CN115400635A - Preparation method and device of carboxyl silicone oil softener - Google Patents

Preparation method and device of carboxyl silicone oil softener Download PDF

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Publication number
CN115400635A
CN115400635A CN202210891226.XA CN202210891226A CN115400635A CN 115400635 A CN115400635 A CN 115400635A CN 202210891226 A CN202210891226 A CN 202210891226A CN 115400635 A CN115400635 A CN 115400635A
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China
Prior art keywords
cylinder
piston
silicone oil
barrel
mounting plate
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CN202210891226.XA
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Chinese (zh)
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CN115400635B (en
Inventor
杨相臣
许达
郭燕
黄作明
邓丽君
盛聪安
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Mianyang Jialide Textile Technology Co ltd
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Mianyang Jialide Textile Technology Co ltd
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/80—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis
    • B01F27/90—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis with paddles or arms 
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F23/00—Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
    • B01F23/50—Mixing liquids with solids
    • B01F23/51—Methods thereof
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F23/00—Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
    • B01F23/50—Mixing liquids with solids
    • B01F23/53—Mixing liquids with solids using driven stirrers
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/05—Stirrers
    • B01F27/11—Stirrers characterised by the configuration of the stirrers
    • B01F27/19—Stirrers with two or more mixing elements mounted in sequence on the same axis
    • B01F27/192—Stirrers with two or more mixing elements mounted in sequence on the same axis with dissimilar elements
    • B01F27/1921—Stirrers with two or more mixing elements mounted in sequence on the same axis with dissimilar elements comprising helical elements and paddles
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/80—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis
    • B01F27/92—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis with helices or screws
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F35/00—Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
    • B01F35/71—Feed mechanisms
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F35/00—Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
    • B01F35/71—Feed mechanisms
    • B01F35/712—Feed mechanisms for feeding fluids
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F35/00—Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
    • B01F35/71—Feed mechanisms
    • B01F35/714—Feed mechanisms for feeding predetermined amounts
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F35/00—Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
    • B01F35/80—Forming a predetermined ratio of the substances to be mixed
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
    • D06M13/144—Alcohols; Metal alcoholates
    • D06M13/148—Polyalcohols, e.g. glycerol or glucose
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
    • D06M13/152—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen having a hydroxy group bound to a carbon atom of a six-membered aromatic ring
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
    • D06M15/03—Polysaccharides or derivatives thereof
    • D06M15/05—Cellulose or derivatives thereof
    • D06M15/09—Cellulose ethers
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
    • D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M15/643—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicon in the main chain
    • D06M15/6433—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicon in the main chain containing carboxylic groups
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
    • D06M2200/50—Modified hand or grip properties; Softening compositions

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Dispersion Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Emergency Medicine (AREA)
  • Accessories For Mixers (AREA)
  • Lubricants (AREA)

Abstract

The invention relates to a preparation device of a carboxyl silicone oil softener, which comprises a mixing drum, a quantifying mechanism and a feeding mechanism, wherein the quantifying mechanism comprises a first mounting plate and a second mounting plate, the first mounting plate and the second mounting plate are fixed through a supporting column, a first cylinder body is arranged in the middle of the second mounting plate, and a plurality of identical second cylinder bodies and third cylinder bodies are arranged on the second mounting plate; in the in-process of carrying out the raw materials and adding, first threaded rod drives the lifter plate and reciprocates, the lifter plate drives the head rod removal this moment, the second piston is synchronous motion in first regulation section of thick bamboo, third piston in the second regulation section of thick bamboo with first regulation section of thick bamboo turn-on connection this moment drives the second connecting rod removal, realize the reciprocating motion of two-sided rack, with the driving gear cooperation of meshing, it is rotatory to drive the transmission shaft, and then it stirs to the raw materials in the feed cylinder to drive helical blade and stirring vane rotation, avoid the raw materials to solidify and appear precipitating.

Description

Preparation method and device of carboxyl silicone oil softener
Technical Field
The invention relates to the technical field of processing of softeners, in particular to a preparation method and a device of a carboxyl silicone oil softener.
Background
The fabric softener acts as if the surface of fabric fibers is uniformly covered with a protective film, because the softener is adsorbed on the surface of the fibers, the friction coefficient among the fibers is reduced, the mobility is enhanced, and the inherent smoothness, extension and compression properties of the fibers are also recovered, so that the fabric becomes softer, fluffy and elastic.
The raw materials of the softener comprise liquid raw materials and powder raw materials, wherein in the process of adding the liquid raw materials according to the proportion, the proportion of the raw materials is easy to deviate, so that the quality of the proportioned softener product is unstable; meanwhile, in the process of storing various liquid raw materials, a special motor is required to be arranged on the storage device for stirring and mixing, otherwise, the liquid raw materials are easy to solidify and precipitate.
Disclosure of Invention
The invention aims to provide a preparation method and a device of a carboxyl silicone oil softener, which solves the problem that the raw materials of the softener comprise liquid raw materials and powdery raw materials, wherein the liquid raw materials are easy to have deviation in the proportioning of the raw materials in the proportional adding process, so that the quality of the proportioned softener product is unstable; meanwhile, in the process of storing various liquid raw materials, a special motor needs to be arranged on the storage device for stirring and mixing, otherwise the technical problems of solidification and precipitation of the liquid raw materials are easy to occur.
In order to achieve the purpose, the invention adopts the following technical scheme:
the preparation device of the carboxyl silicone oil softener comprises a stirring cylinder, a quantifying mechanism and a feeding mechanism, wherein the quantifying mechanism comprises a first mounting plate and a second mounting plate, the first mounting plate and the second mounting plate are fixed through a supporting column, a first cylinder is mounted in the middle of the second mounting plate, a plurality of identical second cylinders and third cylinders are mounted on the second mounting plate, first pistons are slidably mounted in the first cylinders, the second cylinders and the third cylinders, and a first control valve and a second control valve are respectively installed on the bottom sides of the first cylinders, the second cylinders and the third cylinders in a conduction mode;
the feeding mechanism comprises a mounting seat, a plurality of charging tanks are mounted on the mounting seat, connecting valves are mounted at the bottom sides of the charging tanks, and the connecting valves of the plurality of charging tanks are respectively connected with first control valves of the first cylinder, the second cylinder and the third cylinder through connecting pipes;
in the same time, the ratio of the discharge volume of the raw material in the first cylinder to the discharge volume of the raw material in the second cylinder and the discharge volume of the raw material in the third cylinder is 100.
Preferably, the same first screw thread seat, a plurality of second screw thread seat and a plurality of third screw thread seat are installed to the bearing in the first mounting panel, the inside screw thread of first screw thread seat runs through and installs first threaded rod, the inside second threaded rod that runs through and installs of second screw thread seat, third screw thread seat internal thread runs through and installs the third threaded rod, first threaded rod and second threaded rod and third threaded rod are same specification threaded rod.
Preferably, first multilateral post is installed to first threaded rod bottom, second multilateral post is installed to second threaded rod bottom, third multilateral post is installed to third threaded rod bottom, and first multilateral post, second multilateral post and third multilateral post all with first piston connection, and first multilateral post, second multilateral post and third multilateral post respectively with first barrel, the sliding sleeve adaptation in second barrel and the third barrel, and the thickness homogeneous phase of a plurality of first piston is the same.
Preferably, the second cylinder and the third cylinder have the same size, the inner height of the second cylinder is the same as the inner height of the first cylinder, and the ratio of the volume of the second cylinder excluding the first piston to the volume of the first cylinder excluding the first piston is 1.
Preferably, first sprocket and first commentaries on classics tooth are installed to first screw thread seat outside, the motor is installed on first mounting panel top side, and the motor output end installs the initiative tooth with first sprocket meshing, the second sprocket is installed to the second screw thread seat outside, and passes through chain transmission connection between first sprocket and the second sprocket.
Preferably, a plurality of pivot is installed to first barrel top side, and the pivot top installs second commentaries on classics tooth and third commentaries on classics tooth, and the third changes the tooth and meshes with first commentaries on classics tooth, the fourth commentaries on classics tooth is installed to the third screw thread seat outside, and the fourth changes tooth and the meshing of second commentaries on classics tooth, and wherein first commentaries on classics tooth ratio and third commentaries on classics tooth ratio is 1, and second commentaries on classics tooth ratio and fourth commentaries on classics tooth ratio are 1.
Preferably, install the first regulation section of thick bamboo of a plurality of on the second mounting panel, and install the second piston in the first regulation section of thick bamboo, the second piston is connected with the head rod, the head rod top is run through first mounting panel and is connected with the lifter plate, the lifter plate is connected with first threaded rod top.
Preferably, install the limiting plate on the mount pad, horizontal installation has the second to adjust a section of thick bamboo on the limiting plate, and the second adjusts a section of thick bamboo and a first regulation section of thick bamboo turn-on connection, install the third piston in the second is adjusted a section of thick bamboo, and the third piston is connected with the second connecting rod, two-sided rack is installed to second connecting rod outer end.
Preferably, the inside bearing of material jar runs through and installs the transmission shaft, and the transmission shaft top install with two-sided rack toothing's driving gear, the transmission shaft outside is provided with helical blade and stirring vane.
The preparation method of the carboxyl silicone oil softener comprises the following specific operation steps:
the method comprises the following steps: the softener comprises the following raw materials of carboxyl silicone oil, glycerin, eugenol, deionized water, sodium carboxymethylcellulose and a thickening agent, wherein the liquid raw materials comprise the following components in parts by volume: 10 to 15 portions of carboxyl silicone oil, 0.5 to 0.7 portion of glycerol, 2 to 5 portions of eugenol and 100 to 120 portions of deionized water,
step two: carboxyl silicone oil, glycerin, eugenol and deionized water are respectively stored in a charging bucket of the charging mechanism and the first barrel, the second barrel and the third barrel, wherein the deionized water is positioned in the first barrel, the eugenol and the carboxyl silicone oil are positioned in different second barrels, the glycerin is positioned in the third barrel, the driving gear is driven to rotate through the work of a motor and is meshed with the first sprocket to drive the first thread seat and the first rotating tooth to rotate, the first sprocket drives the second sprocket to rotate through a chain to further drive the second thread seat to rotate, the first rotating tooth drives the third rotating tooth on the rotating shaft to rotate, at the moment, the second rotating tooth synchronously rotates to drive the fourth rotating tooth and the third thread seat to rotate, the first threaded rod, the second threaded rod and the third threaded rod which are in threaded connection with the first threaded seat, the second threaded seat and the third threaded seat respectively drive the first polygonal column, the second polygonal column and the third polygonal column to move so as to realize synchronous movement of the first piston, the moving distance of the first piston in the first cylinder and the second cylinder is 10 times of the moving distance of the first piston in the third cylinder in the same time, when the first piston moves downwards, the first control valve is closed, the second control valve is opened, the raw materials are added into the stirring cylinder at the moment, when the second control valve is closed, the first control valve is opened, and the first piston moves so as to realize automatic supplement of the raw materials in the first cylinder, the second cylinder and the third cylinder, and then the raw materials in the stirring cylinder are mixed and stirred for 35-40min to obtain a first mixed liquid;
step three: at the moment, the first mixed solution, the sodium carboxymethyl cellulose and the thickening agent are as follows according to the mass part ratio: 120-140 parts of first mixed solution, 1-3 parts of sodium carboxymethyl cellulose and 5-8 parts of thickening agent, and adding the sodium carboxymethyl cellulose and the thickening agent into a stirring cylinder, and stirring at constant temperature for 20-25min to obtain the carboxyl silicone oil softener.
The invention has the beneficial effects that: drive the initiative tooth through motor work and rotate, it is rotatory to realize first screw thread seat with first sprocket meshing transmission, transmission cooperation through sprocket and chain, it is rotatory to realize second screw thread seat, through the gear drive of different gear ratios, realize the rotation of third screw thread seat, and then drive the threaded rod with screw thread seat threaded connection and remove, drive first piston through multilateral post and remove, the volume of detaching first piston in the second barrel is 1 with the volume ratio of detaching first piston in the first barrel, the moving speed of first piston is the multiple of the moving speed of first piston in the third barrel in first barrel and the second barrel, therefore first barrel, second barrel and third barrel are 100 through the raw materials volume ratio of second control valve toward the churn in the interpolation: 10:1, adding deionized water through a first cylinder, adding eugenol and carboxyl silicone oil through a second different cylinder, glycerol is added through a third cylinder, namely deionized water, eugenol, carboxyl silicon and glycerol are added according to the proportion of 100:10:1, and the first control valve and the second control valve are controlled to open and close, so that the first barrel, the second barrel and the third barrel can be automatically supplemented while the accurate proportioning of the liquid raw materials is realized;
simultaneously carrying out the in-process that the raw materials added, first threaded rod drives the lifter plate and reciprocates, the lifter plate drives the head rod removal this moment, the second piston is synchronous motion in the first regulation section of thick bamboo, the third piston in the second regulation section of thick bamboo with first regulation section of thick bamboo turn-on connection this moment drives the second connecting rod and removes, realize the reciprocating motion of two-sided rack, cooperate with the driving cog of meshing, it is rotatory to drive the transmission shaft, and then it stirs to drive the raw materials in the feed cylinder that helical blade and stirring vane are rotatory, avoid the raw materials to solidify and appear deposiing.
Drawings
FIG. 1 is a schematic view of the structure of the dosing mechanism of the present invention;
FIG. 2 is a schematic view of a first rotary gear mounting arrangement of the present invention;
FIG. 3 is a partial cross-sectional view of the dosing mechanism of the present invention;
FIG. 4 is a schematic view of the chain mounting structure of the present invention;
FIG. 5 is a schematic view of the charging mechanism of the present invention;
fig. 6 is a schematic diagram of the internal structure of the bucket of the present invention.
Illustration of the drawings:
1. a dosing mechanism; 2. a first mounting plate; 3. a second mounting plate; 4. a support pillar; 5. a first cylinder; 6. a second cylinder; 7. a third cylinder; 8. a first threaded seat; 9. a first threaded rod; 10. a second screw seat; 11. a second threaded rod; 12. a third screw seat; 13. a third threaded rod; 14. a first polygonal column; 15. a second polygonal column; 16. a third polygonal column; 17. a sliding sleeve; 18. a first piston; 19. a first control valve; 20. a second control valve; 21. a motor; 22. a driving tooth; 23. a first sprocket; 24. a second sprocket; 25. a first rotating tooth; 26. a rotating shaft; 27. a second rotating tooth; 28. a third rotating tooth; 29. a fourth rotating tooth; 30. a lifting plate; 31. a first adjustment barrel; 32. a second piston; 33. a first connecting rod; 34. a mounting base; 35. a limiting plate; 36. a second adjustment barrel; 37. a third piston; 38. a second connecting rod; 39. a double-sided rack; 40. a charging bucket; 41. a transmission gear; 42. a drive shaft; 43. a helical blade; 44. a stirring blade; 45. and connecting a valve.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Specific examples are given below.
Referring to fig. 1 to 6, the preparation device of the carboxyl silicone oil softener comprises a mixing drum, a quantifying mechanism 1 and a feeding mechanism, wherein the quantifying mechanism 1 comprises a first mounting plate 2 and a second mounting plate 3, the first mounting plate 2 and the second mounting plate 3 are fixed through a support column 4, a first cylinder 5 is mounted in the middle of the second mounting plate 3, a plurality of identical second cylinders 6 and third cylinders 7 are mounted on the second mounting plate 3, first pistons 18 are slidably mounted in the first cylinder 5, the second cylinder 6 and the third cylinder 7, and a first control valve 19 and a second control valve 20 are respectively installed on the bottom sides of the first cylinder 5, the second cylinder 6 and the third cylinder 7 in a conducting manner;
in the same time, the ratio of the discharge volume of the raw materials in the first cylinder 5 to the discharge volume of the raw materials in the second cylinder 6 to the discharge volume of the raw materials in the third cylinder 7 is 100, 10, the top side of the first cylinder 5 is provided with a plurality of rotating shafts 26, the top of the rotating shafts 26 is provided with a second rotating tooth 27 and a third rotating tooth 28, the third rotating tooth 28 is meshed with the first rotating tooth 25, the outer side of the third threaded seat 12 is provided with a fourth rotating tooth 29, and the fourth rotating tooth 29 is meshed with the second rotating tooth 27, wherein the gear ratio of the first rotating tooth 25 to the third rotating tooth 28 is 1: 10:1;
the feeding mechanism comprises a mounting seat 34, a plurality of charging tanks 40 are mounted on the mounting seat 34, connecting valves 45 are mounted at the bottom sides of the charging tanks 40, the connecting valves 45 of the charging tanks 40 are respectively connected with first control valves 19 of a first barrel 5, a second barrel 6 and a third barrel 7 through connecting pipes, a plurality of first adjusting barrels 31 are mounted on a second mounting plate 3, second pistons 32 are mounted in the first adjusting barrels 31, the second pistons 32 are connected with first connecting rods 33, the top ends of the first connecting rods 33 penetrate through the first mounting plate 2 and are connected with lifting plates 30, the lifting plates 30 are connected with the top ends of first threaded rods 9, limiting plates 35 are mounted on the mounting seat 34, second adjusting barrels 36 are horizontally mounted on the limiting plates 35, the second adjusting barrels 36 are in conduction connection with the first adjusting barrels 31, third pistons 37 are mounted in the second adjusting barrels 36, and the third piston 37 is connected with the second connecting rod 38, the outer end of the second connecting rod 38 is provided with a double-sided rack 39, a bearing in the charging bucket 40 is provided with a transmission shaft 42 in a penetrating manner, the top end of the transmission shaft 42 is provided with a transmission gear 41 meshed with the double-sided rack 39, the outer side of the transmission shaft 42 is provided with a helical blade 43 and a stirring blade 44, the first threaded rod 9 drives the lifting plate 30 to move up and down, at the moment, the lifting plate 30 drives the first connecting rod 33 to move, the second piston 32 moves synchronously in the first adjusting cylinder 31, at the moment, the third piston 37 in the second adjusting cylinder 36 in conductive connection with the first adjusting cylinder 31 drives the second connecting rod 38 to move, so that the reciprocating movement of the double-sided rack 39 is realized, the transmission shaft 42 is driven to rotate by matching with the meshed transmission gear 41, and the helical blade 43 and the stirring blade 44 are driven to rotate to stir the raw materials in the charging bucket 40.
The preparation method of the carboxyl silicone oil softener comprises the following specific operation steps:
the method comprises the following steps: the softener comprises the following raw materials of carboxyl silicone oil, glycerin, eugenol, deionized water, sodium carboxymethyl cellulose and a thickening agent, wherein the liquid raw materials comprise the following components in parts by volume: 10-15 parts of carboxyl silicone oil, 0.5-0.7 part of glycerol, 2-5 parts of eugenol and 100-120 parts of deionized water,
step two: carboxyl silicone oil, glycerol, eugenol and deionized water are respectively stored in a charging bucket 40 of the charging mechanism and the first barrel 5, the second barrel 6 and the third barrel 7, wherein the deionized water is positioned in the first barrel 5, the eugenol and the carboxyl silicone oil are positioned in different second barrels 6, the glycerol is positioned in the third barrel 7, the motor 21 works to drive the driving tooth 22 to rotate and be meshed with the first sprocket 23 to drive the first thread seat 8 and the first rotating tooth 25 to rotate, the first sprocket 23 drives the second sprocket 24 to rotate through a chain to further drive the second thread seat 10 to rotate, the first rotating tooth 25 drives the third rotating tooth 28 on the rotating shaft 26 to rotate, at the moment, the second rotating tooth 27 synchronously rotates to drive the fourth rotating tooth 29 and the third thread seat 12 to rotate, at this time, the first threaded rod 9, the second threaded rod 11 and the third threaded rod 13 in threaded connection with the first threaded seat 8, the second threaded seat 10 and the third threaded seat 12 respectively drive the first polygonal column 14, the second polygonal column 15 and the third polygonal column 16 to move so as to realize synchronous movement of the first piston 18, the movement distance of the first piston 18 in the first cylinder 5 and the second cylinder 6 is 10 times of the movement distance of the first piston 18 in the third cylinder 7 in the same time, when the first piston 18 moves downwards, the first control valve 19 is closed, the second control valve 20 is opened, at this time, the raw materials are added into the stirring cylinder, when the second control valve 20 is closed, the first control valve 19 is opened, and the first piston 18 moves, so that automatic replenishment of the raw materials in the first cylinder 5, the second cylinder 6 and the third cylinder 7 is realized, and then the raw materials in the stirring cylinder are mixed and stirred for 35-40min, so as to obtain a first mixed liquid;
step three: at the moment, the first mixed solution, the sodium carboxymethyl cellulose and the thickening agent are as follows according to the mass part ratio: 120-140 parts of first mixed solution, 1-3 parts of sodium carboxymethyl cellulose and 5-8 parts of thickening agent, and adding the sodium carboxymethyl cellulose and the thickening agent into a stirring cylinder, and stirring at constant temperature for 20-25min to obtain the carboxyl silicone oil softener.
The driving gear 22 is driven to rotate through the work of the motor 21, the first thread seat 8 is driven to rotate through the meshing transmission with the first sprocket 23, the second thread seat 10 is driven to rotate through the transmission matching of the sprockets and the chain, the third thread seat 12 is driven to rotate through the gear transmission with different gear ratios, and further the threaded rod in threaded connection with the thread seats is driven to move, the first piston 18 is driven to move through the polygonal column, the volume ratio of the first piston 18 removed in the second cylinder 6 to the volume ratio of the first piston 18 removed in the first cylinder 5 is 1: 10:1, deionized water is added through a first cylinder 5, eugenol and carboxyl silicone oil are added through a second cylinder 6 which is different from the first cylinder, and glycerin is added through a third cylinder 7, namely deionized water, eugenol, carboxyl silicone oil and glycerin are conveniently added in a way that the deionized water, the eugenol, the carboxyl silicone oil and the glycerin are 100:10:1, and the first control valve 19 and the second control valve 20 are controlled to open and close, so that the first barrel 5, the second barrel 6 and the third barrel 7 can be supplemented automatically while the precise proportioning of the liquid raw materials can be realized;
simultaneously in the in-process of carrying out the raw materials and adding, first threaded rod 9 drives lifter plate 30 and reciprocates, lifter plate 30 drives first connecting rod 33 and removes this moment, second piston 32 synchronous motion in first regulation section of thick bamboo 31, third piston 37 in the second regulation section of thick bamboo 36 with first regulation section of thick bamboo 31 turn-on connection drives second connecting rod 38 and removes this moment, realize the reciprocating motion of two-sided rack 39, with the cooperation of engaged driving tooth 41, it is rotatory to drive transmission shaft 42, and then it stirs the raw materials in material jar 40 to drive helical blade 43 and stirring vane 44 rotation, avoid the raw materials to solidify and appear deposiing.
In the process of proportioning the liquid raw materials, 100 parts of deionized water, 15 parts of carboxyl silicone oil, 5 parts of eugenol and 0.7 part of glycerol are proportioned, and the volume ratio of the deionized water to the carboxyl silicone oil to the eugenol to the glycerol is as follows: 1000:150:50:7, the adding volume of the cylinder body is taken as a basic unit every time, at the moment, deionized water of the first cylinder body 5 is added for 10 times, carboxyl silicone oil of the second cylinder body 6 is added for 15 times, eugenol of the second cylinder body 6 is added for 5 times, glycerin of the third cylinder body 7 is added for 7 times, the deionized water is added simultaneously through the work of the motor 21, after the deionized water is added into the 5 th time, the second control valve 20 on the eugenol second cylinder body 6 is closed, after the eugenol is added into the 5 th time, the second control valve 20 on the third cylinder body 7 is closed, after the eugenol is added into the 10 th time, the second control valve 20 on the first cylinder body 5 is closed, after the eugenol is added into the 5 th time, the second control valve 20 on the carboxyl silicone oil second cylinder body 6 is closed, and accurate and automatic adding of liquid raw materials is realized according to different proportions.
The above description is only for the preferred embodiment of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art should be considered as the technical solutions and the inventive concepts of the present invention within the technical scope of the present invention.

Claims (10)

1. The preparation device of the carboxyl silicone oil softener is characterized by comprising a stirring cylinder, a quantifying mechanism (1) and a feeding mechanism, wherein the quantifying mechanism (1) comprises a first mounting plate (2) and a second mounting plate (3), the first mounting plate (2) and the second mounting plate (3) are fixed through a support column (4), a first cylinder (5) is mounted in the middle of the second mounting plate (3), a plurality of identical second cylinders (6) and third cylinders (7) are mounted on the second mounting plate (3), first pistons (18) are mounted inside the first cylinder (5), the second cylinder (6) and the third cylinder (7) in a sliding mode, and a first control valve (19) and a second control valve (20) are respectively installed on the bottom sides of the first cylinder (5), the second cylinder (6) and the third cylinder (7) in a conducting mode;
the feeding mechanism comprises a mounting seat (34), a plurality of charging tanks (40) are mounted on the mounting seat (34), connecting valves (45) are mounted at the bottom sides of the charging tanks (40), and the connecting valves (45) of the plurality of charging tanks (40) are respectively connected with first control valves (19) of a first cylinder (5), a second cylinder (6) and a third cylinder (7) through connecting pipes;
in the same time, the ratio of the discharge volume of the raw material in the first cylinder (5) to the discharge volume of the raw material in the second cylinder (6) and the discharge volume of the raw material in the third cylinder (7) is 100.
2. The preparation facilities of carboxyl silicone oil softener of claim 1, characterized in that, the same first screw thread seat (8), a plurality of second screw thread seat (10) and a plurality of third screw thread seat (12) are installed to first mounting panel (2) inner bearing, first threaded rod (9) is installed through to first screw thread seat (8) internal thread, second threaded rod (11) is installed through to second screw thread seat (10) inside, third screw thread seat (12) internal thread is installed through to third threaded rod (13), first threaded rod (9) and second threaded rod (11) and third threaded rod (13) are same specification threaded rod.
3. The preparation facilities of carboxyl silicone oil softener according to claim 2, characterized in that, first multilateral post (14) is installed to first threaded rod (9) bottom, second multilateral post (15) is installed to second threaded rod (11) bottom, third multilateral post (16) is installed to third threaded rod (13) bottom, and first multilateral post (14), second multilateral post (15) and third multilateral post (16) all are connected with first piston (18), and first multilateral post (14), second multilateral post (15) and third multilateral post (16) respectively with first barrel (5), second barrel (6) and sliding sleeve (17) adaptation in the third barrel (7), and the thickness of a plurality of first piston (18) is all the same.
4. The preparation device of carboxyl silicone oil softener according to claim 1, wherein the second cylinder (6) and the third cylinder (7) are the same in size, the internal height of the second cylinder (6) is the same as that of the first cylinder (5), and the ratio of the volume of the second cylinder (6) excluding the first piston (18) to the volume of the first cylinder (5) excluding the first piston (18) is 1.
5. The preparation device of carboxyl silicone oil softener according to claim 1, wherein a first sprocket (23) and a first rotating tooth (25) are installed on the outer side of the first threaded seat (8), a motor (21) is installed on the top side of the first mounting plate (2), a driving tooth (22) meshed with the first sprocket (23) is installed at the output end of the motor (21), a second sprocket (24) is installed on the outer side of the second threaded seat (10), and the first sprocket (23) and the second sprocket (24) are connected through chain transmission.
6. The preparation device of carboxyl silicone oil softener according to claim 5, characterized in that a plurality of rotating shafts (26) are installed on the top side of the first cylinder (5), a second rotating tooth (27) and a third rotating tooth (28) are installed on the top of the rotating shafts (26), the third rotating tooth (28) is meshed with the first rotating tooth (25), a fourth rotating tooth (29) is installed on the outer side of the third threaded seat (12), and the fourth rotating tooth (29) is meshed with the second rotating tooth (27), wherein the gear ratio of the first rotating tooth (25) to the third rotating tooth (28) is 1.
7. The preparation device of carboxyl silicone oil softener according to claim 1, wherein the second mounting plate (3) is provided with a plurality of first adjusting cylinders (31), the first adjusting cylinders (31) are internally provided with second pistons (32), the second pistons (32) are connected with first connecting rods (33), the top ends of the first connecting rods (33) penetrate through the first mounting plate (2) and are connected with the lifting plate (30), and the lifting plate (30) is connected with the top ends of the first threaded rods (9).
8. The preparation facilities of carboxyl silicone oil softener of claim 5, characterized in that, install limiting plate (35) on mount pad (34), horizontal installation has a second to adjust a section of thick bamboo (36) on limiting plate (35), and a second regulation section of thick bamboo (36) and a first regulation section of thick bamboo (31) turn-on connection, install third piston (37) in the second regulation section of thick bamboo (36), and third piston (37) are connected with second connecting rod (38), two-sided rack (39) are installed to second connecting rod (38) outer end.
9. The preparation device of carboxyl silicone oil softener according to claim 5, characterized in that the inside bearing of the charging bucket (40) is provided with a transmission shaft (42) in a penetrating way, the top end of the transmission shaft (42) is provided with a transmission gear (41) meshed with the double-sided rack (39), and the outer side of the transmission shaft (42) is provided with a helical blade (43) and a stirring blade (44).
10. The preparation method of the carboxyl silicone oil softener according to any one of claims 1 to 9, characterized by comprising the following specific operation steps:
the method comprises the following steps: the softener comprises the following raw materials of carboxyl silicone oil, glycerin, eugenol, deionized water, sodium carboxymethyl cellulose and a thickening agent, wherein the liquid raw materials comprise the following components in parts by volume: 10 to 15 portions of carboxyl silicone oil, 0.5 to 0.7 portion of glycerol, 2 to 5 portions of eugenol and 100 to 120 portions of deionized water,
step two: carboxyl silicone oil, glycerol, eugenol and deionized water are stored in charging bucket (40) and first barrel (5) of feeding mechanism respectively, second barrel (6) and third barrel (7), wherein deionized water is located first barrel (5), eugenol and carboxyl silicone oil are located different second barrel (6), glycerol is located third barrel (7), it is rotatory to drive driving tooth (22) through motor (21) work, mesh with first sprocket (23), it is rotatory to drive first screw thread seat (8) and first commentaries on classics tooth (25), first sprocket (23) drive second sprocket (24) through the chain and rotate, and then drive second screw thread seat (10) and rotate, first commentaries on classics tooth (25) drive third commentaries on classics tooth (28) on pivot (26) and rotate, second commentaries on classics tooth (27) synchronous rotation this moment, drive fourth commentaries on classics tooth (29) and third screw thread seat (12) and rotate, this moment with first screw thread seat (8), second screw thread seat (10) and third screw thread seat (12) drive the same threaded rod (18) and the third screw rod (18) and the synchronous piston (16) of second side of the same side of the first screw rod (11) and the second side of the first screw rod (11) and the second side of the synchronous piston (16), it is realized that the same distance of the barrel (18) and the first side screw rod (11) and the piston (18) move respectively, the piston (16) move, the same side cylinder (16) move, the barrel (14) move, the same side cylinder (18) move, the same side piston (16) move in the barrel (11) and the first side piston (11) of the second side piston (11) move, the piston (16) move, the piston (13) move, the piston is realized The moving distance of a first piston (18) in the three cylinders (7) is 10 times, when the first piston (18) moves downwards, a first control valve (19) is closed, a second control valve (20) is opened, the raw materials are added into the mixing cylinder at the moment, when the second control valve (20) is closed, the first control valve (19) is opened, and the first piston (18) moves, so that the raw materials in the first cylinder (5), the second cylinder (6) and the third cylinder (7) are automatically supplemented, and then the raw materials in the mixing cylinder are mixed and stirred for 35-40min, so that first mixed liquid is obtained;
step three: at the moment, the first mixed solution, the sodium carboxymethyl cellulose and the thickening agent are as follows according to the mass part ratio: 120-140 parts of first mixed solution, 1-3 parts of sodium carboxymethyl cellulose and 5-8 parts of thickening agent, and adding the sodium carboxymethyl cellulose and the thickening agent into a stirring cylinder, and stirring at constant temperature for 20-25min to obtain the carboxyl silicone oil softener.
CN202210891226.XA 2022-07-27 2022-07-27 Preparation method and device of carboxyl silicone oil softener Active CN115400635B (en)

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