CN115287122B - Fresh tobacco baking quality-improving flavoring agent and preparation method and application thereof - Google Patents
Fresh tobacco baking quality-improving flavoring agent and preparation method and application thereof Download PDFInfo
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- CN115287122B CN115287122B CN202210746043.9A CN202210746043A CN115287122B CN 115287122 B CN115287122 B CN 115287122B CN 202210746043 A CN202210746043 A CN 202210746043A CN 115287122 B CN115287122 B CN 115287122B
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- 241000208125 Nicotiana Species 0.000 title claims abstract description 140
- 235000002637 Nicotiana tabacum Nutrition 0.000 title claims abstract description 140
- 239000000796 flavoring agent Substances 0.000 title claims description 24
- 235000013355 food flavoring agent Nutrition 0.000 title claims description 24
- 238000002360 preparation method Methods 0.000 title abstract description 11
- 238000005507 spraying Methods 0.000 claims abstract description 18
- 239000000463 material Substances 0.000 claims abstract description 12
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 12
- 244000026873 Alternanthera philoxeroides Species 0.000 claims abstract description 11
- 235000012907 honey Nutrition 0.000 claims abstract description 11
- 244000242564 Osmanthus fragrans Species 0.000 claims abstract description 9
- 235000019083 Osmanthus fragrans Nutrition 0.000 claims abstract description 9
- 239000000843 powder Substances 0.000 claims description 21
- 238000001035 drying Methods 0.000 claims description 7
- 238000000053 physical method Methods 0.000 claims description 6
- 235000019082 Osmanthus Nutrition 0.000 claims description 5
- 241000333181 Osmanthus Species 0.000 claims description 5
- 238000002156 mixing Methods 0.000 claims description 5
- 238000003756 stirring Methods 0.000 claims description 4
- 239000010902 straw Substances 0.000 claims description 3
- 102000004190 Enzymes Human genes 0.000 claims description 2
- 108090000790 Enzymes Proteins 0.000 claims description 2
- 241000257303 Hymenoptera Species 0.000 claims description 2
- 238000005520 cutting process Methods 0.000 claims description 2
- 238000007865 diluting Methods 0.000 claims description 2
- 238000009837 dry grinding Methods 0.000 claims description 2
- 239000012634 fragment Substances 0.000 claims description 2
- 239000007788 liquid Substances 0.000 claims description 2
- 238000004090 dissolution Methods 0.000 claims 1
- 239000000126 substance Substances 0.000 abstract description 46
- 229910001414 potassium ion Inorganic materials 0.000 abstract description 17
- 238000000034 method Methods 0.000 abstract description 15
- 239000003795 chemical substances by application Substances 0.000 abstract description 2
- 230000015572 biosynthetic process Effects 0.000 abstract 1
- 239000011148 porous material Substances 0.000 abstract 1
- 230000001953 sensory effect Effects 0.000 description 21
- WVDDGKGOMKODPV-UHFFFAOYSA-N Benzyl alcohol Chemical compound OCC1=CC=CC=C1 WVDDGKGOMKODPV-UHFFFAOYSA-N 0.000 description 18
- XPFVYQJUAUNWIW-UHFFFAOYSA-N furfuryl alcohol Chemical compound OCC1=CC=CO1 XPFVYQJUAUNWIW-UHFFFAOYSA-N 0.000 description 18
- 230000007935 neutral effect Effects 0.000 description 18
- 239000000047 product Substances 0.000 description 18
- OHEFFKYYKJVVOX-UHFFFAOYSA-N sulcatol Chemical compound CC(O)CCC=C(C)C OHEFFKYYKJVVOX-UHFFFAOYSA-N 0.000 description 18
- 239000000203 mixture Substances 0.000 description 15
- 238000013441 quality evaluation Methods 0.000 description 14
- IGJQUJNPMOYEJY-UHFFFAOYSA-N 2-acetylpyrrole Chemical compound CC(=O)C1=CC=CN1 IGJQUJNPMOYEJY-UHFFFAOYSA-N 0.000 description 12
- WRMNZCZEMHIOCP-UHFFFAOYSA-N 2-phenylethanol Chemical compound OCCC1=CC=CC=C1 WRMNZCZEMHIOCP-UHFFFAOYSA-N 0.000 description 12
- NIDGCIPAMWNKOA-WOJBJXKFSA-N Neophytadiene Natural products [C@H](CCC[C@@H](CCCC(C)C)C)(CCCC(C=C)=C)C NIDGCIPAMWNKOA-WOJBJXKFSA-N 0.000 description 12
- HUMNYLRZRPPJDN-UHFFFAOYSA-N benzaldehyde Chemical compound O=CC1=CC=CC=C1 HUMNYLRZRPPJDN-UHFFFAOYSA-N 0.000 description 12
- 235000021466 carotenoid Nutrition 0.000 description 12
- 150000001747 carotenoids Chemical class 0.000 description 12
- 229930002875 chlorophyll Natural products 0.000 description 12
- 235000019804 chlorophyll Nutrition 0.000 description 12
- ATNHDLDRLWWWCB-AENOIHSZSA-M chlorophyll a Chemical compound C1([C@@H](C(=O)OC)C(=O)C2=C3C)=C2N2C3=CC(C(CC)=C3C)=[N+]4C3=CC3=C(C=C)C(C)=C5N3[Mg-2]42[N+]2=C1[C@@H](CCC(=O)OC\C=C(/C)CCC[C@H](C)CCC[C@H](C)CCCC(C)C)[C@H](C)C2=C5 ATNHDLDRLWWWCB-AENOIHSZSA-M 0.000 description 12
- HYBBIBNJHNGZAN-UHFFFAOYSA-N furfural Chemical compound O=CC1=CC=CO1 HYBBIBNJHNGZAN-UHFFFAOYSA-N 0.000 description 12
- CDOSHBSSFJOMGT-UHFFFAOYSA-N linalool Chemical compound CC(C)=CCCC(C)(O)C=C CDOSHBSSFJOMGT-UHFFFAOYSA-N 0.000 description 12
- NIDGCIPAMWNKOA-UHFFFAOYSA-N neophytadiene Chemical compound CC(C)CCCC(C)CCCC(C)CCCC(=C)C=C NIDGCIPAMWNKOA-UHFFFAOYSA-N 0.000 description 12
- DTUQWGWMVIHBKE-UHFFFAOYSA-N phenylacetaldehyde Chemical compound O=CCC1=CC=CC=C1 DTUQWGWMVIHBKE-UHFFFAOYSA-N 0.000 description 12
- PQDRXUSSKFWCFA-CFNZNRNTSA-N solanone Chemical group CC(=O)CC[C@@H](C(C)C)\C=C\C(C)=C PQDRXUSSKFWCFA-CFNZNRNTSA-N 0.000 description 12
- PQDRXUSSKFWCFA-UHFFFAOYSA-N solanone Natural products CC(=O)CCC(C(C)C)C=CC(C)=C PQDRXUSSKFWCFA-UHFFFAOYSA-N 0.000 description 12
- UHEPJGULSIKKTP-UHFFFAOYSA-N sulcatone Chemical compound CC(C)=CCCC(C)=O UHEPJGULSIKKTP-UHFFFAOYSA-N 0.000 description 12
- PSQYTAPXSHCGMF-BQYQJAHWSA-N β-ionone Chemical compound CC(=O)\C=C\C1=C(C)CCCC1(C)C PSQYTAPXSHCGMF-BQYQJAHWSA-N 0.000 description 12
- 150000001875 compounds Chemical class 0.000 description 10
- COLNVLDHVKWLRT-QMMMGPOBSA-N L-phenylalanine Chemical compound OC(=O)[C@@H](N)CC1=CC=CC=C1 COLNVLDHVKWLRT-QMMMGPOBSA-N 0.000 description 9
- 238000011282 treatment Methods 0.000 description 9
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 7
- 229910052700 potassium Inorganic materials 0.000 description 7
- 239000011591 potassium Substances 0.000 description 7
- 239000000779 smoke Substances 0.000 description 7
- SFEOKXHPFMOVRM-UHFFFAOYSA-N (+)-(S)-gamma-ionone Natural products CC(=O)C=CC1C(=C)CCCC1(C)C SFEOKXHPFMOVRM-UHFFFAOYSA-N 0.000 description 6
- 239000001490 (3R)-3,7-dimethylocta-1,6-dien-3-ol Substances 0.000 description 6
- CBQXHTWJSZXYSK-DFTQQVSXSA-N (4e)-4-[(e)-but-2-enylidene]-3,5,5-trimethylcyclohex-2-en-1-one Chemical compound C\C=C\C=C1\C(C)=CC(=O)CC1(C)C CBQXHTWJSZXYSK-DFTQQVSXSA-N 0.000 description 6
- CBQXHTWJSZXYSK-VZVVJSHISA-N (4e)-4-[(z)-but-2-enylidene]-3,5,5-trimethylcyclohex-2-en-1-one Chemical compound C\C=C/C=C1/C(C)=CC(=O)CC1(C)C CBQXHTWJSZXYSK-VZVVJSHISA-N 0.000 description 6
- CBQXHTWJSZXYSK-DVIJZSFDSA-N (4z)-4-[(e)-but-2-enylidene]-3,5,5-trimethylcyclohex-2-en-1-one Chemical compound C\C=C\C=C1/C(C)=CC(=O)CC1(C)C CBQXHTWJSZXYSK-DVIJZSFDSA-N 0.000 description 6
- CBQXHTWJSZXYSK-UNKATYBDSA-N (4z)-4-[(z)-but-2-enylidene]-3,5,5-trimethylcyclohex-2-en-1-one Chemical compound C\C=C/C=C1\C(C)=CC(=O)CC1(C)C CBQXHTWJSZXYSK-UNKATYBDSA-N 0.000 description 6
- CDOSHBSSFJOMGT-JTQLQIEISA-N (R)-linalool Natural products CC(C)=CCC[C@@](C)(O)C=C CDOSHBSSFJOMGT-JTQLQIEISA-N 0.000 description 6
- LHORCXXUZJAMPU-UHFFFAOYSA-N 1,7,11-trimethyl-4-(propan-2-yl)cyclotetradecane Chemical compound CC(C)C1CCC(C)CCCC(C)CCCC(C)CC1 LHORCXXUZJAMPU-UHFFFAOYSA-N 0.000 description 6
- IEMMBWWQXVXBEU-UHFFFAOYSA-N 2-acetylfuran Chemical compound CC(=O)C1=CC=CO1 IEMMBWWQXVXBEU-UHFFFAOYSA-N 0.000 description 6
- ROTNQFPVXVZSRL-UHFFFAOYSA-N 4,4,6-trimethyl-7-oxabicyclo[4.1.0]heptan-2-one Chemical compound C1C(C)(C)CC(=O)C2OC21C ROTNQFPVXVZSRL-UHFFFAOYSA-N 0.000 description 6
- OUDFNZMQXZILJD-UHFFFAOYSA-N 5-methyl-2-furaldehyde Chemical compound CC1=CC=C(C=O)O1 OUDFNZMQXZILJD-UHFFFAOYSA-N 0.000 description 6
- DFYRUELUNQRZTB-UHFFFAOYSA-N apocynin Chemical compound COC1=CC(C(C)=O)=CC=C1O DFYRUELUNQRZTB-UHFFFAOYSA-N 0.000 description 6
- 235000019445 benzyl alcohol Nutrition 0.000 description 6
- POIARNZEYGURDG-FNORWQNLSA-N beta-damascenone Chemical compound C\C=C\C(=O)C1=C(C)C=CCC1(C)C POIARNZEYGURDG-FNORWQNLSA-N 0.000 description 6
- POIARNZEYGURDG-UHFFFAOYSA-N beta-damascenone Natural products CC=CC(=O)C1=C(C)C=CCC1(C)C POIARNZEYGURDG-UHFFFAOYSA-N 0.000 description 6
- 229930001594 cembrane Natural products 0.000 description 6
- 238000011156 evaluation Methods 0.000 description 6
- LTUMRKDLVGQMJU-UHFFFAOYSA-N famesylacetone Natural products CC(C)=CCCC(C)=CCCC(C)=CCCC(C)=O LTUMRKDLVGQMJU-UHFFFAOYSA-N 0.000 description 6
- LTUMRKDLVGQMJU-IUBLYSDUSA-N farnesyl acetone Chemical compound CC(C)=CCC\C(C)=C\CC\C(C)=C\CCC(C)=O LTUMRKDLVGQMJU-IUBLYSDUSA-N 0.000 description 6
- HNZUNIKWNYHEJJ-FMIVXFBMSA-N geranyl acetone Chemical compound CC(C)=CCC\C(C)=C\CCC(C)=O HNZUNIKWNYHEJJ-FMIVXFBMSA-N 0.000 description 6
- HNZUNIKWNYHEJJ-UHFFFAOYSA-N geranyl acetone Natural products CC(C)=CCCC(C)=CCCC(C)=O HNZUNIKWNYHEJJ-UHFFFAOYSA-N 0.000 description 6
- 150000002596 lactones Chemical class 0.000 description 6
- 229930007744 linalool Natural products 0.000 description 6
- QNGNSVIICDLXHT-UHFFFAOYSA-N para-ethylbenzaldehyde Natural products CCC1=CC=C(C=O)C=C1 QNGNSVIICDLXHT-UHFFFAOYSA-N 0.000 description 6
- 229940100595 phenylacetaldehyde Drugs 0.000 description 6
- COLNVLDHVKWLRT-UHFFFAOYSA-N phenylalanine Natural products OC(=O)C(N)CC1=CC=CC=C1 COLNVLDHVKWLRT-UHFFFAOYSA-N 0.000 description 6
- 229930007850 β-damascenone Natural products 0.000 description 6
- 230000000052 comparative effect Effects 0.000 description 4
- 238000003306 harvesting Methods 0.000 description 4
- 238000004519 manufacturing process Methods 0.000 description 4
- 230000000694 effects Effects 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 3
- 150000002994 phenylalanines Chemical class 0.000 description 3
- 206010013911 Dysgeusia Diseases 0.000 description 2
- NPYPAHLBTDXSSS-UHFFFAOYSA-N Potassium ion Chemical compound [K+] NPYPAHLBTDXSSS-UHFFFAOYSA-N 0.000 description 2
- 210000004027 cell Anatomy 0.000 description 2
- 238000003912 environmental pollution Methods 0.000 description 2
- 230000007794 irritation Effects 0.000 description 2
- 239000002086 nanomaterial Substances 0.000 description 2
- 238000004383 yellowing Methods 0.000 description 2
- 241000428811 Alternanthera Species 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 238000012271 agricultural production Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000007664 blowing Methods 0.000 description 1
- 230000015556 catabolic process Effects 0.000 description 1
- 239000007857 degradation product Substances 0.000 description 1
- 238000006731 degradation reaction Methods 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 239000000049 pigment Substances 0.000 description 1
- 210000002706 plastid Anatomy 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000002689 soil Substances 0.000 description 1
- 238000009941 weaving Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0003—Compounds of unspecified constitution defined by the chemical reaction for their preparation
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Toxicology (AREA)
- Manufacture Of Tobacco Products (AREA)
Abstract
The invention belongs to the technical field of tobacco quality and aroma enhancement, and particularly relates to a fresh tobacco baking quality and aroma enhancement agent and a preparation method and application thereof. Comprising the following steps: dried 20-50nm nanometer materials of dried stem and leaf of alternanthera philoxeroides, dried fresh osmanthus fragrans, dried orange peel and honey. The preparation is based on film formation after foliage spraying and is absorbed by the foliage, on one hand, certain potassium ions of cured tobacco leaves are provided, the opening of fresh tobacco leaf pores is promoted, the water loss of the fresh tobacco leaves is accelerated, and the curing is facilitated; meanwhile, a certain amount of sugar and aroma substances are provided for fresh tobacco, the aroma substance content and quality of the cured tobacco leaf are improved, and the method has good practicability and application value.
Description
Technical Field
The invention belongs to the technical field of quality and aroma enhancement, and particularly relates to a fresh smoke baking quality and aroma enhancement agent and a preparation method and application thereof.
Background
Tobacco is a warm-loving crop native to america, and is also an important cash crop in the agricultural production of China at present. The quality of tobacco leaves is divided into field quality and baking quality according to production links, wherein the field quality is the basis of the baking quality, and the baking quality is the guarantee of the field quality; the baking quality of tobacco leaves is closely related to the maturity and the moisture content of fresh tobacco, the baking technology and the like; different tobacco planting areas further cause differences in quality of cured tobacco due to differences in ecological environment conditions, tobacco growers production technology levels, tobacco harvesting maturity standards and moisture content of harvested tobacco, as well as differences in curing equipment and curing technology; therefore, on the premise of ensuring the ripe and harvest of the tobacco leaves, the moisture content of the harvested tobacco leaves is properly reduced, and the tobacco leaf baking quality is improved, and the tobacco leaf baking green risk is reduced.
The existing method for reducing the collected high-water-content fresh tobacco in tobacco leaf baking is usually realized by adopting a physical mode of opening a fan for blowing after the fresh tobacco stems are woven into a house, but the mode consumes electric power, easily causes mechanical damage of the tobacco leaves to influence the baking quality, and is difficult to eliminate the adverse effects under a simple and easy method.
Disclosure of Invention
As the current fresh tobacco harvesting and baking has no simple and easy single technical measure which can effectively solve the problem of low tobacco baking quality (such as baking green and hanging ash and the like) caused by high water content of fresh tobacco, the primary aim of the invention is to provide a fresh tobacco baking quality improving flavoring agent. The leaf surface spraying is carried out on the fresh tobacco leaves which are collected, woven and packaged into a house, so that the opening of air holes of fresh tobacco leaf flesh cells is promoted, the moisture content is reduced, and yellowing is easy to occur; meanwhile, potassium ions, aroma substances and sugar are supplemented to improve the potassium content of the cured tobacco leaves and the aroma substances, so that the curing quality of the tobacco leaves is improved and improved. The fresh smoke baking quality-improving flavoring agent has the characteristics of simple production, low cost, convenient use, easy grasp, better effect than the prior art measures, no environmental pollution and the like.
In order to solve the technical problems, the technical scheme of the invention is as follows:
the fresh smoke baking quality-improving flavoring agent comprises the following components in parts by weight: 15-30 parts of dry stem and leaf powder of alternanthera philoxeroides, 20-40 parts of dry fresh osmanthus fragrans powder, 25-40 parts of dry dried orange peel powder and 20-30 parts of honey.
Further preferred is: the fresh tobacco baking quality-improving flavoring agent comprises the following components in parts by weight: 20 parts of alternanthera philoxeroides dry stem and leaf powder, 30 parts of dry fresh osmanthus fragrans powder, 30 parts of dry dried orange peel powder and 20 parts of honey.
Further, the particle size of the dry stem and leaf powder of the alternanthera philoxeroides, the dry fresh osmanthus fragrans powder and the dry dried orange peel powder is 20-50nm.
The dry stem and leaf powder of the alternanthera philoxeroides is prepared by drying stem and leaf of the alternanthera philoxeroides until the moisture content is less than or equal to 5%, and carrying out dry crushing by adopting a physical method to prepare a material with 20-50nm for later use; the dry fresh osmanthus powder is prepared by firstly cutting fresh osmanthus into fragments with the length of 1-2 cm, deactivating enzyme at 102 ℃ for 1h, drying at 70-80 ℃ (drying to water content of < 5%), and carrying out dry crushing by a physical method to prepare a 20-50nm material for later use; the dried orange peel powder is prepared by drying fresh orange peel at 70-80 ℃ until the water content is less than 5%, and performing dry grinding by a physical method to prepare a material with 20-50nm for later use; the honey is produced by bees cultivated by bee farmers.
The invention also provides a preparation method of the fresh smoke baking quality-improving flavoring agent, and the fresh smoke baking quality-improving flavoring agent is prepared by uniformly mixing the components.
The invention also provides an application method of the fresh-tobacco baking quality-improving flavoring agent, which comprises the steps of diluting the fresh-tobacco baking quality-improving flavoring agent, spraying the diluted fresh-tobacco baking quality-improving flavoring agent on the surface of the mature and harvested tobacco leaves, and baking.
The tobacco leaves are fresh tobacco leaves which are picked after rain and are cooked and to be roasted with high water content.
Further, the fresh smoke baking quality-improving flavoring agent and water are mixed according to the following ratio of 1-2: mixing the components in a mass ratio of 100-200, fully stirring and completely dissolving the components to prepare the spraying liquid.
Further, when the harvested mature fresh tobacco leaves are woven into straw and packaged into houses, the diluted fresh tobacco baking quality-improving flavoring agent is sprayed on the surfaces of the tobacco leaves according to the leaf surface spraying amount of 7.5-8.0 g/kg of fresh tobacco leaves.
Preferably, when the harvested mature fresh tobacco leaves are woven into straw and packaged into houses, the diluted fresh tobacco baking quality-improving flavoring agent is sprayed on the surfaces of the tobacco leaves according to the leaf surface spraying amount of 7.5g/kg of fresh tobacco leaves.
The invention has the beneficial effects that:
(1) The preparation of the invention can improve the potassium content and the aroma substance content of the cured tobacco leaves.
(2) The preparation of the invention has wide sources of raw materials and low cost: the dry stem leaves and fresh osmanthus fragrans of the alternanthera philoxeroides can be obtained from wild or planted plants in the natural world; the dried orange peel is produced from fruit trees and purchased in the market; the honey is produced by bee farmers and can be purchased in the market. The materials are wide in sources, low in price and convenient to purchase.
(3) The preparation of the invention is simple and easy in preparation method, and the preparation can be prepared by adding clean water after mixing all the components, and stirring the mixture uniformly and completely to dissolve the components.
According to the fresh tobacco baking quality-improving flavoring agent, leaf surface spraying is carried out on fresh tobacco leaves to be baked in a harvesting, straw-weaving and house-filling mode, so that the opening of air holes of fresh tobacco leaf flesh cells is promoted, the moisture content is reduced, and yellowing is easy to occur; meanwhile, potassium ions, aroma substances and sugar are supplemented to improve the potassium content of the cured tobacco leaves and the aroma substances, so that the curing quality of the tobacco leaves is improved and improved. The fresh smoke baking quality-improving flavoring agent has the characteristics of simple production, low cost, convenient use, easy grasp, better effect than the prior art measures, no environmental pollution and the like, and has better application value.
Detailed Description
The following examples are intended to further illustrate the invention, but not to limit it.
Example 1
The test is carried out in a teaching and scientific research base in Hunan agricultural university in Changsha city. The cured tobacco is cloud tobacco 87, the tobacco leaves are mature fresh tobacco leaves harvested after 2021, 6 months and 10 days of rain, 20 rods are multiplied by 3=60 rods (120 pieces/rod of fresh tobacco leaves), and the cured tobacco is prepared according to the following components: dried fresh osmanthus fragrans nanometer material: pericarpium Citri Reticulatae nanometer material: honey = 20:30:30: after 20 parts by weight "mix, the mixture was mixed with clean water in parts by weight = 1:100, uniformly mixing and stirring, and spraying the mixture on the surface of the fresh tobacco leaves to be cured according to the spraying amount of 30kg/4T of the fresh tobacco leaves to be cured (the spraying amount of 7.5g/kg of the leaf surfaces of the fresh tobacco leaves to be cured); and the tobacco leaves which are picked in the same curing barn in the same period are compared.
Grading the tobacco leaves after baking, taking B2F and C3F tobacco leaves, and referring to GB2635-92 standard, and performing appearance quality such as color, maturity, leaf structure, identity, oil content and chromaticity (see Table 1); the sensory quality of the tobacco leaf, namely the aroma quality, the aroma quantity, the miscellaneous gas, the irritation, the combustibility, the ash content, the aftertaste, the concentration and the strength (see table 2) is evaluated by referring to the YC/T530-2015 standard, and the potassium ion content of the tobacco leaf is measured by adopting a flame photometer; reference Shi Hongzhi et al [1] The method adopts an American HP5890II.5972 gas chromatograph-mass spectrometer to measure and analyze the aroma substances of the tobacco leaf samples.
[1] Shi Hongzhi, gu Shaolong, duan Weidong, etc. different genotypes of cured tobacco plastid pigment degradation and content relation with volatile degradation products of cured tobacco leaf [ J ]. Chinese agricultural science, 2012, 45 (16): 3346-3356.
TABLE 1 appearance quality evaluation index and score
TABLE 2 sensory quality evaluation index and score
TABLE 3 evaluation of overall score for appearance and sensory quality indicators of cured tobacco
As can be seen from the above Table 3, the total appearance quality evaluation scores of C3F and B2F of the cured tobacco leaves treated with the composition of the present invention were successively higher than the control scores of 5.6 and 6.2, respectively, and the total sensory quality evaluation scores of C3F and B2F were successively higher than the control scores of 2.6 and 2.5, respectively, indicating that the improvement of the cured appearance and sensory quality of the tobacco leaves was facilitated. The content of potassium ions in the C3F and B2F tobacco leaves is respectively 5.15 percent and 4.27 percent higher than that in the control, so that the content of potassium ions in the tobacco leaves is improved.
Note that: the percentage (%) increase in treated potassium content compared to the control = [ (percentage value of treated potassium content-percentage value of control potassium content)/(percentage value of control potassium content ] ×100, the same applies below.
TABLE 4 different treatments for neutral volatile aroma content (μg/g)
Note that: 1. the total carotenoid products mainly comprise 17 substances including linalool, 6-methyl-5-hepten-2-ol, 6-methyl-5-hepten-2-one, farnesyl acetone, beta-dihydro-damascenone, beta-damascenone, geranylacetone, beta-ionone, megastigmatrienone 1, megastigmatrienone 2, megastigmatrienone 3, megastigmatrienone 4, 3-hydroxy-beta-dihydro-damascenone, spirodelanone, isophorone oxide, dihydro-kiwi lactone and 4-acetyl-2-methoxyphenol.
2. The total amount of phenylalanine is mainly 4 substances of benzaldehyde, phenylacetaldehyde, phenethyl alcohol and benzyl alcohol.
3. The total amount of the brown products is mainly the content of substances in furfural, 5-methyl furfural, 2-acetyl furan, furfuryl alcohol, 3, 4-dimethyl-2, 5-furan and 2-acetyl pyrrole 6.
4. The cembrane is solanone.
5. Chlorophyll is neophytadiene.
As can be seen from Table 4 above, the total content of neutral volatile aroma substances in the cured tobacco leaves treated with the composition of the present invention, C3F and B2F tobacco leaves, was 17.0% and 16.4%, respectively, higher than that of the control, wherein: the total amount of 17 carotenoid is 28.1% and 23.8% higher than control; the total amount of 4 phenylalanine compounds is 23.3% and 19.5% higher than that of the control; the total amount of the 6 brown products is 15.3% and 18.5% higher than that of the control; the content of the cembrane-like compounds (solanone) is 20.3% and 11.6% higher than that of the control; chlorophyll (neophytadiene) content was 15.3% and 18.5% higher than control, respectively. The method shows that the total content of neutral volatile aroma substances and the content of each main chemical component are improved, and the aroma quality of tobacco leaves is improved.
Example 2
The test is carried out on the soil tobacco field of the paddy field in the Sangzhi county, longtan lawn of Zhang Jiangjia. The cured tobacco is cloud tobacco 87, the tobacco leaves are mature fresh tobacco leaves harvested after 2021, 6 months and 10 days of rain, 20 rods are multiplied by 3=60 rods (120 pieces/rod of fresh tobacco leaves), and the cured tobacco is prepared according to the following components: dried fresh osmanthus fragrans nanometer material: pericarpium Citri Reticulatae nanometer material: honey = 20:35:25: after 20 parts by weight "mix, the mixture was mixed with clean water in parts by weight = 1:400, and spraying the mixture on the surface of the fresh tobacco leaves to be cured according to the spraying amount of 30kg/4.5T (the spraying amount of 6.67g/kg of the leaf surfaces of the fresh tobacco leaves to be cured) of the fresh tobacco leaves to be cured; and the tobacco leaves which are picked in the same curing barn in the same period are compared.
Grading the tobacco leaves after baking, taking B2F and C3F tobacco leaves, and referring to GB2635-92 standard, and performing appearance quality such as color, maturity, leaf structure, identity, oil content and chromaticity (see Table 1); the sensory quality of the tobacco leaf, namely the aroma quality, the aroma quantity, the miscellaneous gas, the irritation, the combustibility, the ash content, the aftertaste, the concentration and the strength (see table 2) is evaluated by referring to the YC/T530-2015 standard, and the potassium ion content of the tobacco leaf is measured by adopting a flame photometer; reference Shi Hongzhi et al [1] The method adopts an American HP5890II.5972 gas chromatograph-mass spectrometer to measure and analyze the aroma substances of the tobacco leaf samples.
TABLE 5 evaluation of overall score for appearance and sensory quality indicators of cured tobacco
As can be seen from Table 5 above, the overall appearance quality evaluation scores of C3F and B2F of the cured tobacco leaves treated with the composition of the present invention were successively higher than the control scores of 7.6 and 8.2, respectively, and the overall sensory quality evaluation scores of C3F and B2F were successively higher than the control scores of 3.8 and 2.8, respectively, indicating that the improvement of the cured appearance and sensory quality of the tobacco leaves was facilitated. The content of potassium ions in the C3F and B2F tobacco leaves is respectively 5.49 percent and 4.17 percent higher than that in the control, so that the content of potassium ions in the tobacco leaves is improved.
TABLE 6 different treatments for neutral volatile aroma content (μg/g)
Note that: 1. the total carotenoid products mainly comprise 17 substances including linalool, 6-methyl-5-hepten-2-ol, 6-methyl-5-hepten-2-one, farnesyl acetone, beta-dihydro-damascenone, beta-damascenone, geranylacetone, beta-ionone, megastigmatrienone 1, megastigmatrienone 2, megastigmatrienone 3, megastigmatrienone 4, 3-hydroxy-beta-dihydro-damascenone, spirodelanone, isophorone oxide, dihydro-kiwi lactone and 4-acetyl-2-methoxyphenol.
2. The total amount of phenylalanine is mainly 4 substances of benzaldehyde, phenylacetaldehyde, phenethyl alcohol and benzyl alcohol.
3. The total amount of the brown products is mainly the content of substances in furfural, 5-methyl furfural, 2-acetyl furan, furfuryl alcohol, 3, 4-dimethyl-2, 5-furan and 2-acetyl pyrrole 6.
4. The cembrane is solanone.
5. Chlorophyll is neophytadiene.
As can be seen from Table 6 above, the total content of neutral volatile aroma substances in the cured tobacco leaves treated with the composition of the present invention, C3F and B2F tobacco leaves, was 11.5% and 11.0%, respectively, higher than that of the control, wherein: the total amount of 17 carotenoid is 22.0% and 20.6% higher than the control; the total amount of 4 phenylalanine groups is 15.7% and 16.2% higher than that of the control; the total amount of the 6 brown products is 15.1% and 12.0% higher than that of the control; the content of the cembrane-like compounds (solanone) is 19.7% and 11.9% higher than that of the control compound; chlorophyll (neophytadiene) content was 9.5% and 9.8% higher than control, respectively. The method shows that the total content of neutral volatile aroma substances and the content of each main chemical component are improved, and the aroma quality of tobacco leaves is improved.
Comparative example 1
The difference from example 1 is that only the nano alternanthera stem and leaf (set as treatment a) is subtracted and the remaining components are no longer used. The test site and time were the same as in test example 1.
TABLE 7 evaluation of overall score for appearance and sensory quality indicators of cured tobacco
As can be seen from Table 7, the total appearance quality evaluation scores of C3F and B2F were successively higher than the controls 0.4 and 0.6 respectively, and the total sensory quality evaluation scores of C3F and B2F were successively higher than the controls 0.3 and 0.4 respectively, indicating that the improvement of the baked appearance and sensory quality of tobacco leaves was facilitated. The content of potassium ions in the C3F and B2F tobacco leaves is respectively 0.34 percent and 0.35 percent higher than that in the control, so that the content of potassium ions in the tobacco leaves is improved.
TABLE 8 different treatments for neutral volatile aroma content (μg/g)
Note that: 1. the total carotenoid products mainly comprise 17 substances including linalool, 6-methyl-5-hepten-2-ol, 6-methyl-5-hepten-2-one, farnesyl acetone, beta-dihydro-damascenone, beta-damascenone, geranylacetone, beta-ionone, megastigmatrienone 1, megastigmatrienone 2, megastigmatrienone 3, megastigmatrienone 4, 3-hydroxy-beta-dihydro-damascenone, spirodelanone, isophorone oxide, dihydro-kiwi lactone and 4-acetyl-2-methoxyphenol.
2. The total amount of phenylalanine is mainly 4 substances of benzaldehyde, phenylacetaldehyde, phenethyl alcohol and benzyl alcohol.
3. The total amount of the brown products is mainly the content of substances in furfural, 5-methyl furfural, 2-acetyl furan, furfuryl alcohol, 3, 4-dimethyl-2, 5-furan and 2-acetyl pyrrole 6.
4. The cembrane is solanone.
5. Chlorophyll is neophytadiene.
As can be seen from Table 8 above, the total content of neutral volatile aroma substances in the cured tobacco leaves treated with the composition of the present invention, C3F and B2F tobacco leaves, was 2.94% and 1.64%, respectively, higher than that of the control, wherein: the total amount of 17 carotenoids was 1.85% and 1.97% higher than the control, respectively; the total amount of 4 phenylalanine groups is respectively 3.38 percent and 5.47 percent higher than that of the control; the total amount of the 6 brown products is 3.29% and 3.77% higher than the control; the content of the cembrane-like compounds (solanone) is 5.45% and 3.39% higher than that of the control compound; chlorophyll (neophytadiene) content was 2.90% and 1.21% higher than control, respectively. The method shows that the total content of neutral volatile aroma substances and the content of each main chemical component are improved, the aroma quality of tobacco leaves is improved, but no embodiment is obvious.
Comparative example 2
The difference from example 1 is that only the dried fresh osmanthus nanomaterial is removed (set as treatment B), and the remaining components are not used any more. The test site and time were the same as in test example 1.
TABLE 9 evaluation of overall score for appearance and sensory quality indicators of cured tobacco
As can be seen from table 9, the total appearance quality evaluation scores of C3F and B2F were higher than those of controls 2.4 and 2.4, respectively, and the total sensory quality evaluation scores of C3F and B2F were higher than controls 1.2 and 0.8, respectively, indicating that improvement of the baked appearance and sensory quality of tobacco leaves was facilitated. The content of potassium ions in the C3F and B2F tobacco leaves is respectively 4.81 percent and 5.30 percent higher than that in the control, so that the content of potassium ions in the tobacco leaves is improved.
Table 10 content of neutral volatile aroma substances (μg/g) for different treatments
Note that: 1. the total carotenoid products mainly comprise 17 substances including linalool, 6-methyl-5-hepten-2-ol, 6-methyl-5-hepten-2-one, farnesyl acetone, beta-dihydro-damascenone, beta-damascenone, geranylacetone, beta-ionone, megastigmatrienone 1, megastigmatrienone 2, megastigmatrienone 3, megastigmatrienone 4, 3-hydroxy-beta-dihydro-damascenone, spirodelanone, isophorone oxide, dihydro-kiwi lactone and 4-acetyl-2-methoxyphenol.
2. The total amount of phenylalanine is mainly 4 substances of benzaldehyde, phenylacetaldehyde, phenethyl alcohol and benzyl alcohol.
3. The total amount of the brown products is mainly the content of substances in furfural, 5-methyl furfural, 2-acetyl furan, furfuryl alcohol, 3, 4-dimethyl-2, 5-furan and 2-acetyl pyrrole 6.
4. The cembrane is solanone.
5. Chlorophyll is neophytadiene.
As can be seen from Table 10 above, the total content of neutral volatile aroma substances in the cured tobacco leaves treated with the composition of the present invention, C3F and B2F tobacco leaves, was 6.79% and 3.72%, respectively, higher than that of the control, wherein: the total amount of 17 carotenoids was 5.16% and 8.32% higher than the control, respectively; the total amount of 4 phenylalanine groups is 9.44% and 11.2% higher than that of the control; the total amount of the 6 brown products is 5.44% and 9.00% higher than that of the control; the content of the cembrane-like compounds (solanone) is 13.1% and 4.13% higher than that of the control; chlorophyll (neophytadiene) content was 6.64% and 2.66% higher than control, respectively. The method shows that the total content of neutral volatile aroma substances and the content of each main chemical component are improved, the aroma quality of tobacco leaves is improved, but no embodiment is obvious.
Comparative example 3
The difference from example 1 is that only the orange peel nanomaterial (process C) was subtracted, the remainder being the same. The test site and time were the same as in test example 1.
Table 11 evaluation of overall score of appearance and sensory quality index of cured tobacco
As can be seen from Table 11, the total appearance quality evaluation scores of C3F and B2F were higher than those of controls 3.9 and 4.4 respectively, and the total sensory quality evaluation scores of C3F and B2F were higher than those of controls 1.2 and 1.4 respectively, indicating that the improvement of the baked appearance and sensory quality of tobacco leaves was facilitated. The content of potassium ions in the C3F and B2F tobacco leaves is respectively 4.24 percent and 4.43 percent higher than that in the control, so that the content of potassium ions in the tobacco leaves is improved.
TABLE 12 different treatments for neutral volatile aroma content (μg/g)
Note that: 1. the total carotenoid products mainly comprise 17 substances including linalool, 6-methyl-5-hepten-2-ol, 6-methyl-5-hepten-2-one, farnesyl acetone, beta-dihydro-damascenone, beta-damascenone, geranylacetone, beta-ionone, megastigmatrienone 1, megastigmatrienone 2, megastigmatrienone 3, megastigmatrienone 4, 3-hydroxy-beta-dihydro-damascenone, spirodelanone, isophorone oxide, dihydro-kiwi lactone and 4-acetyl-2-methoxyphenol.
2. The total amount of phenylalanine is mainly 4 substances of benzaldehyde, phenylacetaldehyde, phenethyl alcohol and benzyl alcohol.
3. The total amount of the brown products is mainly the content of substances in furfural, 5-methyl furfural, 2-acetyl furan, furfuryl alcohol, 3, 4-dimethyl-2, 5-furan and 2-acetyl pyrrole 6.
4. The cembrane is solanone.
5. Chlorophyll is neophytadiene.
As can be seen from Table 12 above, the total content of neutral volatile aroma substances in the cured tobacco leaves treated with the composition of the present invention, C3F and B2F tobacco leaves, was 10.6% and 7.6%, respectively, higher than that of the control, wherein: the total amount of 17 carotenoids was 18.6% and 10.5% higher than the control, respectively; the total amount of 4 phenylalanine compounds is 15.7% and 13.3% higher than that of the control; the total amount of the 6 brown products is 8.51% and 12.5% higher than the control; the content of the cembrane-like compounds (solanone) is 16.6% and 8.24% higher than that of the control compound; chlorophyll (neophytadiene) content was 9.46% and 6.75% higher than control, respectively. The method shows that the total content of neutral volatile aroma substances and the content of each main chemical component are improved, the aroma quality of tobacco leaves is improved, but no embodiment is obvious.
Comparative example 4
The difference from example 1 is that only the honey was subtracted (for treatment D), the remainder being the same. The test site and time were the same as in test example 1.
TABLE 13 evaluation of overall score for appearance and sensory quality indicators of cured tobacco
As can be seen from Table 13, the total appearance quality evaluation scores of C3F and B2F were successively higher than those of controls 4.2 and 4.2, respectively, and the total sensory quality evaluation scores of C3F and B2F were successively higher than controls 1.2 and 1.8, respectively, indicating that it is advantageous to improve the baked appearance and sensory quality of tobacco leaves. The content of potassium ions in the C3F and B2F tobacco leaves is respectively 4.24 percent and 4.73 percent higher than that in the control, so that the content of potassium ions in the tobacco leaves is improved.
TABLE 14 different treatments for neutral volatile aroma content (μg/g)
Note that: 1. the total carotenoid products mainly comprise 17 substances including linalool, 6-methyl-5-hepten-2-ol, 6-methyl-5-hepten-2-one, farnesyl acetone, beta-dihydro-damascenone, beta-damascenone, geranylacetone, beta-ionone, megastigmatrienone 1, megastigmatrienone 2, megastigmatrienone 3, megastigmatrienone 4, 3-hydroxy-beta-dihydro-damascenone, spirodelanone, isophorone oxide, dihydro-kiwi lactone and 4-acetyl-2-methoxyphenol.
2. The total amount of phenylalanine is mainly 4 substances of benzaldehyde, phenylacetaldehyde, phenethyl alcohol and benzyl alcohol.
3. The total amount of the brown products is mainly the content of substances in furfural, 5-methyl furfural, 2-acetyl furan, furfuryl alcohol, 3, 4-dimethyl-2, 5-furan and 2-acetyl pyrrole 6.
4. The cembrane is solanone.
5. Chlorophyll is neophytadiene.
As can be seen from Table 14 above, the total content of neutral volatile aroma substances in the cured tobacco leaves treated with the composition of the present invention, C3F and B2F tobacco leaves, was 7.52% and 7.03%, respectively, higher than the control, wherein: the total amount of 17 carotenoid is 11.7% and 16.9% higher than the control; the total amount of 4 phenylalanine compounds is 8.89% and 7.07% higher than the control; the total amount of the 6 brown products is 11.8% and 5.61% higher than the control; the content of the cembrane-like compounds (solanone) is 11.8% and 5.61% higher than that of the control compound; chlorophyll (neophytadiene) content was 6.14% and 6.86% higher than control, respectively. The method shows that the total content of neutral volatile aroma substances and the content of each main chemical component are improved, the aroma quality of tobacco leaves is improved, but no embodiment is obvious.
After spraying each group of different flavoring agents, the tobacco curing process is carried out under the same condition according to the conventional tobacco curing process.
Claims (4)
1. The application of the quality-improving flavoring agent in tobacco quality-improving flavoring is characterized in that the quality-improving flavoring agent comprises the following components in parts by weight: 15-30 parts of dry stem and leaf powder of alternanthera philoxeroides, 20-40 parts of dry fresh osmanthus fragrans powder, 25-40 parts of dry dried orange peel powder and 20-30 parts of honey; the dry stem and leaf powder of the alternanthera philoxeroides is prepared by drying stem and leaf of the alternanthera philoxeroides until the moisture content is less than or equal to 5%, and carrying out dry crushing by adopting a physical method to prepare a material with 20-50nm for later use; the dry fresh osmanthus powder is prepared by firstly cutting fresh osmanthus into fragments with the length of 1-2 cm, deactivating enzyme at 102 ℃ for 1h, drying at 70-80 ℃ until the water content is less than 5%, and carrying out dry crushing by adopting a physical method to prepare a 20-50nm material for later use; the dried orange peel powder is prepared by drying fresh orange peel at 70-80 ℃ until the water content is less than 5%, and performing dry grinding by a physical method to prepare a material with 20-50nm for later use; the honey is produced by bees cultivated by bee farmers; the quality-improving flavoring agent and water are mixed according to the proportion of 1-2: mixing 100-200 mass percent, fully stirring, and preparing spraying liquid after complete dissolution; and (3) diluting the quality-improving flavoring agent, spraying the diluted quality-improving flavoring agent on the surface of the mature and harvested tobacco leaves, and baking the tobacco leaves.
2. Use according to claim 1, characterized in that it comprises the following components in parts by weight: 20 parts of alternanthera philoxeroides dry stem and leaf powder, 30 parts of dry fresh osmanthus fragrans powder, 30 parts of dry dried orange peel powder and 20 parts of honey.
3. The use according to claim 1, wherein the diluted quality-improving flavoring agent is sprayed on the surface of the tobacco leaves according to the leaf surface spraying amount of 7.5-8.0 g/kg of fresh tobacco leaves when the harvested mature fresh tobacco leaves are woven into a straw house.
4. The use according to claim 3, wherein the diluted quality-improving flavoring agent is sprayed on the surface of the tobacco leaves according to the leaf surface spraying amount of 7.5g/kg of fresh tobacco leaves when the harvested mature fresh tobacco leaves are woven into a house.
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| US20030131857A1 (en) * | 2002-01-16 | 2003-07-17 | Kim Hong Bin | Nicotine free cigarette substitute |
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| GB676646A (en) * | 1949-09-05 | 1952-07-30 | Maurice Alec Arnold | Improvements in or relating to herbal smoking mixtures |
| CN1370474A (en) * | 2002-03-18 | 2002-09-25 | 吴昊 | Tobacco flue-curing and amending agent |
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