CN115119956B - Sustained-release herbal lip cigarette - Google Patents
Sustained-release herbal lip cigarette Download PDFInfo
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- CN115119956B CN115119956B CN202210725882.2A CN202210725882A CN115119956B CN 115119956 B CN115119956 B CN 115119956B CN 202210725882 A CN202210725882 A CN 202210725882A CN 115119956 B CN115119956 B CN 115119956B
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/183—Treatment of tobacco products or tobacco substitutes sterilization, preservation or biological decontamination
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
- B65B—MACHINES, APPARATUS OR DEVICES FOR, OR METHODS OF, PACKAGING ARTICLES OR MATERIALS; UNPACKING
- B65B53/00—Shrinking wrappers, containers, or container covers during or after packaging
- B65B53/02—Shrinking wrappers, containers, or container covers during or after packaging by heat
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
- B65B—MACHINES, APPARATUS OR DEVICES FOR, OR METHODS OF, PACKAGING ARTICLES OR MATERIALS; UNPACKING
- B65B61/00—Auxiliary devices, not otherwise provided for, for operating on sheets, blanks, webs, binding material, containers or packages
- B65B61/04—Auxiliary devices, not otherwise provided for, for operating on sheets, blanks, webs, binding material, containers or packages for severing webs, or for separating joined packages
- B65B61/06—Auxiliary devices, not otherwise provided for, for operating on sheets, blanks, webs, binding material, containers or packages for severing webs, or for separating joined packages by cutting
- B65B61/10—Auxiliary devices, not otherwise provided for, for operating on sheets, blanks, webs, binding material, containers or packages for severing webs, or for separating joined packages by cutting using heated wires or cutters
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
- B65B—MACHINES, APPARATUS OR DEVICES FOR, OR METHODS OF, PACKAGING ARTICLES OR MATERIALS; UNPACKING
- B65B61/00—Auxiliary devices, not otherwise provided for, for operating on sheets, blanks, webs, binding material, containers or packages
- B65B61/26—Auxiliary devices, not otherwise provided for, for operating on sheets, blanks, webs, binding material, containers or packages for marking or coding completed packages
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- Manufacture Of Tobacco Products (AREA)
Abstract
A slow release type herbal lip cigarette relates to lip cigarette technical field, the formula raw materials include: 20-25 parts of tea powder, 15-18 parts of microcrystalline cellulose, 37-42 parts of xylitol, 18-21 parts of essence and 3-6 parts of nicotine salt. The tea powder can be of various varieties such as black tea, green tea, pu' er tea and the like, can be used without grade requirement according to the flavor requirement, and can carry tea stems, and due to the special fiber structure of the tea powder, after organic matters are extracted and separated, fiber hole structures which are convenient for adsorbing nicotine salt particles are just formed, so that the nicotine salt particles are adsorbed more uniformly and firmly, and microcrystalline cellulose acts as a slow release agent; the lip cigarette manufactured by adopting the formula can keep stable taste for 35-45 minutes, and has longer duration, so that the lip cigarette has softer, more stable and full taste.
Description
Technical Field
The invention relates to the technical field of lip cigarettes, in particular to a slow-release herbal lip cigarette.
Background
Lip tobacco today can be divided into two main categories depending on the manner of packaging, one being in a pouch (powder), one being a LOOSE powder (LOOSE) which appears to be more primitive, and another important category division for wet lip tobacco is based on the amount of tobacco juice in wet lip tobacco. The white lip tobacco can be basically classified into primary taste and white lip tobacco, and the white lip tobacco is dry and has relatively less juice, so that the mouth water can be relatively less spit.
At present, the lip cigarette in the prior art can be used for 30 minutes at a time, namely, the nicotine salt can be slowly released for about 30 minutes, so that the requirement of nicotine intake of a traditional cigarette is met, and the adsorption quantity and uniformity of the nicotine salt are different due to the difference of fiber components used as a nicotine salt (nicotine) carrier, so that the stability of the taste is greatly different, the lip cigarette in the market has large taste variation in the use process, the taste experience is unstable, the concentration of the nicotine salt is poor in continuous stability, and the full taste cannot be kept within 30-40 minutes of normal taste time introduced in the specification.
Disclosure of Invention
In order to solve the problems that the stability of taste is greatly different due to different adsorption amounts and uniformity of the used fiber components serving as the nicotine salt (nicotine) carriers, the taste of lip cigarettes on the market is greatly changed, the taste experience is unstable, the nicotine salt concentration is continuously poor in stability, and full taste cannot be maintained within 30-40 minutes of normal taste time introduced in the specification, the invention provides a slow-release type herbal lip cigarette and a production process thereof. The following technical scheme is adopted:
a slow-release herbal lip cigarette comprises the following raw materials: 20-25 parts of tea powder, 15-18 parts of microcrystalline cellulose, 37-42 parts of xylitol, 18-21 parts of essence and 3-6 parts of nicotine salt.
The tea powder can be of various varieties such as black tea, green tea, pu' er tea and the like, can be used without grade requirement according to the flavor requirement, and can be provided with tea stems, and due to the special fiber structure of the tea powder, after organic matters are extracted and separated, fiber hole structures which are convenient for adsorbing nicotine salt particles are just formed, so that the nicotine salt particles are adsorbed more uniformly and firmly, microcrystalline cellulose acts as a slow release agent, active substances enter a porous structure of a carrier in the slow release process, the active substances are contained by intermolecular hydrogen bonds, and the active substances are fixed after drying. When the active substance is released, swelling is caused by diffusion of water in the capillary system of the polymer carrier, the compound bond between the carrier and the immobilized active substance is broken, and the active substance is slowly released. The lip cigarette manufactured by adopting the formula can keep stable taste for 35-45 minutes, so that the release of the nicotine salt is more uniform, the duration time is longer, and the overlarge taste deviation caused by nonuniform release of the nicotine salt is avoided.
Optionally, 0.01-0.1 part of antioxidant, 0.01-0.1 part of preservative, 0.1-1 part of sour regulator, 0.5-2 parts of sweetener, 1.5-3.5 parts of cooling agent and 1-3 parts of humectant are added.
Optionally, the formula raw materials comprise: 22-23.5 parts of tea powder, 16-17 parts of microcrystalline cellulose, 38-41 parts of xylitol, 19-20 parts of essence, 3.5-5 parts of nicotine salt, 0.03-0.08 part of antioxidant, 0.03-0.08 part of preservative, 0.03-0.08 part of sour regulator, 0.8-1.5 parts of sweetener, 1.8-3 parts of cooling agent and 1-2.5 parts of humectant.
Optionally, the xylitol is xylitol powder, and the particle size of the powder is 50-150 meshes.
Through the technical scheme, the xylitol has better low-temperature tasting effect, and the sweetness of the xylitol can reach 1.2 times of that of sucrose. The xylitol is easy to dissolve in water and absorbs a certain amount of heat when dissolved, so that the xylitol powder with the particle size of more than 50 meshes is added into lip cigarettes to effectively improve the taste of the lip cigarettes, and meanwhile, the xylitol powder plays a role in uniformly dispersing nicotine salt, so that the taste of the nicotine salt is less irritative.
Optionally, the microcrystalline cellulose has a particle size of 50-100 μm.
Through the technical scheme, microcrystalline cellulose can be better mixed with each component by 50-100 mu m, can be better compounded with tea powder, and plays a role of a sustained release agent to the greatest extent.
Optionally, the tea powder comprises the following components in parts by weight: and (3) extracting and drying the dried tea, water and 65-degree alcohol at a ratio of 10:3.5.
Optionally, the specific manufacturing method of the tea powder comprises the following steps:
step1, extracting with water for the first time, taking the weight parts of dry tea, crushing the dry tea by a crusher for 120 meshes to obtain dry tea powder, pouring the dry tea powder into a stainless steel stirring tank, adding water which is half of the weight parts of the dry tea, stirring for 5-10 minutes until the water is uniform, putting into an ultrasonic vibration rod, performing ultrasonic extraction for 50-70 minutes, taking out the mixed solution, pouring into a centrifuge, and centrifuging for 30 minutes;
step2, water is added again after the second water extraction, the water is added in half by weight, the mixed solution is taken out after ultrasonic extraction is carried out again for 50-70 minutes, and is poured into a centrifuge for centrifugation, and the mixed solution is taken out after 25-35 minutes, so that 0.6-0.8 weight part of tea powder after water extraction is obtained;
step3, drying, namely placing the tea powder after water extraction into a dryer for drying treatment for 30 minutes to obtain dry tea powder after primary extraction;
and 4, putting the dry tea powder into a reaction kettle, adding 65-degree alcohol in parts by weight, stirring and heating at 75-80 ℃ for 4-6 hours, putting into a centrifuge for 30 minutes, centrifuging, taking out the mixture, putting into a dryer for 30 minutes, and drying to obtain 0.4-0.6 part of finally extracted tea powder.
According to the technical scheme, the dried tea parts required by the preparation process of the tea herbal granules prepared from the black tea/green tea/Pu' er tea/etc. dried tea can be removed from the dried tea by twice water extraction and finally alcohol extraction, so that a mesh structure is formed, and a stable and reliable carrier is provided for subsequent absorption of nicotine salt.
A production process of slow-release herbal lip tobacco comprises the following steps of Step1, putting tea powder, microcrystalline cellulose powder, xylitol powder, essence and nicotine salt in parts by weight into a low-speed stirrer to be uniformly mixed for 20-30 minutes;
step2, adding the antioxidant, the preservative, the acidity regulator, the sweetener and the cooling agent in parts by weight, and continuously stirring for 20-30 minutes until the mixture is uniform;
step3, adding the humectant in the weight parts, and stirring for 5-10 minutes until the humectant is uniform;
step4, adding the uniform mixture in Step3 into a lip tobacco powder split charging machine for packaging with the package size of 1.2cm x 3cm, wherein each package is 0.5 g+/-0.1 g;
through the technical scheme, the slow-release herbal lip cigarettes can be produced by single package of the non-woven fabrics with higher automation degree, the specification of the single package is suitable for users, single use can be ensured, and the taste is stable and kept for more than 40 minutes.
Optionally, a sterilization process is also provided, and the sterilization process specifically comprises the Step of conveying the packaging lip cigarette produced by Step4 to an ultraviolet sterilization furnace for 18-22 seconds.
According to the technical scheme, ultraviolet sterilization and disinfection are that ultraviolet rays with proper wavelength can destroy the molecular structure of DNA (deoxyribonucleic acid) or RNA (ribonucleic acid) in microorganism organism cells, so that growing cells die and/or regenerative cells die, and the sterilization and disinfection effects are achieved. The ultraviolet disinfection technology is based on modern epidemic prevention, medicine and photodynamics, and utilizes specially designed high-efficiency, high-intensity and long-service-life UVC-band ultraviolet light to irradiate running water so as to directly kill various bacteria, viruses, parasites, algae and other pathogens in the lip smoke non-woven fabric packet.
The slow release type herbal lip tobacco production process also comprises a boxing process, wherein the boxing process specifically comprises the following steps of:
s1, conveying the materials to a counting boxing machine for 25-pack one-pack split charging;
s2, conveying the box-packed lip cigarettes to a labeling machine for labeling up and down and spraying production dates;
s3, transmitting the label to a side label labeling machine for side label sticking and sealing;
s4, conveying the film to a film cutting machine for packaging and cutting the heat shrinkage film;
s5, conveying the film to a thermal shrinkage furnace for thermal shrinkage film coating;
s6, conveying the materials to a box filling machine for filling.
In summary, the present invention includes at least one of the following beneficial technical effects:
the invention provides a slow-release herbal lip cigarette and a production process thereof, wherein tea powder can be of various varieties such as black tea, green tea, pu' er and the like, can be used without grade requirements according to flavor requirements, and can be provided with tea stems. When the active substance is released, swelling is caused by diffusion of water in the capillary system of the polymer carrier, the compound bond between the carrier and the immobilized active substance is broken, and the active substance is slowly released. The lip cigarette manufactured by adopting the formula can keep stable taste for 35-45 minutes, so that the release of the nicotine salt is more uniform, the duration is longer, the release of the nicotine salt is more uniform and stable, the duration is longer, and the taste of the lip cigarette is softer, more stable and full.
The slow-release herbal lip tobacco provided by the invention adopts tea as the raw material, has low requirements on the quality of the tea, does not need to be new tea or tender tea, can be used as long as the tea is wide in raw material source, contains some beneficial components, is beneficial to health, and is environment-friendly and green.
Drawings
Fig. 1 shows a slow-release herbal lip cigarette obtained by the implementation of the invention.
Description of the embodiments
The present invention will be described in further detail with reference to examples.
The embodiment of the invention discloses a slow-release herbal lip cigarette and a production process thereof.
A slow-release herbal lip cigarette comprises the following raw materials: 20-25 parts of tea powder, 15-18 parts of microcrystalline cellulose, 37-42 parts of xylitol, 18-21 parts of essence and 3-6 parts of nicotine salt.
The tea powder can be of various varieties such as black tea, green tea, pu' er tea and the like, can be used without grade requirement according to the flavor requirement, and can be provided with tea stems, and due to the special fiber structure of the tea powder, after organic matters are extracted and separated, fiber hole structures which are convenient for adsorbing nicotine salt particles are just formed, so that the nicotine salt particles are adsorbed more uniformly and firmly, microcrystalline cellulose acts as a slow release agent, active substances enter a porous structure of a carrier in the slow release process, the active substances are contained by intermolecular hydrogen bonds, and the active substances are fixed after drying. When the active substance is released, swelling is caused by diffusion of water in the capillary system of the polymer carrier, the compound bond between the carrier and the immobilized active substance is broken, and the active substance is slowly released. The lip cigarette manufactured by adopting the formula can keep stable taste for 35-45 minutes, so that the release of the nicotine salt is more uniform, the duration time is longer, and the overlarge taste deviation caused by nonuniform release of the nicotine salt is avoided.
Also comprises 0.01-0.1 part of antioxidant, 0.01-0.1 part of preservative, 0.1-1 part of sour regulator, 0.5-2 parts of sweetener, 1.5-3.5 parts of cooling agent and 1-3 parts of humectant.
The formula comprises the following raw materials: 22-23.5 parts of tea powder, 16-17 parts of microcrystalline cellulose, 38-41 parts of xylitol, 19-20 parts of essence, 3.5-5 parts of nicotine salt, 0.03-0.08 part of antioxidant, 0.03-0.08 part of preservative, 0.03-0.08 part of sour regulator, 0.8-1.5 parts of sweetener, 1.8-3 parts of cooling agent and 1-2.5 parts of humectant.
Xylitol is xylitol powder with particle size of 50-150 mesh.
Xylitol has better low-temperature tasting effect, and the sweetness of the xylitol can reach 1.2 times of that of sucrose. The xylitol is easy to dissolve in water and absorbs a certain amount of heat when dissolved, so that the xylitol powder with the particle size of more than 50 meshes is added into lip cigarettes to effectively improve the taste of the lip cigarettes, and meanwhile, the xylitol powder plays a role in uniformly dispersing nicotine salt, so that the taste of the nicotine salt is less irritative.
The grain size of the microcrystalline cellulose is 50-100 μm.
Microcrystalline cellulose can be better mixed with each component by 50-100 mu m, can be better compounded with tea powder, and plays a role of a slow release agent to the greatest extent.
The tea powder comprises the following components in parts by weight: and (3) extracting and drying the dried tea, water and 65-degree alcohol at a ratio of 10:3.5.
The specific manufacturing method of the tea powder comprises the following steps:
step1, extracting with water for the first time, taking weight parts of dry tea, crushing the dry tea by a crusher with 120 meshes to obtain dry tea powder, pouring the dry tea powder into a stainless steel stirring tank, adding water which is half of the weight parts of the dry tea, stirring for 5-10 minutes until the water is uniform, putting into an ultrasonic vibration rod, performing ultrasonic extraction for 50-70 minutes, taking out the mixed solution, pouring into a centrifuge, and centrifuging for 30 minutes;
step2, water extraction is carried out for the second time, water is added again, half of the water by weight is added again, ultrasonic extraction is carried out for 50-70 minutes again, the mixed solution is taken out and poured into a centrifugal machine for centrifugation, and after 25-35 minutes, the mixed solution is taken out, so that 0.6-0.8 weight of tea powder after water extraction is obtained;
step3, drying, namely placing the tea powder after water extraction into a dryer for drying treatment for 30 minutes to obtain dry tea powder after primary extraction;
and 4, putting the dry tea powder into a reaction kettle, adding 65-degree alcohol in parts by weight, stirring and heating at 75-80 ℃ for 4-6 hours, putting into a centrifuge for 30 minutes and centrifuging, taking out the mixture, putting into a dryer for 30 minutes and drying to obtain 0.4-0.6 part of finally extracted tea powder.
The method can realize that the dried tea parts required by the preparation process of the dried tea of black tea/green tea/Pu' er tea/etc. into the tea herbal granules are extracted by water twice, and finally various organic matters in the dried tea are removed by alcohol extraction to form a mesh structure, so that a stable and reliable carrier is provided for the subsequent absorption of nicotine salt.
A production process of slow-release herbal lip tobacco comprises the following steps of Step1, putting tea powder, microcrystalline cellulose powder, xylitol powder, essence and nicotine salt in a low-speed stirrer to uniformly mix for 20-30 minutes;
step2, adding antioxidant, preservative, acidity regulator, sweetener and cooling agent in parts by weight, and continuously stirring for 20-30 minutes until uniform;
step3, adding the humectant in parts by weight, and stirring for 5-10 minutes until the humectant is uniform;
step4, adding the uniform mixture in Step3 into a lip tobacco powder split charging machine for packaging with the package size of 1.2cm x 3cm, wherein each package is 0.5 g+/-0.1 g;
the slow-release herbal lip cigarettes can be produced by single package of non-woven fabrics with higher automation degree, the specification of single package is suitable for users, single use can be ensured, and the taste is stable and kept for more than 40 minutes.
And a sterilization process, which is to transfer the packaging lip cigarette produced by Step4 to an ultraviolet sterilization furnace for 18-22 seconds.
Ultraviolet sterilization and disinfection is to destroy the molecular structure of DNA (deoxyribonucleic acid) or RNA (ribonucleic acid) in the cells of the microorganism organism by utilizing ultraviolet rays with proper wavelength, thereby causing the death of growing cells and/or the death of regenerative cells and achieving the effect of sterilization and disinfection. The ultraviolet disinfection technology is based on modern epidemic prevention, medicine and photodynamics, and utilizes specially designed high-efficiency, high-intensity and long-service-life UVC-band ultraviolet light to irradiate running water so as to directly kill various bacteria, viruses, parasites, algae and other pathogens in the lip smoke non-woven fabric packet.
The slow release type herbal lip tobacco production process also comprises a boxing process, wherein the boxing process specifically comprises the following steps of:
s1, conveying the materials to a counting boxing machine for 25-pack one-pack split charging;
s2, conveying the box-packed lip cigarettes to a labeling machine for labeling up and down and spraying production dates;
s3, transmitting the label to a side label labeling machine for side label sticking and sealing;
s4, conveying the film to a film cutting machine for packaging and cutting the heat shrinkage film;
s5, conveying the film to a thermal shrinkage furnace for thermal shrinkage film coating;
s6, conveying the materials to a box filling machine for filling.
In the first embodiment of the invention:
the formula comprises the following raw materials:
23.2 parts of tea powder, 16.8 parts of microcrystalline cellulose, 40.8 parts of xylitol, 20 parts of essence, 4.8 parts of nicotine salt, 0.05 part of antioxidant, 0.05 part of preservative, 0.4 part of sour regulator, 1.2 parts of sweetener, 2.6 parts of cooling agent and 2 parts of humectant.
Firstly, preparing the tea powder with the weight portions,
taking the dry tea in parts by weight, and crushing the dry tea by 120 meshes of a crusher to obtain dry tea powder;
pouring the dry tea powder obtained by STEP1 into a stainless steel stirring tank, adding half of water by weight, and stirring for 8 minutes until uniformity;
placing a 300w ultrasonic vibration rod, performing ultrasonic extraction for 60 minutes, taking out the mixed solution, and pouring the mixed solution into a centrifuge for centrifugation for 35 minutes;
and adding half of the water by weight, performing ultrasonic extraction again for 60 minutes, taking out the mixed solution, pouring the mixed solution into a centrifuge for centrifugation, and taking out the mixed solution after 35 minutes to obtain the extracted tea powder with higher water content.
The obtained tea powder is put into a dryer for drying treatment for 30 minutes, and 0.7 weight part of dry tea powder after primary extraction is obtained;
and (3) putting the dry tea powder into a reaction kettle, adding the alcohol with the weight portions, stirring and heating at the low temperature of 80 ℃ for 5 hours, putting into a centrifuge for 30 minutes, centrifuging, taking out the mixture, putting into a dryer for 30 minutes, drying to obtain 0.5 portion of the finally extracted tea powder, and measuring that the water content of the extracted tea powder is 4.2%.
Preparing lip tobacco, namely placing the tea powder, the microcrystalline cellulose powder, the xylitol powder, the essence and the nicotine salt in the low-speed stirrer to uniformly mix for 25 minutes;
adding antioxidant, preservative, acidity regulator, sweetener and cooling agent, and stirring for 25 min to uniformity;
adding humectant in weight parts, and stirring for 8 minutes until the mixture is uniform;
adding the uniform mixture into a lip tobacco powder split charging machine for packaging with 0.5 g+/-0.1 g of each package, wherein the package adopts food-grade non-woven fabrics, and the package size is 1.2cm x 3cm; and conveying the produced packaging lip cigarettes to an ultraviolet sterilizing furnace for 18-22 seconds. Thus, the finished lip cigarette product which can be used is finished.
The obtained qualified product is subjected to product performance test, and the performance parameters are shown in table 1.
The appearance of the obtained lip gloss product is shown in figure 1, the obtained lip gloss powder is uniform white powder, the outer package is also white woven cloth, and the stability of the obtained lip gloss product and the white powder are ensured by adopting the process.
The specific contents of each evaluation index are as follows:
taste uniformity in mouth: the comprehensive feeling of taste and smell of the user is scored with the score of 0-10, the user places the single-pack lip cigarette between the upper gum and the lips, the mouth feel test is carried out for 60 minutes, the test participants are 10 persons, the mouth feel evaluation is carried out every 5 minutes, the average value is taken, the mouth feel of the mouth is greatly reduced along with the change of time, and the mouth feel of the mouth is uneven.
Nicotine salt release uniformity refers to: in the use process, the release stability of nicotine salt concentration and the like in the liquid outside the packaging lip cigarette along with time is specifically indicated by measuring the nicotine salt concentration in the liquid extracted from the food-grade non-woven fabric outside the packaging lip cigarette at intervals of 5 minutes, taking the extract of the non-woven fabric on the lip cigarette containing nicotine and nicotine salt, diluting with water with pH=7-9, extracting with an equal volume of organic solvent containing an internal standard, fully oscillating for 30-120 minutes, measuring the amount of free nicotine by a gas phase method, wherein the nicotine salt concentration change of two adjacent 5 minutes exceeds 5%, and the release of the nicotine salt is considered to be uneven.
Nicotine salt release persistence refers to: in the use process, the duration time such as the sensory intensity of the nicotine salt felt by a user is long, the specific index is that the lip cigarette starts in 20 minutes, every 5 minutes, the ratio of the nicotine salt concentration in the current cigarette to the nicotine salt concentration in the use process of 5 minutes is lower than 50%, and the nicotine salt concentration is considered to be unsuitable for continuous use and needs to be discarded, so that the lip cigarette experience is avoided.
The performance parameters are shown in Table 1
TABLE 1
| Time index | For 5 minutes | For 10 minutes | 15 minutes | 20 minutes | 25 minutes | 30 minutes |
| Taste in mouth | 9.5 | 9.6 | 9.5 | 9.4 | 9.4 | 9.2 |
| Concentration of nicotine salt | 0.023mg/mL | 0.023mg/mL | 0.022mg/mL | 0.022mg/mL | 0.021mg/mL | 0.020mg/mL |
| Sustained release of nicotine salts | 0.957 | 0.913 | 0.870 | |||
| 35 minutes | 40 minutes | 45 minutes | 50 minutes | 55 minutes | 60 minutes | |
| Taste in mouth | 9.0 | 8.8 | 8.7 | 8.2 | 7.5 | 6.5 |
| Concentration of nicotine salt | 0.018mg/mL | 0.016mg/mL | 0.014mg/mL | 0.012mg/mL | 0.010mg/mL | 0.008mg/mL |
| Sustained release of nicotine salts | 0.783 | 0.696 | 0.609 | 0.522 | 0.435 | 0.348 |
Therefore, the lip cigarette produced by the formula and the process in the first embodiment has higher evaluation on the taste of a user, and has small change of the taste along with time change, and can maintain average evaluation of 8.8 minutes before 40 minutes, so that the taste is full, stable and soft.
The uniformity of the release of the nicotine salt is good, and the concentration of the nicotine salt slowly decreases with the increase of time after the concentration of the nicotine salt reaches the peak at 5 minutes.
The release durability of the nicotine salt is good, the nicotine salt concentration in the smoke can reach 95.7% at 5 minutes after 20 minutes, which is the root cause of stable taste evaluation, the nicotine salt concentration in the external packaging non-woven fabric still reaches 52.2% at 5 minutes by 50 minutes, the nicotine salt concentration in the smoke can still be stably used, and the nicotine salt concentration in the smoke is reduced to 43.5% at 5 minutes by 55 minutes, so that the taste experience is not suggested to be influenced by continuous use.
Therefore, the lip tobacco produced by the formula and the process of the first embodiment has soft and full taste, good uniformity of releasing nicotine salt and good durability of releasing nicotine salt, at least can meet the requirement that the normal use time of a user exceeds 50 minutes, and like products on the market cannot be used continuously after 30 minutes, so that the tea leaf herbal lip tobacco prepared by the formula and the process of the first embodiment has advantages in the durability of releasing nicotine salt.
In the second embodiment of the invention:
the formula comprises the following raw materials:
30 parts of tea powder, 10 parts of microcrystalline cellulose, 40.8 parts of xylitol, 20 parts of essence, 4.8 parts of nicotine salt, 0.05 part of antioxidant, 0.05 part of preservative, 0.4 part of sour regulator, 1.2 parts of sweetener, 2.6 parts of cooling agent and 2 parts of humectant.
Firstly, preparing the tea powder with the weight portions,
taking the dry tea in parts by weight, and crushing the dry tea by 120 meshes of a crusher to obtain dry tea powder;
pouring the dry tea powder obtained by STEP1 into a stainless steel stirring tank, adding half of water by weight, and stirring for 8 minutes until uniformity;
placing a 300w ultrasonic vibration rod, performing ultrasonic extraction for 60 minutes, taking out the mixed solution, and pouring the mixed solution into a centrifuge for centrifugation for 35 minutes;
and adding half of the water by weight, performing ultrasonic extraction again for 60 minutes, taking out the mixed solution, pouring the mixed solution into a centrifuge for centrifugation, and taking out the mixed solution after 35 minutes to obtain the extracted tea powder with higher water content.
The obtained tea powder is put into a dryer for drying treatment for 30 minutes, and 0.7 weight part of dry tea powder after primary extraction is obtained;
and (3) putting the dry tea powder into a reaction kettle, adding the alcohol with the weight portions, stirring and heating at the low temperature of 80 ℃ for 5 hours, putting into a centrifuge for 30 minutes, centrifuging, taking out the mixture, putting into a dryer for 30 minutes, drying to obtain 0.5 portion of the finally extracted tea powder, and measuring that the water content of the extracted tea powder is 4.2%.
Preparing lip tobacco, namely placing the tea powder, the microcrystalline cellulose powder, the xylitol powder, the essence and the nicotine salt in the low-speed stirrer to uniformly mix for 25 minutes;
adding antioxidant, preservative, acidity regulator, sweetener and cooling agent, and stirring for 25 min to uniformity;
adding humectant in weight parts, and stirring for 8 minutes until the mixture is uniform;
adding the uniform mixture into a lip tobacco powder split charging machine for packaging with 0.5 g+/-0.1 g of each package, wherein the package adopts food-grade non-woven fabrics, and the package size is 1.2cm x 3cm; and conveying the produced packaging lip cigarettes to an ultraviolet sterilizing furnace for 18-22 seconds. Thus, the finished lip cigarette product which can be used is finished.
The obtained qualified product is subjected to product performance test, and the performance parameters are shown in Table 2
For each evaluation index, see embodiment one.
TABLE 2
| Time index | For 5 minutes | For 10 minutes | 15 minutes | 20 minutes | 25 minutes | 30 minutes |
| Taste in mouth | 9.0 | 9.2 | 9.2 | 9.0 | 8.8 | 8.7 |
| Concentration of nicotine salt | 0.023mg/mL | 0.023mg/mL | 0.022mg/mL | 0.021mg/mL | 0.020mg/mL | 0.018mg/mL |
| Sustained release of nicotine salts | 0.913 | 0.870 | 0.783 | |||
| 35 minutes | 40 minutes | 45 minutes | 50 minutes | 55 minutes | 60 minutes | |
| Taste in mouth | 8.5 | 8 | 8 | 7.8 | 7.5 | 7 |
| Concentration of nicotine salt | 0.018mg/mL | 0.017mg/mL | 0.015mg/mL | 0.012mg/mL | 0.010mg/mL | 0.008mg/mL |
| Sustained release of nicotine salts | 0.783 | 0.739 | 0.652 | 0.522 | 0.435 | 0.348 |
Therefore, compared with the first embodiment, the formula and the lip cigarette produced by the process of the second embodiment greatly improve the dosage proportion of the tea powder and greatly reduce microcrystalline cellulose.
The taste is evaluated higher by users, and the taste changes little with time, and the average evaluation of 8 minutes can be maintained before 40 minutes, so that the taste is full, stable and soft.
The uniformity of nicotine salt release was better, but the nicotine salt concentration decreased too rapidly at 20-25 minutes with some downslide over the examples.
The release durability of the nicotine salt is better, the nicotine salt concentration in the smoke can reach 91.3% of the nicotine salt concentration in the smoke in 5 minutes after 20 minutes, and the nicotine salt concentration in the smoke is reduced to 43.5% of the nicotine salt concentration in the smoke in 5 minutes after 55 minutes, so that the continuous use is not recommended, and the taste experience is affected.
Therefore, the lip tobacco produced by the formula and the process of the second embodiment has soft, full and stable taste, general uniformity of nicotine salt release and general durability of nicotine salt release, and the tea herbal lip tobacco prepared by the formula and the process of the second embodiment has no advantages in taste, uniformity of nicotine salt release and durability of nicotine salt release.
The third embodiment of the invention:
the formula comprises the following raw materials:
10 parts of tea powder, 30 parts of microcrystalline cellulose, 40.8 parts of xylitol, 20 parts of essence, 4.8 parts of nicotine salt, 0.05 part of antioxidant, 0.05 part of preservative, 0.4 part of sour regulator, 1.2 parts of sweetener, 2.6 parts of cooling agent and 2 parts of humectant.
Firstly, preparing the tea powder with the weight portions,
taking the dry tea in parts by weight, and crushing the dry tea by 120 meshes of a crusher to obtain dry tea powder;
pouring the dry tea powder obtained by STEP1 into a stainless steel stirring tank, adding half of water by weight, and stirring for 8 minutes until uniformity;
placing a 300w ultrasonic vibration rod, performing ultrasonic extraction for 60 minutes, taking out the mixed solution, and pouring the mixed solution into a centrifuge for centrifugation for 35 minutes;
and adding half of the water by weight, performing ultrasonic extraction again for 60 minutes, taking out the mixed solution, pouring the mixed solution into a centrifuge for centrifugation, and taking out the mixed solution after 35 minutes to obtain the extracted tea powder with higher water content.
The obtained tea powder is put into a dryer for drying treatment for 30 minutes, and 0.7 weight part of dry tea powder after primary extraction is obtained;
and (3) putting the dry tea powder into a reaction kettle, adding the alcohol with the weight portions, stirring and heating at the low temperature of 80 ℃ for 5 hours, putting into a centrifuge for 30 minutes, centrifuging, taking out the mixture, putting into a dryer for 30 minutes, drying to obtain 0.5 portion of the finally extracted tea powder, and measuring that the water content of the extracted tea powder is 4.2%.
Preparing lip tobacco, namely placing the tea powder, the microcrystalline cellulose powder, the xylitol powder, the essence and the nicotine salt in the low-speed stirrer to uniformly mix for 25 minutes;
adding antioxidant, preservative, acidity regulator, sweetener and cooling agent, and stirring for 25 min to uniformity;
adding humectant in weight parts, and stirring for 8 minutes until the mixture is uniform;
adding the uniform mixture into a lip tobacco powder split charging machine for packaging with 0.5 g+/-0.1 g of each package, wherein the package adopts food-grade non-woven fabrics, and the package size is 1.2cm x 3cm; and conveying the produced packaging lip cigarettes to an ultraviolet sterilizing furnace for 18-22 seconds. Thus, the finished lip cigarette product which can be used is finished.
The obtained qualified product is subjected to product performance test, and the performance parameters are shown in Table 3
For each evaluation index, see embodiment one.
TABLE 3 Table 3
| Time index | For 5 minutes | For 10 minutes | 15 minutes | 20 minutes | 25 minutes | 30 minutes |
| Taste in mouth | 8.5 | 8.6 | 8.3 | 8 | 8 | 8.1 |
| Concentration of nicotine salt | 0.023mg/mL | 0.022mg/mL | 0.022mg/mL | 0.020mg/mL | 0.018mg/mL | 0.019mg/mL |
| Sustained release of nicotine salts | 0.870 | 0.783 | 0.826 | |||
| 35 minutes | 40 minutes | 45 minutes | 50 minutes | 55 minutes | 60 minutes | |
| Taste in mouth | 7.8 | 7.5 | 7.3 | 7.2 | 7 | 7 |
| Concentration of nicotine salt | 0.016mg/mL | 0.015mg/mL | 0.013mg/mL | 0.011mg/mL | 0.009mg/mL | 0.007mg/mL |
| Sustained release of nicotine salts | 0.696 | 0.652 | 0.565 | 0.478 | 0.391 | 0.304 |
Therefore, compared with the first embodiment, the lip cigarette produced by adopting the formula and the process in the third embodiment has the advantages that the consumption ratio of tea powder is greatly reduced, and microcrystalline cellulose is greatly improved.
The mouthfeel is generally evaluated by users, and the mouthfeel changes rapidly with time.
The nicotine salt release uniformity is poor.
The release durability of the nicotine salt is poor, the nicotine salt concentration in the smoke can reach 87% in 5 minutes after 20 minutes, and the nicotine salt concentration in the smoke is reduced to 47.8% in 5 minutes after 50 minutes, so that the continuous use is not recommended, and the taste experience is affected.
Therefore, the lip tobacco produced by the formula and the process of the third embodiment has the advantages of general taste, poor uniformity of nicotine salt release and poor durability of nicotine salt release, and the tea herbal lip tobacco prepared by the formula and the process of the third embodiment has no advantages in taste, uniformity of nicotine salt release and durability of nicotine salt release.
The fourth embodiment of the invention:
the formula comprises the following raw materials:
40 parts of microcrystalline cellulose, 40.8 parts of xylitol, 20 parts of essence, 4.8 parts of nicotine salt, 0.05 part of antioxidant, 0.05 part of preservative, 0.4 part of sour regulator, 1.2 parts of sweetener, 2.6 parts of cooling agent and 2 parts of humectant.
Preparing lip tobacco, namely placing the microcrystalline cellulose powder, the xylitol powder, the essence and the nicotine salt in the weight parts into a low-speed stirrer to be uniformly mixed for 25 minutes;
adding antioxidant, preservative, acidity regulator, sweetener and cooling agent, and stirring for 25 min to uniformity;
adding humectant in weight parts, and stirring for 8 minutes until the mixture is uniform;
adding the uniform mixture into a lip tobacco powder split charging machine for packaging with 0.5 g+/-0.1 g of each package, wherein the package adopts food-grade non-woven fabrics, and the package size is 1.2cm x 3cm; and conveying the produced packaging lip cigarettes to an ultraviolet sterilizing furnace for 18-22 seconds. Thus, the finished lip cigarette product which can be used is finished.
The obtained qualified product is subjected to product performance test, and the performance parameters are shown in Table 4
For each evaluation index, see embodiment one.
TABLE 4 Table 4
| Time index | For 5 minutes | For 10 minutes | 15 minutes | 20 minutes | 25 minutes | 30 minutes |
| Taste in mouth | 7.5 | 7.2 | 7 | 7 | 6.8 | 6.7 |
| Concentration of nicotine salt | 0.023mg/mL | 0.020mg/mL | 0.021mg/mL | 0.020mg/mL | 0.017mg/mL | 0.019mg/mL |
| Sustained release of nicotine salts | 0.870 | 0.739 | 0.826 | |||
| 35 minutes | 40 minutes | 45 minutes | 50 minutes | 55 minutes | 60 minutes | |
| Taste in mouth | 6.5 | 6.2 | 6 | 6 | 5.8 | 5.5 |
| Concentration of nicotine salt | 0.016mg/mL | 0.014mg/mL | 0.012mg/mL | 0.010mg/mL | 0.009mg/mL | 0.007mg/mL |
| Sustained release of nicotine saltsSex characteristics | 0.696 | 0.609 | 0.521 | 0.435 | 0.391 | 0.304 |
Therefore, compared with the first embodiment, the lip cigarette produced by adopting the formula and the process in the fourth embodiment has the advantages that the consumption ratio of tea powder is greatly reduced, and microcrystalline cellulose is greatly improved.
The mouthfeel was poorly evaluated by the user and varied over time with a fluctuation in mouthfeel.
The nicotine salt release uniformity is poor.
The release durability of the nicotine salt is poor, the nicotine salt concentration in the smoke can reach 87% in 5 minutes after 20 minutes, and the nicotine salt concentration in the smoke is reduced to 43.5% in 5 minutes after 50 minutes, so that the continuous use is not recommended, and the taste experience is affected.
Therefore, the lip tobacco produced by the formula and the process of the fourth embodiment has poor taste, poor uniformity of nicotine salt release and poor durability of nicotine salt release, and the tea herbal lip tobacco prepared by the formula and the process of the fourth embodiment has no advantages in taste, uniformity of nicotine salt release and durability of nicotine salt release.
Fifth embodiment of the invention:
the formula comprises the following raw materials:
40 parts of citrus powder, 40.8 parts of xylitol, 20 parts of essence, 4.8 parts of nicotine salt, 0.05 part of antioxidant, 0.05 part of preservative, 0.4 part of sour regulator, 1.2 parts of sweetener, 2.6 parts of cooling agent and 2 parts of humectant.
First, the citrus powder is prepared in parts by weight,
taking weight parts of dried citrus peel, and crushing the dried citrus peel by a crusher with 120 meshes to obtain dried citrus powder;
pouring the dry tea powder obtained by STEP1 into a stainless steel stirring tank, adding half of water by weight, and stirring for 8 minutes until uniformity;
placing a 300w ultrasonic vibration rod, performing ultrasonic extraction for 60 minutes, taking out the mixed solution, and pouring the mixed solution into a centrifuge for centrifugation for 35 minutes;
and adding half of the water by weight again, performing ultrasonic extraction again for 60 minutes, taking out the mixed solution, pouring the mixed solution into a centrifuge for centrifugation, and taking out the mixed solution after 35 minutes to obtain the extracted citrus powder with higher water content.
The obtained tea powder is put into a dryer for drying treatment for 30 minutes, and 0.7 weight part of dried citrus powder after primary extraction is obtained;
and (3) putting dry orange powder into a reaction kettle, adding the alcohol in parts by weight, stirring and heating at a low temperature of 80 ℃ for 5 hours, putting into a centrifuge for 30 minutes, centrifuging, taking out the mixture, putting into a dryer for 30 minutes, drying to obtain 0.5 part of finally extracted orange powder, and measuring that the water content of the extracted orange powder is 4.2%.
Preparing lip tobacco, namely placing the citrus powder, xylitol powder, essence and nicotine salt in the weight parts into a low-speed stirrer to be uniformly mixed for 25 minutes;
adding antioxidant, preservative, acidity regulator, sweetener and cooling agent, and stirring for 25 min to uniformity;
adding humectant in weight parts, and stirring for 8 minutes until the mixture is uniform;
adding the uniform mixture into a lip tobacco powder split charging machine for packaging with 0.5 g+/-0.1 g of each package, wherein the package adopts food-grade non-woven fabrics, and the package size is 1.2cm x 3cm; and conveying the produced packaging lip cigarettes to an ultraviolet sterilizing furnace for 18-22 seconds. Thus, the finished lip cigarette product which can be used is finished.
The obtained qualified product is subjected to product performance test, and the performance parameters are shown in Table 5
For each evaluation index, see embodiment one.
TABLE 5
| Time index | For 5 minutes | For 10 minutes | 15 minutes | 20 minutes | 25 minutes | 30 minutes |
| Taste in mouth | 7 | 7 | 6.8 | 6.5 | 6.5 | 6 |
| Concentration of nicotine salt | 0.022mg/mL | 0.023mg/mL | 0.020mg/mL | 0.019mg/mL | 0.021mg/mL | 0.017mg/mL |
| Sustained release of nicotine salts | 0.864 | 0.955 | 0.773 | |||
| 35 minutes | 40 minutes | 45 minutes | 50 minutes | 55 minutes | 60 minutes | |
| Taste in mouth | 6 | 6 | 5.5 | 5.5 | 5 | 4.5 |
| Concentration of nicotine salt | 0.018mg/mL | 0.014mg/mL | 0.015mg/mL | 0.012mg/mL | 0.008mg/mL | 0.006mg/mL |
| Sustained release of nicotine salts | 0.818 | 0.636 | 0.682 | 0.545 | 0.364 | 0.273 |
It can be seen that the lip cigarette produced by the formulation and process of the fifth embodiment is replaced with the citrus fiber powder in comparison with the first embodiment.
The mouthfeel obtained was poorly evaluated by the user, and the mouthfeel was greatly changed with time.
The uniformity of nicotine salt release is poor and the nicotine salt concentration fluctuates with time.
The release durability of the nicotine salt is generally that after 20 minutes, the nicotine salt concentration in the smoke can only reach 86.4% at 5 minutes, and when the nicotine salt concentration in the smoke reaches 55 minutes, the nicotine salt concentration in the smoke can only reach 36.4% at 5 minutes, and the continuous use is not recommended, so that the taste experience is affected.
Therefore, the lip tobacco produced by the formula and the process of the fifth embodiment has poor taste and poor uniformity of nicotine salt release, and the nicotine salt release durability is general, so that the tea herbal lip tobacco prepared by the formula and the process of the fifth embodiment has no advantages in taste, nicotine salt release uniformity and nicotine salt release durability.
The sixth embodiment of the invention:
the formula comprises the following raw materials:
40 parts of corn fiber powder, 40.8 parts of xylitol, 20 parts of essence, 4.8 parts of nicotine salt, 0.05 part of antioxidant, 0.05 part of preservative, 0.4 part of sour regulator, 1.2 parts of sweetener, 2.6 parts of cooling agent and 2 parts of humectant.
First the corn flour of the weight part is prepared,
taking weight parts of dry corns, and crushing the dry corns by a crusher with 120 meshes to obtain dry corn powder;
pouring the dry corn flour obtained by STEP1 into a stainless steel stirring tank, adding half of the water by weight, and stirring for 8 minutes until the corn flour is uniform;
placing a 300w ultrasonic vibration rod, performing ultrasonic extraction for 60 minutes, taking out the mixed solution, and pouring the mixed solution into a centrifuge for centrifugation for 35 minutes;
and adding half of the water by weight again, performing ultrasonic extraction again for 60 minutes, taking out the mixed solution, pouring the mixed solution into a centrifuge for centrifugation, and taking out the mixed solution after 35 minutes to obtain the extracted corn flour with higher water content.
Putting the obtained corn powder into a dryer for drying treatment for 30 minutes to obtain 0.7 weight part of dry corn powder after preliminary extraction;
and (3) putting the dry corn powder into a reaction kettle, adding the alcohol in parts by weight, stirring and heating at a low temperature of 80 ℃ for 5 hours, putting into a centrifuge for 30 minutes, centrifuging, taking out the mixture, putting into a dryer for 30 minutes, drying to obtain 0.5 part of the finally extracted corn powder, and measuring that the water content of the extracted corn powder is 4.2%.
Preparing lip tobacco, namely placing the corn flour, the xylitol powder, the essence and the nicotine salt in the weight parts into a low-speed stirrer to be uniformly mixed for 25 minutes;
adding antioxidant, preservative, acidity regulator, sweetener and cooling agent, and stirring for 25 min to uniformity;
adding humectant in weight parts, and stirring for 8 minutes until the mixture is uniform;
adding the uniform mixture into a lip tobacco powder split charging machine for packaging with 0.5 g+/-0.1 g of each package, wherein the package adopts food-grade non-woven fabrics, and the package size is 1.2cm x 3cm; and conveying the produced packaging lip cigarettes to an ultraviolet sterilizing furnace for 18-22 seconds. Thus, the finished lip cigarette product which can be used is finished.
The obtained qualified product is subjected to product performance test, and the performance parameters are shown in Table 6
For each evaluation index, see embodiment one.
TABLE 6
| Time index | For 5 minutes | For 10 minutes | 15 minutes | 20 minutes | 25 minutes | 30 minutes |
| Taste in mouth | 7 | 6.8 | 7 | 6.5 | 6.2 | 6.2 |
| Concentration of nicotine salt | 0.023mg/mL | 0.022mg/mL | 0.019mg/mL | 0.020mg/mL | 0.021mg/mL | 0.016mg/mL |
| Sustained release of nicotine salts | 0.870 | 0.913 | 0.696 | |||
| 35 minutes | 40 minutes | 45 minutes | 50 minutes | 55 minutes | 60 minutes | |
| Taste in mouth | 6 | 5.5 | 5.3 | 5.2 | 5 | 4.5 |
| Concentration of nicotine salt | 0.014mg/mL | 0.015mg/mL | 0.012mg/mL | 0.010mg/mL | 0.008mg/mL | 0.006mg/mL |
| Sustained release of nicotine salts | 0.609 | 0.652 | 0.522 | 0.435 | 0.348 | 0.261 |
It can be seen that the lip cigarette produced by the formulation and process of example six is replaced by corn meal in comparison with the composition of tea meal and microcrystalline cellulose of example one.
The mouthfeel obtained was poorly evaluated by the user, and the mouthfeel was greatly changed with time.
The uniformity of nicotine salt release is poor and the nicotine salt concentration fluctuates with time.
The release durability of the nicotine salt is generally that after 20 minutes, the nicotine salt concentration in the smoke can only reach 87% at 5 minutes, and after 50 minutes, the nicotine salt concentration in the smoke can only reach 43.5% at 5 minutes, and the continuous use is not recommended, so that the taste experience is affected.
Therefore, the lip cigarette produced by the formula and the process in the sixth embodiment has poor taste and poor uniformity of nicotine salt release, and the nicotine salt release durability is general, so that the tea herbal lip cigarette prepared by the formula and the process in the fifth embodiment has no advantages in taste, nicotine salt release uniformity and nicotine salt release durability.
The above embodiments are not intended to limit the scope of the present invention, so: all equivalent changes in structure, shape and principle of the invention should be covered in the scope of protection of the invention.
Claims (7)
1. A slow release type herbal lip cigarette is characterized in that: the formula comprises the following raw materials: 20-25 parts of tea powder, 15-18 parts of microcrystalline cellulose, 37-42 parts of xylitol, 18-21 parts of essence and 3-6 parts of nicotine salt; the lip gloss is white powder; the tea powder comprises the following components in parts by weight: the tea powder is prepared by extracting and drying dry tea, water and 65-degree alcohol in a ratio of 10:3.5, and the preparation method of the tea powder comprises the following steps:
step1, extracting with water for the first time, taking the dry tea, crushing the dry tea with a crusher for 120 meshes to obtain dry tea powder, pouring the dry tea powder into a stainless steel stirring tank, adding half of water by weight, stirring for 5-10 minutes until the water is uniform, putting into an ultrasonic vibration rod, performing ultrasonic extraction for 50-70 minutes, taking out the mixed solution, pouring into a centrifuge, and centrifuging for 30 minutes;
step2, water extraction is carried out for the second time, half of the water by weight is added again, ultrasonic extraction is carried out again for 50-70 minutes, then the mixed solution is taken out, poured into a centrifuge for centrifugation, and taken out after 25-35 minutes, thus obtaining 0.6-0.8 weight part of tea powder after water extraction;
step3, drying, namely placing the tea powder after water extraction into a dryer for drying treatment for 30 minutes to obtain dry tea powder after primary extraction;
and 4, placing the dry tea powder after preliminary extraction into a reaction kettle, adding 65-degree alcohol according to the weight parts, stirring and heating at 75-80 ℃ for 4-6 hours, placing into a centrifuge for 30 minutes and centrifuging, taking out the mixture, and placing into a dryer for 30 minutes and drying to obtain the finally extracted tea powder.
2. The slow release herbal lip cigarette according to claim 1, wherein: also comprises 0.01-0.1 part of antioxidant, 0.01-0.1 part of preservative, 0.1-1 part of sour regulator, 0.5-2 parts of sweetener, 1.5-3.5 parts of cooling agent and 1-3 parts of humectant.
3. The slow release herbal lip cigarette according to claim 2, wherein: the xylitol is xylitol powder, and the particle size of the powder is 50-150 meshes.
4. A slow release herbal lip cigarette according to claim 3, wherein: the grain size of the microcrystalline cellulose is 50-100 mu m.
5. A process for producing a slow-release herbal lip cigarette according to any one of claims 2 to 4, which is characterized in that:
step1, placing the tea powder, the microcrystalline cellulose powder, the xylitol powder, the essence and the nicotine salt in a low-speed stirrer to uniformly mix for 20-30 minutes;
step2, adding the antioxidant, the preservative, the acidity regulator, the sweetener and the cooling agent in parts by weight, and continuously stirring for 20-30 minutes until the mixture is uniform;
step3, adding the humectant in the weight parts, and stirring for 5-10 minutes until the humectant is uniform;
step4, adding the uniform mixture in Step3 into a lip tobacco powder split charging machine for packaging with the package size of 1.2cm multiplied by 3cm, wherein each package is 0.5 g+/-0.1 g.
6. The process for producing slow release type herbal lip cigarette according to claim 5, wherein: and a sterilization process, which is to transfer the packaging lip cigarette produced by Step4 to an ultraviolet sterilization furnace for 18-22 seconds.
7. The process for producing slow release type herbal lip cigarette according to claim 6, wherein: the boxing process comprises the following steps:
s1, conveying the materials to a counting boxing machine for 25-pack one-pack split charging;
s2, conveying the box-packed lip cigarettes to a labeling machine for labeling up and down and spraying production dates;
s3, transmitting the label to a side label labeling machine for side label sticking and sealing;
s4, conveying the film to a film cutting machine for packaging and cutting the heat shrinkage film;
s5, conveying the film to a thermal shrinkage furnace for thermal shrinkage film coating;
s6, conveying the materials to a box filling machine for filling.
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