CN115400635B - Preparation method and device of carboxyl silicone oil softener - Google Patents

Preparation method and device of carboxyl silicone oil softener Download PDF

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Publication number
CN115400635B
CN115400635B CN202210891226.XA CN202210891226A CN115400635B CN 115400635 B CN115400635 B CN 115400635B CN 202210891226 A CN202210891226 A CN 202210891226A CN 115400635 B CN115400635 B CN 115400635B
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cylinder
piston
threaded rod
rotating tooth
mounting plate
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CN115400635A (en
Inventor
杨相臣
许达
郭燕
黄作明
邓丽君
盛聪安
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Mianyang Jialide Textile Technology Co ltd
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Mianyang Jialide Textile Technology Co ltd
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/80—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis
    • B01F27/90—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis with paddles or arms 
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F23/00—Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
    • B01F23/50—Mixing liquids with solids
    • B01F23/51—Methods thereof
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F23/00—Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
    • B01F23/50—Mixing liquids with solids
    • B01F23/53—Mixing liquids with solids using driven stirrers
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/05—Stirrers
    • B01F27/11—Stirrers characterised by the configuration of the stirrers
    • B01F27/19—Stirrers with two or more mixing elements mounted in sequence on the same axis
    • B01F27/192—Stirrers with two or more mixing elements mounted in sequence on the same axis with dissimilar elements
    • B01F27/1921—Stirrers with two or more mixing elements mounted in sequence on the same axis with dissimilar elements comprising helical elements and paddles
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/80—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis
    • B01F27/92—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis with helices or screws
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F35/00—Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
    • B01F35/71—Feed mechanisms
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F35/00—Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
    • B01F35/71—Feed mechanisms
    • B01F35/712—Feed mechanisms for feeding fluids
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F35/00—Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
    • B01F35/71—Feed mechanisms
    • B01F35/714—Feed mechanisms for feeding predetermined amounts
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F35/00—Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
    • B01F35/80—Forming a predetermined ratio of the substances to be mixed
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
    • D06M13/144—Alcohols; Metal alcoholates
    • D06M13/148—Polyalcohols, e.g. glycerol or glucose
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
    • D06M13/152—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen having a hydroxy group bound to a carbon atom of a six-membered aromatic ring
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
    • D06M15/03—Polysaccharides or derivatives thereof
    • D06M15/05—Cellulose or derivatives thereof
    • D06M15/09—Cellulose ethers
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
    • D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M15/643—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicon in the main chain
    • D06M15/6433—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicon in the main chain containing carboxylic groups
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
    • D06M2200/50—Modified hand or grip properties; Softening compositions

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Dispersion Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Emergency Medicine (AREA)
  • Accessories For Mixers (AREA)
  • Lubricants (AREA)

Abstract

The invention relates to a preparation device of a carboxyl silicone oil softener, which comprises a stirring cylinder, a quantifying mechanism and a feeding mechanism, wherein the quantifying mechanism comprises a first mounting plate and a second mounting plate, the first mounting plate and the second mounting plate are fixed through a support column, a first cylinder is arranged in the middle of the second mounting plate, and a plurality of identical second cylinders and third cylinders are arranged on the second mounting plate; in the process of raw material adding, the first threaded rod drives the lifter plate to move up and down, the lifter plate drives the first connecting rod to move at the moment, the second piston synchronously moves in the first adjusting cylinder, at the moment, the third piston in the second adjusting cylinder connected with the first adjusting cylinder in a conducting way drives the second connecting rod to move, reciprocating movement of the double-sided rack is achieved, the double-sided rack is matched with the meshed transmission teeth, the transmission shaft is driven to rotate, and then the helical blades and the stirring blades are driven to rotate to stir raw materials in the charging bucket, so that raw material solidification and precipitation are avoided.

Description

Preparation method and device of carboxyl silicone oil softener
Technical Field
The invention relates to the technical field of softener processing, in particular to a preparation method and a device of carboxyl silicone oil softener.
Background
The fabric softener has the functions of uniformly coating a protective film on the surface of the fabric fiber, and the surface of the fiber is reduced in friction coefficient and enhanced in mobility due to the adsorption of the softener, and the inherent smoothness, elongation and compression performance of the fiber are restored, so that the fabric becomes softer, fluffy and elastic.
The raw materials of the softener comprise liquid raw materials and powdery raw materials, wherein in the process of adding the liquid raw materials according to the proportion, deviation of the proportion of the raw materials is easy to occur, and the quality of the proportioned softener product is unstable; meanwhile, in the process of storing various liquid raw materials, a special motor is required to be arranged on a storage device for stirring and mixing, otherwise solidification and precipitation of the liquid raw materials are easy to occur.
Disclosure of Invention
The invention solves the problems of providing a preparation method and a preparation device of a carboxyl silicone oil softener, solving the problems that the raw materials of the softener comprise liquid raw materials and powdery raw materials, wherein in the process of adding the liquid raw materials according to a proportion, deviation of the proportion of the raw materials is easy to occur, and the quality of a proportioned softener product is unstable; meanwhile, in the process of storing various liquid raw materials, a special motor is required to be arranged on a storage device for stirring and mixing, otherwise, the technical problems of solidification and precipitation of the liquid raw materials are easy to occur.
In order to achieve the above purpose, the present invention adopts the following technical scheme:
the preparation device of the carboxyl silicone oil softener comprises a stirring cylinder, a quantifying mechanism and a feeding mechanism, wherein the quantifying mechanism comprises a first mounting plate and a second mounting plate, the first mounting plate and the second mounting plate are fixed through a supporting column, a first cylinder body is arranged in the middle of the second mounting plate, a plurality of identical second cylinder bodies and third cylinder bodies are arranged on the second mounting plate, first pistons are slidably arranged in the first cylinder bodies, the second cylinder bodies and the third cylinder bodies, and a first control valve and a second control valve are respectively arranged at the bottom sides of the first cylinder bodies, the second cylinder bodies and the third cylinder bodies in a conducting mode;
the charging mechanism comprises a mounting seat, a plurality of charging tanks are mounted on the mounting seat, connecting valves are mounted on the bottom sides of the charging tanks, and the connecting valves of the charging tanks are respectively connected with the first control valves of the first cylinder, the second cylinder and the third cylinder through connecting pipes;
and in the same time, the ratio of the discharge volume of the raw materials in the first cylinder to the discharge volume of the raw materials in the second cylinder and the discharge volume of the raw materials in the third cylinder is 100:10:1.
Preferably, the same first thread seat, a plurality of second thread seat and a plurality of third thread seat are installed to first mounting panel internal bearing, first threaded rod is installed in the inside screw thread penetration of first thread seat, the second threaded rod is installed in the inside penetration of second thread seat, the third threaded rod is installed in the penetration of third thread seat internal thread, first threaded rod and second threaded rod and third threaded rod are the same specification threaded rod.
Preferably, the first polygonal column is installed to first threaded rod bottom, the second polygonal column is installed to the second threaded rod bottom, the third polygonal column is installed to the third threaded rod bottom, and first polygonal column, second polygonal column and third polygonal column all are connected with first piston, and first polygonal column, second polygonal column and third polygonal column respectively with first barrel, second barrel and third barrel in sliding sleeve adaptation, and the thickness of a plurality of first piston is the same.
Preferably, the second cylinder and the third cylinder are the same in size, the inner height of the second cylinder is the same as that of the first cylinder, and the volume ratio of the volume of the second cylinder except for the first piston to the volume of the first cylinder except for the first piston is 1:10.
Preferably, first sprocket and first rotating tooth are installed in the first screw thread seat outside, the motor is installed to first mounting panel top side, and motor output installs the initiative tooth with first sprocket meshing, the second sprocket is installed in the second screw thread seat outside, and is connected through chain transmission between first sprocket and the second sprocket.
Preferably, the top side of the first cylinder is provided with a plurality of rotating shafts, the top of each rotating shaft is provided with a second rotating tooth and a third rotating tooth, the third rotating tooth is meshed with the first rotating tooth, the outer side of the third thread seat is provided with a fourth rotating tooth, the fourth rotating tooth is meshed with the second rotating tooth, the tooth ratio of the first rotating tooth to the third rotating tooth is 1:2, and the tooth ratio of the second rotating tooth to the fourth rotating tooth is 1:5.
Preferably, a plurality of first adjusting cylinders are mounted on the second mounting plate, a second piston is mounted in the first adjusting cylinders and connected with a first connecting rod, the top end of the first connecting rod penetrates through the first mounting plate to be connected with a lifting plate, and the lifting plate is connected with the top end of a first threaded rod.
Preferably, the limiting plate is arranged on the mounting seat, the second adjusting cylinder is horizontally arranged on the limiting plate and is connected with the first adjusting cylinder in a conducting mode, the third piston is arranged in the second adjusting cylinder and is connected with the second connecting rod, and the double-sided rack is arranged at the outer end of the second connecting rod.
Preferably, a transmission shaft is installed in the material tank in a penetrating mode, transmission teeth meshed with the double-sided racks are installed at the top end of the transmission shaft, and spiral blades and stirring blades are arranged on the outer side of the transmission shaft.
The preparation method of the carboxyl silicone oil softener comprises the following specific operation steps:
step one: the softener comprises the following raw materials in parts by volume: 10-15 parts of carboxyl silicone oil, 0.5-0.7 part of glycerol, 2-5 parts of eugenol and 100-120 parts of deionized water,
step two: carboxyl silicone oil, glycerol, eugenol and deionized water are respectively stored in a charging mechanism charging tank, a first cylinder, a second cylinder and a third cylinder, wherein the deionized water is positioned in the first cylinder, the eugenol and the carboxyl silicone oil are positioned in different second cylinders, the glycerol is positioned in the third cylinder, the motor works to drive a driving tooth to rotate, the driving tooth is meshed with a first sprocket to drive a first thread seat and a first rotating tooth to rotate, the first sprocket drives a second sprocket to rotate through a chain to drive the second thread seat to rotate, the first rotating tooth drives a third rotating tooth on a rotating shaft to rotate, at the moment, the second rotating tooth synchronously rotates to drive a fourth rotating tooth and the third thread seat to rotate, at the moment, a first threaded rod, a second threaded rod and a third threaded rod which are in threaded connection with the first threaded seat, the second threaded seat and the third threaded seat respectively drive the first polygonal column, the second polygonal column and the third polygonal column to move, so that synchronous movement of the first piston is realized, the moving distance of the first piston in the first cylinder and the second cylinder is 10 times that of the first piston in the third cylinder within the same time, when the first piston moves downwards, the first control valve is closed, the second control valve is opened, at the moment, raw materials are added into the mixing cylinder, when the second control valve is closed, the first control valve is opened, the first piston moves, automatic replenishment of the raw materials in the first cylinder, the second cylinder and the third cylinder is realized, and then the raw materials in the mixing cylinder are mixed and stirred for 35-40min, so that a first mixed solution is obtained;
step three: at the moment, the first mixed solution, sodium carboxymethyl cellulose and a thickening agent are prepared from the following components in parts by weight: 120-140 parts of first mixed solution, 1-3 parts of sodium carboxymethyl cellulose and 5-8 parts of thickener, and adding the sodium carboxymethyl cellulose and the thickener into a stirring barrel, and stirring at constant temperature for 20-25min to obtain the carboxyl silicone oil softener.
The beneficial effects of the invention are as follows: the motor works to drive the driving teeth to rotate, the driving teeth are meshed with the first sprocket to drive the first thread seat to rotate, the second thread seat is driven to rotate through the transmission cooperation of the sprocket and the chain, the third thread seat is driven to rotate through the gear transmission of different tooth ratios, the threaded rod connected with the thread seat is driven to move, the polygonal column drives the first piston to move, the volume ratio of the volume of removing the first piston in the second cylinder to the volume of removing the first piston in the first cylinder is 1:10, the moving speed of the first piston in the first cylinder and the second cylinder is multiple of the moving speed of the first piston in the third cylinder, and therefore the volume ratio of raw materials added into the mixing cylinder through the second control valve is 100:10:1, deionized water is added through a first barrel, eugenol and carboxyl silicone oil are added through a second barrel which is different, and glycerin is added through a third barrel, namely deionized water, eugenol, carboxyl silicone and glycerin are convenient to be added according to 100:10:1, and the first control valve and the second control valve are used for controlling the opening and closing of the first barrel, the second barrel and the third barrel to realize the automatic feeding of the first barrel, the second barrel and the third barrel while realizing the accurate proportioning of the liquid raw materials;
simultaneously at the in-process that carries out the raw materials and add, first threaded rod drives the lifter plate and reciprocates, and the lifter plate drives the head rod and removes this moment, and the second piston is synchronous to be removed in first regulation section of thick bamboo, and the third piston in the second regulation section of thick bamboo that is connected with first regulation section of thick bamboo switch on this moment drives the second connecting rod and removes, realizes the reciprocating motion of two-sided rack, cooperates with the transmission tooth of meshing, drives the transmission shaft and rotates, and then drives helical blade and stirring vane rotation and stir the raw materials in the material jar, avoids the raw materials to solidify and appear precipitating.
Drawings
FIG. 1 is a schematic view of the structure of the present invention;
FIG. 2 is a schematic view of a first tooth mounting structure according to the present invention;
FIG. 3 is a partial cross-sectional view of a dosing mechanism of the present invention;
FIG. 4 is a schematic view of a chain mounting structure of the present invention;
FIG. 5 is a schematic view of the structure of the feeding mechanism of the present invention;
fig. 6 is a schematic view of the internal structure of the charging bucket according to the present invention.
Legend description:
1. a dosing mechanism; 2. a first mounting plate; 3. a second mounting plate; 4. a support column; 5. a first cylinder; 6. a second cylinder; 7. a third cylinder; 8. a first screw seat; 9. a first threaded rod; 10. a second screw seat; 11. a second threaded rod; 12. a third thread seat; 13. a third threaded rod; 14. a first polygonal column; 15. a second polygonal column; 16. a third polygonal column; 17. a sliding sleeve; 18. a first piston; 19. a first control valve; 20. a second control valve; 21. a motor; 22. a driving tooth; 23. a first sprocket; 24. a second sprocket; 25. a first rotating tooth; 26. a rotating shaft; 27. a second rotating tooth; 28. a third rotating tooth; 29. a fourth rotating tooth; 30. a lifting plate; 31. a first adjustment cylinder; 32. a second piston; 33. a first connecting rod; 34. a mounting base; 35. a limiting plate; 36. a second adjustment cylinder; 37. a third piston; 38. a second connecting rod; 39. double-sided racks; 40. a charging bucket; 41. a drive tooth; 42. a transmission shaft; 43. a helical blade; 44. stirring blades; 45. and a connecting valve.
Detailed Description
The following description of the embodiments of the present invention will be made clearly and completely with reference to the accompanying drawings, in which it is apparent that the embodiments described are only some embodiments of the present invention, but not all embodiments. All other embodiments, which can be made by those skilled in the art based on the embodiments of the invention without making any inventive effort, are intended to be within the scope of the invention.
Specific examples are given below.
Referring to fig. 1-6, the preparation device of the carboxyl silicone oil softener comprises a stirring cylinder, a quantifying mechanism 1 and a feeding mechanism, wherein the quantifying mechanism 1 comprises a first mounting plate 2 and a second mounting plate 3, the first mounting plate 2 and the second mounting plate 3 are fixed through a support column 4, a first cylinder 5 is arranged in the middle of the second mounting plate 3, a plurality of identical second cylinders 6 and third cylinders 7 are arranged on the second mounting plate 3, a first piston 18 is slidably arranged in each of the first cylinder 5, the second cylinder 6 and the third cylinder 7, and a first control valve 19 and a second control valve 20 are respectively arranged on the bottom sides of the first cylinder 5, the second cylinder 6 and the third cylinder 7 in a conducting manner;
in the same time, the ratio of the discharge volume of the raw materials in the first cylinder 5 to the discharge volume of the raw materials in the second cylinder 6 and the discharge volume of the raw materials in the third cylinder 7 is 100:10:1, the same first threaded seat 8, a plurality of second threaded seats 10 and a plurality of third threaded seats 12 are arranged in the first mounting plate 2 in a bearing manner, the first threaded rod 9 is arranged in the first threaded seat 8 in a penetrating manner, the second threaded rod 11 is arranged in the second threaded seat 10 in a penetrating manner, the third threaded rod 13 is arranged in the third threaded seat 12 in a penetrating manner, the first threaded rod 9, the second threaded rod 11 and the third threaded rod 13 are threaded rods with the same specification, the first polygonal column 14 is arranged at the bottom end of the first threaded rod 9, the second polygonal column 15 is arranged at the bottom end of the second threaded rod 11, the third polygonal column 16 is arranged at the bottom end of the third threaded rod 13, the first polygonal column 14, the second polygonal column 15 and the third polygonal column 16 are all connected with the first piston 18, the first polygonal column 14, the second polygonal column 15 and the third polygonal column 16 are respectively matched with sliding sleeves 17 in the first cylinder 5, the second cylinder 6 and the third cylinder 7, the thicknesses of a plurality of first pistons 18 are the same, the second cylinder 6 and the third cylinder 7 are the same in size, the inner height of the second cylinder 6 is the same as the inner height of the first cylinder 5, the volume ratio of the volume of the first cylinder 6 except for the first piston 18 to the volume of the first cylinder 5 except for the first piston 18 is 1:10, a first sprocket 23 and a first rotating tooth 25 are arranged outside the first threaded seat 8, a motor 21 is arranged on the top side of the first mounting plate 2, a driving tooth 22 meshed with the first sprocket 23 is arranged at the output end of the motor 21, a second sprocket 24 is arranged outside the second threaded seat 10, the first sprocket 23 and the second sprocket 24 are connected through chain transmission, a plurality of rotating shafts 26 are arranged on the top side of the first cylinder body 5, a second rotating tooth 27 and a third rotating tooth 28 are arranged on the top of the rotating shaft 26, the third rotating tooth 28 is meshed with the first rotating tooth 25, a fourth rotating tooth 29 is arranged on the outer side of the third thread seat 12, the fourth rotating tooth 29 is meshed with the second rotating tooth 27, the gear ratio of the first rotating tooth 25 to the third rotating tooth 28 is 1:2, the gear ratio of the second rotating tooth 27 to the fourth rotating tooth 29 is 1:5, the driving tooth 22 is driven to rotate through the operation of the motor 21, the first thread seat 8 is realized through the meshing transmission of the first sprocket 23, the second thread seat 10 is realized through the transmission cooperation of the sprocket and a chain, through the gear transmission of different gear ratios, realize the rotation of third screw seat 12, and then drive the threaded rod that is connected with screw seat screw thread and remove, drive first piston 18 with the excessive side post and remove, the volume ratio of removing first piston 18 in the second barrel 6 and removing first piston 18 in the first barrel 5 is 1:10, the velocity of movement of first piston 18 in first barrel 5 and the second barrel 6 is 10 times of the velocity of movement of first piston 18 in the third barrel 7, consequently, the volume ratio of raw materials that first barrel 5, second barrel 6 and third barrel 7 add through second control valve 20 to churn is 100:10:1, a step of;
the charging mechanism comprises a mounting seat 34, a plurality of charging tanks 40 are mounted on the mounting seat 34, a connecting valve 45 is mounted at the bottom side of the charging tanks 40, the connecting valve 45 of the charging tanks 40 is respectively connected with a first cylinder 5, a second cylinder 6 and a first control valve 19 of a third cylinder 7 through connecting pipes, a plurality of first adjusting cylinders 31 are mounted on a second mounting plate 3, a second piston 32 is mounted in the first adjusting cylinders 31, the second piston 32 is connected with a first connecting rod 33, the top end of the first connecting rod 33 penetrates through the first mounting plate 2 and is connected with a lifting plate 30, the lifting plate 30 is connected with the top end of a first threaded rod 9, a limiting plate 35 is mounted on the mounting seat 34, a second adjusting cylinder 36 is horizontally mounted on the limiting plate 35, the second adjusting cylinders 36 are connected with the first adjusting cylinders 31 in a conducting manner, a third piston 37 is mounted in the second adjusting cylinders 36, and the third piston 37 is connected with the second connecting rod 38, the double-sided rack 39 is installed at the outer end of the second connecting rod 38, the transmission shaft 42 is installed in a penetrating manner in the inner bearing of the charging bucket 40, the transmission teeth 41 meshed with the double-sided rack 39 are installed at the top end of the transmission shaft 42, the spiral blades 43 and the stirring blades 44 are arranged on the outer side of the transmission shaft 42, the first threaded rod 9 drives the lifting plate 30 to move up and down, the lifting plate 30 drives the first connecting rod 33 to move at the moment, the second piston 32 synchronously moves in the first adjusting cylinder 31, at the moment, the third piston 37 in the second adjusting cylinder 36 connected with the first adjusting cylinder 31 in a conducting manner drives the second connecting rod 38 to move, the reciprocating movement of the double-sided rack 39 is realized, the transmission teeth 41 meshed with the transmission shaft 42 are matched, the transmission shaft 42 is driven to rotate, and the spiral blades 43 and the stirring blades 44 are driven to rotate to stir raw materials in the charging bucket 40.
The preparation method of the carboxyl silicone oil softener comprises the following specific operation steps:
step one: the softener comprises the following raw materials in parts by volume: 10-15 parts of carboxyl silicone oil, 0.5-0.7 part of glycerol, 2-5 parts of eugenol and 100-120 parts of deionized water,
step two: carboxyl silicone oil, glycerol, eugenol and deionized water are respectively stored in a charging mechanism charging bucket 40, a first barrel 5, a second barrel 6 and a third barrel 7, wherein the deionized water is positioned in the first barrel 5, the eugenol and carboxyl silicone oil are positioned in different second barrels 6, the glycerol is positioned in the third barrel 7, a motor 21 works to drive a driving tooth 22 to rotate, the driving tooth is meshed with a first sprocket 23 to drive a first thread seat 8 and a first rotating tooth 25 to rotate, the first sprocket 23 drives a second sprocket 24 to rotate through a chain, the second thread seat 10 is driven to rotate, the first rotating tooth 25 drives a third rotating tooth 28 on a rotating shaft 26 to rotate, at the moment, the second rotating tooth 27 synchronously rotates to drive a fourth rotating tooth 29 and the third thread seat 12 to rotate, at this time, the first threaded rod 9, the second threaded rod 11 and the third threaded rod 13 which are in threaded connection with the first threaded seat 8, the second threaded seat 10 and the third threaded seat 12 respectively drive the first polygonal column 14, the second polygonal column 15 and the third polygonal column 16 to move so as to realize synchronous movement of the first piston 18, the moving distance of the first piston 18 in the first cylinder 5 and the second cylinder 6 is 10 times of the moving distance of the first piston 18 in the third cylinder 7 within the same time, when the first piston 18 moves downwards, the first control valve 19 is closed, the second control valve 20 is opened, at this time, raw materials are added into the mixing cylinder, when the second control valve 20 is closed, the first control valve 19 is opened, and the first piston 18 moves so as to realize automatic replenishment of the raw materials in the first cylinder 5, the second cylinder 6 and the third cylinder 7, and then the raw materials in the mixing cylinder are mixed and stirred for 35-40min, so as to obtain a first mixed solution;
step three: at the moment, the first mixed solution, sodium carboxymethyl cellulose and a thickening agent are prepared from the following components in parts by weight: 120-140 parts of first mixed solution, 1-3 parts of sodium carboxymethyl cellulose and 5-8 parts of thickener, and adding the sodium carboxymethyl cellulose and the thickener into a stirring barrel, and stirring at constant temperature for 20-25min to obtain the carboxyl silicone oil softener.
The motor 21 works to drive the driving teeth 22 to rotate, the driving teeth 23 are meshed with the first chain teeth to drive the first thread seat 8 to rotate, the chain teeth are matched with the chain to drive the second thread seat 10 to rotate, the gears with different gear ratios drive the third thread seat 12 to rotate, the threaded rod connected with the thread seat is driven to move, the polygonal column drives the first piston 18 to move, the volume ratio of the volume of the second cylinder 6 except the first piston 18 to the volume of the first cylinder 5 except the first piston 18 is 1:10, the moving speed of the first piston 18 in the first cylinder 5 and the second cylinder 6 is 10 times that of the first piston 18 in the third cylinder 7, and therefore the volume ratio of raw materials added into the stirring cylinder by the first cylinder 5, the second cylinder 6 and the third cylinder 7 through the second control valve 20 is 100:10:1, deionized water is added through a first cylinder 5, eugenol and carboxyl silicone oil are added through a second cylinder 6 which is different, and glycerin is added through a third cylinder 7, namely, deionized water, eugenol, carboxyl silicone and glycerin are convenient to be added according to 100:10:1, and the first control valve 19 and the second control valve 20 are used for controlling the opening and closing, so that the accurate proportioning of liquid raw materials can be realized, and the automatic feeding of the first cylinder 5, the second cylinder 6 and the third cylinder 7 can be realized;
meanwhile, in the process of raw material addition, the first threaded rod 9 drives the lifting plate 30 to move up and down, at the moment, the lifting plate 30 drives the first connecting rod 33 to move, the second piston 32 synchronously moves in the first adjusting cylinder 31, at the moment, the third piston 37 in the second adjusting cylinder 36 connected with the first adjusting cylinder 31 in a conducting way drives the second connecting rod 38 to move, the reciprocating movement of the double-sided rack 39 is realized, the double-sided rack is matched with the meshed transmission teeth 41, the transmission shaft 42 is driven to rotate, and the helical blade 43 and the stirring blade 44 are driven to rotate to stir raw materials in the charging bucket 40, so that raw materials are prevented from being solidified and precipitating.
In the liquid raw material proportioning process, the deionized water, the carboxyl silicone oil, the eugenol and the glycerol are proportioned according to 100 parts of deionized water, 15 parts of carboxyl silicone oil, 5 parts of eugenol and 0.7 part of glycerol, and at the moment, the volume ratio of the deionized water, the carboxyl silicone oil, the eugenol and the glycerol is as follows: 1000:150:50:7, according to the unit of the adding volume of each barrel, deionized water of the first barrel 5 is added for 10 times, carboxyl silicone oil of the second barrel 6 is added for 15 times, eugenol of the second barrel 6 is added for 5 times, glycerin of the third barrel 7 is added for 7 times, the adding is started simultaneously through the operation of a motor 21, when the second control valve 20 on the second barrel 6 of eugenol is closed after the 5 th time, the second control valve 20 on the third barrel 7 is closed after the 7 th time, the second control valve 20 on the first barrel 5 is closed after the 10 th time, the second control valve 20 on the second barrel 6 of carboxyl silicone oil is closed after the 15 th time, and accurate automatic adding of liquid raw materials is realized according to different proportions.
The foregoing is only a preferred embodiment of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art, who is within the scope of the present invention, should make equivalent substitutions or modifications according to the technical scheme of the present invention and the inventive concept thereof, and should be covered by the scope of the present invention.

Claims (4)

1. The preparation device of the carboxyl silicone oil softener is characterized by comprising a stirring cylinder, a quantifying mechanism (1) and a feeding mechanism, wherein the quantifying mechanism (1) comprises a first mounting plate (2) and a second mounting plate (3), the first mounting plate (2) and the second mounting plate (3) are fixed through a support column (4), a first cylinder (5) is arranged in the middle of the second mounting plate (3), a plurality of identical second cylinders (6) and third cylinders (7) are arranged on the second mounting plate (3), a first piston (18) is slidably arranged in each of the first cylinder (5), the second cylinder (6) and the third cylinder (7), and a first control valve (19) and a second control valve (20) are respectively arranged at the bottoms of the first cylinder (5), the second cylinder (6) and the third cylinder (7) in a conducting manner;
the feeding mechanism comprises a mounting seat (34), a plurality of charging tanks (40) are mounted on the mounting seat (34), connecting valves (45) are mounted on the bottom sides of the charging tanks (40), and the connecting valves (45) of the charging tanks (40) are respectively connected with first control valves (19) of a first cylinder body (5), a second cylinder body (6) and a third cylinder body (7) through connecting pipes;
in the same time, the ratio of the discharge volume of the raw materials in the first cylinder (5) to the discharge volume of the raw materials in the second cylinder (6) to the discharge volume of the raw materials in the third cylinder (7) is 100:10:1;
the bearing is arranged in the first mounting plate (2) and is provided with the same first thread seat (8), a plurality of second thread seats (10) and a plurality of third thread seats (12), a first threaded rod (9) is arranged in the first thread seat (8) in a penetrating mode, a second threaded rod (11) is arranged in the second thread seat (10) in a penetrating mode, a third threaded rod (13) is arranged in the third thread seat (12) in a penetrating mode, and the first threaded rod (9), the second threaded rod (11) and the third threaded rod (13) are identical in specification;
a first polygonal column (14) is arranged at the bottom end of the first threaded rod (9), a second polygonal column (15) is arranged at the bottom end of the second threaded rod (11), a third polygonal column (16) is arranged at the bottom end of the third threaded rod (13), the first polygonal column (14), the second polygonal column (15) and the third polygonal column (16) are all connected with a first piston (18), and the first polygonal column (14), the second polygonal column (15) and the third polygonal column (16) are respectively matched with sliding sleeves (17) in the first cylinder (5), the second cylinder (6) and the third cylinder (7), and the thicknesses of a plurality of first pistons (18) are the same;
the second cylinder (6) and the third cylinder (7) are the same in size, the inner height of the second cylinder (6) is the same as that of the first cylinder (5), and the volume ratio of the volume of the second cylinder (6) except for the first piston (18) to the volume of the first cylinder (5) except for the first piston (18) is 1:10;
a first sprocket (23) and a first rotating tooth (25) are arranged on the outer side of the first thread seat (8), a motor (21) is arranged on the top side of the first mounting plate (2), a driving tooth (22) meshed with the first sprocket (23) is arranged at the output end of the motor (21), a second sprocket (24) is arranged on the outer side of the second thread seat (10), and the first sprocket (23) and the second sprocket (24) are in transmission connection through a chain;
a plurality of rotating shafts (26) are arranged on the top side of the first cylinder body (5), a second rotating tooth (27) and a third rotating tooth (28) are arranged on the top of each rotating shaft (26), the third rotating tooth (28) is meshed with the first rotating tooth (25), a fourth rotating tooth (29) is arranged on the outer side of the third thread seat (12), the fourth rotating tooth (29) is meshed with the second rotating tooth (27), the tooth number ratio of the first rotating tooth (25) to the third rotating tooth (28) is 1:2, and the tooth number ratio of the second rotating tooth (27) to the fourth rotating tooth (29) is 1:5;
install a plurality of first adjustment section of thick bamboo (31) on second mounting panel (3), and install second piston (32) in first adjustment section of thick bamboo (31), second piston (32) are connected with head rod (33), head rod (33) top runs through first mounting panel (2) and is connected with lifter plate (30), lifter plate (30) are connected with first threaded rod (9) top.
2. The preparation device of the carboxyl silicone oil softener according to claim 1, characterized in that a limiting plate (35) is installed on the installation seat (34), a second adjusting cylinder (36) is horizontally installed on the limiting plate (35), the second adjusting cylinder (36) is in conductive connection with the first adjusting cylinder (31), a third piston (37) is installed in the second adjusting cylinder (36), the third piston (37) is connected with a second connecting rod (38), and a double-sided rack (39) is installed at the outer end of the second connecting rod (38).
3. The preparation device of the carboxyl silicone oil softener according to claim 2, wherein a transmission shaft (42) is installed in the charging bucket (40) in a penetrating manner, transmission teeth (41) meshed with the double-sided rack (39) are installed at the top end of the transmission shaft (42), and spiral blades (43) and stirring blades (44) are arranged on the outer side of the transmission shaft (42).
4. A preparation method of a carboxyl silicone oil softener, which adopts the preparation device of the carboxyl silicone oil softener as defined in any one of claims 1 to 3, and is characterized by comprising the following specific operation steps:
step one: the softener comprises the following raw materials in parts by volume: 10-15 parts of carboxyl silicone oil, 0.5-0.7 part of glycerol, 2-5 parts of eugenol and 100-120 parts of deionized water;
step two: carboxyl silicone oil, glycerol, eugenol and deionized water are respectively stored in a charging mechanism charging tank (40) and a first cylinder (5), a second cylinder (6) and a third cylinder (7), wherein the deionized water is positioned in the first cylinder (5), the eugenol and the carboxyl silicone oil are positioned in different second cylinders (6), the glycerol is positioned in the third cylinder (7), the motor (21) works to drive a driving tooth (22) to rotate and meshed with a first sprocket (23), the first thread seat (8) and the first rotating tooth (25) are driven to rotate, the first sprocket (23) drives a second sprocket (24) to rotate through a chain, the second rotating tooth (25) drives a third rotating tooth (28) on a rotating shaft (26) to rotate, at the moment, the second rotating tooth (27) synchronously rotates, the fourth rotating tooth (29) and the third thread seat (12) are driven to rotate, at the moment, the driving threaded rods (8, the second thread seat (10) and the third threaded seat (12) are connected with the first thread seat (9), the second threaded rod (13) and the third threaded rod (13) are driven to move synchronously, the threaded rods (13) and the threaded rods (13) are respectively, and the threaded rods (13) are driven to move synchronously, and the threaded rods (13) are respectively, and the threaded rods are moved synchronously, the moving distance of a first piston (18) in the first cylinder (5) and the second cylinder (6) is 10 times of the moving distance of the first piston (18) in the third cylinder (7), when the first piston (18) moves downwards, a first control valve (19) is closed, a second control valve (20) is opened, raw materials are added into the mixing cylinder at the moment, when the second control valve (20) is closed, the first control valve (19) is opened, the first piston (18) moves, raw materials in the first cylinder (5), the second cylinder (6) and the third cylinder (7) are automatically replenished, and then the raw materials in the mixing cylinder are mixed and stirred for 35-40min, so that a first mixed liquid is obtained;
step three: at the moment, the first mixed solution, sodium carboxymethyl cellulose and a thickening agent are prepared from the following components in parts by weight: 120-140 parts of first mixed solution, 1-3 parts of sodium carboxymethyl cellulose and 5-8 parts of thickener, and adding the sodium carboxymethyl cellulose and the thickener into a stirring barrel, and stirring at constant temperature for 20-25min to obtain the carboxyl silicone oil softener.
CN202210891226.XA 2022-07-27 2022-07-27 Preparation method and device of carboxyl silicone oil softener Active CN115400635B (en)

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