CN115350119B - 一种双色搭配、表面雕花的护肤膏体及其制备方法 - Google Patents

一种双色搭配、表面雕花的护肤膏体及其制备方法 Download PDF

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CN115350119B
CN115350119B CN202210882511.5A CN202210882511A CN115350119B CN 115350119 B CN115350119 B CN 115350119B CN 202210882511 A CN202210882511 A CN 202210882511A CN 115350119 B CN115350119 B CN 115350119B
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CN115350119A (zh
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孟铁钢
卢海珍
聂小凤
邱孟德
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Guangzhou Q Max Cosmetics Co ltd
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Abstract

本发明涉及一种双色搭配、表面雕花的护肤膏体及其制备方法，所述双色搭配、表面雕花的护肤膏体由组分A和组分B共混得到，所述组分A和所述组分B均包括质量分数如下的成分：稳定剂0.01‑5％、彩色活性功效物、增稠剂0.01‑5％、保湿剂0.1‑20％、润肤剂0.5‑30％、乳化剂0.1‑10％、防腐剂0.1‑5％、皮肤调理剂0.0001‑20％、溶剂余量；其中，所述稳定剂包括PEG‑240/HDI共聚物双‑癸基十四醇聚醚‑20醚、藻酸钠和蜂蜡。本发明通过复配而成的稳定剂使膏体表面图案清晰、美观，同时显著提升了产品的稳定性，大大增强了产品体验，具有良好的应用前景。

Description

一种双色搭配、表面雕花的护肤膏体及其制备方法
技术领域
本发明涉及护肤品技术领域，特别是涉及一种双色搭配、表面雕花的护肤膏体及其制备方法。
背景技术
随着科技的进步和人们的水平的提高，人们对护肤品的要求越来越高，无论是从功效上还是从护肤品的包装或料体外观状态或使用形式上的要求。目前市场上护肤品的形态也有各式各样，都有从不同的角度吸引消费者的眼球。形态外观的特显，也能让消费者更深刻认知护肤功效物的艺术性。
然而当前的护肤品中，以多种颜色搭配进行雕花工艺的产品效果较差，无法达到图案边界清晰、膏体外观稳定、产品细腻美观的效果，因此难以得到市场和消费者的认可，造成了产品的缺失。
综上所述，亟需研发一种新的技术方案，以解决现有技术中存在的缺陷。
发明内容
基于此，本发明开发了一种双色搭配、表面雕花的护肤膏体及其制备方法，本发明采用多种天然绿色的彩色活性功效物赋予产品双色搭配雕花的效果，并通过PEG-240/HDI共聚物双-癸基十四醇聚醚-20醚、藻酸钠、蜂蜡复配为稳定剂，使膏体表面图案清晰、美观，同时显著提升了产品的稳定性，大大增强了产品体验。
本发明的一个目的在于，提供一种双色搭配、表面雕花的护肤膏体，所述双色搭配、表面雕花的护肤膏体由组分A和组分B共混得到，所述组分A和所述组分B均包括质量分数如下的成分：
Figure BDA0003764750750000011
Figure BDA0003764750750000021
且
组分A中还包括彩色活性功效物0.0001-20％；
组分B中还包括彩色活性功效物0.0001-20％；
其中，所述稳定剂包括PEG-240/HDI共聚物双-癸基十四醇聚醚-20醚、藻酸钠和蜂蜡。
PEG-240/HDI共聚物双-癸基十四醇聚醚-20醚是一种缔合性的高分子，具有自我形态恢复功能的增稠稳定剂；藻酸钠水溶凝胶后具有独特的交联网状结构，有较好的延伸性，同时是一种高温不可逆凝胶，有粘合和悬浮稳定的作用；蜂蜡熔点为62-65℃，质地柔润，是一种具有自乳化能力的天然蜡；令人意外的发现，这三种物质复配而成的稳定剂能够产生良好的协同效应，并且与彩色活性功效物的相容性较好，可以有效改善膏体的流变性以及自我形态修复的效果，使产品能在多种条件下保持稳定、美观、均匀的外观。
进一步地，所述组分A和所述组分B均包括质量分数如下的成分：
Figure BDA0003764750750000022
且
组分A中还包括彩色活性功效物0.0001-20％；
组分B中还包括彩色活性功效物0.0001-20％。
优选地，组分A中还包括彩色活性功效物1-3％；
优选地，组分B中还包括彩色活性功效物0.01-0.5％。
进一步地，所述彩色活性功效物选自蓝铜肽、虾青素、花青素、孔雀石、沙棘果油、叶绿素、玫瑰果油、炭粉、生物活性提取物中的一种或多种。
进一步地，所述组分A中的彩色活性功效物和所述组分B中的彩色活性功效物具有不同颜色。
进一步地，所述保湿剂选自甘油、甲基丙二醇、丁二醇和透明质酸钠中的一种或多种。
进一步地，所述增稠剂选自丙烯酰二甲基牛磺酸铵/VP共聚物、黄原胶、羟乙基纤维素和水解小核菌胶中的一种或多种。
进一步地，所述润肤剂选自辛酸/癸酸甘油三酯、聚二甲基硅氧烷、C12-15醇苯甲酸酯、牛油果树果脂、异壬酸异壬酯中的一种或多种。
进一步地，所述乳化剂选自鲸蜡硬脂醇、鲸蜡硬脂基葡糖苷、PEG-100硬脂酸酯、甘油硬脂酸酯、鲸蜡醇磷酸酯钾中的一种或多种。
进一步地，所述防腐剂选自对羟基苯乙酮、1,2-己二醇、甘油辛酸酯和辛酰羟肟酸中的一种或多种。
进一步地，所述溶剂为去离子水。
本发明的另一个目的在于，提供上述双色搭配、表面雕花的护肤膏体的制备方法，包括如下步骤：
S1.将溶剂、保湿剂、增稠剂混合并加热溶解，得到组分1；
S2.将润肤剂、乳化剂混合并加热溶解，得到组分2；
S3.将组分1和组分2趁热混合后，进行均质乳化，然后加入稳定剂，降温后加入其他剩余成分，搅拌均匀得到组分A；
S4.采用相同方法制备组分B，然后将所述组分A和所述组分B共混，得到所述双色搭配、表面雕花的护肤膏体。
本发明具有以下有益效果：
本发明采用天然绿色的活性功效物为原料制备了具有不同颜色的两种组分A和B，通过组分A和B的混合使产品具有双色搭配雕花的效果，并通过PEG-240/HDI共聚物双-癸基十四醇聚醚-20醚、藻酸钠、蜂蜡复配产生协同作用，改善膏体的流变性以及自我形态修复的效果，使不同颜色组分混合后保持均匀、相容性好，同时显著提升了产品的稳定性，在多种条件下均能保持膏体均一、光滑、铺展性良好，保证了产品的美观和流动性，大大增强了产品的使用体验，具有良好的应用前景。
附图说明
图1示出了测试例2中侧放稳定性测试结果图；
其中，
图1(a)为实施例1样品测试前形貌图；图1(b)为实施例1样品倒立放置24h后结果图；
图1(c)为实施例2样品测试前形貌图；图1(d)为实施例2样品倒立放置24h后结果图；
图1(e)为实施例3样品测试前形貌图；图1(f)为实施例3样品倒立放置24h后结果图；
图1(g)为实施例4样品测试前形貌图；图1(h)为实施例4样品倒立放置24h后结果图；
图1(i)为对比例1样品测试前形貌图；图1(j)为对比例1样品倒立放置24h后结果图；
图1(k)为对比例2样品测试前形貌图；图1(l)为对比例2样品倒立放置24h后结果图；
图1(m)为对比例3样品测试前形貌图；图1(n)为对比例3样品倒立放置24h后结果图。
具体实施方式
为了更清楚地说明本发明的技术方案，列举如下实施例。实施例中所出现的原料、反应和后处理手段，除非特别声明，均为市面上常见原料，以及本领域技术人员所熟知的技术手段。
本发明实施例中的材料均购买自市场。
实施例1-4双色搭配、表面雕花的护肤膏体中各个成分和相应质量分数，如表1所示。
表1实施例1-4中各成分及其质量分数(含量)
Figure BDA0003764750750000041
Figure BDA0003764750750000051
实施例1-4双色搭配、表面雕花的护肤膏体的制备方法均为：
S1.按上述质量分数，将溶剂、保湿剂、增稠剂混合并加热至85℃溶解，得到组分1；
S2.将润肤剂、乳化剂混合并加热至80℃溶解，得到组分2；
S3.温度接近一致时，将组分1和组分2趁热混合并进行均质乳化，然后保温20min加入稳定剂，降温至45℃后加入其他剩余成分，搅拌均匀得到外观黑色的组分A；
S4.采用相同方法制备外观白色的组分B，然后将所述组分A和所述组分B共混，得到所述双色搭配、表面雕花的护肤膏体。
基于实施例1设置对比例1-3，对比例1-3中各个成分和相应质量分数，如表2所示。
表2对比例1-3中各成分及其质量分数(含量)
Figure BDA0003764750750000052
Figure BDA0003764750750000061
对比例1-3的与实施例1的区别在于：对稳定剂中的成分进行了替换，其他制备方法和步骤均相同。
测试例1
对实施例1-4和对比例1-3制备的双色搭配、表面雕花的护肤膏体进行高低温稳定性测试。
测试方法：
取实施例1-4和对比例1-3制备的双色搭配、表面雕花的护肤膏体各50g分别置于广口瓶中，分为7组，每组设置3个样品，密封后，分别置于室温、48℃烘箱、-18℃冰箱中，每周取出一次放置至室温后，观察并记录样品外观的变化，测试时间共3个月。
测试结果如表3所示。
表3稳定性测试结果
Figure BDA0003764750750000062
根据表1可以看出，实施例1-4制备的样品具有良好的稳定性，能够维持多种组分间较好的相容性，从而保证产品在高低温环境下均能保持流畅、光滑的形貌，且延展性较好；而对比例1-3将PEG-240/HDI共聚物双-癸基十四醇聚醚-20醚、藻酸钠或蜂蜡替换为同类稳定剂后，样品的稳定性降低，外观产生了析出、粗糙、浑浊等变化，大大降低了产品的使用体验和效果，说明上述三种成分复配后能够产生良好的协同效应，有效提高了产品的稳定性，对维持产品形态具有重要作用。
测试例2
对实施例1-4和对比例1-3制备的双色搭配、表面雕花的护肤膏体进行侧放稳定性测试。
测试方法：
取实施例1-4和对比例1-3制备的双色搭配、表面雕花的护肤膏体各50g分别置于广口瓶中，分为4组，每个样品均倒立放置24h，观察并记录样品外观的变化。
测试结果如图1所示。
图1示出了侧放稳定性测试结果图；
其中，
图1(a)为实施例1样品测试前形貌图；图1(b)为实施例1样品倒立放置24h后结果图；
图1(c)为实施例2样品测试前形貌图；图1(d)为实施例2样品倒立放置24h后结果图；
图1(e)为实施例3样品测试前形貌图；图1(f)为实施例3样品倒立放置24h后结果图；
图1(g)为实施例4样品测试前形貌图；图1(h)为实施例4样品倒立放置24h后结果图；
图1(i)为对比例1样品测试前形貌图；图1(j)为对比例1样品倒立放置24h后结果图；
图1(k)为对比例2样品测试前形貌图；图1(l)为对比例2样品倒立放置24h后结果图；
图1(m)为对比例3样品测试前形貌图；图1(n)为对比例3样品倒立放置24h后结果图。
根据图1可以得出，对比例1倒立放置24h后表面有蜡析出、不光滑，对比例2-3无法保持稳定、清晰的分界，产品中的组分无法形成稳定的外观，而实施例1-4由于加入了PEG-240/HDI共聚物双-癸基十四醇聚醚-20醚、藻酸钠、蜂蜡复配的稳定剂，通过其协同作用大大提升了产品的侧放稳定性，优于替换了成分的对比例，外观保持清晰、美观、均匀，本发明具有良好的应用前景。
对于本领域技术人员而言，显然本发明不限于上述示范性实施例的细节，而且在不背离本发明的精神或基本特征的情况下，能够以其他的具体形式实现本发明。因此，无论从哪一点来看，均应将实施例看作是示范性的，而且是非限制性的，本发明的范围由所附权利要求而不是上述说明限定，因此旨在将落在权利要求的等同要件的含义和范围内的所有变化囊括在本发明内。
此外，应当理解，虽然本说明书按照实施方式加以描述，但并非每个实施方式仅包含一个独立的技术方案，说明书的这种叙述方式仅仅是为清楚起见，本领域技术人员应当将说明书作为一个整体，各实施例中的技术方案也可以经适当组合，形成本领域技术人员可以理解的其他实施方式。

Claims (3)

1.一种双色搭配、表面雕花的护肤膏体，其特征在于，所述双色搭配、表面雕花的护肤膏体由组分A和组分B共混得到，所述组分A和所述组分B均包括质量分数如下的成分：
Figure FDA0004223987050000011
且
组分A中还包括彩色活性功效物1％；
组分B中还包括彩色活性功效物0.1％；
其中，所述稳定剂包括PEG-240/HDI共聚物双-癸基十四醇聚醚-20醚、藻酸钠和蜂蜡；
所述组分A中的彩色活性功效物和所述组分B中的彩色活性功效物具有不同颜色；
所述保湿剂选自甘油、甲基丙二醇、丁二醇和透明质酸钠中的一种或多种；
所述增稠剂选自丙烯酰二甲基牛磺酸铵/VP共聚物、黄原胶、羟乙基纤维素和水解小核菌胶中的一种或多种；
所述润肤剂选自辛酸/癸酸甘油三酯、聚二甲基硅氧烷、C12-15醇苯甲酸酯、牛油果树果脂、异壬酸异壬酯中的一种或多种；
所述乳化剂选自鲸蜡硬脂醇、鲸蜡硬脂基葡糖苷、PEG-100硬脂酸酯、甘油硬脂酸酯、鲸蜡醇磷酸酯钾中的一种或多种；
所述防腐剂选自对羟基苯乙酮、1,2-己二醇、甘油辛酸酯和辛酰羟肟酸中的一种或多种；
所述溶剂为去离子水。
2.根据权利要求1所述双色搭配、表面雕花的护肤膏体，其特征在于，所述彩色活性功效物选自蓝铜肽、虾青素、花青素、孔雀石、沙棘果油、叶绿素、玫瑰果油、炭粉、白松露菌提取物中的一种或多种。
3.权利要求1-2任一项所述双色搭配、表面雕花的护肤膏体的制备方法，其特征在于，包括如下步骤：
S1.将溶剂、保湿剂、增稠剂混合并加热溶解，得到组分1；
S2.将润肤剂、乳化剂混合并加热溶解，得到组分2；
S3.将组分1和组分2趁热混合后，进行均质乳化，然后加入稳定剂，降温后加入其他剩余成分，搅拌均匀得到组分A；
S4.采用相同方法制备组分B，然后将所述组分A和所述组分B共混，得到所述双色搭配、表面雕花的护肤膏体。
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