CN115531249A - Smearing mask with oil control effect and preparation method thereof - Google Patents

Smearing mask with oil control effect and preparation method thereof Download PDF

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Publication number
CN115531249A
CN115531249A CN202211260114.0A CN202211260114A CN115531249A CN 115531249 A CN115531249 A CN 115531249A CN 202211260114 A CN202211260114 A CN 202211260114A CN 115531249 A CN115531249 A CN 115531249A
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oil control
percent
oil
facial mask
skin
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李莹
马晓钰
侯亚东
鲁朝刚
李想
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Shaanxi HuiKang Bio Tech Co Ltd
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Shaanxi HuiKang Bio Tech Co Ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/84Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34Alcohols
    • A61K8/345Alcohols containing more than one hydroxy group
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/36Carboxylic acids; Salts or anhydrides thereof
    • A61K8/362Polycarboxylic acids
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/36Carboxylic acids; Salts or anhydrides thereof
    • A61K8/365Hydroxycarboxylic acids; Ketocarboxylic acids
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    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/36Carboxylic acids; Salts or anhydrides thereof
    • A61K8/368Carboxylic acids; Salts or anhydrides thereof with carboxyl groups directly bound to carbon atoms of aromatic rings
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/37Esters of carboxylic acids
    • A61K8/375Esters of carboxylic acids the alcohol moiety containing more than one hydroxy group
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/64Proteins; Peptides; Derivatives or degradation products thereof
    • A61K8/66Enzymes
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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    • A61K8/987Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
    • A61K8/988Honey; Royal jelly, Propolis
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/008Preparations for oily skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/20Chemical, physico-chemical or functional or structural properties of the composition as a whole
    • A61K2800/24Thermal properties
    • A61K2800/242Exothermic; Self-heating; Heating sensation

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Abstract

The invention discloses an applying facial mask with an oil control effect and a preparation method thereof, wherein the facial mask comprises the following components in percentage by mass: 0.1 to 15 percent of base raw material, 20 to 95 percent of polyol, 3 to 15 percent of emulsifier, 1 to 10 percent of emollient and 0.01 to 5 percent of oil control compound. The facial mask has special jam-like appearance by compounding the emulsifier, the emollient, the polyalcohol and the like, and can be changed from jam shape to cream shape by gentle massage in the using process, visual appearance change is realized, redundant grease on the surface of the skin can be emulsified, the use is mild, the facial mask is safe and non-irritant, in addition, the temperature of the surface of the skin is raised by heat emitted by the facial mask, the emulsification of the redundant grease on the surface of the skin is facilitated, and the redundant grease secreted on the surface of the skin is taken away. Meanwhile, the oil control composite component is matched, so that the water-oil balance of skin can be adjusted after long-term use, and the oil control is long-acting.

Description

Smearing mask with oil control effect and preparation method thereof
Technical Field
The invention belongs to the technical field of cosmetics, and particularly relates to an applying facial mask with an oil control effect and a preparation method of the applying facial mask.
Background
The demand of consumers for the skin care products of 'nature and health' is more and more intense, and the texture of the food for beautifying the kitchen is also well received by people. Most people are relatively exclusive to substances such as preservatives, pigments, essences and the like added in the formula, and people pay more attention to the appearance and the mild use safety of the product while pursuing beauty. Therefore, the product similar to the food appearance is free of pigments, essences and preservatives and can cater to the market.
The number of the facial masks with variable temperature is small in the facial mask market, substances which can generate heat along with the temperature rise are zeolite, sodium aluminate, capsaicin, capsicum extracts, vanillyl butyl ether and the like, the main mechanisms of the components are similar to the mechanism of human allergy, and the components have high skin irritation in the use process. Meanwhile, because the use of electronic products is increased, the skin grease is exuberantly secreted in the face of the electronic products, so that redundant grease on the surface of the skin is emulsified through massage in the using process, visual emulsification change is realized, and meanwhile, the oil control effect is achieved by matching with other oil control active ingredients for long-term use.
At present, the smearing facial mask mainly comprises mud, cream, tearing, gel and foam. The mud type smearing facial mask has strong cleaning effect, but the main component of the facial mask is a powder type raw material, so that the facial mask is generally poor in ductility, troublesome to clean and easy to block pores. Cream type facial masks usually have the effects of moisturizing, resisting aging and the like, but are thick and heavy in texture, and can feel greasy and even feel stuffy and acne when being used. The tearing type smearing mask also has the main effect of cleaning, can powerfully remove blackheads, but has a slightly rough use mode and is easy to damage the skin when being improperly used. The gel type facial mask has the effects of relieving and moisturizing, but the facial mask generally contains high-content polymers, is sticky in skin feel, and is easy to make the skin feel close after being used. The foam type facial masks generally have two types, one type is foam-shaped after being directly extruded, and the other type is foam-shaped after being contacted with air, and the two types have cleaning effects, but the substrate is weak alkaline generally and has certain irritation to skin.
Disclosure of Invention
The invention aims to provide a smearing facial mask with an oil control effect, which can emulsify redundant oil on the surface of skin in use and has a long-acting oil control effect.
The invention also aims to provide a preparation method of the smearing type facial mask.
The technical scheme adopted by the invention is that the smearing facial mask with the oil control effect comprises the following components in percentage by mass: 0.1 to 15 percent of base raw material, 20 to 95 percent of polyol, 3 to 15 percent of emulsifier, 1 to 10 percent of emollient and 0.01 to 5 percent of oil control compound.
The present invention is also characterized in that,
the composite material comprises the following components in percentage by mass: 2 to 12 percent of base raw material, 70 to 90 percent of polyol, 5 to 10 percent of emulsifier, 3 to 8 percent of emollient and 1 to 3.5 percent of oil control compound.
The base material comprises the following components in parts by weight: 0.1 to 4 portions of water, 0.1 to 2.5 portions of panthenol, 0.01 to 0.3 portion of allantoin and 0.01 to 0.5 portion of nicotinamide.
The polyol is prepared from the following components in percentage by mass of 45-85: 10-30 of glycerin and diglycerin.
The emulsifier is polyglycerol-10 stearate.
The emollient is prepared from the following components in a mass ratio of 1-4: 0.1 to 1:0.1 to 1: 0.05-0.4 of caprylic/capric triglyceride, sweet almond oil, hydrogenated vegetable oil and tangerine peel oil.
The oil control compound is prepared from the following components in a mass ratio of 0.001-0.2: 0.1 to 2:0.1 to 2:0.1 to 2:0.01 to 0.3:0.01 to 0.5 of azelaic acid, grapefruit fruit extract, propolis extract, 10-hydroxydecanoic acid compound, lysozyme and encapsulated salicylic acid.
The invention adopts another technical scheme that a preparation method of the smearing facial mask with the oil control effect is implemented according to the following steps:
step 1, weighing the following components in percentage by mass: 0.1-15% of base raw material, 20-95% of polyalcohol, 3-15% of emulsifier, 1-10% of emollient and 0.01-5% of oil control compound;
the base stock comprises water, panthenol, allantoin and nicotinamide; the oil control compound is prepared by mixing azelaic acid, grapefruit fruit extract, propolis extract, 10-hydroxydecanoic acid compound, lysozyme and encapsulated salicylic acid;
step 2, mixing polyalcohol, emulsifier, panthenol in the basic raw material, allantoin, azelaic acid in the oil control compound and coated salicylic acid, heating to 80-85 ℃ under the stirring state, and keeping the temperature for 8-10 min; then adding the emollient, heating to 80-85 ℃ under the stirring state, and preserving the heat for 5-8 min;
step 3, adding water and nicotinamide in the basic raw materials, heating to 80-85 ℃ under a stirring state, and preserving heat for 8-10 min; and then cooling, sequentially adding the grapefruit fruit extract, the propolis extract, the 10-hydroxydecanoic acid compound and the lysozyme in the oil-controlling compound when the temperature is reduced to 45-55 ℃, continuously stirring uniformly, cooling to 30-45 ℃, and discharging to obtain the smearing facial mask.
The invention has the beneficial effects that:
1. the facial mask has special jam-like appearance by compounding the emulsifier, the emollient, the polyalcohol and the like, and can be changed from jam to cream by gentle massage in the use process, visual appearance change is realized, redundant grease on the surface of skin can be emulsified, the facial mask is mild in use, safe and non-irritant, has a long-acting oil control effect in the long-term use process, can brighten the skin, and is suitable for any skin;
2. the facial mask selects two polyols of glycerin and diglycerin, wherein the two polyols have good moisturizing effect and contain more hydroxyl groups, and hydrogen in the hydroxyl groups reacts with oxygen atoms in the air in the using process to form hydrogen bonds, so that the hydrogen bonds release heat and are sensed by skin nerves, thereby having warm feeling, reducing stimulation to the skin, opening pores of the skin due to the warm skin feeling and being beneficial to absorption of skin care nutrient substances.
3. The heat emitted by the facial mask disclosed by the invention can raise the temperature of the skin surface, and is more beneficial to emulsifying redundant grease on the skin surface, so that the redundant grease secreted on the skin surface is taken away. Meanwhile, the oil control composite component is matched, so that the water-oil balance of skin can be adjusted after long-term use, and the oil control is long-acting.
Drawings
Fig. 1 is an external view of the application mask of the present invention;
fig. 2 is a view showing the state of application of the application mask of the present invention.
Fig. 3 is a state diagram of the smearing mask of the present invention after being emulsified by smearing, massaging.
Detailed Description
The present invention will be described in detail with reference to the following embodiments.
The invention relates to an applying facial mask with an oil control effect, which comprises the following components in percentage by mass: 0.1-15% of base raw material, 20-95% of polyalcohol, 3-15% of emulsifier, 1-10% of emollient and 0.01-5% of oil control compound;
preferably, the smearing mask comprises the following components in percentage by mass: 2 to 12 percent of base raw material, 70 to 90 percent of polyol, 5 to 10 percent of emulsifier, 3 to 8 percent of emollient and 1 to 3.5 percent of oil control compound;
the base material comprises the following components in parts by weight: 0.1 to 4 portions of water, 0.1 to 2.5 portions of panthenol, 0.01 to 0.3 portion of allantoin and 0.01 to 0.5 portion of nicotinamide;
preferably, the composition comprises the following components in parts by weight: 1 to 3 parts of water, 0.5 to 1.5 parts of panthenol, 0.05 to 0.15 part of allantoin and 0.05 to 0.2 part of nicotinamide;
in order to have good skin-smearing feeling and temperature change during massage, the polyol is prepared from the following components in a mass ratio of 45-85: 10-30 of glycerin and diglycerin; preferably, the mass ratio of glycerol to diglycerol is 13:4;
for the purpose of changing appearance when being smeared, the emulsifier is selected from polyglycerol-10 stearate;
in order to have the appearance color and fruit fragrance of the jam, the emollient is prepared from the following components in a mass ratio of 1-4: 0.1 to 1:0.1 to 1: 0.05-0.4 of caprylic/capric triglyceride, sweet almond (PRUNUS AMYGDALUS DULCIS) oil, hydrogenated vegetable oil, and mandarin orange (CITRUS TANGERINA) peel oil;
preferably, the emollient is prepared from a mixture of 2.5:0.6:0.6:0.15 of caprylic/capric triglyceride, sweet almond oil, hydrogenated vegetable oil, and tangerine peel oil;
in order to have the oil control effect, the oil control compound is prepared by mixing the following components in a mass ratio of 0.001-0.2: 0.1 to 2:0.1 to 2:0.1 to 2:0.01 to 0.3:0.01 to 0.5 of azelaic acid, grapefruit fruit extract, propolis extract, 10-hydroxydecanoic acid compound, lysozyme and encapsulated salicylic acid;
preferably, the oil control compound is prepared from a mixture of 0.05:1:1:1:0.1:0.2 of azelaic acid, grapefruit fruit extract, propolis extract, 10-hydroxydecanoic acid compound, lysozyme and encapsulated salicylic acid;
the smearing mask disclosed by the invention is prepared by selecting stable, safe and good-skin-feel raw materials and matching the raw materials through an emulsifier, an emollient, a polyalcohol and the like, so that the mask has a special jam-like appearance as shown in figure 1, and visual appearance change can be realized by slight massage in the using process and changing from a jam shape to a cream shape as shown in figures 2 and 3.
In the mask of the invention, each component has different functions, and the whole combination has fragrance, appearance and temperature change through the synergistic effect among the components. The basic raw material is a skin conditioner, except water, other materials can be replaced according to skin feeling effects, and the water is a basic solvent and is beneficial to later-stage smearing and emulsification. The polyhydric alcohol has good moisturizing effect, and can release heat when being applied to the skin to achieve warm feeling and soft and smooth feeling. The emulsifier plays a role of a bridge, can well connect and stabilize incompatible polyol, basic raw materials and emollient, and can make the product more similar to the texture of food in appearance and similar to the texture of food. The emollient has good effects of moistening and lubricating skin, and can make the facial mask have color and flavor and have the characteristics of jam. The oil control compound is an effective component, and can inhibit sebum secretion, control oil and resist acne, regulate water and oil balance of skin, clear pores and promote epidermis renewal of skin through synergistic effect of a plurality of components. Through the cooperative matching of the components, the whole mask has the appearance and fragrance of jam, and visual appearance change and temperature change are smeared.
The invention relates to a preparation method of a smearing facial mask with an oil control effect, which is implemented according to the following steps:
step 1, weighing the following components in percentage by mass: 0.1-15% of base raw material, 20-95% of polyalcohol, 3-15% of emulsifier, 1-10% of emollient and 0.01-5% of oil control compound;
the base material comprises the following components in parts by weight: 0.1 to 4 portions of water, 0.1 to 2.5 portions of panthenol, 0.01 to 0.3 portion of allantoin and 0.01 to 0.5 portion of nicotinamide;
the oil control compound is prepared from the following components in a mass ratio of 0.001-0.2: 0.1 to 2:0.1 to 2:0.1 to 2:0.01 to 0.3:0.01 to 0.5 of azelaic acid, grapefruit fruit extract, propolis extract, 10-hydroxydecanoic acid compound, lysozyme and encapsulated salicylic acid;
step 2, mixing polyalcohol, emulsifier, panthenol in the basic raw material, allantoin, azelaic acid in the oil control compound and coated salicylic acid, heating to 80-85 ℃ under stirring, and keeping the temperature for 8-10 min until the mixture is completely dissolved; then adding the emollient, heating to 80-85 ℃ under the stirring state, and preserving the heat for 5-8 min until the mixture is uniformly mixed.
Step 3, adding water and nicotinamide in the basic raw materials, heating to 80-85 ℃ under a stirring state, and keeping the temperature for 8-10 min until the components are completely dissolved and uniformly mixed; and then cooling by starting cooling water, sequentially adding the grapefruit fruit extract, the propolis extract, the 10-hydroxydecanoic acid compound and the lysozyme in the oil control compound when the temperature is reduced to 45-55 ℃, continuously stirring uniformly, cooling to 30-45 ℃, and discharging to obtain the smearing facial mask.
Example 1
Taking the preparation of 1000g of a mask as an example, it consists of 379.5g of glycerin, 400g of diglycerin, 120g of polyglycerin-10 stearate, 10g of caprylic/capric triglyceride, 5.4g of sweet almond (PRUNUS AMYGDALUS DULCIS) oil, 5.4g of hydrogenated vegetable oil, 1.2g of tangerine (CITRUS TANGERINA) peel oil, 35g of water, 8g of panthenol, 1g of allantoin, 1g of niacinamide, 0.5g of azelaic acid, 10g of grapefruit fruit extract, 10g of propolis extract, 10g of 10-hydroxydecanoic acid, 1g of lysozyme, 2g of coated salicylic acid, and it is prepared as follows:
1. adding glycerol, diglycerol, polyglycerol-10 stearate, panthenol, allantoin, azelaic acid, and coated salicylic acid into an emulsifying pot in sequence, closing the emulsifying pot, heating to 80 deg.C under stirring, and keeping the temperature for 8min until completely dissolved.
2. Adding caprylic/capric triglyceride, sweet almond (PRUNUS AMYGDALUS DULCIS) oil, hydrogenated vegetable oil, and pericarpium Citri Tangerinae (Citrus TANGERINA) oil into emulsifying pan, heating to 80 deg.C under stirring, and maintaining the temperature for 5min until mixing.
3. Adding water and nicotinamide into the emulsifying pot, heating to 80 deg.C under stirring, and maintaining for 8min until completely dissolved and mixed uniformly.
4. Cooling with cooling water, adding grapefruit fruit extract, propolis extract, 10-hydroxydecanoic acid and lysozyme when the temperature is reduced to 45 deg.C, stirring, cooling to 30 deg.C, and discharging to obtain the final product.
Example 2
Taking the preparation of 1000g of mask as an example, it is composed of 500.5g of glycerin, 300g of diglycerin, 100g of polyglycerin-10 stearate, 15g of caprylic/capric triglyceride, 5.4g of sweet almond (PRUNUS AMYGDALUS DULCIS) oil, 5.4g of hydrogenated vegetable oil, 1.2g of tangerine (CITRUS TANGERINA) peel oil, 30g of water, 8g of panthenol, 1g of allantoin, 1g of niacinamide, 0.5g of azelaic acid, 10g of grapefruit fruit extract, 10g of propolis extract, 10g of 10-hydroxydecanoic acid, 1g of lysozyme, 2g of coated salicylic acid, and its preparation method is as follows:
1. adding glycerol, diglycerol, polyglycerol-10 stearate, panthenol, allantoin, azelaic acid, and coated salicylic acid into an emulsifying pot in sequence, closing the emulsifying pot, heating to 85 deg.C under stirring, and keeping the temperature for 10min until completely dissolved.
2. Adding caprylic/capric triglyceride, sweet almond (PRUNUS AMYGDALUS DULCIS) oil, hydrogenated vegetable oil, and pericarpium Citri Tangerinae (Citrus TANGERINA) oil into emulsifying pan, heating to 85 deg.C under stirring, and maintaining the temperature for 8min until mixing.
3. Adding water and nicotinamide into the emulsifying pot, heating to 85 deg.C under stirring, and maintaining for 10min until completely dissolved and mixed.
4. Cooling with cooling water, adding grapefruit fruit extract, propolis extract, 10-hydroxydecanoic acid and lysozyme when the temperature is reduced to 55 deg.C, stirring, cooling to 45 deg.C, and discharging to obtain the final product.
Example 3
Taking the preparation of 1000g of a mask as an example, it consists of 620.5g of glycerin, 200g of diglycerin, 80g of polyglycerin-10 stearate, 25g of caprylic/capric triglyceride, 5.4g of sweet almond (PRUNUS AMYGDALUS DULCIS) oil, 5.4g of hydrogenated vegetable oil, 1.2g of tangerine (CITRUS TANGERINA) peel oil, 20g of water, 8g of panthenol, 1g of allantoin, 1g of niacinamide, 0.5g of azelaic acid, 10g of grapefruit fruit extract, 10g of propolis extract, 10g of 10-hydroxydecanoic acid, 1g of lysozyme, 2g of coated salicylic acid, and it is prepared as follows:
1. adding glycerol, diglycerol, polyglycerol-10 stearate, panthenol, and allantoin into an emulsifying pan in sequence
And after the azelaic acid and the salicylic acid are wrapped, closing an emulsifying pot, heating to 80 ℃ under the stirring state, and keeping the temperature for 10min until the azelaic acid and the salicylic acid are completely dissolved.
2. Adding caprylic/capric triglyceride, sweet almond (PRUNUS AMYGDALUS DULCIS) oil, hydrogenated vegetable oil, and pericarpium Citri Tangerinae (Citrus TANGERINA) oil into emulsifying pan, heating to 85 deg.C under stirring, and maintaining the temperature for 8min until mixing.
3. Adding water and nicotinamide into the emulsifying pot, heating to 85 deg.C under stirring, and maintaining for 10min until completely dissolved and mixed uniformly.
4. Cooling with cooling water, adding grapefruit fruit extract, propolis extract, 10-hydroxydecanoic acid and lysozyme when the temperature is reduced to 55 deg.C, stirring, cooling to 30 deg.C, and discharging to obtain the final product.
Example 4
Taking the preparation of 1000g of mask as an example, it is composed of 750.5g of glycerin, 100g of diglycerin, 50g of polyglycerin-10 stearate, 40g of caprylic/capric triglyceride, 5.4g of sweet almond (PRUNUS AMYGDALUS DULCIS) oil, 5.4g of hydrogenated vegetable oil, 1.2g of tangerine (CITRUS TANGERINA) peel oil, 5g of water, 8g of panthenol, 1g of allantoin, 1g of niacinamide, 0.5g of azelaic acid, 10g of grapefruit fruit extract, 10g of propolis extract, 10g of 10-hydroxydecanoic acid, 1g of lysozyme, 2g of coated salicylic acid, and its preparation method is as follows:
1. adding glycerol, diglycerol, polyglycerol-10 stearate, panthenol, allantoin, azelaic acid, and coated salicylic acid into an emulsifying pot in sequence, closing the emulsifying pot, heating to 80 deg.C under stirring, and keeping the temperature for 8min until completely dissolved.
2. Adding caprylic/capric triglyceride, sweet almond (PRUNUS AMYGDALUS DULCIS) oil, hydrogenated vegetable oil, and pericarpium Citri Tangerinae (Citrus TANGERINA) oil into emulsifying pan, heating to 80 deg.C under stirring, and maintaining the temperature for 8min until mixing.
3. Adding water and nicotinamide into the emulsifying pot, heating to 85 deg.C under stirring, and keeping the temperature for 8min until completely dissolved and mixed uniformly.
4. Cooling with cooling water, adding grapefruit fruit extract, propolis extract, 10-hydroxydecanoic acid and lysozyme when the temperature is reduced to 45 deg.C, stirring, cooling to 30 deg.C, and discharging to obtain the final product.
In order to determine the raw material composition of the mask of the invention, a large number of laboratory research tests were carried out, the specific test conditions were as follows:
1. selection of polyol component
0.3g of glycerin, butanediol, glyceryl polyether-26, 1,3-propylene glycol, 1,2-pentanediol and diglycerin are respectively dropped on the surface of the skin, the skin is gently massaged, the change condition of the temperature on the surface of the skin is sensed, the result is shown in table 1, and the glycerin and the diglycerin are selected as the polyol component according to the test result.
TABLE 1 polyol feed Screen
Figure BDA0003891230920000111
2. Selection of emulsifiers
Preparing 100g of samples according to the mass percentage of the raw materials in the table 2, and observing the appearance of the obtained samples and the change condition of the appearance after smearing, wherein the results are shown in the table 3;
table 2 screening of emulsifier materials
Figure BDA0003891230920000121
TABLE 3 results of emulsifier raw material screening experiment
Figure BDA0003891230920000122
Figure BDA0003891230920000131
According to the test results of Table 3, the emulsifier of the present invention was selected as polyglyceryl-10 stearate.
In order to prove the beneficial effects of the invention, a large number of laboratory efficacy research tests are carried out, and the specific test conditions are as follows:
(1) In order to screen for excellent skin feel, the use skin feel of the masks prepared in examples 1 to 4 was evaluated by the following methods: the skin feeling of the product is comprehensively evaluated by 8 volunteers in a questionnaire mode, and the skin feeling is like or dislike for 1-10 points, and the average is finally averaged to be the highest. The results are shown in Table 4.
Table 4 example sensory evaluation
Group of Example 1 Example 2 Example 3 Example 4
Skin feel evaluation (average score) 6.8 7.2 8.6 8
(2) In order to prove the beneficial effects of the invention, the mask with the highest score in the examples was subjected to mild safety evaluation: human skin patch test of 20 persons. The results are shown in Table 5;
TABLE 5 evaluation of safety of formulations- -human skin Patch test
Figure BDA0003891230920000132
Note: skin closed patch test skin reaction grading standard-general product judgment standard: stage 0: negative reaction; level 1: suspicious reaction, only weak erythema exists, the number of the reaction people is less than or equal to 2, the result is judged to be passed, otherwise, the result is not passed; and 2, stage: weak positive reaction (erythema reaction): erythema, infiltration, edema and pimple, the number of the reaction people is less than or equal to 1 (note: no other 1-grade reaction can occur), the judgment is that the disease passes, otherwise, the disease does not pass; and 3, level: strong positive reaction (herpes reaction): erythema, infiltration, edema, pimples, herpes; the reaction may be beyond the test area; 4, level: very strong positive reaction (fusogenic herpes reaction); obvious erythema, severe infiltration, edema, and fusional herpes; the reaction goes beyond the test area. Once the 3 rd and 4 th order reactions have occurred, it is judged to fail.
(3) In order to prove the beneficial effects of the invention, the mask with the highest score in the examples was subjected to sensory evaluation of 20 persons, and the evaluation method was as follows: the questionnaire mode was used by 20 volunteers to perform a comprehensive assessment of the appearance, spreadability, moisture retention, oil control, degree of ease of rinsing, etc. of the product. The score criterion is that 7-10 points represent satisfaction; scores 4-7 represent general; scores 1-4 indicate unsatisfactory results. The results are shown in Table 6.
TABLE 6 mean values of sensory skin feel evaluation
Figure BDA0003891230920000141
(4) In order to prove the beneficial effects of the invention, the facial mask with the highest score in the examples was subjected to a long-term efficacy test of 4 persons, and the evaluation method was as follows: after 4 volunteers used for one month, the long-term efficacy evaluation of the product on the moisture retention and oil control effects of the product for one month is carried out. The results are shown in tables 7 to 8.
TABLE 7 summary of 30-day skin moisture data for 4 subjects
Figure BDA0003891230920000151
TABLE 8 summary of skin oil data of 30 days for 4 subjects
Figure BDA0003891230920000152
As can be seen from the test data and the attached drawings, the mask disclosed by the invention has the advantages of good skin feel evaluation, mild and safe formula, good humidity retention and oil control effects in long-term efficacy test, stable formula and visual appearance change phenomenon in use, solves the problem that the temperature change can be realized only by using a chemical heating agent in the traditional temperature change mask, is safe and non-irritant, and is suitable for any skin type.

Claims (8)

1. The smearing mask with the oil control effect is characterized by comprising the following components in percentage by mass: 0.1 to 15 percent of base raw material, 20 to 95 percent of polyol, 3 to 15 percent of emulsifier, 1 to 10 percent of emollient and 0.01 to 5 percent of oil control compound.
2. The smearing mask with the oil control effect as claimed in claim 1, which is characterized by comprising the following components in percentage by mass: 2 to 12 percent of base raw material, 70 to 90 percent of polyol, 5 to 10 percent of emulsifier, 3 to 8 percent of emollient and 1 to 3.5 percent of oil control compound.
3. The facial mask with the oil control effect as claimed in claim 1 or 2, wherein the base material comprises the following components in parts by weight: 0.1 to 4 portions of water, 0.1 to 2.5 portions of panthenol, 0.01 to 0.3 portion of allantoin and 0.01 to 0.5 portion of nicotinamide.
4. The facial mask with the oil control function according to claim 1 or 2, wherein the polyol is prepared from the following components in a mass ratio of 45-85: 10-30 of glycerin and diglycerin.
5. The facial mask with oil control function as claimed in claim 1 or 2, wherein the emulsifier is polyglycerol-10 stearate.
6. The facial mask with the oil control function according to claim 1 or 2, wherein the emollient is prepared from the following components in a mass ratio of 1-4: 0.1 to 1:0.1 to 1: 0.05-0.4 of caprylic/capric triglyceride, sweet almond oil, hydrogenated vegetable oil and tangerine peel oil.
7. The facial mask with oil control function according to claim 1 or 2, wherein the oil control compound is prepared from the following components in a mass ratio of 0.001-0.2: 0.1 to 2:0.1 to 2:0.1 to 2:0.01 to 0.3:0.01 to 0.5 of azelaic acid, grapefruit fruit extract, propolis extract, 10-hydroxydecanoic acid compound, lysozyme and encapsulated salicylic acid.
8. A preparation method of a smearing mask with an oil control effect is characterized by comprising the following steps:
step 1, weighing the following components in percentage by mass: 0.1-15% of base raw material, 20-95% of polyalcohol, 3-15% of emulsifier, 1-10% of emollient and 0.01-5% of oil control compound;
the base stock comprises water, panthenol, allantoin and nicotinamide; the oil control compound is prepared by mixing azelaic acid, grapefruit fruit extract, propolis extract, 10-hydroxydecanoic acid compound, lysozyme and encapsulated salicylic acid;
step 2, mixing polyalcohol, emulsifier, panthenol in the basic raw material, allantoin, azelaic acid in the oil control compound and coated salicylic acid, heating to 80-85 ℃ under the stirring state, and keeping the temperature for 8-10 min; then adding an emollient, heating to 80-85 ℃ under a stirring state, and keeping the temperature for 5-8 min;
step 3, adding water and nicotinamide in the basic raw materials, heating to 80-85 ℃ under a stirring state, and preserving heat for 8-10 min; and then cooling, when the temperature is reduced to 45-55 ℃, sequentially adding the grapefruit fruit extract, the propolis extract, the 10-hydroxydecanoate compound and the lysozyme in the oil control compound, continuously stirring uniformly, cooling to 30-45 ℃, and discharging to obtain the smearing facial mask.
CN202211260114.0A 2022-10-14 2022-10-14 Smearing mask with oil control effect and preparation method thereof Pending CN115531249A (en)

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Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103191027A (en) * 2013-04-27 2013-07-10 珀莱雅化妆品股份有限公司 Solid makeup removing cream having warm sense in using process
CN104434720A (en) * 2014-11-11 2015-03-25 彤阳生技(杭州)有限公司 Spontaneous type temperature sensing mask and preparation method thereof
KR20160061784A (en) * 2014-11-24 2016-06-01 주식회사 엘지생활건강 Heating compositions for personal cleansing containing powdered surfactant and natural powder
CN112315850A (en) * 2020-10-13 2021-02-05 广州妮趣化妆品有限公司 Self-heating gel mask cream and preparation method thereof
CN112569177A (en) * 2021-02-05 2021-03-30 东晟源研究院(广州)有限公司 Formula and preparation method of one-time emulsion luminescent mask paste

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103191027A (en) * 2013-04-27 2013-07-10 珀莱雅化妆品股份有限公司 Solid makeup removing cream having warm sense in using process
CN104434720A (en) * 2014-11-11 2015-03-25 彤阳生技(杭州)有限公司 Spontaneous type temperature sensing mask and preparation method thereof
KR20160061784A (en) * 2014-11-24 2016-06-01 주식회사 엘지생활건강 Heating compositions for personal cleansing containing powdered surfactant and natural powder
CN112315850A (en) * 2020-10-13 2021-02-05 广州妮趣化妆品有限公司 Self-heating gel mask cream and preparation method thereof
CN112569177A (en) * 2021-02-05 2021-03-30 东晟源研究院(广州)有限公司 Formula and preparation method of one-time emulsion luminescent mask paste

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
国产普通化妆品备案信息: "悦木集菁纯蜜养面膜", pages 1 - 2, Retrieved from the Internet <URL:https://hzpba.nmpa.gov.cn/gccx/chakan.html?prodId=973558209530822656&gb=G> *

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