下根、地上根等から上記抽出溶媒を用いて、例えば以下
の方法で抽出することが可能である。Examples of the organic solvent include various solvents, ethers, ketones, alcohols, etc., and particularly, lower alcohols having 1 to 3 carbon atoms, glycerin, propylene glycol, 1,3-butylene glycol, polyethylene glycol, and It is preferable to use those aqueous solutions. The plant extract used in the present invention can be extracted from the leaves, subterranean roots, aboveground roots, etc. of each plant using the above-mentioned extraction solvent, for example, by the following method.
【0014】すなわち、植物の葉、地下根、地上根等を
細切りにし、粉砕器で粉砕し、これにエタノールを加
え、一昼夜撹拌抽出したのち濾過する。残渣にさらにエ
タノールを加え同様に抽出を行い全抽出液をあわせて減
圧濃縮を行い、抽出液のエタノール含量を日局精製水及
び日局エタノールを加えて適当に調整する。さらに、数
日若しくは数十日間冷暗所に放置して熟成させ、この工
程で生ずるオリや沈殿を濾過して除去して植物抽出液を
得ることが可能である。That is, plant leaves, subterranean roots, above-ground roots, etc. are cut into small pieces, ground with a grinder, ethanol is added thereto, and the mixture is stirred and extracted for 24 hours, and then filtered. Ethanol is added to the residue and extraction is performed in the same manner. All the extracts are combined and concentrated under reduced pressure, and the ethanol content of the extracts is adjusted appropriately by adding purified water of JP and ethanol of JP. Further, it is possible to leave it in a cool dark place for several days or several tens of days for aging, and to remove the sediment or precipitate generated in this step by filtration to obtain a plant extract.
【0015】本発明においては上記植物抽出液の消臭組
成物への配合量は任意であるが、抽出液の総配合量が組
成物全体の0.0001〜10重量%、特に0.001
〜5重量%であることが好適である。配合量が、0.0
001%未満であると、十分な消臭効果を示すことがで
きず、一方、10重量%以上配合すると植物抽出液の臭
いが顕在化してしまい好ましくなく、特に好ましくは5
重量%までである。In the present invention, the amount of the above plant extract added to the deodorant composition is arbitrary, but the total amount of the extract added is 0.0001 to 10% by weight, particularly 0.001% of the total composition.
It is preferably ˜5% by weight. The amount is 0.0
If it is less than 001%, a sufficient deodorizing effect cannot be exhibited, while if it is blended in an amount of 10% by weight or more, the odor of the plant extract becomes apparent, which is not preferable, and particularly preferably 5
% By weight.
【0016】本発明の消臭化粧料及び消臭剤には、前記
必須成分の他、必要に応じ一般に化粧料及び消臭剤に配
合される他の成分を配合することができる。それらの成
分としては、流動パラフィン、スクワラン、ラノリン誘
導体、高級アルコール、各種エステル油、シリコーン
油、ポリアルキレングリコールポリエーテル及びその他
カルボン酸、オリゴエステル化合物、テルペン系炭化水
素油等の油分、界面活性剤、紫外線吸収剤、紫外線錯乱
剤、アクリル系樹脂、シリコーン樹脂、ポリビニルピロ
リドン等の樹脂類、大豆タンパク、ゼラチン、コラーゲ
ン、絹フィブロイン、エラスチン等のタンパク又はタン
パク分解物、エチルパラベン、ブチルパラベン等の防腐
剤、ビオチン、パントテン酸誘導対等の賦活剤、エタノ
ール、イソプロパノール、テトラクロジフルオロエタン
トルエン等の希釈剤、カルボキシビニルポリマー等の増
粘剤、キレート剤、酸化防止剤、保湿剤、薬剤、香料、
色剤、顔料等が挙げられる。In addition to the above-mentioned essential components, the deodorant cosmetic composition and deodorant composition of the present invention may contain, if necessary, other components generally contained in cosmetic compositions and deodorant compositions. Examples of such components include liquid paraffin, squalane, lanolin derivatives, higher alcohols, various ester oils, silicone oils, polyalkylene glycol polyethers and other carboxylic acids, oligoester compounds, oil components such as terpene hydrocarbon oils, and surfactants. , UV absorbers, UV confusion agents, acrylic resins, silicone resins, polyvinylpyrrolidone and other resins, soy protein, gelatin, collagen, silk fibroin, elastin and other proteins or proteolytic products, ethylparaben, butylparaben and other preservatives Agents, biotin, activators such as pantothenic acid-derived pairs, ethanol, isopropanol, diluents such as tetraclodifluoroethanetoluene, thickeners such as carboxyvinyl polymers, chelating agents, antioxidants, humectants, drugs, fragrances,
Colorants, pigments, etc. may be mentioned.
【0017】また、本発明の消臭化粧料及び消臭剤の剤
形は任意であり、可溶化系、乳化系、粉末分散系、油−
水の2相系、油−水−粉末の3相系等、いずれの系でも
用いることが可能であり、各種添加剤を加えて化粧水、
乳液、クリーム、リキッドファンデーション、ヘアリキ
ッド、ヘアスプレー、ヘアムース、ヘアジェル、ヘアシ
ャンプー、ヘアリンス、ヘアトリートメント、ヘアクリ
ーム、ヘアミスト(ノンガスタイプ)、ルームコロン等
とすることができる。The dosage form of the deodorant cosmetic composition and deodorant of the present invention is arbitrary, including a solubilizing system, an emulsifying system, a powder dispersion system and an oil
It is possible to use any system such as a two-phase system of water and a three-phase system of oil-water-powder. To the skin lotion by adding various additives,
It can be emulsion, cream, liquid foundation, hair liquid, hair spray, hair mousse, hair gel, hair shampoo, hair rinse, hair treatment, hair cream, hair mist (non-gas type), room colon, and the like.
【0018】[0018]
【実施例】以下、植物抽出についての実施例を挙げて説
明する。なお、本発明に用いられる植物抽出液の抽出方
法がこれにより限定されるものではない。[Examples] Examples of plant extraction will be described below. The method for extracting the plant extract used in the present invention is not limited to this.
【0019】植物抽出実施例1 ニンジン オタネニンジン Panax ginseng C.A Meyer (Panax schi
nseng Nees)(Araliaceae) の5〜6年根25kgを細
切りし、粉砕器で細砕し、これに50v/v%エタノー
ル100lを加え、一昼夜撹拌抽出したのち濾過する。
残渣は50v/v%エタノール75lを加え同様に抽出
を行い、全抽出液をあわせ、約50℃にて減圧濃縮を行
い、抽出液のエタノール含量が10v/v%になるよう
に日局精製水及び日局エタノールを加えて調整する。さ
らに、7〜10日間冷所に放置して熟成させ、この工程
で生ずるオリや沈殿を濾過して除去すると同時に10v
/v%エタノールを追加して製品100lを得る。 Plant Extraction Example 1 Carrot Panax ginseng CA Meyer (Panax schi
25 kg of 5- to 6-year-old roots of nseng Nees) (Araliaceae) are shredded, shredded with a grinder, and 100 l of 50 v / v% ethanol is added thereto, and the mixture is extracted with stirring for 24 hours and then filtered.
The residue was extracted in the same manner by adding 75 l of 50 v / v% ethanol, and all the extracts were combined and concentrated under reduced pressure at about 50 ° C. to make the ethanol content of the extracts 10 v / v%. And adjust by adding JP ethanol. Furthermore, it is left to stand in a cool place for 7 to 10 days for aging, and the sediment or precipitate generated in this step is removed by filtration and at the same time 10v.
/ V% ethanol is added to obtain 100 l of product.
【0020】植物抽出実施例2 アロエ 採取したアロエ:Aloe ferox Miller 又はこれとAloe a
fricana Millern 又はAloe spicata Bakerとの雑種(li
liaceae)の新鮮葉176〜180kgを約5cmの長
さに切り、これを圧搾し、全液汁約90〜100lを集
め布こしする。この液を水浴上撹拌しながら濃縮し、反
流動体となし、これを蒸発用バットに移し120〜13
0℃にて約15時間加熱し、暗褐色の固形物とする。 Plant Extraction Example 2 Aloe Aloe collected: Aloe ferox Miller or this and Aloe a
hybrid with fricana Millern or Aloe spicata Baker (li
liaceae) fresh leaves 176 to 180 kg are cut into a length of about 5 cm, and this is squeezed, and about 90 to 100 l of the whole sap is collected and rubbed. This liquid was concentrated on a water bath while stirring to form an anti-fluid, which was transferred to an evaporation vat 120 to 13
Heat at 0 ° C. for about 15 hours to give a dark brown solid.
【0021】これを粉砕した後、粉砕器にかけ約1kg
の粉末を得る。この粉末に日局精製水10lを加えよく
撹拌しながら7〜10℃にて72時間抽出する。これを
吸引濾過した後、冷暗所にて10日間放置する。不純物
を濾過して除き、得られた濾液に日局無水エタノールを
加えて30v/v%エタノール溶液となし、よく撹拌し
た後、再び冷暗所に7日間放置して濾過し、製品15l
を得る。After crushing this, it is put into a crusher and about 1 kg.
To obtain a powder of. To this powder, 10 l of purified water of Japanese Pharmacopoeia is added, and the mixture is extracted at 7 to 10 ° C for 72 hours while stirring well. This is suction filtered and then left standing in a cool dark place for 10 days. Impurities were removed by filtration, and the filtrate obtained was mixed with Japanese Pharmacopoeia absolute ethanol to form a 30 v / v% ethanol solution. After stirring well, the mixture was left standing in a cool dark place for 7 days and filtered.
Get.
【0022】植物抽出実施例3 ヨモギ ガイヨウ(艾葉):ヨモギ Artemisia princeps Pampan
iniのは又はモウコヨモギ Amongolia Fischerの葉:1
0kgを細切りにし、これに30v/v%エタノール5
0lを加え、20から25℃にて約2週間浸漬したのち
濾過する。残渣は30v/v%エタノール30lで同様
に抽出し、抽出液を減圧濃縮し、軟エキスを得る。さら
に得られた抽出液に、この軟エキスを加えて溶かしたの
ち、常温にて約10日間静置する。これを濾過し、冷暗
所にて10日間静置し、必要ならば濾過紙、最後に30
v/v%エタノールを追加して製品50lを得る。[0022] The plant extracts Example 3 mugwort Overview (AiYo): mugwort Artemisia princeps Pampan
leaves of ini or mugwort Amongolia Fischer: 1
0 kg is chopped into 30 v / v% ethanol 5
0 l is added and the mixture is immersed at 20 to 25 ° C. for about 2 weeks and then filtered. The residue is similarly extracted with 30 l of 30 v / v% ethanol, and the extract is concentrated under reduced pressure to obtain a soft extract. Further, this soft extract is added to the obtained extract to dissolve it, and the mixture is allowed to stand at room temperature for about 10 days. This is filtered and allowed to stand in a cool dark place for 10 days, if necessary filter paper, and finally 30
Add 50% v / v% ethanol to give 50 l of product.
【0023】植物抽出実施例4 チャ チャ:Thea sinensis L. の新鮮葉(Theaceac):を乾
燥し、天日乾燥にて5〜10分ごとに茶葉を集め、軽く
反転し、約30〜60分間で重量20%まで乾燥させ
る。さらに室内に移し、茶葉の撹拌を静置作業と交互に
数時間繰り返す。重量の減少を約30%まで進め、茶葉
のまわりが紅褐色に代わり、芳香を発するようになった
ら、200〜230℃の釜に入れて茶葉を炒り、乾燥す
る。この乾燥葉10kgに30v/v%エタノール55
lを加え、20〜25℃にて2時間浸漬したのち濾過す
る。残渣は、30v/v%エタノール30lで同様に抽
出を行い、抽出液を減圧濃縮し軟エキスを得る。先に得
られた抽出液に、この軟エキスを加えて溶かしたのち、
常温にて10日間静置する。これを濾過し、冷暗所にて
10日間静置し、必要ならば濾過し、最後に30v/v
%エタノールを追加して製品50lを得る。The plant extracts in Example 4 Cha Cha: Thea fresh leaves sinensis L. (Theaceac): dried, tea leaves collected in solar drying every 5-10 minutes, gently inverting, about 30 to 60 minutes To 20% weight. Furthermore, it is moved to the room and the stirring of tea leaves is repeated for several hours alternately with the static work. When the weight reduction is promoted to about 30% and the tea leaves are replaced by reddish brown and emit an aroma, the tea leaves are put in a pot at 200 to 230 ° C., and the tea leaves are roasted and dried. 30 kg of 30% v / v% ethanol to 10 kg of this dried leaf
1 is added, the mixture is immersed at 20 to 25 ° C. for 2 hours, and then filtered. The residue is similarly extracted with 30 l of 30 v / v% ethanol, and the extract is concentrated under reduced pressure to obtain a soft extract. After adding and dissolving this soft extract to the extract obtained earlier,
Let stand for 10 days at room temperature. This is filtered, left in a cool dark place for 10 days, filtered if necessary, and finally 30 v / v
% Ethanol is added to obtain 50 l of product.
【0024】植物抽出実施例5 ビワ 局外生規ビワヨウ(枇杷葉):ビワ Eriobotrya japoni
ca Lindlの葉:10kgを細切りにし、これに30v/
v%エタノール55lを加え、20〜25℃にて2時間
浸漬したのち、濾過する。残渣は、30v/v%エタノ
ール30lで同様に抽出を行い、抽出液を減圧濃縮し軟
エキスを得る。先に得られた抽出液に、この軟エキスを
加えて溶かしたのち、常温にて10日間静置する。これ
を濾過し、冷暗所にて10日間静置し、必要ならば濾過
紙、最後に30v/v%エタノールを追加して製品50
lを得る。 Plant Extraction Example 5 Loquat Officinalis Loquat Loquat (Silver Leaf): Loquat Eriobotrya japoni
ca Lindl leaves: cut 10kg into 30v /
55% of v% ethanol is added and the mixture is immersed at 20 to 25 ° C. for 2 hours and then filtered. The residue is similarly extracted with 30 l of 30 v / v% ethanol, and the extract is concentrated under reduced pressure to obtain a soft extract. The soft extract is added to the previously obtained extract to dissolve it, and the mixture is allowed to stand at room temperature for 10 days. This is filtered, left standing in a cool and dark place for 10 days, and if necessary, a filter paper is added, and finally 30 v / v% ethanol is added to the product 50.
get l.
【0025】植物抽出実施例6 シソ シソPerilla frutescens Britton var. acuta Kudoまた
はその他近縁植物(Labiatae)の葉及び枝先:10kg
を細かく砕き、これに30v/v%エタノール50lを
加え、緩やかに加温したのち濾過する。残渣はさらに3
0v/v%エタノール50lずつで2回同様に抽出を行
い、全抽出液を併せて50℃で減圧濃縮を行い、濃縮液
約20lを得る。この液に粧原基精製水及び粧原基無水
エタノールを加えアルコール濃度を30v/v%とし、
全量約45lとする。冷所に7〜10日間放置して熟成
させ、この工程で生ずるオリや沈殿を濾過して除去する
と同時に30v/v%エタノールを追加して製品50l
を得る。. [0025] plant extracts EXAMPLE 6 Perilla Perilla Perilla frutescens Britton var acuta Kudo or leaves and Edasaki other closely related plants (Labiatae): 10 kg
Is crushed finely, 50 l of 30 v / v% ethanol is added thereto, and the mixture is gently heated and then filtered. 3 more residues
The same extraction is performed twice with 50 l of 0 v / v% ethanol, and all the extracts are combined and concentrated under reduced pressure at 50 ° C. to obtain about 20 l of concentrated solution. To this liquid, purified water of cosmetic original material and anhydrous ethanol of cosmetic original material are added to make the alcohol concentration 30 v / v%,
The total volume is about 45 liters. Let stand for 7-10 days in a cool place for aging, and remove the sediment or precipitate generated in this step by filtration, and at the same time add 30 v / v% ethanol to give 50 l of product.
Get.
【0026】植物抽出実施例7 ゲンノショウコ ゲンノショウコ:ゲンノショウコ Geranium thunbergii
Siebold et Zuccarini(Geraniaceae)の地上部:10k
gを細切りにし、これに90v/v%エタノール150
lを加え、緩やかに加熱抽出したのち濾過する。残渣に
90v/v%エタノール150lを加え同様に処理して
得られた濾液を先の濾液と合わせ、50℃で減圧濃縮を
行い、濃縮液10lを得る。この液に適量の粧原基精製
水及び粧原基無水エタノールを加え、エタノール濃度を
50v/v%及び全量約50lに調整する。これを7〜
10日間冷所に放置して熟成させ、この工程で生ずるオ
リや沈殿を濾過して除去すると同時に50v/v%エタ
ノールを追加して製品50lを得る。 Plant Extraction Example 7 Gingernium thunbergii Geranium thunbergii
Above-ground part of Siebold et Zuccarini (Geraniaceae): 10k
g, cut into pieces, and add 90 v / v% ethanol 150 to it.
1 is added, the mixture is gently heated and extracted, and then filtered. The filtrate obtained by adding 150 v of 90 v / v% ethanol to the residue and treating it in the same manner is combined with the above-mentioned filtrate and concentrated under reduced pressure at 50 ° C. to obtain a concentrated liquid of 10 l. To this solution, appropriate amounts of purified water for cosmetic base and anhydrous ethanol for cosmetic base are added to adjust the ethanol concentration to 50 v / v% and the total amount of about 50 l. This is 7 ~
The product is left to stand in a cold place for 10 days for aging, and the sediment or precipitate generated in this step is removed by filtration, and 50 v / v% ethanol is added at the same time to obtain 50 l of a product.
【0027】次に上述の植物抽出液を用いた本発明の実
施例を示す。なお、本発明はこれによって限定されるも
のではない。なお、配合量はとくに示さない限り重量%
である。Next, examples of the present invention using the above-mentioned plant extract will be shown. The present invention is not limited by this. Unless otherwise specified, the blending amount is% by weight.
It is.
【0028】表1及び表2に示す処方によりヘアミスト
(ノンガスタイプ)を調整した。表中各植物抽出物は上
記各植物抽出の実施例で抽出したものである。得られた
ヘアミストのタバコ臭消臭効果を下記の方法にて評価し
た。結果は併せて表1及び表2に記載する。Hair mists (non-gas type) were prepared according to the formulations shown in Tables 1 and 2. Each plant extract in the table is extracted in the above-mentioned examples of plant extraction. The tobacco odor eliminating effect of the obtained hair mist was evaluated by the following method. The results are also shown in Table 1 and Table 2.
【0029】[評価方法] 1.毛束1gにヘアミスト約0.3gを塗布し、ブラッ
シングしてよくのばした。 2.室温にて1時間乾燥させた。 3.毛束を200ml三角フラスコに移し、さらにタバ
コの煙(フィルター側からシリンジで吸引収集)を5ml
注入して15分間放置した。 4.毛束をシャーレに移し、その臭いを専門パネル5名
により官能評価した。評価は5段階で行った。対象とし
て、上記操作でサンプル未塗布のものを1、タバコの煙
を注入しないものを5と評価した。なお、各表に示した
評価は各パネルの評価の平均値である。また、表中のヘ
アミストは以下の方法製造した。[Evaluation Method] 1. About 0.3 g of hair mist was applied to 1 g of a hair bundle, and brushed and spread well. 2. It was dried at room temperature for 1 hour. 3. Transfer the tufts to a 200 ml Erlenmeyer flask and 5 ml of tobacco smoke (suction collected from the filter side with a syringe).
It was injected and left for 15 minutes. 4. The hair bundle was transferred to a petri dish, and the odor was sensory evaluated by 5 expert panels. The evaluation was performed in five stages. In the above operation, the sample not coated was evaluated as 1 and the sample not injected with cigarette smoke was evaluated as 5. The evaluation shown in each table is an average value of the evaluation of each panel. The hair mist in the table was manufactured by the following method.
【0030】[製法]プロピレングリコール、ポリオキ
シエチレン(9)ラウリルエーテル、ジメチルポリシロ
キサン(8cs)を混合溶解し、ホモミキサーで均一に
乳化する。イオン交換水にエタノール、先の乳化パーツ
及び各抽出液を撹拌混合溶解して得た。[Production Method] Propylene glycol, polyoxyethylene (9) lauryl ether and dimethylpolysiloxane (8 cs) are mixed and dissolved, and the mixture is uniformly emulsified with a homomixer. Ethanol, the above emulsified part, and each extract were stirred and mixed and dissolved in ion-exchanged water.
【0031】[0031]
【表1】 ──────────────────────────────────── 実 施 例 1 2 3 4 5 6 7 8 9 ────────────────────────────────────フ゜ロヒ゜レンク゛リコール 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0ホ゜リオキシエチレン (9) ラウリルエーテル 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5シ゛メチル ホ゜リシロキサン (8cs) 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5ニンシ゛ン 抽出液 - 0.7 - - 0.7 - - 0.467 0.2アロエ 抽出液 - 0.7 - - - 0.467 - - 0.2ヨモキ゛ 抽出液 0.7 - 0.7 - - 0.467 - - 0.2チャ 抽出液 - - 0.7 - - 0.467 - 0.467 0.2ヒ゛ワ 抽出液 0.7 - - 0.7 - - 0.467 - 0.2シソ 抽出液 - - - 0.7 - - 0.467 0.467 0.2ケ゛ンノショウコ 抽出液 - - - - 0.7 - 0.467 - 0.2エタノール 60.0 60.0 60.0 60.0 60.0 60.0 60.0 60.0 60.0イオン 交換水 残余 残余 残余 残余 残余 残余 残余 残余 残余 ──────────────────────────────────── 評価 2.8 3.0 3.0 2.6 2.8 3.4 3.2 3.6 4.2 ────────────────────────────────────[Table 1] ──────────────────────────────────── Actual Example 1 2 3 4 5 6 7 8 9 ──────────────────────────────────── PROPOLEGEN RECALL 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 Oxyethylene (9) Lauryl ether 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 Dimethylpolysiloxane (8cs) 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 Ningen extract-0.7--0.7--0.467 0.2 Aloe extract-0.7-- -0.467--0.2 Momogyi extract 0.7-0.7--0.467--0.2 Tea extract--0.7--0.467-0.467 0.2 Biwa extract 0.7--0.7--0.467-0.2 Perilla extract---0.7-- 0.467 0.467 0.2 White ginger extract----0.7-0.467-0.2 Ethanol 60.0 60.0 60.0 60.0 60.0 60.0 60.0 60.0 60.0 Ion-exchanged water Residual Residual Residual Residual Residual Residual Residual Residual ──────────────────────────────────── Rating 2.8 3.0 3.0 2.6 2.8 3.4 3.2 3.6 4.2 ─ ───────────────────────────────────
【0032】[0032]
【表2】 ──────────────────────────────────── 比 較 例 1 2 3 4 5 6 7 ────────────────────────────────────フ゜ロヒ゜レンク゛リコール 1.0 1.0 1.0 1.0 1.0 1.0 1.0ホ゜リオキシエチレン (9) ラウリルエーテル 0.5 0.5 0.5 0.5 0.5 0.5 0.5シ゛メチル ホ゜リシロキサン (8cs) 2.5 2.5 2.5 2.5 2.5 2.5 2.5ニンシ゛ン 抽出液 1.4 - - - - - - アロエ 抽出液 - 1.4 - - - - - ヨモキ゛ 抽出液 - - 1.4 - - - - チャ 抽出液 - - - 1.4 - - - ヒ゛ワ 抽出液 - - - - 1.4 - - シソ 抽出液 - - - - - 1.4 - ケ゛ンノショウコ 抽出液 - - - - - - 1.4エタノール 60.0 60.0 60.0 60.0 60.0 60.0 60.0イオン 交換水 残余 残余 残余 残余 残余 残余 残余 ──────────────────────────────────── 評価 1.8 1.6 1.6 1.8 1.4 1.6 1.6 ────────────────────────────────────[Table 2] ──────────────────────────────────── Comparative Examples 1 2 3 4 5 6 7 ──────────────────────────────────── Fluoropolyene recall 1.0 1.0 1.0 1.0 1.0 1.0 1.0 Polyoxyethylene (9 ) Lauryl ether 0.5 0.5 0.5 0.5 0.5 0.5 0.5 Dimethylpolysiloxane (8cs) 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 Ningen extract 1.4------Aloe extract-1.4-----Yomog extract--1.4- ---Cha extract---1.4---Biwa extract----1.4--Perilla extract-----1.4-Kensho extract------1.4 Ethanol 60.0 60.0 60.0 60.0 60.0 60.0 60.0 Ion-exchanged water Residual residual Residual residual Residual residual ──────────────────────────────────── Evaluation 1.8 1.6 1.6 1.8 1.4 1.6 1.6 ────────────────────────────────────
【0033】表1に記載する本発明の各実施例は、いず
れも評価が2.0以上となり、臭いの付着が少ないこと
が示唆される。一方、表2に示す各植物抽出液の一種の
みを配合した各比較例においては、いずれの評価も2.
0未満となり、臭いの付着が著しいことが示唆される。
したがって、各植物抽出液を単独で配合したのでは、消
臭効果が弱く、各植物抽出液を2種以上同時に配合する
ことにより、高い消臭効果を示すことが明らかとなっ
た。In each of the examples of the present invention shown in Table 1, the evaluation was 2.0 or more, which suggests that the odor is less attached. On the other hand, in each comparative example in which only one kind of each plant extract shown in Table 2 was blended, each evaluation was 2.
It is less than 0, which suggests that the odor is significantly attached.
Therefore, it was clarified that the deodorizing effect was weak when each plant extract was blended alone, and a high deodorizing effect was exhibited by simultaneously blending two or more plant extracts.
【0034】次に本発明者らは、植物抽出液の総配合量
について検討を行った。なお、ここで言う植物抽出液の
総配合量とは、各実施例、比較例に配合される各植物抽
出液の配合量の総和を意味する。また、評価及び製法は
表1及び表2と同じである。処方と評価を表3〜5に示
す。Next, the present inventors examined the total blending amount of the plant extract. The total amount of the plant extract liquids referred to here means the sum of the amounts of the plant extract liquids compounded in each Example and Comparative Example. The evaluation and manufacturing method are the same as those in Tables 1 and 2. The prescription and evaluation are shown in Tables 3-5.
【0035】[0035]
【表3】 ──────────────────────────────────── 実 施 例 10 11 12 13 14 15 ────────────────────────────────────フ゜ロヒ゜レンク゛リコール 1.0 1.0 1.0 1.0 1.0 1.0 ホ゜リオキシエチレン (9) ラウリルエーテル 0.5 0.5 0.5 0.5 0.5 0.5 シ゛メチル ホ゜リシロキサン (8cs) 2.5 2.5 2.5 2.5 2.5 2.5 ニンシ゛ン 抽出液 0.00005 - - 0.0005 - 0.0005 アロエ 抽出液 0.00005 - - - 0.0005 - ヨモキ゛ 抽出液 - 0.00005 - - - - チャ 抽出液 - 0.00005 - - - 0.0005 ヒ゛ワ 抽出液 - - 0.00005 - 0.0005 - シソ 抽出液 - - 0.00005 - - - ケ゛ンノショウコ 抽出液 - - - 0.0005 - 0.0005 エタノール 60.0 60.0 60.0 60.0 60.0 60.0 イオン 交換水 残余 残余 残余 残余 残余 残余 ──────────────────────────────────── 総配合量 0.0001 0.0001 0.0001 0.001 0.001 0.0015 ──────────────────────────────────── 評価 2.0 2.0 2.1 2.6 2.4 2.6 ────────────────────────────────────[Table 3] ──────────────────────────────────── Actual Example 10 11 12 13 14 15 ─ ─────────────────────────────────── Fluoropolyene recall 1.0 1.0 1.0 1.0 1.0 1.0 Polyoxyethylene (9) Lauryl Ether 0.5 0.5 0.5 0.5 0.5 0.5 Dimethylpolysiloxane (8cs) 2.5 2.5 2.5 2.5 2.5 2.5 Ningen extract 0.00005--0.0005-0.0005 Aloe extract 0.00005---0.0005-Momo extract-0.00005----Cha extract- 0.00005---0.0005 Biwa extract--0.00005-0.0005-Perilla extract--0.00005---Ginger extract---0.0005-0.0005 Ethanol 60.0 60.0 60.0 60.0 60.0 60.0 Ion-exchanged water Residual Residual Residual ── ──────────────────────── ────────── Total amount 0.0001 0.0001 0.0001 0.001 0.001 0.0015 ─────────────────────────────── ───── Evaluation 2.0 2.0 2.1 2.6 2.4 2.6 ─────────────────────────────────────
【0036】[0036]
【表4】 ──────────────────────────────────── 実 施 例 16 17 18 19 20 21 22 23 24 ────────────────────────────────────フ゜ロヒ゜レンク゛リコール 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0ホ゜リオキシエチレン (9) ラウリルエーテル 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5シ゛メチル ホ゜リシロキサン (8cs) 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5ニンシ゛ン 抽出液 - 0.005 0.01 0.02 0.5 0.5 1.0 1.0 1.0アロエ 抽出液 - 0.005 0.01 0.01 0.5 1.0 - 1.0 1.0ヨモキ゛ 抽出液 0.005 - 0.01 0.01 0.5 0.5 - 1.0 2.0チャ 抽出液 - - - 0.02 0.5 1.0 - 1.0 1.0ヒ゛ワ 抽出液 - 0.005 0.01 0.01 0.5 1.0 2.0 1.0 1.0シソ 抽出液 0.005 - - 0.02 0.5 0.5 - 1.0 2.0ケ゛ンノショウコ 抽出液 - - 0.01 0.01 0.5 0.5 2.0 1.0 2.0エタノール 60.0 60.0 60.0 60.0 60.0 60.0 60.0 60.0 60.0イオン 交換水 残余 残余 残余 残余 残余 残余 残余 残余 残余 ──────────────────────────────────── 総配合量 0.01 0.015 0.05 0.1 3.5 5.0 5.0 7.0 10.0 ──────────────────────────────────── 評価 2.4 2.6 3.0 3.4 4.2 4.4 4.4 4.4 4.6 ────────────────────────────────────[Table 4] ──────────────────────────────────── Example 16 17 18 19 19 20 21 22 23 24 ──────────────────────────────────── Prologen recall 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 Oxyethylene (9) Lauryl ether 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 Dimethylpolysiloxane (8cs) 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 Ningen extract-0.005 0.01 0.02 0.5 0.5 1.0 1.0 1.0 Aloe extract-0.005 0.01 0.01 0.5 1.0-1.0 1.0 Momo extract 0.005-0.01 0.01 0.5 0.5-1.0 2.0 Cha extract---0.02 0.5 1.0-1.0 1.0 Biwa extract-0.005 0.01 0.01 0.5 1.0 2.0 1.0 1.0 Perilla extract 0.005--0.02 0.5 0.5 -1.0 2.0 Ginger extract--0.01 0.01 0.5 0.5 2.0 1.0 2.0 Ethanol 60.0 60.0 60.0 60.0 60.0 60.0 60.0 60.0 60.0 Ion-exchanged water Residual residual Residual residual Residual residual Residual residual ────────────────────────────────────── Total 0.01 0.015 0.05 0.1 3.5 5.0 5.0 7.0 10.0 ──────────────────────────────────── Evaluation 2.4 2.6 3.0 3.4 4.2 4.4 4.4 4.4 4.6 ────────────────────────────────────
【0037】[0037]
【表5】 ──────────────────────────────────── 比 較 例 8 9 10 ────────────────────────────────────フ゜ロヒ゜レンク゛リコール 1.0 1.0 1.0 ホ゜リオキシエチレン (9)ラウリルエーテル 0.5 0.5 0.5 シ゛メチルホ゜リシロキサン (8cs) 2.5 2.5 2.5 ニンシ゛ン 抽出液 0.00002 - 0.00001 アロエ 抽出液 0.00003 - 0.00001 ヨモキ゛ 抽出液 - - 0.00001チャ 抽出液 - 0.00003 0.00001ヒ゛ワ 抽出液 - - 0.00001シソ 抽出液 - 0.00003 0.00001ケ゛ンノショウコ 抽出液 - - 0.00001エタノール 60.0 60.0 60.0 イオン 交換水 残余 残余 残余 ──────────────────────────────────── 総配合量 0.00005 0.00006 0.00007 ──────────────────────────────────── 評価 1.0 1.2 1.2 ────────────────────────────────────[Table 5] ──────────────────────────────────── Comparative Examples 8 9 10 ──── ──────────────────────────────── Fluoropolyene glycol 1.0 1.0 1.0 Polyoxyethylene (9) Lauryl ether 0.5 0.5 0.5 Dimethylpolyol Siloxane (8cs) 2.5 2.5 2.5 Ninjin extract 0.00002-0.00001 Aloe extract 0.00003-0.00001 Yomogi extract--0.00001 Cha extract-0.00003 0.00001 Biwa extract--0.00001 Perilla extract-0.00003 0.00001 White pepper extract--0.00001 Ethanol 60.0 60.0 60.0 Ion-exchanged water Residual residue Residual residue ──────────────────────────────────── Total compounding amount 0.00005 0.00006 0.00007 ──────────────────────────── ─────── evaluation 1.0 1.2 1.2 ────────────────────────────────────
【0038】以上の結果より明らかなように、総配合量
が0.0001重量%未満では、良好な消臭効果を発揮
することができない。一方、総配合量が0.0001重
量%以上とすると、評価が2.0以上となり、消臭効果
が認められる。さらに、総配合量が0.001重量%以
上とすると、消臭効果に優れたヘアミストを得ることが
できる。As is clear from the above results, if the total content is less than 0.0001% by weight, a good deodorizing effect cannot be exhibited. On the other hand, when the total content is 0.0001% by weight or more, the evaluation is 2.0 or more, and the deodorizing effect is recognized. Furthermore, when the total content is 0.001% by weight or more, a hair mist excellent in deodorizing effect can be obtained.
【0039】ただし、総配合量が10重量%をこえる
と、各植物抽出液の臭いが顕在化し、特に好ましくは、
5重量%までである。したがって、植物抽出液の総配合
量が、0.0001〜10重量%、特に、0.001〜
5重量%であることが好ましい。However, when the total content exceeds 10% by weight, the odor of each plant extract becomes apparent, and particularly preferably,
Up to 5% by weight. Therefore, the total blending amount of the plant extract is 0.0001 to 10% by weight, particularly 0.001 to 10% by weight.
Preferably it is 5% by weight.
【0040】以下、本発明の配合例を挙げて本発明をさ
らに詳細に説明する。本発明はこれによって限定される
ものではない。また、配合量は特に示さない限り重量%
で示す。Hereinafter, the present invention will be described in more detail with reference to formulation examples of the present invention. The present invention is not limited by this. Unless otherwise specified, the blending amount is% by weight.
Indicated by
【0041】配合例1 ヘアスプレー(圧縮ガススプレー) プロピレングリコール 2.0重量% ポリオキシエチレン(40)硬化ヒマシ油 0.5 ジメチルポリシロキサン(8cs) 3.0 ニンジン抽出液 0.8 アロエ抽出液 0.8 チャ抽出液 0.8 ビワ抽出液 0.8 シソ抽出液 0.8 ゲンノショウコ抽出液 0.8 エタノール 60.0 イオン交換水 29.7 窒素ガス 適 量 ──────────────────────────────────── 合計:100.0重量% Formulation Example 1 Hair spray (compressed gas spray) Propylene glycol 2.0% by weight Polyoxyethylene (40) hydrogenated castor oil 0.5 Dimethylpolysiloxane (8cs) 3.0 Carrot extract 0.8 Aloe extract 0.8 Tea extract 0.8 Loquat extract 0.8 Perilla extract 0.8 Genso ginger extract 0.8 Ethanol 60.0 Ion-exchanged water 29.7 Nitrogen gas Appropriate amount ────────── ─────────────────────────── Total: 100.0% by weight
【0042】[製法]プロピレングリコール、ポリオキ
シエチレン(40)硬化ヒマシ油、ジメチルポリシロキ
サン(8cs)を混合溶解し、ホモミキサーで均一に乳
化する(乳化相)。イオン交換水にエタノール、先の乳
化相及び各抽出液を撹拌混合溶解する。ガスの充填は、
管に原液を充填し、バルブ装着後、ガスを充填する。[Manufacturing Method] Propylene glycol, polyoxyethylene (40) hydrogenated castor oil, and dimethylpolysiloxane (8cs) are mixed and dissolved, and uniformly emulsified by a homomixer (emulsion phase). Ethanol, the above emulsified phase and each extract are mixed by stirring and dissolved in ion-exchanged water. The gas filling is
Fill the tube with stock solution, install the valve, and then fill with gas.
【0043】配合例2 ヘアムース 1,3−ブチレングリコール 3.0重量% ポリエチレン(40)硬化ヒマシ油 1.0 合成イソパラフィン 3.0 流動パラフィン 3.0 ポリビニルピロリドン/酢酸ビニル共重合体 3.0 ニンジン抽出液 0.2 ヨモギ抽出液 0.2 ビワ抽出液 0.2 エタノール 10.0 イオン交換水 66.6 L.P.G(40kg/cm2at20℃) 10.0 香料 適 量 ──────────────────────────────────── 合計:100.0重量% Formulation 2 Hair Mousse 1,3-Butylene Glycol 3.0 wt% Polyethylene (40) hydrogenated castor oil 1.0 Synthetic isoparaffin 3.0 Liquid paraffin 3.0 Polyvinylpyrrolidone / vinyl acetate copolymer 3.0 Carrot Extract solution 0.2 Wormwood extract solution 0.2 Loquat extract solution 0.2 Ethanol 10.0 Ion-exchanged water 66.6 L. P. G (40kg / cm2at20 ℃) 10.0 Perfume Suitable amount ──────────────────────────────────── Total : 100.0% by weight
【0044】[製法]1,3−ブチレングリコール、ポ
リエチレン硬化ヒマシ油、合成イソパラフィン、流動パ
ラフィンを混合溶解し、ホモミキサーで均一に乳化する
(乳化相)。ポリビニルピロリドン/酢酸ビニル共重合
体、香料をアルコールに溶解する(アルコール相)。イ
オン交換水に先の乳化相、アルコール相及び各抽出液を
撹拌混合溶解する。ガスの充填は、管に原液を充填し、
バルブ装着後、ガスを充填する。[Production Method] 1,3-butylene glycol, polyethylene hardened castor oil, synthetic isoparaffin, and liquid paraffin are mixed and dissolved, and uniformly emulsified by a homomixer (emulsion phase). A polyvinylpyrrolidone / vinyl acetate copolymer and a fragrance are dissolved in alcohol (alcohol phase). The above-mentioned emulsified phase, alcohol phase and each extract are mixed by stirring and dissolved in ion-exchanged water. To fill the gas, fill the tube with the stock solution,
After installing the valve, fill it with gas.
【0045】配合例3 ヘアリキッド ポリエチレングリコール(1500) 2.0重量% ポリオキシエチレン(5)デシルテトラデシルエーテル 2.0 ポリオキシエチレンポリオキシプロピレンオリゴサクシネート (3.E.O)(20.P.O) 2.0 アロエ抽出液 0.1 ビワ抽出液 0.1 シソ抽出液 0.1 エタノール 65.0 イオン交換水 28.7 香料 適 量 ──────────────────────────────────── 合計:100.0重量% Formulation Example 3 Hair Liquid Polyethylene Glycol (1500) 2.0 wt% Polyoxyethylene (5) decyl tetradecyl ether 2.0 Polyoxyethylene polyoxypropylene oligosuccinate (3.EO) (20. P.O) 2.0 Aloe extract 0.1 Loquat extract 0.1 Perilla extract 0.1 Ethanol 65.0 Ion-exchanged water 28.7 Fragrance Suitable amount ──────────── ──────────────────────── Total: 100.0% by weight
【0046】[製法]精製水に各抽出液を溶解する(水
相)。エチルアルコールにそれ以外のものを溶解する
(アルコール相)。アルコール相に水相を添加し、濾紙
などで濾過する。[Production Method] Each extract is dissolved in purified water (aqueous phase). Others are dissolved in ethyl alcohol (alcohol phase). The aqueous phase is added to the alcohol phase and the mixture is filtered with filter paper or the like.
【0047】配合例4 ヘアシャンプー ラウリルポリオキシエチレン(3) 硫酸エステルナトリウム塩 30.0重量% ラウリル硫酸エステルナトリウム塩(30%水溶液) 10.0 ヤシ油脂肪酸ジエタノールアミド 4.0 グリセリン 1.0 チャ抽出液 1.0 ビワ抽出液 1.0 シソ抽出液 1.0 ゲンノショウコ抽出液 1.0 イオン交換水 51.0 クエン酸 適 量 クエン酸ナトリウム 適 量 エデト酸塩 適 量 窒素ガス 適 量 ──────────────────────────────────── 合計:100.0重量% Formulation Example 4 Hair shampoo Lauryl polyoxyethylene (3) Sulfate sodium salt 30.0% by weight Lauryl sulfate sodium salt (30% aqueous solution) 10.0 Coconut oil fatty acid diethanolamide 4.0 Glycerin 1.0 Cha Extraction liquid 1.0 Loquat extract liquid 1.0 Perilla extract liquid 1.0 Genus ginger extract liquid 1.0 Deionized water 51.0 Citric acid proper amount Sodium citrate proper amount Edetate proper amount Nitrogen gas proper amount ─── ───────────────────────────────── Total: 100.0% by weight
【0048】[製法]イオン交換水を70℃に加熱し、
他の成分を加えて均一に溶解したのち、冷却する。[Production Method] Ion-exchanged water is heated to 70 ° C.,
After adding other ingredients and dissolving uniformly, it is cooled.
【0049】配合例5 ヘアリンス グリセリン 3.0重量% ジメチルポリシロキサン(20cs) 3.0 流動パラフィン 1.0 セチルアルコール 1.5 ステアリルアルコール 1.0 塩化ステアリルトリメチルアンモニウム 0.7 ニンジン抽出液 0.5 ヨモギ抽出液 0.5 チャ抽出液 0.5 シソ抽出液 0.5 ゲンノショウコ抽出液 0.5 イオン交換水 87.3 香料 適 量 ──────────────────────────────────── 合計:100.0重量% Formulation 5 Hairrins Glycerin 3.0% by weight Dimethylpolysiloxane (20cs) 3.0 Liquid paraffin 1.0 Cetyl alcohol 1.5 Stearyl alcohol 1.0 Stearyltrimethylammonium chloride 0.7 Carrot extract 0.5 Mugwort extract 0.5 Cha extract 0.5 Perilla extract 0.5 Genshosho extract 0.5 Ion-exchanged water 87.3 Perfume Suitable amount ────────────────── ─────────────────── Total: 100.0% by weight
【0050】[製法]イオン交換水に塩化ステアリルト
リメチルアンモニウム、グリセリンを加え、70℃に保
ち(水相)、他の成分を混合し、加熱融解し70℃に保
つ(油相)。水相に油相を加えホモミキサーで乳化後撹
拌しながら冷却する。[Production Method] Stearyltrimethylammonium chloride and glycerin were added to ion-exchanged water, and the mixture was kept at 70 ° C (aqueous phase), other components were mixed, heated and melted and kept at 70 ° C (oil phase). The oil phase is added to the aqueous phase and the mixture is emulsified with a homomixer and then cooled with stirring.
【0051】配合例6 化粧水 グリセリン 5.0重量% オレイルアルコール 0.1 ポリオキシエチレン(20) ソルビタンモノラウリン酸エステル 0.5 アロエ抽出液 0.08 ビワ抽出液 0.05 ゲンノショウコ抽出液 0.02 エタノール 10.0 イオン交換水 84.25 香料 適 量 ──────────────────────────────────── 合計:100.0重量% Formulation Example 6 Lotion glycerin 5.0% by weight Oleyl alcohol 0.1 Polyoxyethylene (20) Sorbitan monolaurate 0.5 Aloe extract 0.08 Loquat extract 0.05 Geno ginger extract 0.02 Ethanol 10.0 Deionized water 84.25 Fragrance Suitable amount ──────────────────────────────────── Total : 100.0% by weight
【0052】[製法]精製水にオレイルアルコール、各
抽出液を室温にて溶解し水相とする。エタノールに香
料、グリセリン、ポリオキシエチレン(20)ソルビタ
ンモノラウリン酸エステルを溶解し、先の水相に混合化
する。[Production Method] Oleyl alcohol and each extract are dissolved in purified water at room temperature to obtain an aqueous phase. A perfume, glycerin, and polyoxyethylene (20) sorbitan monolaurate are dissolved in ethanol and mixed with the above aqueous phase.
【0053】配合例7 乳液 ジプロピレングリコール 5.0重量% ポリエチレングリコール1500 3.0 ステアリン酸 2.0 セチルアルコール 1.5 ワセリン 4.0 スクワラン 5.0 グリセロールトリ2エチルへキサン酸エステル 2.0 ソルビタンモノオレイン酸エステル 2.0 トリエタノールアミン 1.0 ニンジン抽出液 0.05 アロエ抽出液 0.1 ビワ抽出液 0.05 イオン交換水 74.3 香料 適 量 ──────────────────────────────────── 合計:100.0重量% Blending Example 7 Emulsion Dipropylene glycol 5.0% by weight Polyethylene glycol 1500 3.0 Stearic acid 2.0 Cetyl alcohol 1.5 Vaseline 4.0 Squalane 5.0 Glycerol tri-2-ethylhexanoate 2.0 Sorbitan monooleate 2.0 Triethanolamine 1.0 Carrot extract 0.05 Aloe extract 0.1 Loquat extract 0.05 Ion-exchanged water 74.3 Perfume Suitable amount ────────── ─────────────────────────── Total: 100.0% by weight
【0054】[製法]各抽出液を溶解したイオン交換水
にジプロピレングリコール、ポリエチレングリコール、
トリエタノールアミンを加え70℃に加熱調整する(水
相)。ステアリン酸、セチルアルコール、ワセリン、ス
クワラン、グリセロールトリ2エチルへキサン酸エステ
ルを溶解し、コレステロールエステルに、ソルビタンモ
ノオレイン酸エステル、香料を加え70℃に調整する
(油相)。この油相を先に調整した水相に加え呼び乳化
を行う。ホモミキサーにて乳化粒子を均一にした後、脱
気、濾過、冷却する。[Manufacturing method] Dipropylene glycol, polyethylene glycol,
Triethanolamine is added and the temperature is adjusted to 70 ° C. (aqueous phase). Stearic acid, cetyl alcohol, petrolatum, squalane, and glycerol tri-2-ethylhexanoate are dissolved, and sorbitan monooleate and a fragrance are added to cholesterol ester to adjust the temperature to 70 ° C (oil phase). The oil phase is added to the previously prepared water phase to emulsify. After homogenizing the emulsified particles with a homomixer, deaeration, filtration and cooling are performed.
【0055】配合例8 クリーム 1,3−ブチレングリコール 6.0重量% ポリエチレングリコール1500 4.0 ステアリルアルコール 6.0 ステアリン酸 2.0 水添ラノリン 4.0 スクワラン 9.0 オクチルドデカノール 10.0 ポリオキシエチレン(25)セチルアルコールエーテル 3.0 モノステアリン酸グリセリン 2.0 ヨモギ抽出液 0.1 ゲンノショウコ抽出液 0.1 イオン交換水 53.8 香料 適 量 ──────────────────────────────────── 合計:100.0重量% Formulation 8 Cream 1,3-butylene glycol 6.0% by weight Polyethylene glycol 1500 4.0 Stearyl alcohol 6.0 Stearic acid 2.0 Hydrogenated lanolin 4.0 Squalane 9.0 Octyldodecanol 10.0 Polyoxyethylene (25) Cetyl alcohol ether 3.0 Glycerin monostearate 2.0 Mugwort extract 0.1 Ginseng extract 0.1 Deionized water 53.8 Perfume proper amount ─────────── ────────────────────────── Total: 100.0% by weight
【0056】[製法]各抽出液を溶解したイオン交換水
に、1,3−ブチレングリコール、ポリエチレングリコ
ールを加え70℃に加熱調整する(水相)。ステアリル
アルコール、ステアリン酸、水添ラノリン、スクワラ
ン、オクテルドデカノールを加熱溶解後、ポリオキシエ
チレン(25)セチルアルコールエーテル、モノステア
リン酸グリセリン、香料を加え70℃に調整する(油
相)。これを先の水相に加えて、ホモミキサーにて乳化
粒子を均一にして、脱気、濾過、冷却する。[Production Method] 1,3-butylene glycol and polyethylene glycol are added to ion-exchanged water in which each extract solution is dissolved, and the temperature is adjusted to 70 ° C. (aqueous phase). Stearyl alcohol, stearic acid, hydrogenated lanolin, squalane, and octerdodecanol are heated and dissolved, and then polyoxyethylene (25) cetyl alcohol ether, glyceryl monostearate, and a fragrance are added to adjust the temperature to 70 ° C. (oil phase). This is added to the above aqueous phase, the emulsified particles are made uniform by a homomixer, and deaerated, filtered and cooled.
【0057】配合例9 ルームコロン ポリオキシエチレン(60)硬化ヒマシ油 1.5重量% アロエ抽出液 1.0 チャ抽出物 2.0 シソ抽出物 1.0 ゲンノショウコ抽出液 2.0 イオン交換水 87.5 香料 5.0 ──────────────────────────────────── 合計:100.0重量% Formulation 9 Room colon polyoxyethylene (60) hydrogenated castor oil 1.5% by weight Aloe extract 1.0 Tea extract 2.0 Perilla extract 1.0 Geno ginger extract 2.0 Ion-exchanged water 87 .5 Fragrance 5.0 ──────────────────────────────────── Total: 100.0% by weight
【0058】[製法]イオン交換水に加温融解したポリ
オキシエチレン(60)硬化ヒマシ油を溶解し、そこに
香料を徐添する。これに各抽出液を溶解する。[Production Method] Polyoxyethylene (60) hydrogenated castor oil melted by heating in ion-exchanged water is dissolved, and a fragrance is gradually added thereto. Each extract is dissolved in this.
【0059】[0059]
【発明の効果】以上説明したように、本発明の消臭剤、
消臭組成物および消臭化粧料は、ニンジン、アロエ、ヨ
モギ、チャ、ビワ、シソ、ゲンノショウコの7種の植物
群より選択される2種以上の植物抽出液を含むことによ
り、消臭効果に優れた効果を発揮する。As described above, the deodorant of the present invention,
The deodorant composition and the deodorant cosmetic composition have two or more kinds of plant extract liquids selected from the seven kinds of plant groups of carrot, aloe, mugwort, tea, loquat, perilla, and ginkgo biloba, thereby improving the deodorant effect. Shows excellent effects.
───────────────────────────────────────────────────── フロントページの続き (72)発明者 中村 祥二 神奈川県横浜市港北区新羽町1050番地 株 式会社資生堂第一リサーチセンター内 (72)発明者 鈴木 あい子 神奈川県横浜市港北区新羽町1050番地 株 式会社資生堂第一リサーチセンター内 (72)発明者 難波 富幸 神奈川県横浜市港北区新羽町1050番地 株 式会社資生堂第一リサーチセンター内 (72)発明者 中根 俊彦 神奈川県横浜市港北区新羽町1050番地 株 式会社資生堂第一リサーチセンター内 (72)発明者 井上 正春 大阪府大阪市旭区千林2丁目15番17号 環 境科学開発株式会社内 ─────────────────────────────────────────────────── ─── Continuation of the front page (72) Shoji Nakamura, 1050, Shinba-cho, Kohoku-ku, Yokohama-shi, Kanagawa Inside Shiseido Daiichi Research Center, Inc. (72) Inventor, Aiko Suzuki, 1050, Niiba-cho, Kohoku-ku, Yokohama-shi, Kanagawa Incorporated Shiseido Daiichi Research Center (72) Inventor Tomiyuki Nanba, 1050 Shinba-cho, Kohoku-ku, Yokohama-shi, Kanagawa Incorporated Shiseido Daiichi Research Center (72) Inventor Toshihiko Nakane, Niigata, Kohoku-ku, Yokohama-shi, Kanagawa 1050, Machi Incorporated company Shiseido Daiichi Research Center (72) Inventor Masaharu Inoue 2-15-17 Senbayashi, Asahi-ku, Osaka Prefecture Osaka Environmental Science Development Co., Ltd.
Claims (9)
ワ、シソ、ゲンノショウコの7種の植物群より選択され
る2種以上の植物抽出液を含むことを特徴とする消臭
剤。1. A deodorant comprising two or more plant extracts selected from seven plant groups of carrot, aloe, mugwort, tea, loquat, perilla, and ginger ginger.
徴とする消臭組成物。2. A deodorant composition comprising the deodorant according to claim 1.
出液の総配合量が、組成物全量中の0.0001〜10
重量%であることを特徴とする消臭組成物。3. The deodorant according to claim 2, wherein the total amount of the plant extract is 0.0001 to 10 in the total amount of the composition.
A deodorant composition, characterized in that the composition is in a weight percentage.
いて、タバコ臭の消臭効果を有することを特徴とする消
臭組成物。4. The deodorant composition according to claim 2 or 3, which has a deodorizing effect on tobacco odor.
成物を含むことを特徴とする消臭化粧料。5. A deodorant cosmetic comprising the deodorant composition according to any one of claims 2 to 4.
あることを特徴とする毛髪用消臭化粧料。6. A deodorant cosmetic for hair, wherein the deodorant cosmetic according to claim 5 is for hair.
あることを特徴とする皮膚用消臭化粧料。7. A deodorant cosmetic for skin, wherein the deodorant cosmetic according to claim 5 is for skin.
ップ用であることを特徴とするメーキャップ用消臭化粧
料。8. A deodorant cosmetic composition for makeup, wherein the deodorant cosmetic composition according to claim 5 is for makeup composition.
用であることを特徴とする室内用消臭組成物。9. An indoor deodorant composition, wherein the deodorant composition according to any one of claims 2 to 4 is for indoor use.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP7317239A JPH09131393A (en) | 1995-11-10 | 1995-11-10 | Deodorant, deodorizing composition, and deodorizing cosmetic |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP7317239A JPH09131393A (en) | 1995-11-10 | 1995-11-10 | Deodorant, deodorizing composition, and deodorizing cosmetic |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| JPH09131393A true JPH09131393A (en) | 1997-05-20 |
Family
ID=18086040
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP7317239A Pending JPH09131393A (en) | 1995-11-10 | 1995-11-10 | Deodorant, deodorizing composition, and deodorizing cosmetic |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPH09131393A (en) |
Cited By (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH11228325A (en) * | 1998-02-17 | 1999-08-24 | Hiromi Nishii | Liquid composition containing plant extract |
| KR20010000243A (en) * | 2000-08-28 | 2001-01-05 | 김명훈 | A Deodorizer Composition |
| JP2006025943A (en) * | 2004-07-13 | 2006-02-02 | Nozaki Seika Kk | Additive for deodorization and functional article containing the same |
| JP2007290983A (en) * | 2006-04-21 | 2007-11-08 | Lion Corp | Deodorant composition and deodorant agent |
| JP2010053058A (en) * | 2008-08-27 | 2010-03-11 | Hoyu Co Ltd | Hair-treating composition |
| US8236291B2 (en) | 2007-04-04 | 2012-08-07 | Es Fiber Visions Co., Ltd. | Antibacterial and deodorant fiber, fiber formed article, and fiber product |
| JP2012147984A (en) * | 2011-01-20 | 2012-08-09 | Tango Orimono Kogyo Kumiai | Deodorant, method of manufacturing the deodorant, and deodorant product containing the deodorant |
| JP2014034527A (en) * | 2012-08-07 | 2014-02-24 | Oshima Tsubaki Honpo:Kk | Cosmetics containing young leaf extract of camellia japonica |
| JP2015086183A (en) * | 2013-10-31 | 2015-05-07 | ポーラ化成工業株式会社 | Composition for skin photoaging prevention |
| WO2019225755A1 (en) * | 2018-05-25 | 2019-11-28 | 株式会社 資生堂 | Deodorant and deactivating agent |
| US20230042771A1 (en) * | 2021-07-23 | 2023-02-09 | Colgate-Palmolive Company | Personal Care Compositions Incorporating Natural Benefit Agents and Methods for the Same |
-
1995
- 1995-11-10 JP JP7317239A patent/JPH09131393A/en active Pending
Cited By (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH11228325A (en) * | 1998-02-17 | 1999-08-24 | Hiromi Nishii | Liquid composition containing plant extract |
| KR20010000243A (en) * | 2000-08-28 | 2001-01-05 | 김명훈 | A Deodorizer Composition |
| JP2006025943A (en) * | 2004-07-13 | 2006-02-02 | Nozaki Seika Kk | Additive for deodorization and functional article containing the same |
| JP2007290983A (en) * | 2006-04-21 | 2007-11-08 | Lion Corp | Deodorant composition and deodorant agent |
| US8236291B2 (en) | 2007-04-04 | 2012-08-07 | Es Fiber Visions Co., Ltd. | Antibacterial and deodorant fiber, fiber formed article, and fiber product |
| JP2010053058A (en) * | 2008-08-27 | 2010-03-11 | Hoyu Co Ltd | Hair-treating composition |
| JP2012147984A (en) * | 2011-01-20 | 2012-08-09 | Tango Orimono Kogyo Kumiai | Deodorant, method of manufacturing the deodorant, and deodorant product containing the deodorant |
| JP2014034527A (en) * | 2012-08-07 | 2014-02-24 | Oshima Tsubaki Honpo:Kk | Cosmetics containing young leaf extract of camellia japonica |
| JP2015086183A (en) * | 2013-10-31 | 2015-05-07 | ポーラ化成工業株式会社 | Composition for skin photoaging prevention |
| WO2019225755A1 (en) * | 2018-05-25 | 2019-11-28 | 株式会社 資生堂 | Deodorant and deactivating agent |
| JPWO2019225755A1 (en) * | 2018-05-25 | 2021-07-26 | 株式会社 資生堂 | Deodorant and inactivating agent |
| US20230042771A1 (en) * | 2021-07-23 | 2023-02-09 | Colgate-Palmolive Company | Personal Care Compositions Incorporating Natural Benefit Agents and Methods for the Same |
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