CN113350235A - Lip care composition and preparation and application of cosmetics thereof - Google Patents
Lip care composition and preparation and application of cosmetics thereof Download PDFInfo
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- CN113350235A CN113350235A CN202110693833.0A CN202110693833A CN113350235A CN 113350235 A CN113350235 A CN 113350235A CN 202110693833 A CN202110693833 A CN 202110693833A CN 113350235 A CN113350235 A CN 113350235A
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- 239000000203 mixture Substances 0.000 title claims abstract description 38
- 239000002537 cosmetic Substances 0.000 title claims abstract description 25
- 238000002360 preparation method Methods 0.000 title abstract description 11
- 229940006284 undaria pinnatifida extract Drugs 0.000 claims description 27
- 241000130781 Arnebia Species 0.000 claims description 25
- 238000002156 mixing Methods 0.000 claims description 21
- 241001071917 Lithospermum Species 0.000 claims description 18
- 238000000605 extraction Methods 0.000 claims description 17
- 239000003921 oil Substances 0.000 claims description 16
- 235000019198 oils Nutrition 0.000 claims description 16
- 241000199919 Phaeophyceae Species 0.000 claims description 15
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims description 12
- 239000007788 liquid Substances 0.000 claims description 12
- 239000011259 mixed solution Substances 0.000 claims description 12
- 238000003756 stirring Methods 0.000 claims description 12
- 238000005303 weighing Methods 0.000 claims description 12
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- 239000000463 material Substances 0.000 claims description 9
- 238000000926 separation method Methods 0.000 claims description 9
- 239000000243 solution Substances 0.000 claims description 9
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- 239000003974 emollient agent Substances 0.000 claims description 8
- 241000675108 Citrus tangerina Species 0.000 claims description 7
- 238000000034 method Methods 0.000 claims description 7
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- 235000012545 Vaccinium macrocarpon Nutrition 0.000 claims description 6
- 235000002118 Vaccinium oxycoccus Nutrition 0.000 claims description 6
- 229910002092 carbon dioxide Inorganic materials 0.000 claims description 6
- 239000001569 carbon dioxide Substances 0.000 claims description 6
- 235000004634 cranberry Nutrition 0.000 claims description 6
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- 239000000843 powder Substances 0.000 claims description 6
- 239000002562 thickening agent Substances 0.000 claims description 6
- 235000015112 vegetable and seed oil Nutrition 0.000 claims description 6
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- 239000004006 olive oil Substances 0.000 claims description 5
- LADGBHLMCUINGV-UHFFFAOYSA-N tricaprin Chemical compound CCCCCCCCCC(=O)OCC(OC(=O)CCCCCCCCC)COC(=O)CCCCCCCCC LADGBHLMCUINGV-UHFFFAOYSA-N 0.000 claims description 5
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 4
- HGKOWIQVWAQWDS-UHFFFAOYSA-N bis(16-methylheptadecyl) 2-hydroxybutanedioate Chemical compound CC(C)CCCCCCCCCCCCCCCOC(=O)CC(O)C(=O)OCCCCCCCCCCCCCCCC(C)C HGKOWIQVWAQWDS-UHFFFAOYSA-N 0.000 claims description 4
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- 238000010438 heat treatment Methods 0.000 claims description 4
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- 235000019271 petrolatum Nutrition 0.000 claims description 4
- PRAKJMSDJKAYCZ-UHFFFAOYSA-N squalane Chemical compound CC(C)CCCC(C)CCCC(C)CCCCC(C)CCCC(C)CCCC(C)C PRAKJMSDJKAYCZ-UHFFFAOYSA-N 0.000 claims description 4
- 239000004166 Lanolin Substances 0.000 claims description 3
- 244000044822 Simmondsia californica Species 0.000 claims description 3
- 235000004433 Simmondsia californica Nutrition 0.000 claims description 3
- 235000018936 Vitellaria paradoxa Nutrition 0.000 claims description 3
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- FOLJTMYCYXSPFQ-CJKAUBRRSA-N [(2r,3s,4s,5r,6r)-6-[(2s,3s,4s,5r)-3,4-dihydroxy-5-(hydroxymethyl)-2-(octadecanoyloxymethyl)oxolan-2-yl]oxy-3,4,5-trihydroxyoxan-2-yl]methyl octadecanoate Chemical compound O[C@@H]1[C@@H](O)[C@H](O)[C@@H](COC(=O)CCCCCCCCCCCCCCCCC)O[C@@H]1O[C@@]1(COC(=O)CCCCCCCCCCCCCCCCC)[C@@H](O)[C@H](O)[C@@H](CO)O1 FOLJTMYCYXSPFQ-CJKAUBRRSA-N 0.000 claims description 3
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- 238000002791 soaking Methods 0.000 claims description 3
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- 239000008158 vegetable oil Substances 0.000 claims description 3
- DSEKYWAQQVUQTP-XEWMWGOFSA-N (2r,4r,4as,6as,6as,6br,8ar,12ar,14as,14bs)-2-hydroxy-4,4a,6a,6b,8a,11,11,14a-octamethyl-2,4,5,6,6a,7,8,9,10,12,12a,13,14,14b-tetradecahydro-1h-picen-3-one Chemical compound C([C@H]1[C@]2(C)CC[C@@]34C)C(C)(C)CC[C@]1(C)CC[C@]2(C)[C@H]4CC[C@@]1(C)[C@H]3C[C@@H](O)C(=O)[C@@H]1C DSEKYWAQQVUQTP-XEWMWGOFSA-N 0.000 claims description 2
- ULQISTXYYBZJSJ-UHFFFAOYSA-N 12-hydroxyoctadecanoic acid Chemical compound CCCCCCC(O)CCCCCCCCCCC(O)=O ULQISTXYYBZJSJ-UHFFFAOYSA-N 0.000 claims description 2
- KIHBGTRZFAVZRV-UHFFFAOYSA-N 2-Hydroxyoctadecanoic acid Natural products CCCCCCCCCCCCCCCCC(O)C(O)=O KIHBGTRZFAVZRV-UHFFFAOYSA-N 0.000 claims description 2
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- 235000018330 Macadamia integrifolia Nutrition 0.000 claims description 2
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- 235000000539 Rosa canina Nutrition 0.000 claims description 2
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- PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Natural products C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 claims description 2
- FGUZFFWTBWJBIL-XWVZOOPGSA-N [(1r)-1-[(2s,3r,4s)-3,4-dihydroxyoxolan-2-yl]-2-hydroxyethyl] 16-methylheptadecanoate Chemical compound CC(C)CCCCCCCCCCCCCCC(=O)O[C@H](CO)[C@H]1OC[C@H](O)[C@H]1O FGUZFFWTBWJBIL-XWVZOOPGSA-N 0.000 claims description 2
- 235000021302 avocado oil Nutrition 0.000 claims description 2
- 239000008163 avocado oil Substances 0.000 claims description 2
- 235000013871 bee wax Nutrition 0.000 claims description 2
- 239000012166 beeswax Substances 0.000 claims description 2
- 239000004204 candelilla wax Substances 0.000 claims description 2
- 235000013868 candelilla wax Nutrition 0.000 claims description 2
- 229940073532 candelilla wax Drugs 0.000 claims description 2
- 239000004203 carnauba wax Substances 0.000 claims description 2
- 235000013869 carnauba wax Nutrition 0.000 claims description 2
- 229960000541 cetyl alcohol Drugs 0.000 claims description 2
- 235000019868 cocoa butter Nutrition 0.000 claims description 2
- 229940110456 cocoa butter Drugs 0.000 claims description 2
- 235000018597 common camellia Nutrition 0.000 claims description 2
- 125000000118 dimethyl group Chemical group [H]C([H])([H])* 0.000 claims description 2
- HQQADJVZYDDRJT-UHFFFAOYSA-N ethene;prop-1-ene Chemical group C=C.CC=C HQQADJVZYDDRJT-UHFFFAOYSA-N 0.000 claims description 2
- 235000008524 evening primrose extract Nutrition 0.000 claims description 2
- 239000010475 evening primrose oil Substances 0.000 claims description 2
- 229940089020 evening primrose oil Drugs 0.000 claims description 2
- 229940087068 glyceryl caprylate Drugs 0.000 claims description 2
- 239000008169 grapeseed oil Substances 0.000 claims description 2
- IUJAMGNYPWYUPM-UHFFFAOYSA-N hentriacontane Chemical compound CCCCCCCCCCCCCCCCCCCCCCCCCCCCCCC IUJAMGNYPWYUPM-UHFFFAOYSA-N 0.000 claims description 2
- 229940119170 jojoba wax Drugs 0.000 claims description 2
- 239000010487 meadowfoam seed oil Substances 0.000 claims description 2
- 239000004200 microcrystalline wax Substances 0.000 claims description 2
- 235000019808 microcrystalline wax Nutrition 0.000 claims description 2
- JXTPJDDICSTXJX-UHFFFAOYSA-N n-Triacontane Natural products CCCCCCCCCCCCCCCCCCCCCCCCCCCCCC JXTPJDDICSTXJX-UHFFFAOYSA-N 0.000 claims description 2
- 239000010466 nut oil Substances 0.000 claims description 2
- AEIJTFQOBWATKX-UHFFFAOYSA-N octane-1,2-diol Chemical compound CCCCCCC(O)CO AEIJTFQOBWATKX-UHFFFAOYSA-N 0.000 claims description 2
- 239000012188 paraffin wax Substances 0.000 claims description 2
- 235000019809 paraffin wax Nutrition 0.000 claims description 2
- 229940066842 petrolatum Drugs 0.000 claims description 2
- 229920001083 polybutene Polymers 0.000 claims description 2
- 229920000573 polyethylene Polymers 0.000 claims description 2
- GHBFNMLVSPCDGN-UHFFFAOYSA-N rac-1-monooctanoylglycerol Chemical compound CCCCCCCC(=O)OCC(O)CO GHBFNMLVSPCDGN-UHFFFAOYSA-N 0.000 claims description 2
- 239000000377 silicon dioxide Substances 0.000 claims description 2
- 229940057429 sorbitan isostearate Drugs 0.000 claims description 2
- 229940032094 squalane Drugs 0.000 claims description 2
- 235000020238 sunflower seed Nutrition 0.000 claims description 2
- 125000000383 tetramethylene group Chemical group [H]C([H])([*:1])C([H])([H])C([H])([H])C([H])([H])[*:2] 0.000 claims description 2
- 235000019489 Almond oil Nutrition 0.000 claims 1
- 240000002299 Symphytum officinale Species 0.000 claims 1
- 235000005865 Symphytum officinale Nutrition 0.000 claims 1
- 239000008168 almond oil Substances 0.000 claims 1
- 239000001993 wax Substances 0.000 claims 1
- 230000000694 effects Effects 0.000 abstract description 14
- 208000007287 cheilitis Diseases 0.000 abstract description 7
- 230000003020 moisturizing effect Effects 0.000 abstract description 5
- 238000013329 compounding Methods 0.000 abstract description 4
- 230000008439 repair process Effects 0.000 abstract description 4
- 230000003110 anti-inflammatory effect Effects 0.000 abstract description 3
- 230000009044 synergistic interaction Effects 0.000 abstract description 3
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- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 description 3
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 3
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- 230000002354 daily effect Effects 0.000 description 2
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- 239000007934 lip balm Substances 0.000 description 2
- 238000005259 measurement Methods 0.000 description 2
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- GLDOVTGHNKAZLK-UHFFFAOYSA-N octadecan-1-ol Chemical compound CCCCCCCCCCCCCCCCCCO GLDOVTGHNKAZLK-UHFFFAOYSA-N 0.000 description 2
- 229920000728 polyester Polymers 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- ULSUXBXHSYSGDT-UHFFFAOYSA-N tangeretin Chemical compound C1=CC(OC)=CC=C1C1=CC(=O)C2=C(OC)C(OC)=C(OC)C(OC)=C2O1 ULSUXBXHSYSGDT-UHFFFAOYSA-N 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- 244000175448 Citrus madurensis Species 0.000 description 1
- 235000017317 Fortunella Nutrition 0.000 description 1
- 244000062730 Melissa officinalis Species 0.000 description 1
- 235000010654 Melissa officinalis Nutrition 0.000 description 1
- 241001465754 Metazoa Species 0.000 description 1
- 235000010337 Rosa dumalis Nutrition 0.000 description 1
- IECRXMSGDFIOEY-UHFFFAOYSA-N Tangeretin Natural products COC=1C(OC)=C(OC)C(OC)=C(C(C=2)=O)C=1OC=2C1=CC=C(O)C=C1 IECRXMSGDFIOEY-UHFFFAOYSA-N 0.000 description 1
- 241001261506 Undaria pinnatifida Species 0.000 description 1
- 206010048222 Xerosis Diseases 0.000 description 1
- 239000013566 allergen Substances 0.000 description 1
- 239000001140 aloe barbadensis leaf extract Substances 0.000 description 1
- 229940069638 aloe vera leaf extract Drugs 0.000 description 1
- 239000003963 antioxidant agent Substances 0.000 description 1
- 230000003078 antioxidant effect Effects 0.000 description 1
- 235000020221 chamomile extract Nutrition 0.000 description 1
- 229940119217 chamomile extract Drugs 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
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- 238000001816 cooling Methods 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 210000002615 epidermis Anatomy 0.000 description 1
- 229940093499 ethyl acetate Drugs 0.000 description 1
- 235000019439 ethyl acetate Nutrition 0.000 description 1
- 238000004880 explosion Methods 0.000 description 1
- 210000000245 forearm Anatomy 0.000 description 1
- 239000003205 fragrance Substances 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 239000000865 liniment Substances 0.000 description 1
- 150000002632 lipids Chemical class 0.000 description 1
- GOQYKNQRPGWPLP-UHFFFAOYSA-N n-heptadecyl alcohol Natural products CCCCCCCCCCCCCCCCCO GOQYKNQRPGWPLP-UHFFFAOYSA-N 0.000 description 1
- 239000000049 pigment Substances 0.000 description 1
- 239000003755 preservative agent Substances 0.000 description 1
- 239000001944 prunus armeniaca kernel oil Substances 0.000 description 1
- 230000003716 rejuvenation Effects 0.000 description 1
- 239000010666 rose oil Substances 0.000 description 1
- 210000003491 skin Anatomy 0.000 description 1
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Images
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9706—Algae
- A61K8/9711—Phaeophycota or Phaeophyta [brown algae], e.g. Fucus
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/001—Preparations for care of the lips
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
Abstract
The invention discloses a lip care composition and preparation and application of cosmetics thereof. The composition selects natural oil and oil-soluble active matters, achieves good anti-inflammatory repair, moisturizing and moistening effects through reasonable compounding and synergistic interaction, and comprehensively and effectively prevents the problems of dry lips, peeling, cracking and cheilitis caused by frequent use of lip color cosmetics.
Description
Technical Field
The invention relates to the field of daily cosmetics, and relates to a lip care composition, preparation and application of cosmetics of the lip care composition, in particular to a natural lip care composition with orange fragrance, and a preparation method and application of a lip care cosmetic containing the natural lip care composition.
Background
The development of color cosmetic products has been diversified in recent years, and the market growth of lip color cosmetics has been also noted. The explosion of lip color cosmetics has benefited from the need for lip color cosmetics becoming more regular and from audience rejuvenation. More and more consumers are used to improve their own color every day by using lip color cosmetics, thereby improving their own confidence. The efficient distribution of the internet also allows more and more young consumers to recognize and reach the emerging lip color.
However, the high frequency of lip color cosmetics causes the lips to be dried, peeled, cracked and the like, and the pigments, preservatives or animal-derived components in the lip color cosmetics can become allergens, so that the lips are attacked by cheilitis. The moisturizing lip balms used on a daily basis have failed to meet the increasing consumer demands for lip care, and there is a need to develop a lip care product that is natural enough and can provide effective centralized care and repair of the lips.
Disclosure of Invention
According to the application, natural oil and oil-soluble active matters are selected, and through reasonable compounding and synergistic interaction, good anti-inflammatory repair, moisturizing and moistening effects are achieved, and the problems of dry lips, peeling, cracking and cheilitis caused by frequent use of lip color cosmetics are comprehensively and effectively prevented.
In order to achieve the purpose, the invention provides the following technical scheme:
the invention provides a lip care composition which comprises, by mass, 2-40 parts of cranberry fat, 0.1-4 parts of lithospermum extract and 0.1-0.4 part of undaria pinnatifida extract.
The health-care food further comprises 2-40 parts of the following tangerine peel, 0.1-4 parts of lithospermum extract and 0.1-0.4 part of undaria pinnatifida extract in parts by mass. The tangerines ester: and (3) extracting the lithospermum: the weight portion ratio of the undaria pinnatifida extract is (20-100): 1-10): 1.
The health-care food further comprises 2-40 parts of the following tangerine peel, 0.1-4 parts of lithospermum extract and 0.1-0.4 part of undaria pinnatifida extract in parts by mass. The tangerines ester: and (3) extracting the lithospermum: the weight portion ratio of the undaria pinnatifida extract is (50-80): 5-8): 1.
Further, the lithospermum extract is extracted from the root of lithospermum erythrorhizon in Xinjiang, and the extraction method is a micro-jet extraction method, and comprises the following steps:
step one, crushing Sinkiang arnebia root into powder with the particle size of not more than 5 mm;
step two, mixing the Sinkiang arnebia root powder and the vegetable oil in a proportion of 1: (3-20) mixing the solid-liquid ratio of g/ml in a material mixing tank to obtain a Sinkiang arnebia root mixed solution;
guiding the Sinkiang arnebia root mixed solution into a micro-jet extractor at a feeding speed of 8L/min-18L/min for micro-jet extraction at normal temperature to obtain Sinkiang arnebia root extracting solution;
and step four, guiding the Sinkiang arnebia root extracting solution into a centrifugal machine, centrifuging at the rotating speed of 5000-12000 rpm for solid-liquid separation, collecting separated liquid, and purifying the separated liquid by using a 300-700 nm ceramic membrane to obtain the Sinkiang arnebia root extract.
Further, the undaria pinnatifida extract is extracted from roots of French brown algae by a supercritical carbon dioxide extraction method, and comprises the following steps of:
firstly, breaking the walls of brown algae roots, crushing, and soaking in an edible ethanol solution for 12-36 hours to obtain a mixed solution;
adding the mixed solution into an extraction kettle, introducing carbon dioxide in a supercritical state into the extraction kettle, controlling the temperature at 30-45 ℃, controlling the pressure at 20-40 Mpa, and controlling the time at 1.5-3.5 hours;
and step three, introducing the carbon dioxide fluid containing the brown algae oil flowing out of the extraction kettle into a separation kettle for decompression separation to obtain the brown algae oil, and mixing the brown algae oil with caprylic/capric triglyceride to obtain the undaria pinnatifida extract.
The invention also provides a cosmetic containing the composition, which comprises, by mass, 2-40 parts of the following tangerines lipid, 0.1-4 parts of lithospermum extract, 0.1-0.4 part of undaria pinnatifida extract, 60-80 parts of an emollient and 10-30 parts of a thickening agent.
Further, the emollient is selected from jojoba oil, macadamia nut oil, sunflower seed oil, meadowfoam seed oil, grape seed oil, camellia seed oil, olive oil, dog rose oil, apricot kernel oil, avocado oil, evening primrose oil, shea butter, avocado butter, jojoba butter, cocoa butter, mango seed butter, squalane, petrolatum, lanolin, sorbitan isostearate, diisostearyl malate, glycerol tri (ethylacetate), polyglycerol-2 triisostearate, caprylic/capric triglyceride, hydrogenated polyisobutene (and) ethylene/propylene/styrene copolymers (and) butylene/ethylene/styrene copolymers, acetylated (sucrose distearate), hydroxystearic acid, phytosterol/isostearyl alcohol/cetyl alcohol/stearyl alcohol/behenyl alcohol dilinoleate, phytosterol/isostearyl alcohol/ethylene/styrene copolymers, acetylated (sucrose distearate), and mixtures thereof, Any one or a combination of at least two of glyceryl caprylate, caprylyl glycol, diisostearyl malate (and) dimethyl silylated silica.
Further, the thickening agent is selected from one or a combination of at least two of polyethylene, polybutene, microcrystalline wax, beeswax, paraffin wax, ozokerite, candelilla wax, carnauba wax and hydrogenated olive oil;
further, the cosmetic is lipstick, lip mask, lip glaze or lip gloss.
The invention also provides a preparation method of the cosmetic, which comprises the following steps:
weighing the components of the thickening agent and part of the emollient according to mass fractions, heating to 85-90 ℃ until the components are uniformly melted, and mixing and stirring for 5-10 min until the components are completely uniform;
step two, weighing and adding the rest of components of the emollient according to parts by weight, and mixing and stirring for 10-15 min at the temperature of 70-75 ℃ until the components are completely uniform;
step three, weighing and adding the components of the scarlet orange fat, the Sinkiang lithospermum extract and the undaria pinnatifida extract according to parts by weight, and uniformly mixing and stirring for 5-10 min at the temperature of 70-75 ℃;
and step four, defoaming and discharging, and filling at the temperature of 60-65 ℃ to obtain a finished product.
Compared with the prior art, the application can obtain the following technical effects:
the invention relates to a natural lip care composition containing kumquat ester, Sinkiang arnebia root extract and undaria pinnatifida extract and a lip care cosmetic containing the composition. The composition selects natural oil and oil-soluble active matters, achieves good anti-inflammatory repair, moisturizing and moistening effects through reasonable compounding and synergistic interaction, can be matched with other natural oil or synthetic oil, is applied to lipstick, lip mask, lip glaze, lip gloss and other formulations, and can prevent the problems of dryness, peeling, cracks, cheilitis and the like of lips.
Drawings
Figure 1 shows the lip condition of different volunteers after use.
Detailed Description
Embodiments of the present application will be described in detail by examples, so that how to apply technical means to solve technical problems and achieve technical effects of the present application can be fully understood and implemented.
The lithospermum extract is extracted from the root of arnebia euchroma (Royle) Johnst, the extraction method is a micro-jet extraction method, and the method comprises the following steps:
step one, crushing Sinkiang arnebia root into powder with the particle size of not more than 5 mm;
step two, mixing the Sinkiang arnebia root powder and the vegetable oil in a proportion of 1: mixing the solid-liquid ratio of 10g/ml in a material mixing tank to obtain Sinkiang arnebia root mixed solution;
guiding the Sinkiang arnebia root mixed solution into a micro-jet extractor at a feeding speed of 12L/min for micro-jet extraction at normal temperature to obtain Sinkiang arnebia root extracting solution;
and step four, guiding the Sinkiang arnebia root extracting solution into a centrifugal machine, centrifuging at the rotating speed of 8000rpm for solid-liquid separation, collecting separated liquid, and purifying the separated liquid by using a 700nm ceramic membrane to obtain the Sinkiang arnebia root extract.
The undaria pinnatifida extract is extracted from roots of French brown algae by a supercritical carbon dioxide extraction method, and comprises the following steps of:
firstly, breaking the wall of the root of brown algae, crushing, and soaking in an edible ethanol solution for 36 hours to obtain a mixed solution;
adding the mixed solution into an extraction kettle, introducing carbon dioxide in a supercritical state into the extraction kettle, controlling the temperature at 35 ℃, controlling the pressure at 35Mpa and controlling the time at 3 hours;
and step three, introducing the carbon dioxide fluid containing the brown algae oil flowing out of the extraction kettle into a separation kettle for decompression separation to obtain the brown algae oil, and mixing the brown algae oil with caprylic/capric triglyceride to obtain the undaria pinnatifida extract.
The raw materials and equipment used in the present application are all common raw materials and equipment in the field, and are all from commercially available products, unless otherwise specified. The methods used in this application are conventional in the art unless otherwise indicated.
Examples
The examples were prepared in the following manner according to the compounding ratios shown in tables 1 and 2.
The specific method comprises the following steps:
step one, weighing and adding the phase A substances according to parts by weight, heating to 85-90 ℃ until the phase A substances are uniformly melted, and mixing and stirring for 5-10 min until the phase A substances are completely uniform;
step two, weighing and adding the phase B substances according to parts by weight, and mixing and stirring for 10-15 min at the temperature of 70-75 ℃ until the mixture is completely uniform;
step three, weighing and adding the phase C substances according to the weight parts, and uniformly mixing and stirring for 5-10 min at the temperature of 70-75 ℃;
and step four, defoaming and discharging, and filling at the temperature of 60-65 ℃.
TABLE 1
TABLE 2
Comparative example
A 6-pair comparative was prepared according to the following procedure.
Wherein:
comparative example 1: this comparative example provides a lip base composition which, compared to example 11, does not contain scarlet polyester, arnebia euchroma extract, undaria pinnatifida extract, and the remaining ingredients and preparation method are the same as example 11.
Comparative example 2: this comparative example provides a lip base composition which, compared to example 11, does not contain arnebia euchroma extract and undaria pinnatifida extract, and the remaining ingredients and preparation method are the same as example 11.
Comparative example 3: this comparative example provides a lip base composition which, compared to example 11, does not contain scarlet polyester, undaria pinnatifida extract, and the remaining components and preparation method are the same as example 11.
Comparative example 4: this comparative example provides a lip base composition which, compared to example 11, does not contain the cranberry ester and arnebia euchroma extract, and the remaining ingredients and preparation method are the same as example 11.
In addition, comparative examples 5-6 were prepared by replacing different lip care compositions and using different preparation methods.
Comparative examples 5-6 were prepared as follows, with the specific material formulations shown in Table 3:
step one, weighing and adding the group A materials according to parts by weight, heating to 80-85 ℃, and uniformly stirring until the materials are completely dissolved;
step two, weighing and adding the group B materials according to parts by weight, keeping the temperature at 70-75 ℃, and uniformly stirring until the materials are completely dissolved;
weighing and adding the group C materials in parts by weight, keeping the temperature at 70-75 ℃, and uniformly stirring;
and step four, defoaming and discharging, insulating at 75 ℃, filling, cooling to 5-10 ℃, and demolding.
TABLE 3
Comparative example 5 is a common lip balm, with shea butter as the lip care composition, along with aloe vera leaf extract and olive oil.
Comparative example 6 is another common lip balm on the market, lanolin was selected as a lip care composition together with chamomile extract and jojoba seed oil.
Effect example 1: 8h moisture test
Test samples: examples 1 to 15 and the commercially available A, B were selected as test samples
Testing an instrument: CorneometeterMPA 580 skin epidermis tester
Test objects: female volunteers between the ages of 20-40 years, 5 persons per group
The test method comprises the following steps:
1. selecting a test area of 2x2 cm2 on the curved side of the forearm of a subject, and uniformly coating the product on the area to be tested;
2. measurements were performed using a Corneometer at 0h, 2h, 4h and 8h before and after use, respectively;
3. the same spot was measured 5 times, and 3 average values were recorded excluding the maximum and minimum values.
The moisture increase/decrease rate is the difference between the moisture content before and after use/the moisture content before use/100%.
Wherein the water content measurements are reported in table 4, the stratum corneum water loss and gain calculated by the above formula are reported in table 5, and the units in table 5 are%.
TABLE 4
TABLE 5
As can be seen from the test results, the examples to which the natural lip care composition was added all had better moisturizing effects than the comparative examples.
Effect example 2: lip print improvement test
Test samples: the samples of example 11 and comparative examples 1 to 6 were selected as test samples
Testing an instrument: antera 3D (Miravex, Ireland)
Test objects: female volunteers between the ages of 20-40 years, 5 persons per group
The test method comprises the following steps:
1. measuring lip wrinkles by using an Antera 3D, selecting the deepest wrinkle of the lips of each subject, analyzing the wrinkle depth and the average cross-sectional area of each subject, and taking the average value of each group of volunteers as an initial value;
2. smearing the test sample in the morning, at noon and at night every day, and smearing the test sample for 2 times back and forth each time;
3. lip wrinkles were measured 1 week and 2 weeks after product use using an andrera 3D, respectively, wrinkle depth and average cross-sectional area at the same location were analyzed, and the average of each group of volunteers was taken as one-week and two-week values;
4. the rate of change of the wrinkle depth and average cross-sectional area of the lip skin after the corresponding test sample was used was calculated for each group of volunteers.
The rate of change of the wrinkle area is shown in table 6, and the rate of change of the wrinkle depth is shown in table 7.
TABLE 6
| Before | 1w | Rate of change | 2w | Rate of change | |
| Example 11 | 4.48 | 3.56 | -20.54％ | 3.02 | -32.59％ |
| Comparative example 1 | 3.89 | 3.44 | -11.57％ | 3.65 | -6.17％ |
| Comparative example 2 | 5.95 | 5.24 | -11.93％ | 5.13 | -13.78％ |
| Comparative example 3 | 4.17 | 3.69 | -11.51％ | 3.52 | -15.59％ |
| Comparative example 4 | 4.74 | 4.21 | -11.18％ | 3.96 | -16.46％ |
| Comparative example 5 | 4.28 | 3.64 | -14.95％ | 3.19 | -25.47％ |
| Comparative example 6 | 5.04 | 4.47 | -11.31％ | 4.02 | -20.24％ |
TABLE 7
| Before | 1w | Variations inRate of change | 2w | Rate of change | |
| Example 11 | 0.0298 | 0.0247 | -17.11％ | 0.0217 | -27.18％ |
| Comparative example 1 | 0.0261 | 0.0255 | -2.30％ | 0.0248 | -4.98％ |
| Comparative example 2 | 0.0390 | 0.0364 | -6.67％ | 0.0349 | -10.51％ |
| Comparative example 3 | 0.0271 | 0.0249 | -8.12％ | 0.0238 | -12.18％ |
| Comparative example 4 | 0.0290 | 0.0264 | -8.97％ | 0.0251 | -13.45％ |
| Comparative example 5 | 0.0267 | 0.0238 | -10.86％ | 0.0218 | -18.35％ |
| Comparative example 6 | 0.0344 | 0.0311 | -9.59％ | 0.0292 | -15.12％ |
According to the test results, the lip wrinkle improvement effect of the example 11 added with the natural lip care composition is remarkable, and is superior to comparative examples 1-4 in which the composition is not added, the scarlet orange ester is added alone, the Sinkiang arnebia root extract is added alone or the undaria pinnatifida extract is added alone, so that the scarlet orange ester, the Sinkiang arnebia root extract and the undaria pinnatifida extract have a synergistic effect. Meanwhile, the lip wrinkle improvement effect of the composition of the scarlet orange ester, the Sinkiang arnebia root extract and the undaria pinnatifida is far superior to that of the common lip functional composition as shown in comparative examples 5 and 6 in the lip wrinkle improvement effect of the composition of the example 11.
Effect example 3: cheilitis improvement test
Test samples: example 11
Testing an instrument: C-CUBE (PIXIENCE, France)
Test objects: 5 volunteers with cheilitis
The test method comprises the following steps:
1. the lips of the volunteers were photographed using C-CUBE;
2. smearing the test sample in the morning, at noon and at night every day, and smearing the test sample for 2 times back and forth each time;
3. the lips of the volunteers were photographed 2 weeks, 4 weeks after the product use, again using C-CUBE.
The comparison before and after use is shown in figure 1 as follows:
as can be seen from the test results, the natural lip care composition prepared by the invention has a remarkable improvement effect on the phenomena of exfoliative cheilitis and xerosis after 4 weeks, and all the subjects give satisfactory evaluation after the test is finished.
Effect example 4: test of stability to sunlight
Test samples: example 11 and comparative examples 1 to 6
The test method comprises the following steps:
1. placing 20-30 g of each group of samples in a 50ml transparent glass bottle container, and placing the container in a test environment with sufficient sunlight;
2. observing the stability of the color, smell, appearance and the like of the sample every other week for 4 weeks in total;
3. the evaluation was performed by a score of 0 to 3, and the higher the score, the larger the change in properties, and the results are shown in the following table.
TABLE 8
TABLE 9
The test results show that the stability of the sunshine for 4 weeks in the example 11 is superior to that of the comparative examples 1-6 under the condition that no additional antioxidant is added, and the compound of the tangeretin, the lithospermum extract and the undaria pinnatifida extract is more resistant to the sunshine.
There are many other possible embodiments of the present invention, which are not listed here, and the embodiments claimed in the claims of the present invention can be implemented.
The details not described in the specification of the present application belong to the common general knowledge of those skilled in the art.
In the following description and in the claims, the terms "include" and "comprise" are used in an open-ended fashion, and thus should be interpreted to mean "include, but not limited to. "substantially" means within an acceptable error range, and a person skilled in the art can solve the technical problem within a certain error range to substantially achieve the technical effect.
It is also noted that the terms "comprises," "comprising," or any other variation thereof, are intended to cover a non-exclusive inclusion, such that a good or system that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such good or system. Without further limitation, an element defined by the phrase "comprising an … …" does not exclude the presence of other like elements in a commodity or system that includes the element.
The foregoing description shows and describes several preferred embodiments of the present application, but as aforementioned, it is to be understood that the application is not limited to the forms disclosed herein, but is not to be construed as excluding other embodiments and is capable of use in various other combinations, modifications, and environments and is capable of changes within the scope of the inventive concept as expressed herein, commensurate with the above teachings, or the skill or knowledge of the relevant art. And that modifications and variations may be effected by those skilled in the art without departing from the spirit and scope of the application, which is to be protected by the claims appended hereto.
Claims (10)
1. A lip care composition is characterized by comprising, by mass, 2-40 parts of cranberry fat, 0.1-4 parts of lithospermum extract and 0.1-0.4 part of undaria pinnatifida extract.
2. The lip care composition according to claim 1, comprising 2 to 40 parts by mass of cranberry fat, 0.1 to 4 parts by mass of lithospermum extract, and 0.1 to 0.4 part by mass of undaria pinnatifida extract; the tangerines ester: and (3) extracting the lithospermum: the weight portion ratio of the undaria pinnatifida extract is (20-100): 1-10): 1.
3. The lip care composition according to claim 2, comprising 2 to 40 parts by mass of cranberry fat, 0.1 to 4 parts by mass of lithospermum extract, and 0.1 to 0.4 part by mass of undaria pinnatifida extract; the tangerines ester: and (3) extracting the lithospermum: the weight portion ratio of the undaria pinnatifida extract is (50-80): 5-8): 1.
4. The lip care composition according to claim 1, wherein the comfrey extract is extracted from arnebia euchroma root by a microfluidization extraction method comprising the steps of:
step one, crushing Sinkiang arnebia root into powder with the particle size of not more than 5 mm;
step two, mixing the Sinkiang arnebia root powder and the vegetable oil in a proportion of 1: (3-20) mixing the solid-liquid ratio of g/ml in a material mixing tank to obtain a Sinkiang arnebia root mixed solution;
guiding the Sinkiang arnebia root mixed solution into a micro-jet extractor at a feeding speed of 8L/min-18L/min for micro-jet extraction at normal temperature to obtain Sinkiang arnebia root extracting solution;
and step four, guiding the Sinkiang arnebia root extracting solution into a centrifugal machine, centrifuging at the rotating speed of 5000-12000 rpm for solid-liquid separation, collecting separated liquid, and purifying the separated liquid by using a 300-700 nm ceramic membrane to obtain the Sinkiang arnebia root extract.
5. The lip care composition according to claim 1, wherein said Undaria pinnatifida extract is extracted from root of French brown algae by supercritical carbon dioxide extraction comprising the steps of:
firstly, breaking the walls of brown algae roots, crushing, and soaking in an edible ethanol solution for 12-36 hours to obtain a mixed solution;
adding the mixed solution into an extraction kettle, introducing carbon dioxide in a supercritical state into the extraction kettle, controlling the temperature at 30-45 ℃, controlling the pressure at 20-40 Mpa, and controlling the time at 1.5-3.5 hours;
and step three, introducing the carbon dioxide fluid containing the brown algae oil flowing out of the extraction kettle into a separation kettle for decompression separation to obtain the brown algae oil, and mixing the brown algae oil with caprylic/capric triglyceride to obtain the undaria pinnatifida extract.
6. A cosmetic containing the composition according to claim 1, characterized by comprising 2-40 parts by mass of cranberry fat, 0.1-4 parts by mass of lithospermum extract, 0.1-0.4 part by mass of undaria pinnatifida extract, 60-80 parts by mass of an emollient and 10-30 parts by mass of a thickener.
7. Cosmetic product according to claim 6, characterized in that the emollient is chosen from jojoba oil, macadamia nut oil, sunflower seed oil, meadowfoam seed oil, grape seed oil, camellia seed oil, olive oil, rosa canina oil, almond oil, avocado oil, evening primrose oil, shea butter, avocado butter, jojoba fat, cocoa butter, mango seed fat, squalane, petrolatum, lanolin, sorbitan isostearate, diisostearyl malate, glycerol tri (ethylacetate) ester, polyglycerol-2 triisostearate, caprylic/capric triglyceride, hydrogenated polyisobutene (and) ethylene/propylene/styrene copolymers (and) butylene/ethylene/styrene copolymers, acetylated (sucrose distearate), hydroxystearic acid, phytosterol/isostearyl alcohol/cetyl alcohol/behenyl alcohol dilinoleate, phytosterol/isostearyl alcohol/behenic alcohol dilinoleate, hydrogenated polyisobutene, and mixtures thereof, Any one or a combination of at least two of glyceryl caprylate, caprylyl glycol, diisostearyl malate (and) dimethyl silylated silica.
8. The cosmetic according to claim 6, wherein the thickener is selected from one or a combination of at least two of polyethylene, polybutene, microcrystalline wax, beeswax, paraffin wax, ozokerite wax, candelilla wax, carnauba wax, and hydrogenated olive oil.
9. The cosmetic of claim 6, wherein the cosmetic is a lipstick, lip mask, lip glaze or lip gloss.
10. A method for preparing the cosmetic according to claim 6, comprising the steps of:
weighing the components of the thickening agent and part of the emollient according to mass fractions, heating to 85-90 ℃ until the components are uniformly melted, and mixing and stirring for 5-10 min until the components are completely uniform;
step two, weighing and adding the rest of components of the emollient according to parts by weight, and mixing and stirring for 10-15 min at the temperature of 70-75 ℃ until the components are completely uniform;
step three, weighing and adding the components of the scarlet orange fat, the Sinkiang lithospermum extract and the undaria pinnatifida extract according to parts by weight, and uniformly mixing and stirring for 5-10 min at the temperature of 70-75 ℃;
and step four, defoaming and discharging, and filling at the temperature of 60-65 ℃ to obtain a finished product.
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