CN115317411B - Plant repairing composition and lip product containing same - Google Patents

Plant repairing composition and lip product containing same Download PDF

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Publication number
CN115317411B
CN115317411B CN202211065598.3A CN202211065598A CN115317411B CN 115317411 B CN115317411 B CN 115317411B CN 202211065598 A CN202211065598 A CN 202211065598A CN 115317411 B CN115317411 B CN 115317411B
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China
Prior art keywords
wax
plant
lip
composition
repairing composition
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CN202211065598.3A
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CN115317411A (en
Inventor
苗锋
沈玲玲
刘冉
姚瑶
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Shanghai Yingcai Biotechnology Co ltd
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Shanghai Yingcai Biotechnology Co ltd
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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • A61K8/25—Silicon; Compounds thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • A61K8/26—Aluminium; Compounds thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/31—Hydrocarbons
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34—Alcohols
    • A61K8/342—Alcohols having more than seven atoms in an unbroken chain
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/37—Esters of carboxylic acids
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • A61Q19/001—Preparations for care of the lips
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59—Mixtures
    • A61K2800/592—Mixtures of compounds complementing their respective functions
    • A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18

Abstract

The application relates to the technical field of cosmetics, in particular to the field of IPC A61K8, and more particularly relates to a plant repairing composition and a lip product containing the composition. The plant repairing composition comprises the following components in percentage by weight: 30-70% of sunflower seed oil, 15-35% of jojoba seed oil and 15-35% of squalane. The lip product containing the plant repairing composition comprises the following components in percentage by weight: 10-30% of a forming agent, 1-6% of a plant repairing composition, 60-80% of a skin conditioning agent and 2-10% of a filling agent. The natural plant component is selected as the main component of the plant repairing composition, so that the natural plant repairing composition can provide good safety for lip products such as lip products containing the composition, has a certain repairing and moisturizing effect, can improve the condition of cracks of lips, and has excellent stability.

Description

Plant repairing composition and lip product containing same
Technical Field
The application relates to the technical field of cosmetics, in particular to the field of IPC A61K8, and more particularly relates to a plant repairing composition and a lip product containing the composition.
Background
Compared with facial skin, the lips skin has the following characteristics: 1) The cuticle resisting external stimulus is very thin, and the facial skin is generally 15-16 layers, but the lip skin is only 1/3, namely 3-4 layers; 2) There are no sweat glands and sebaceous glands, so the lip skin cannot be protected by secreting sweat and sebaceous glands; 3) No hair; 4) The skin has weak barrier function, and the percutaneous water loss speed is far higher than that of facial skin; because of these features of the lip skin, it is very dry, dull, lose elasticity, age faster, produce various lip problems such as inflammation, chapping, etc.
The main components of the common lip balm are grease and wax, and the main components of raw materials used in the lip balm products on the market are beeswax, ceresin, castor oil, lanolin, vaseline and the like, namely the main components are the wax raw materials and animal or mineral grease. Although the lip balm prepared by the method can temporarily and effectively relieve the problem of dryness and water loss of lips, the sustained effect lasts for a short time, long-term and effective care and deep care cannot be performed on the skin of the lips, and the skin cannot be effectively improved; in addition, the lip balm prepared by taking the wax raw materials and animal or mineral grease as main materials is easy to have chemical residues after long-term use, is easy to cause lip allergy, brings more serious injury to lip skin, and is suitable for light people to peel, dry and crack, red, swelling and itching, even causes lesions and canceration and threatens the health of people.
Due to the repetition of new crown epidemic situations of the COVID 19, the demand of consumers for green components is increasing; at the same time, the mask becomes an indispensable daily commodity, and the lip skin becomes more sensitive due to the moisture-sealed environment under the mask, so the requirement for the safety of raw materials in the lipstick formula becomes higher. Consumers are also more inclined to use natural or plant-derived materials as the base system for the formulation.
In the prior art, the patent document with the authority of publication number CN106726706B discloses a full-oil lip gloss containing water or water-soluble components and a preparation method thereof, and the prepared lip product containing the composition has lasting moisturizing effect and good stability, but has limited repairing effect on lips.
Patent document CN111494250B discloses a plant lip balm and a preparation method thereof, and by adding natural plant wax base, natural plant oil and plant oil derivatives, a plant lip balm with good stability and high moisturizing durability is obtained, but the lip balm has limited repairing effect on lips.
Disclosure of Invention
In order to solve the problems, the first aspect of the application provides a plant repairing composition, which comprises the following components in percentage by weight: 30-70% of sunflower (HELIANTHUS ANNUUS) seed oil, 15-35% of jojoba (SIMMONDSIA CHINENSIS) seed oil and 15-35% of squalane.
Preferably, the weight ratio of jojoba seed oil to squalane is (1-2.1): 1.
in some preferred embodiments, the sunflower seed oil is purchased from plicon corporation as SUNFLOWER OIL HIGH OLEIC.
In some preferred embodiments, the JOJOBA seed oil is purchased from Vantage Specialty Ingredients, inc.
In some preferred embodiments, the squalane is purchased from SOPHIM corporation
Preferably, the plant repair composition is prepared by the following steps: mixing the raw materials according to weight percentage, and stirring uniformly at 75-85 ℃.
The applicant has found unexpectedly that the weight ratio is chosen to be (1-2.1): the jojoba seed oil and squalane which are used as main components of the plant repairing composition can play a synergistic effect in a system with sunflower seed oil as a solvent, so that the prepared composition has remarkable moisturizing and repairing effects, can be applied to lip products to improve the moisturizing and moisturizing properties and reduce the skin irritation of the lip products, and is of plant origin and green and mild in components. However, if it is to be applied to lip balm, only the plant care composition is not shaped.
The second aspect of the present application provides a lip product of the plant repair composition comprising, in weight percent: 10-30% of a forming agent, 1-6% of a plant repairing composition, 60-80% of a skin conditioning agent and 2-10% of a filling agent.
Preferably, the shaping agent is one or more of candelilla (EUPHORBIA CERIFERA) wax, carnauba (COPERNICIA CERIFERA) wax, compound wax, sunflower (HELIANTHUS ANNUUS) seed wax, myrgeese longifolia (myrgescellentum abuch) -ham) wax, rhos vaccinum (RHUS vaccadanea) fruit wax; further preferred are candelilla wax, carnauba wax, sunflower seed wax and compound waxes.
Preferably, the weight ratio of candelilla wax, carnauba wax, sunflower seed wax and composite wax is (8-12): (3-6): (2-5): 1, a step of; further preferred is 10:5:4:1.
Preferably, the candelilla wax has a melting point of 65-75deg.C and a hydrocarbon content of 45-55wt%; further preferably, the candelilla wax has a melting point of 68-73 ℃ and a hydrocarbon content of 50wt%.
Preferably, the melting point of the carnauba wax is 80-90 ℃; further preferably, the temperature is 82-86 ℃.
Preferably, the sunflower seed wax has a melting point of 70-80 ℃; further preferably, the temperature is 74-80 ℃.
Preferably, the compound wax comprises, by weight, 50-75% of jojoba esters, 25-50% of sunflower seed wax, 1-5% of wattle (ACACIA DECURRRENS) flower wax, 5-3 1% of polyglycerol and 0.02% of tocopherol; further preferably, the compound wax comprises 62% of jojoba esters, 32% of sunflower seed wax, 2.98% of vitex negundo flower wax, 33% of polyglycerol and 0.02% of tocopherol in percentage by weight.
In some preferred embodiments, the candelilla wax is purchased from Henan Fumei corporationCandelilla wax 5501.
In some preferred embodiments, the carnauba wax is purchased from Henan Fumei corporationCarnauba wax 2012.
In some preferred embodiments, the sunflower seed wax is purchased from Henan FumeiSunflower wax 5301.
In some preferred embodiments, the composite wax is purchased from ACTICIRE MB, manufactured by the company of the carnauba company.
The applicant found that the selection of specific candelilla wax, carnauba wax and sunflower seed wax as the shaping agent can produce a lip balm with suitable hardness and good skin-moistening properties. This is probably due to the fact that candelilla wax, carnauba wax and sunflower seed wax are all purely natural vegetable waxes and have close melting points, so that not only are the three waxes well compatible, but also the excellent oil binding ability of the candelilla wax and the sunflower seed wax enables the candelilla wax and the plant repairing composition to have good compatibility, so that the hardness and crystal structure of the formula can be improved, the film forming property of the prepared lip balm is improved, and the water locking and moisturizing capabilities of the lip balm are further improved. However, lip balms prepared from only three kinds of waxes have rough and sticky touch feeling when used. The applicant has unexpectedly found that the use of a complex wax of specific composition and when the candelilla wax, carnauba wax, sunflower seed wax and complex wax are in a weight ratio of (8-12): (3-6): (2-5): 1, the prepared lip balm not only has excellent film forming property and skin moisturizing property, but also has soft and light touch feeling, and reduces sticky feeling, thereby improving sensory effect.
Preferably, the skin conditioning agent is one or more of polyglycerol-2 triisostearate, caprylic/capric/myristic/stearic triglycerides, octyldodecanol, caprylic/capric triglycerides, botanical extracts, hydrogenated lecithin, ceramide, nicotinamide, polypeptides, fullerenes, salicylic acid; further preferred are polyglycerol-2 triisostearate, caprylic/capric/myristic/stearic triglycerides, octyldodecanol, caprylic/capric triglycerides.
Preferably, the weight ratio of the polyglycerol-2 triisostearate, caprylic/capric/myristic/stearic triglyceride, octyldodecanol and caprylic/capric triglyceride is (15-25): (1-3): (1-2): 1, a step of; further preferred is 55:7:5:3.
In some preferred embodiments, the polyglycerol-2 triisostearate is purchased from COSMOL 43V, manufactured by The Nisshin OilliO Group, ltd.
In some advantagesIn an alternative, the caprylic/capric/myristic/stearic triglyceride is purchased from IOI oils Inc378。
In some preferred embodiments, the octyldodecanol is purchased from RISONOL 20SP, manufactured by kokokoyou.
In some preferred embodiments, the caprylic/capric triglyceride is purchased from BASF318RC。
The applicant has found unexpectedly that the weight ratio is selected to be (15-25): (1-3): (1-2): the polyglyceryl-2 triisostearate, caprylic acid/capric acid/myristic acid/stearic acid triglyceride, octyl dodecanol and caprylic acid/capric acid triglyceride of the formula 1 are used as skin conditioning agents, so that the stability of the lip balm can be improved, and meanwhile, the moisturizing capability of the lip balm can be further improved. The inorganic filler can be well dispersed in the grease system due to the synergistic effect of the polyglycerol-2 triisostearate, the octyl dodecanol and the caprylic/capric triglyceride, so that the stability of the prepared lip balm is improved, and the condition that the lip balm is easy to sweat at high temperature is avoided; the caprylic acid/capric acid/myristic acid/stearic acid triglyceride and caprylic acid/capric acid triglyceride can improve the penetrability of skin, and the effective components such as the phytoremediation composition can permeate into the deep skin of lips to achieve the effects of deep repair and moisture retention, so that the moistening and moisture retention capacity of the skin is further improved; in addition, the octyl dodecanol can promote the film forming property of caprylic acid/capric acid/myristic acid/stearic acid triglyceride, improve skin feel, avoid greasiness and play a role in deeply moistening and locking water. However, if the caprylic acid/capric acid/myristic acid/stearic acid triglyceride is added too much, the risk of acne may occur due to too high blocking degree, so that the inventor can prevent the acne phenomenon caused by too high blocking degree while deeply locking water by controlling the adding amount of the caprylic acid/capric acid/myristic acid/stearic acid triglyceride and adding a proper amount of non-blocking softener caprylic acid/capric acid triglyceride, so that the lip skin can be locked and moisturized and the skin is not blocked.
Preferably, the filler is one or more of silica, mica, talc, kaolin, bentonite, rutile and calcite; further preferred are silica and mica.
Preferably, the silica has an average particle size of 2 to 15 μm and an oil absorption value of 0.5 to 2.0cc/g; further preferably, the silica has an average particle size of 7 μm and an oil absorption value of 0.9 to 1.3cc/g.
In some preferred embodiments, the silica is purchased from SUNSIL 130 manufactured by SUNJIN.
Preferably, the mica is one or more of sericite, common mica and synthetic mica; further preferably, sericite is used.
Preferably, the whiteness of the sericite is 80-90%, and the median particle diameter is 2-10 mu m; further preferably, the whiteness of the sericite is 85%, and the median particle diameter is 6 μm.
In some preferred embodiments, the sericite is purchased from sericite LX-001 manufactured by Anhui glargine mining Co., ltd.
Preferably, the weight ratio of the silica to the mica is (1-2): (1-2); further preferably, it is 2:3.
Specific silica and mica are selected as filler, and the weight ratio of the silica to the mica is (1-2): in the case of (1-2), the stability of the formulation and the spreadability on the skin can be improved, and the lip balm prepared by the method has a certain improvement effect on the cracking of lips. This is probably due to the fact that the compatibility between specific silica and mica and grease is good, so that the dispersity of the specific silica and mica in the system is improved, the stability of the formula is further improved, the particle size of the specific silica and mica is proper, and the specific mica is not harmful to the skin of lips during use, and meanwhile, the specific mica has a certain effect of improving cracks. When the lips are cracked and peeled, the lip balm prepared by the filler can remove dead skin on the surfaces of lips, and meanwhile, the plant repairing composition in the lip balm can penetrate deep into the skin of the mouth, so that the effects of effectively improving the cracks and repairing the skin of the lips are achieved.
Preferably, the method for preparing the lip product comprises the following steps:
s1, heating the forming agent to 90-95 ℃ in a manufacturing pot, and continuously stirring until the system is uniform, wherein the stirring speed is 500-800rpm;
s2, after the temperature of the manufacturing pot is reduced to 75-85 ℃, adding the plant repairing composition and the skin conditioning agent into the manufacturing pot, and keeping the temperature of 75-85 ℃ and continuously stirring until the system is uniform, wherein the stirring speed is 500-800rpm;
s3, putting the filling agent into a manufacturing pot, maintaining the temperature of 75-85 ℃ and stirring at the stirring speed of 800-1000rpm until the system is uniform, thus obtaining the high-strength concrete.
The beneficial effects are that:
1. the weight ratio is (1-2.1): the jojoba seed oil and squalane which are used as main components of the plant repairing composition can ensure that the prepared composition has obvious moisturizing and repairing effects in a system with sunflower seed oil as a solvent, can be applied to lip products to improve the moisturizing and moisturizing properties and reduce the skin irritation of the lip products, and are all of plant sources, and the components are green and mild.
2. By selecting specific candelilla wax, carnauba wax and sunflower seed wax as the shaping agent, a lip product containing a plant repairing composition with proper hardness can be prepared, and good skin-moistening property can be achieved.
3. The weight ratio of the components is (8-12): (3-6): (2-5): 1 candelilla wax, carnauba wax, sunflower seed wax and compound wax are used as forming agents, and the prepared lip product containing the plant repairing composition has excellent film forming property and skin moistening property, soft and smooth touch, and reduced sticky feel, thereby improving sensory effect.
4. The weight ratio of the components is (15-25): (1-3): (1-2): 1, caprylic/capric/myristic/stearic triglyceride, octyldodecanol, caprylic/capric triglyceride as skin conditioning agent, and can further improve the moisturizing ability of the lip product containing the plant repairing composition while improving the stability of the lip product.
5. By selecting specific silica and mica as filler, the weight ratio of the silica to the mica is (1-2): in the case of (1-2), the lip product containing the plant-repairing composition can be improved in the stability of the formulation and the spreadability on the skin, and can be improved in the effect of improving the cracking of lips.
6. The natural plant component is selected as the main component of the plant repairing composition, so that the natural plant repairing composition can provide good safety for lip products such as lip products containing the composition, has a certain repairing and moisturizing effect, can improve the condition of cracks of lips, and has excellent stability.
Drawings
FIG. 1 shows the results of the change in moisture content of the lip skin with time after the lip products prepared in examples 1 to 8 and comparative examples 1 to 6, respectively.
Detailed Description
Examples
Example 1
Example 1 provides a plant repair composition comprising the following components in percentage by weight: 30% of sunflower seed oil, 35% of jojoba seed oil and 35% of squalane.
The weight ratio of jojoba seed oil to squalane is 1:1.
the sunflower seed oil was purchased from plicon company as SUNFLOWER OIL HIGH OLEIC.
The JOJOBA seed oil was purchased from Vantage Specialty Ingredients, inc.
The squalane is purchased from SOPHIM company
The preparation method of the plant repairing composition comprises the following steps: mixing the raw materials according to weight percentage, and stirring uniformly at 80 ℃.
In a second aspect, this embodiment provides a lip product comprising the plant-repairing composition, comprising, in weight percent: 20% of a forming agent, 5% of a plant repairing composition, 70% of a skin conditioning agent and 5% of a filler.
The forming agent is candelilla wax, carnauba wax, sunflower seed wax and compound wax.
The weight ratio of candelilla wax to carnauba wax to sunflower seed wax to composite wax is 10:5:4:1.
The melting point of the candelilla wax is 68-73 ℃ and the hydrocarbon content is 50wt%.
The melting point of the carnauba wax is 82-86 ℃.
The sunflower seed wax has a melting point of 74-80deg.C.
The compound wax comprises, by weight, 62% of jojoba esters, 32% of sunflower seed wax, 2.98% of vitex negundo flower wax, polyglycerol-3 3% and 0.02% of tocopherol.
The candelilla wax was purchased from Henan Fumei corporationCandelilla wax 5501.
The carnauba wax was purchased from Henan Fumei companyCarnauba wax 2012.
The sunflower seed wax is purchased from Henan Fumei companySunflower wax 5301.
The composite wax was purchased from ACTICIRE MB, manufactured by the company of the lion, law.
The skin conditioning agent is polyglycerol-2 triisostearate, caprylic/capric/myristic/stearic triglyceride, octyldodecanol, caprylic/capric triglyceride.
The weight ratio of the polyglycerol-2 triisostearate, caprylic acid/capric acid/myristic acid/stearic acid triglyceride and octyl dodecanol to caprylic acid/capric acid triglyceride is 55:7:5:3.
The polyglycerol-2 triisostearate was purchased from COSMOL 43V manufactured by The Nisshin OilliO Group, ltd.
The caprylic/capric/myristic/stearic triglyceride is purchased from IOI oils Inc378。
The octyldodecanol was purchased from RISONOL 20SP, manufactured by kokokoyou.
The caprylic/capric triglyceride is purchased from BASF318RC。
The filler is silica or mica.
The silica has an average particle size of 7 μm and an oil absorption value of 0.9 to 1.3cc/g.
The silica was purchased from SUNSIL 130 manufactured by SUNJIN.
The mica is sericite.
The whiteness of the sericite is 85%, and the median particle diameter is 6 mu m.
The sericite was purchased from sericite LX-001 manufactured by Anhui gracilis mining limited liability company.
The weight ratio of the silica to the mica is 2:3.
The preparation method of the lip product comprises the following steps:
s1, heating a forming agent to 95 ℃ in a manufacturing pot, and continuously stirring until the system is uniform, wherein the stirring speed is 600rpm;
s2, after the temperature of the manufacturing pot is reduced to 80 ℃, adding the plant repairing composition and the skin conditioning agent into the manufacturing pot, and keeping the temperature of 80 ℃ and continuously stirring until the system is uniform, wherein the stirring speed is 600rpm;
s3, putting the filling agent into a manufacturing pot, maintaining the temperature of 80 ℃ and stirring at the stirring speed of 900rpm until the system is uniform, thus obtaining the high-temperature-resistant filler.
Example 2
Example 2 provides a plant repair composition, the specific embodiment of which is the same as example 1, except that: the plant repairing composition comprises the following components in percentage by weight: 62.5% of sunflower seed oil, 22.5% of jojoba seed oil and 15% of squalane.
The weight ratio of jojoba seed oil to squalane is 1.5:1.
example 3
Example 3 provides a plant repair composition, the specific embodiment of which is the same as example 1, except that: the plant repairing composition comprises the following components in percentage by weight: 55% of sunflower seed oil, 30% of jojoba seed oil and 15% of squalane.
The weight ratio of jojoba seed oil to squalane is 2:1.
example 4
Example 4 provides a plant repair composition, the specific embodiment of which is the same as example 1, except that: the plant repairing composition comprises the following components in percentage by weight: 53.5% of sunflower seed oil, 31.5% of jojoba seed oil and 15% of squalane.
The weight ratio of jojoba seed oil to squalane is 2.1:1.
example 5
Example 5 provides a plant repair composition, the specific embodiment of which is the same as example 1, except that: the lip product containing the plant repairing composition comprises the following components in percentage by weight: 20% of a forming agent, 4.5% of a plant repairing composition, 70.5% of a skin conditioning agent and 5% of a filler.
The weight ratio of the polyglycerol-2 triisostearate, the caprylic acid/capric acid/myristic acid/stearic acid triglyceride and the octyl dodecanol to the caprylic acid/capric acid triglyceride is 55:7:5:3.5.
Example 6
Example 6 provides a plant repair composition, the specific embodiment of which is the same as example 1, except that: the lip product containing the plant repairing composition comprises the following components in percentage by weight: 20% of a forming agent, 6% of a plant repairing composition, 69% of a skin conditioning agent and 5% of a filler.
The weight ratio of the polyglycerol-2 triisostearate, caprylic acid/capric acid/myristic acid/stearic acid triglyceride and octyl dodecanol to caprylic acid/capric acid triglyceride is 55:7:5:2.
Example 7
Example 7 provides a plant repair composition, the specific embodiment being the same as example 1, except that: the lip product containing the plant repairing composition comprises the following components in percentage by weight: 23% of a forming agent, 5% of a plant repairing composition, 67% of a skin conditioning agent and 5% of a filler.
The weight ratio of candelilla wax to carnauba wax to sunflower seed wax to composite wax is 10:8:4:1.
The weight ratio of the polyglycerol-2 triisostearate, caprylic acid/capric acid/myristic acid/stearic acid triglyceride and octyl dodecanol to caprylic acid/capric acid triglyceride is 50:10:5:2.
Example 8
Example 8 provides a plant repair composition, the specific embodiment of which is the same as example 1, except that: the lip product containing the plant repairing composition comprises the following components in percentage by weight: 23% of a forming agent, 6% of a plant repairing composition, 66% of a skin conditioning agent and 5% of a filler.
The weight ratio of candelilla wax to carnauba wax to sunflower seed wax to composite wax is 10:8:4:1.
The weight ratio of the polyglycerol-2 triisostearate, the caprylic acid/capric acid/myristic acid/stearic acid triglyceride and the octyl dodecanol to the caprylic acid/capric acid triglyceride is 50:10:5:1.
Comparative example 1
Comparative example 1 provides a plant repair composition, the specific embodiment is the same as example 1, except that: the plant repairing composition comprises the following components in percentage by weight: 52% of sunflower seed oil, 33% of jojoba seed oil and 15% of squalane.
The weight ratio of jojoba seed oil to squalane is 2.2:1.
comparative example 2
Comparative example 2 provides a plant repair composition, the specific embodiment is the same as example 1, except that: the plant repairing composition comprises the following components in percentage by weight: 50.5% of sunflower seed oil, 34.5% of jojoba seed oil and 15% of squalane.
The weight ratio of jojoba seed oil to squalane is 2.3:1.
comparative example 3
Comparative example 3 provides a plant repair composition, the specific embodiment is the same as example 1, except that: the plant repairing composition comprises the following components in percentage by weight: 70% of sunflower seed oil and 30% of jojoba seed oil.
Comparative example 4
Comparative example 4 provides a plant repair composition, the specific embodiment being the same as example 1, except that: the plant repairing composition comprises the following components in percentage by weight: 70% of sunflower seed oil and 30% of squalane.
Comparative example 5
Comparative example 5 provides a plant repair composition, the specific embodiment being the same as example 1, except that: the lip product containing the plant repairing composition comprises the following components in percentage by weight: 20% of a forming agent, 75% of a skin conditioning agent and 5% of a filler.
The forming agent is candelilla wax, carnauba wax and compound wax.
The weight ratio of candelilla wax to carnauba wax to composite wax is 10:9:1.
The skin conditioning agent is polyglycerol-2 triisostearate, caprylic/capric/myristic/stearic triglyceride, and octyldodecanol.
The weight ratio of the polyglycerol-2 triisostearate to the caprylic acid/capric acid/myristic acid/stearic acid triglyceride to the octyldodecanol is 60:7:8.
Comparative example 6
Comparative example 6 provides a plant repair composition, the specific embodiment being the same as example 1, except that: the forming agent is candelilla wax and carnauba wax.
The weight ratio of candelilla wax to carnauba wax is 1:1.
The skin conditioning agent is polyglycerol-2 triisostearate, caprylic/capric/myristic/stearic triglyceride.
The weight ratio of the polyglycerol-2 triisostearate, caprylic acid/capric acid/myristic acid/stearic acid triglyceride is 6:1.
Performance test method
1. Sanitary safety detection
The toxic substances of the lip products prepared in examples 1 to 8 and comparative examples 1 to 6 were detected according to the detection method of 2015 edition "cosmetic hygienic Standard Specification"; the lip products prepared in examples 1 to 8 and comparative examples 1 to 6 were examined for microorganisms according to the method of GB 7918.2-87 Standard detection method for microorganisms for cosmetic-total bacterial count measurement, and the examination results are shown in Table 1.
As shown in Table 1, the heavy metal content and the total colony count in the lip product prepared by the application completely meet the national relevant standards, and meet the safety requirements.
2. Moisture retention test
The lip products prepared in examples 1 to 8 and comparative examples 1 to 6 were examined for moisturizing ability according to cosmetic moisturizing efficacy evaluation guidelines QB/T4256-2011, and the results are shown in Table 2.
[ test purpose ]: measuring the improvement value control of the tested part of the test subject and the blank control area by using the test subject by using the sample and an instrument test method, and evaluating the moisturizing efficacy of the product;
test method selected healthy volunteers on the skin of the lips, each sample was tested for use by 5 persons. Each sample was applied to the lips, the moisture content of the outer layer of the skin cornified film of the lips was measured by a skin moisture tester, the skin moisture content of the lips before use (0 h) and after use (1 h, 3h, 6 h) was measured, and the average value was calculated, and the experimental results are shown in table 2 and fig. 1;
[ subject information ]: female volunteers 21-45 years old;
[ detection Environment ]: the temperature is 20-22 ℃, and the humidity is as follows: 40% -60% RH;
[ detecting instrument ]:CM825 stratum corneum moisture content tester;
[ test item ]: and (5) moisturizing.
As can be seen from Table 2, examples 1 to 8 compare with comparative examples 1 to 6, jojoba seed oil in the repair compositions of examples 1 to 4: the mass ratio of squalane is in the range of (1-2.1): 1, while the comparative examples 1-2 are out of the range of (1-2.1): 1, and the skin moisture increase amount of examples 1-4 is significantly higher than that of comparative examples 1-2, indicating that lip balm prepared by the repairing composition of the present application has more moisturizing and repairing effects. The lip balm prepared in comparative example 5, without adding the restoration composition, cannot increase the moisture content of the skin, but also accelerates the loss of the moisture of the skin after use. Of the above examples of the present application, example 4 had the best moisturizing and repairing effect.
3. Effect of sensory test of application
70 female volunteers aged 20-25 years were selected, randomly divided into 14 groups by 5 persons, and lip products containing the composition of each of test examples 1-8 and comparative examples 1-6 were each used for 2 months, and each effect was scored (full score 5 min, 1 min worst, average result) and the test results are shown in table 3.
As can be seen from Table 3, each of the sensory test evaluations of examples 1 to 8 was higher than that of the comparative examples, wherein examples 1 to 8 were compared with comparative examples 1 to 6 in which jojoba seed oil was used in the repair compositions of examples 1 to 4: the squalane mass ratio was in the range of (1-2.1): 1, while comparative examples 1-6 were outside the range of (1-2.1): 1, and the results of sensory evaluation of the lip products prepared in examples 1-6 were all higher than comparative examples 1-6, indicating that in the formulation of the present application, jojoba seed oil: the mass ratio of squalane directly affects various properties of the lip product, and the components can act together only when the mass ratio of squalane and the lip product is in a specified proportion, so that the best effect is achieved.
Comparative example 5 was free of the addition of a restorative composition, and the lip product prepared therefrom had the lowest moisturizing effect, crack-improving effect, and moisture retention, and could not meet consumer use demands. Examples 1 and 7 were identical in the number of parts of the repair composition to comparative example 6, but the components of the other raw materials were different, and the effects were also different.
The best results of the sensory tests for the lip product of example 4 are shown in table 3.
TABLE 1 sanitary safety test data
Object of detection Colony count Lead Arsenic (As) Mercury Cadmium (Cd)
Limiting amount/ppm ≤500CFU/g 10 2 1 5
Example 1 ≤5 Not detected Not detected Not detected Not detected
Example 2 ≤20 Not detected Not detected Not detected Not detected
Example 3 ≤25 Not detected Not detected Not detected Not detected
Example 4 ≤20 Not detected Not detected Not detected Not detected
Example 5 ≤15 Not detected Not detected Not detected Not detected
Example 6 ≤25 Not detected Not detected Not detected Not detected
Example 7 ≤30 Not detected Not detected Not detected Not detected
Example 8 ≤20 Not detected Not detected Not detected Not detected
Comparative example 1 ≤15 Not detected Not detected Not detected Not detected
Comparative example 2 ≤20 Not detected Not detected Not detected Not detected
Comparative example 3 ≤25 Not detected Not detected Not detected Not detected
Comparative example 4 ≤25 Not detected Not detected Not detected Not detected
Comparative example 5 ≤35 Not detected Not detected Not detected Not detected
Comparative example 6 ≤15 Not detected Not detected Not detected Not detected
Table 2 moisture test data
TABLE 3 data on sensory test effects of smear
Detecting item/group Moisturizing effect Crack improving effect Moisture retention
Example 1 5 4.8 4.9
Example 2 5 4.9 4.9
Example 3 5 4.8 5
Example 4 5 5 5
Example 5 4.9 4.7 4.8
Example 6 4.9 4.8 4.9
Implementation of the embodimentsExample 7 4.8 4.9 4.8
Example 8 4.8 4.9 4.8
Comparative example 1 4.8 4.7 4.7
Comparative example 2 4.9 4.7 4.7
Comparative example 3 4.3 3.5 4.5
Comparative example 4 4 3.6 4.3
Comparative example 5 3.9 4.3 4.5
Comparative example 6 4.7 4.6 4.8

Claims (6)

1. The lip product of the plant repairing composition is characterized by comprising the following components in percentage by weight: 10-30% of a forming agent, 1-6% of a plant repairing composition, 60-80% of a skin conditioner and 2-10% of a filler; the plant repairing composition comprises the following components in percentage by weight: 30-70% of sunflower seed oil, 15-35% of jojoba seed oil and 15-35% of squalane; the weight ratio of jojoba seed oil to squalane is (1-2.1): 1, a step of; the forming agent is candelilla wax, carnauba wax, sunflower seed wax and compound wax; the weight ratio of candelilla wax, carnauba wax, sunflower seed wax and compound wax is (8-12): (3-6): (2-5): 1.
2. lip product according to claim 1, characterized in that the skin conditioning agent is one or more of polyglycerol-2 triisostearate, caprylic/capric/myristic/stearic triglycerides, octyldodecanol, caprylic/capric triglycerides, vegetable extracts, hydrogenated lecithins, ceramides, nicotinamide, polypeptides, fullerenes, salicylic acid.
3. Lip product according to claim 1, characterized in that the filler is one or more of silica, mica, talc, kaolin, bentonite, rutile, calcite.
4. A lip product according to claim 3, characterized in that the silica has an average particle size of 2-15 μm and an oil absorption value of 0.5-2.0cc/g.
5. The lip product according to claim 4, wherein the mica is one or more of sericite, plain mica, synthetic mica.
6. A method of producing a lip product according to any one of claims 1-5, comprising the steps of:
s1, heating the forming agent to 90-95 ℃ in a manufacturing pot, and continuously stirring until the system is uniform, wherein the stirring speed is 500-800rpm;
s2, after the temperature of the manufacturing pot is reduced to 75-85 ℃, adding the plant repairing composition and the skin conditioning agent into the manufacturing pot, and keeping the temperature of 75-85 ℃ and continuously stirring until the system is uniform, wherein the stirring speed is 500-800rpm;
s3, putting the filling agent into a manufacturing pot, maintaining the temperature of 75-85 ℃ and stirring at the stirring speed of 800-1000rpm until the system is uniform, thus obtaining the high-strength concrete.
CN202211065598.3A 2022-08-29 2022-08-29 Plant repairing composition and lip product containing same Active CN115317411B (en)

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Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105326671A (en) * 2015-12-02 2016-02-17 共聚生化科技（昆山）有限公司 Natural nourishing lip beautifying and protecting oil
CN107281031A (en) * 2017-06-30 2017-10-24 广州澳希亚实业有限公司 A kind of lip gloss of long-acting moisturizing and nourishing injury repair and preparation method thereof
CN107595679A (en) * 2017-10-09 2018-01-19 澳宝化妆品（惠州）有限公司 A kind of color-changing lipstick and preparation method thereof
CN111214397A (en) * 2020-03-13 2020-06-02 广东密尚生物科技有限公司 Plant skin moistening composition, preparation method thereof and lip balm
CN114917138A (en) * 2022-06-09 2022-08-19 上海臻臣化妆品有限公司 Whole-plant water-containing lipstick and preparation method thereof

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105326671A (en) * 2015-12-02 2016-02-17 共聚生化科技（昆山）有限公司 Natural nourishing lip beautifying and protecting oil
CN107281031A (en) * 2017-06-30 2017-10-24 广州澳希亚实业有限公司 A kind of lip gloss of long-acting moisturizing and nourishing injury repair and preparation method thereof
CN107595679A (en) * 2017-10-09 2018-01-19 澳宝化妆品（惠州）有限公司 A kind of color-changing lipstick and preparation method thereof
CN111214397A (en) * 2020-03-13 2020-06-02 广东密尚生物科技有限公司 Plant skin moistening composition, preparation method thereof and lip balm
CN114917138A (en) * 2022-06-09 2022-08-19 上海臻臣化妆品有限公司 Whole-plant water-containing lipstick and preparation method thereof

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