CN115104673A - Preparation process and device of selenium-rich saccharicterpenin - Google Patents
Preparation process and device of selenium-rich saccharicterpenin Download PDFInfo
- Publication number
- CN115104673A CN115104673A CN202210781685.2A CN202210781685A CN115104673A CN 115104673 A CN115104673 A CN 115104673A CN 202210781685 A CN202210781685 A CN 202210781685A CN 115104673 A CN115104673 A CN 115104673A
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- Prior art keywords
- filter
- saccharicterpenin
- wall
- pipe
- worm
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- 239000011669 selenium Substances 0.000 title claims abstract description 20
- BUGBHKTXTAQXES-UHFFFAOYSA-N Selenium Chemical compound [Se] BUGBHKTXTAQXES-UHFFFAOYSA-N 0.000 title claims abstract description 19
- 229910052711 selenium Inorganic materials 0.000 title claims abstract description 19
- 238000002360 preparation method Methods 0.000 title claims abstract description 18
- 238000003756 stirring Methods 0.000 claims abstract description 37
- 238000004140 cleaning Methods 0.000 claims abstract description 19
- 241001122767 Theaceae Species 0.000 claims abstract description 15
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 59
- 235000012054 meals Nutrition 0.000 claims description 32
- 240000001548 Camellia japonica Species 0.000 claims description 31
- 235000018597 common camellia Nutrition 0.000 claims description 31
- 238000001914 filtration Methods 0.000 claims description 28
- 238000002156 mixing Methods 0.000 claims description 15
- 238000003466 welding Methods 0.000 claims description 12
- 241000526900 Camellia oleifera Species 0.000 claims description 10
- 229930182490 saponin Natural products 0.000 claims description 10
- 150000007949 saponins Chemical class 0.000 claims description 10
- 235000017709 saponins Nutrition 0.000 claims description 10
- 238000007789 sealing Methods 0.000 claims description 9
- 239000000706 filtrate Substances 0.000 claims description 6
- 239000002244 precipitate Substances 0.000 claims description 6
- 230000000295 complement effect Effects 0.000 claims description 5
- 238000010438 heat treatment Methods 0.000 claims description 5
- 239000007788 liquid Substances 0.000 claims description 5
- 230000008878 coupling Effects 0.000 claims description 4
- 238000010168 coupling process Methods 0.000 claims description 4
- 238000005859 coupling reaction Methods 0.000 claims description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 4
- 229920001661 Chitosan Polymers 0.000 claims description 3
- 238000004108 freeze drying Methods 0.000 claims description 3
- 238000000227 grinding Methods 0.000 claims description 3
- 238000002386 leaching Methods 0.000 claims description 3
- 239000000463 material Substances 0.000 claims description 3
- 239000001397 quillaja saponaria molina bark Substances 0.000 claims description 3
- 239000002994 raw material Substances 0.000 claims description 3
- 238000001694 spray drying Methods 0.000 claims description 3
- 239000006228 supernatant Substances 0.000 claims description 3
- 238000007599 discharging Methods 0.000 abstract description 8
- 230000009347 mechanical transmission Effects 0.000 abstract description 5
- 238000004064 recycling Methods 0.000 abstract description 5
- 230000009286 beneficial effect Effects 0.000 abstract description 2
- 239000000243 solution Substances 0.000 description 19
- 230000002349 favourable effect Effects 0.000 description 4
- QGJOPFRUJISHPQ-UHFFFAOYSA-N Carbon disulfide Chemical compound S=C=S QGJOPFRUJISHPQ-UHFFFAOYSA-N 0.000 description 3
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 3
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 description 3
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 description 3
- 244000309464 bull Species 0.000 description 3
- 239000002893 slag Substances 0.000 description 3
- 150000008130 triterpenoid saponins Chemical class 0.000 description 3
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 2
- 150000001720 carbohydrates Chemical class 0.000 description 2
- 239000012141 concentrate Substances 0.000 description 2
- 230000003068 static effect Effects 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 229960000583 acetic acid Drugs 0.000 description 1
- TXHIDIHEXDFONW-UHFFFAOYSA-N benzene;propan-2-one Chemical compound CC(C)=O.C1=CC=CC=C1 TXHIDIHEXDFONW-UHFFFAOYSA-N 0.000 description 1
- 230000000975 bioactive effect Effects 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 238000005520 cutting process Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 239000012362 glacial acetic acid Substances 0.000 description 1
- 238000010030 laminating Methods 0.000 description 1
- 239000011259 mixed solution Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 150000007524 organic acids Chemical class 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 238000007493 shaping process Methods 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
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Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K10/00—Animal feeding-stuffs
- A23K10/30—Animal feeding-stuffs from material of plant origin, e.g. roots, seeds or hay; from material of fungal origin, e.g. mushrooms
- A23K10/37—Animal feeding-stuffs from material of plant origin, e.g. roots, seeds or hay; from material of fungal origin, e.g. mushrooms from waste material
- A23K10/38—Animal feeding-stuffs from material of plant origin, e.g. roots, seeds or hay; from material of fungal origin, e.g. mushrooms from waste material from distillers' or brewers' waste
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/10—Organic substances
- A23K20/163—Sugars; Polysaccharides
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23N—MACHINES OR APPARATUS FOR TREATING HARVESTED FRUIT, VEGETABLES OR FLOWER BULBS IN BULK, NOT OTHERWISE PROVIDED FOR; PEELING VEGETABLES OR FRUIT IN BULK; APPARATUS FOR PREPARING ANIMAL FEEDING- STUFFS
- A23N17/00—Apparatus specially adapted for preparing animal feeding-stuffs
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D29/00—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor
- B01D29/50—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor with multiple filtering elements, characterised by their mutual disposition
- B01D29/56—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor with multiple filtering elements, characterised by their mutual disposition in series connection
- B01D29/58—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor with multiple filtering elements, characterised by their mutual disposition in series connection arranged concentrically or coaxially
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D29/00—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor
- B01D29/62—Regenerating the filter material in the filter
- B01D29/64—Regenerating the filter material in the filter by scrapers, brushes, nozzles, or the like, acting on the cake side of the filtering element
- B01D29/6407—Regenerating the filter material in the filter by scrapers, brushes, nozzles, or the like, acting on the cake side of the filtering element brushes
- B01D29/6423—Regenerating the filter material in the filter by scrapers, brushes, nozzles, or the like, acting on the cake side of the filtering element brushes with a translational movement with respect to the filtering element
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D29/00—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor
- B01D29/96—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor in which the filtering elements are moved between filtering operations; Particular measures for removing or replacing the filtering elements; Transport systems for filters
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Polymers & Plastics (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Food Science & Technology (AREA)
- Animal Husbandry (AREA)
- Zoology (AREA)
- Health & Medical Sciences (AREA)
- Biotechnology (AREA)
- Botany (AREA)
- Molecular Biology (AREA)
- Mycology (AREA)
- Physiology (AREA)
- Extraction Or Liquid Replacement (AREA)
Abstract
The invention discloses a preparation process and a device of selenium-rich saccharicterpenin, which relate to the field of agricultural resource recycling and comprise a collecting box, a filter pipe, a stirring bin, a second motor, a stirring rod, a guide plate and a discharge mechanism; and the auxiliary mechanism is used for cleaning residues falling below the first filter plate. According to the automatic oil tea seed residue discharging device, the discharging mechanism is arranged, the output end of the first motor rotates to drive the first filter plate to rotate upwards through mechanical transmission, the first filter plate rotates to drive oil tea seed residue accumulated at the top end of the first filter plate to move upwards, the guide plate cuts the moved oil tea seed residue, the first worm rotates to drive the first baffle plate to move through mechanical transmission, the cut residue is moved out of the inside of the filter pipe through the residue outlet, and the automatic oil tea seed residue discharging device is beneficial to automatic oil tea seed residue discharging operation inside the filter pipe through the structure.
Description
Technical Field
The invention relates to the field of agricultural resource recycling, in particular to a preparation process and a device of selenium-rich saccharicterpenin.
Background
Saccharicterpenin is mainly developed by using saccharides and triterpenoid saponins in theaceae plants as main bodies, triterpenoid saponins in seed cakes of theaceae plants are bioactive substances consisting of organic acid-ligand-saccharides, are stable in chemical properties, can be dissolved in warm water, carbon disulfide and ethyl acetate, are easily dissolved in aqueous methanol, aqueous ethanol, n-butyl alcohol and glacial acetic acid but are not dissolved in solvents such as diethyl ether, acetone benzene and the like, are resistant to high temperature and are brownish yellow and ashless fine crystals, the saccharicterpenin mainly consists of saccharides (more than 30 percent), triterpenoid saponins (more than or equal to 30 percent) and organic acid, and the addition amount of the saccharicterpenin in feed is 0.2-0.5 mg/kg.
At present, selenium-rich saccharicterpenin is in the preparation process, through mixing camellia seed meal and ethanol of certain volume proportion, then carry out the operation of stirring through the poking bar, the stirring is finished and is obtained concentrate and camellia seed meal residue after static for a period of time, present staff is collecting the back to the concentrate, mostly carry out the operation of taking out through artifical manual camellia seed meal residue on filter top, open the filter tube earlier when taking out, take off the filter again, clear up the collection to the residue on filter top, later install the filter to the filter tube on, close the filter tube again, because add the filterable step of ethanol heating and need repeat many times, manual operation has reduced the preparation efficiency of device, and staff's work load has also been increased.
Disclosure of Invention
The invention aims to: in order to solve the problem that filtered residues cannot be automatically discharged, a preparation process of selenium-rich saccharicterpenin and a device thereof are provided.
In order to achieve the purpose, the invention provides the following technical scheme: a preparation process and a device of selenium-rich saccharicterpenin comprise a collecting box, wherein a filter pipe is fixedly welded at the top end of the collecting box, a solenoid valve is arranged at the joint of the filter pipe and a stirring bin, the top end of the filter pipe is fixedly welded with the stirring bin, a second motor is fixedly arranged at the top end of the stirring bin through a bolt, the output end of the second motor is connected with a stirring rod extending into the stirring bin through a coupling, a guide plate is fixedly welded on the inner wall of the filter pipe, and a discharge mechanism is arranged in the filter pipe;
the discharge mechanism comprises a first motor fixed at one end of the filter pipe through a bolt, the output end of the first motor is connected with a first worm extending into the filter pipe through a coupling, a first worm wheel is meshed at the top end of the first worm, a connecting column is fixed on one side of the first worm wheel through welding, the outer wall of the connecting column is fixedly connected with a first filter plate, one end of the first worm is fixedly provided with a rotating rod through welding, a first bevel gear is fixedly connected with the outer wall of the rotating rod, a second bevel gear is meshed with the top end of the first bevel gear, a first screw rod is fixed at the top end of the second bevel gear through welding, the outer wall of the first screw rod is connected with a connecting rod through threads, the bottom of connecting rod is through welded fastening has first baffle, one side of spliced pole is provided with complementary unit for the operation of clearing up the residue that drops to first filter below.
As a still further scheme of the invention: the auxiliary mechanism includes the third bevel gear through welded fastening in spliced pole one side, the bottom meshing of third bevel gear has the fourth bevel gear, welded fastening has the second worm in the bottom of fourth bevel gear, one side meshing of second worm has the second worm wheel, the one end of second worm wheel has the second lead screw through welded fastening, the outer wall of second lead screw has the cleaning brush through threaded connection, there is the fixed block one end of cleaning brush through bolted connection, the filter tube inner wall have with the second filter of cleaning brush bottom laminating through bolted connection, the one end that the cleaning brush was kept away from to the filter tube inner wall is connected with the bull stick through the bearing, the outer wall fixedly connected with second baffle of bull stick.
As a still further scheme of the invention: the second worm and the second screw rod are rotatably connected with the inner wall of the filter pipe through bearings, and the second worm wheel is rotatably connected with the inner wall of the filter pipe through a rotating shaft.
As a still further scheme of the invention: the inside shaping of filter tube has and removes the orbit assorted sliding tray of brush, just the fixed block is in same level with the second baffle, the inside of filter tube is provided with rotates the orbit assorted rotation groove with the second baffle, the junction of bull stick and filter tube is provided with the sealing member.
As a still further scheme of the invention: the first worm is provided with two, and symmetric distribution is at the both ends of dwang, first filter is provided with two, first filter is located the top of second filter.
As a still further scheme of the invention: the spliced pole passes through the bearing with first lead screw and is connected with the inner wall rotation of filter tube, the spliced pole is provided with the sealing member with the junction of filter tube, one side of first worm wheel is connected with the pivot, the pivot is connected with the fixed plate through the bearing, the inner wall fixed connection of fixed plate and filter tube.
As a still further scheme of the invention: the inside of filter tube is provided with connecting rod assorted sliding tray, the inside of filter tube be provided with first baffle assorted spout, and the junction of first baffle and filter tube is provided with the sealing member.
As a still further scheme of the invention: a preparation process of selenium-rich saccharicterpenin comprises the following steps:
step 1, crushing raw materials: carrying out ultrafine grinding on the degreased camellia seed meal to 100 meshes;
step 4, preparing the oil tea total sugar: adding water in a ratio of 1:10 into the oil tea seed meal filtration residue filtered in the step 2, extracting for 2 times at the temperature of 80 ℃, extracting for 2 hours each time, combining the filtrates, filtering, concentrating to obtain a concentrated solution, adding ethanol with the volume fraction of 3 times being 85%, standing for 24 hours, removing the supernatant, leaving a precipitate, and freeze-drying to obtain oil tea total sugar;
As a still further scheme of the invention: and 2, mixing the camellia seed meal powder and the ethanol and filtering camellia seed meal residues through the collecting box, the filtering pipe and the stirring bin.
Compared with the prior art, the invention has the beneficial effects that:
1. through the arrangement of the discharging mechanism, the output end of the first motor rotates to drive the first filter plate to rotate upwards through mechanical transmission, the first filter plate rotates and drives the camellia seed meal residues accumulated at the top end of the first filter plate to move upwards, the guide plate cuts the moved camellia seed meal residues, the first worm rotates and drives the first baffle plate to move through mechanical transmission, the cut residues are moved out of the inside of the filter pipe through the residue outlet, the automatic discharging operation of the camellia seed meal residues in the filter pipe is facilitated through the structure, and compared with the traditional manual discharging, the working efficiency of the device is improved;
2. through setting up complementary unit, the spliced pole rotates and drives the removal of clearance brush through mechanical transmission simultaneously, the clearance brush removes and will pile up the one end on second filter top at the partial residue on second filter top, the fixed block removes and promotes the rotation of second baffle, later the clearance brush removes and passes through the inside of the second slag notch discharge filter tube on second filter one end with the residue on second filter top, be favorable to carrying out whole exhaust operations to the inside residue of filter tube through this structure, avoid the accumulational condition of residue to appear on the top of second filter, the normal use of second filter has been guaranteed.
Drawings
FIG. 1 is a schematic structural view of the present invention;
FIG. 2 is a schematic view of a first perspective structure inside the filtering pipe and the stirring bin according to the present invention;
FIG. 3 is an enlarged view of the structure at A in FIG. 2 according to the present invention;
FIG. 4 is a second perspective view of the filter tube and the interior of the stirring chamber according to the present invention;
FIG. 5 is an enlarged view of the structure at B in FIG. 4 according to the present invention;
FIG. 6 is a third view structural diagram of the interior of the filtering pipe and the stirring bin of the present invention;
fig. 7 is an enlarged view of the structure of fig. 6 at C according to the present invention.
In the figure: 1. a collection box; 2. a filter tube; 3. a stirring bin; 4. a discharge mechanism; 401. a first motor; 402. a first worm; 403. a first worm gear; 404. connecting columns; 405. a first filter plate; 406. rotating the rod; 407. a first bevel gear; 408. a second bevel gear; 409. a first lead screw; 410. a connecting rod; 411. a first baffle; 5. an auxiliary mechanism; 501. a third bevel gear; 502. a fourth bevel gear; 503. a second worm; 504. a second worm gear; 505. a second lead screw; 506. cleaning a brush; 507. a fixed block; 508. a second filter plate; 509. a rotating rod; 510. a second baffle; 6. a stirring rod; 7. a baffle; 8. a second motor.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. Based on the embodiments of the present invention, all other embodiments obtained by a person of ordinary skill in the art of agricultural resource recycling without creative efforts belong to the protection scope of the present invention.
In the description of the present invention, it should be noted that the terms "center", "upper", "lower", "left", "right", "vertical", "horizontal", "inner", "outer", etc., indicate orientations or positional relationships based on the orientations or positional relationships shown in the drawings, and are only for convenience of description and simplicity of description, but do not indicate or imply that the device or element being referred to must have a particular orientation, be constructed and operated in a particular orientation, and thus, should not be construed as limiting the present invention. Furthermore, the terms "first," "second," and "third" are used for descriptive purposes only and are not to be construed as indicating or implying relative importance. In the description of the present invention, it should be noted that, unless otherwise explicitly specified or limited, the terms "mounted," "connected," and "disposed" are to be construed broadly, e.g., as meaning either a fixed connection, a removable connection, or an integral connection; can be mechanically or electrically connected; they may be connected directly or indirectly through intervening media, or they may be interconnected between two elements. The specific meaning of the above terms in the present invention can be understood in specific cases to those of ordinary skill in the art of agricultural resource recycling. The following describes an embodiment of the present invention based on its overall structure.
Referring to fig. 1 to 7, in the embodiment of the invention, a preparation process of selenium-rich saccharicterpenin and a device thereof comprise a collection box 1, wherein a filter pipe 2 is fixedly welded at the top end of the collection box 1, an electromagnetic valve is arranged at the joint of the filter pipe 2 and a stirring bin 3, the stirring bin 3 is fixedly welded at the top end of the filter pipe 2, a second motor 8 is fixedly arranged at the top end of the stirring bin 3 through a bolt, the output end of the second motor 8 is connected with a stirring rod 6 extending into the stirring bin 3 through a coupler, a guide plate 7 is fixedly welded on the inner wall of the filter pipe 2, and a discharge mechanism 4 is arranged in the filter pipe 2;
discharge mechanism 4 includes the first motor 401 of being fixed in filter tube 2 one end through the bolt, the output of first motor 401 has the first worm 402 that extends to filter tube 2 inside through the coupling joint, the top meshing of first worm 402 has first worm wheel 403, one side of first worm wheel 403 has spliced pole 404 through welded fastening, the outer wall fixedly connected with first filter 405 of spliced pole 404, the one end of first worm 402 has dwang 406 through welded fastening, the outer wall fixedly connected with first bevel gear 407 of dwang 406, the top meshing of first bevel gear 407 has second bevel gear 408, the top of second bevel gear 408 has first lead screw 409 through welded fastening, the outer wall of first lead screw 409 has connecting rod 410 through threaded connection, the bottom of connecting rod 410 has first baffle 411 through welded fastening, one side of spliced pole 404 is provided with complementary unit 5, be used for the operation of clearing up the residue that drops to first filter 405 below.
In this embodiment: the stirring rod 6 is used for stirring and mixing the camellia seed meal and the ethanol, the collecting box 1 is used for collecting the concentrated solution, the mixed solution in the stirring bin 3 can flow into the filtering pipe 2 by opening the electromagnetic valve, the flowing solution can be divided by the guide plate 7 to uniformly flow to the upper part of the first filtering plate 405, the residue in the solution can be filtered by the first filter plate 405, and when the solution is completely discharged, the automatic discharge operation of the camellia seed meal residues in the filter pipe 2 can be carried out through the matching of other parts of the discharge mechanism 4, compared with the traditional manual discharge, the working efficiency of the device is improved, through setting up complementary unit 5 and being favorable to carrying out whole exhaust operations to the inside residue of filter tube 2, avoid the top of second filter 508 the accumulational condition of residue to appear, guaranteed the normal use of second filter 508.
Please refer to fig. 2 to 5, the auxiliary mechanism 5 includes a third bevel gear 501 fixed to one side of the connecting column 404 by welding, a fourth bevel gear 502 is engaged with the bottom end of the third bevel gear 501, a second worm 503 is fixed to the bottom end of the fourth bevel gear 502 by welding, a second worm wheel 504 is engaged with one side of the second worm 503, a second lead screw 505 is fixed to one end of the second worm wheel 504 by welding, a cleaning brush 506 is connected to the outer wall of the second lead screw 505 by a thread, a fixing block 507 is connected to one end of the cleaning brush 506 by a bolt, a second filter plate 508 attached to the bottom end of the cleaning brush 506 is fixed to the inner wall of the filter tube 2 by a bolt, a rotating rod 509 is connected to one end of the inner wall of the filter tube 2, which is far away from the cleaning brush 506, by a bearing, and a second baffle plate 510 is fixedly connected to the outer wall of the rotating rod 509; the second worm 503 and the second lead screw 505 are rotatably connected with the inner wall of the filter pipe 2 through a bearing, and the second worm wheel 504 is rotatably connected with the inner wall of the filter pipe 2 through a rotating shaft; a sliding groove matched with the moving track of the cleaning brush 506 is formed in the inner wall of the filter pipe 2, the fixing block 507 and the second baffle 510 are at the same horizontal height, a rotating groove matched with the rotating track of the second baffle 510 is formed in the filter pipe 2, and a sealing element is arranged at the joint of the rotating rod 509 and the filter pipe 2.
In this embodiment: the camellia seed meal residue part falls to the top end of a second filter plate 508 through a space between two rotated first filter plates 405, a connecting column 404 rotates and drives a third bevel gear 501 to rotate, the third bevel gear 501 rotates and drives a fourth bevel gear 502 to rotate, the fourth bevel gear 502 rotates and drives a second worm 503 to rotate, the second worm 503 rotates and drives a second worm wheel 504 to rotate, the second worm wheel 504 rotates and drives a second screw rod 505 to rotate, the second screw rod 505 rotates and drives a cleaning brush 506 to move, the cleaning brush 506 moves and pushes part of residue accumulated at the top end of the second filter plate 508 to one end of the top end of the second filter plate 508, when a fixed block 507 is in contact with the second baffle plate 510, the fixed block 507 continues to move and pushes the second baffle plate 510 to rotate, then the cleaning brush 506 moves and discharges the residue at the top end of the second filter plate 508 out of the filter pipe 2 through a second residue outlet at one end of the second filter plate 508, through this structure be favorable to carrying out whole exhaust operations to the inside residue of filter tube 2, avoid the accumulational condition of residue to appear in the top of second filter 508, guaranteed the normal use of second filter 508.
Please refer to fig. 1, 2, 6, and 7, the first worm 402 is provided with two worms and symmetrically distributed at two ends of the rotating rod 406, the first filter plate 405 is provided with two worms, and the first filter plate 405 is located above the second filter plate 508; the connecting column 404 and the first screw rod 409 are rotatably connected with the inner wall of the filter pipe 2 through a bearing, a sealing element is arranged at the connecting position of the connecting column 404 and the filter pipe 2, one side of the first worm gear 403 is connected with a rotating shaft, the rotating shaft is connected with a fixing plate through a bearing, and the fixing plate is fixedly connected with the inner wall of the filter pipe 2; the inside of filter tube 2 is provided with the sliding tray with connecting rod 410 assorted, the inside of filter tube 2 be provided with first baffle 411 assorted spout, and the junction of first baffle 411 and filter tube 2 is provided with the sealing member.
In this embodiment: in the step 2, firstly, the electromagnetic valve at the joint of the filter pipe 2 and the stirring bin 3 is closed, then ethanol with a certain volume is added into the stirring bin 3 through the feeding pipe at the top end of the stirring bin 3, then the camellia seed meal is added into the stirring bin 3 through the feeding hole, the second motor 8 works, the output end of the second motor 8 rotates and drives the stirring rod 6 to rotate, the stirring rod 6 rotates and stirs the camellia seed meal and the ethanol, then a worker observes the mixing condition of the camellia seed meal and the ethanol through the transparent window at one side of the filter pipe 2, when the mixing requirement is met and the mixture is static for a period of time, the electromagnetic valve inside the filter pipe 2 is opened, the concentrated liquid flows into the collection box 1 through the electromagnetic valve, the first motor 401 is opened after the concentrated liquid completely flows into the collection box 1, the output end of the first motor 401 rotates and drives the first worm 402 to rotate, the first worm 402 rotates to drive the first worm wheel 403 to rotate, the first worm wheel 403 rotates to drive the connecting column 404 to rotate, the connecting column 404 rotates to drive the first filter plate 405 to rotate upwards, the first filter plate 405 rotates and drives the camellia seed meal residues accumulated on the top end of the first filter plate 405 to move upwards, the guide plate 7 performs cutting operation on the moved camellia seed meal residues, the first worm 402 rotates and drives the rotating rod 406 to rotate, the rotating rod 406 rotates and drives the first bevel gear 407 to rotate, the first bevel gear 407 rotates and drives the second bevel gear 408 to rotate, the second bevel gear 408 rotates and drives the first lead screw 409 to rotate, the first lead screw 409 rotates and drives the connecting rod 410 to move upwards, the connecting rod 410 moves and drives the first baffle 411 to move, the first baffle 411 moves and opens slag outlets at two ends of the filter tube 2, at the moment, the first filter plate 405 inclines and the cut residues move out of the interior of the filter tube 2 through the slag outlets, through this structure be favorable to carrying out automatic discharge's operation to the inside oil tea seed dregs residue of filter tube 2, compare in traditional artifical manual discharge, improved the efficiency of device work.
A preparation process of selenium-rich saccharicterpenin comprises the following steps:
step 1, crushing raw materials: carrying out ultrafine grinding on the degreased camellia seed meal to 100 meshes;
step 4, preparing the oil tea total sugar: adding water in a ratio of 1:10 into the residues filtered from the camellia seed meal in the step 2, extracting for 2 times at the temperature of 80 ℃ for 2 hours each time, combining the filtrates, filtering, concentrating to obtain a concentrated solution, adding ethanol with a volume fraction of 85% 3 times, standing for 24 hours, removing the supernatant, leaving a precipitate, and freeze-drying to obtain camellia total sugar;
In this embodiment: the concentrated solution required by the preparation of the total saponins of camellia oleifera is obtained by mixing camellia seed meal and ethanol according to a certain proportion and then heating at a constant temperature.
Please refer to fig. 1, in step 2, the mixing operation of the camellia seed meal and the ethanol and the filtering operation of the camellia seed meal residue are performed through the collecting box 1, the filtering pipe 2 and the stirring bin 3.
In this embodiment: through the structure, the full mixing of the camellia seed meal and the ethanol is facilitated, and the automatic discharging operation of the filtered camellia seed meal residues is facilitated.
The above description is only for the preferred embodiment of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art of agricultural resource recycling in the art should be covered by the present invention, and the technical solutions and the inventive concepts thereof according to the present invention should be equally replaced or changed within the technical scope of the present invention.
Claims (9)
1. A preparation device of selenium-rich saccharicterpenin comprises a collection box (1), wherein a filter pipe (2) is fixedly welded at the top end of the collection box (1), an electromagnetic valve is arranged at the joint of the filter pipe (2) and a stirring bin (3), the stirring bin (3) is fixedly welded at the top end of the filter pipe (2), a second motor (8) is fixedly arranged at the top end of the stirring bin (3) through a bolt, the output end of the second motor (8) is connected with a stirring rod (6) extending into the stirring bin (3) through a coupler, and a guide plate (7) is fixedly welded on the inner wall of the filter pipe (2), and is characterized in that a discharge mechanism (4) is arranged in the filter pipe (2);
the discharge mechanism (4) comprises a first motor (401) fixed at one end of the filter pipe (2) through a bolt, the output end of the first motor (401) is connected with a first worm (402) extending to the inside of the filter pipe (2) through a coupling joint, the top end of the first worm (402) is meshed with a first worm wheel (403), one side of the first worm wheel (403) is fixedly provided with a connecting column (404) through welding, the outer wall of the connecting column (404) is fixedly connected with a first filter plate (405), one end of the first worm (402) is fixedly provided with a rotating rod (406) through welding, the outer wall of the rotating rod (406) is fixedly connected with a first bevel gear (407), the top end of the first bevel gear (407) is meshed with a second bevel gear (408), the top end of the second bevel gear (408) is fixedly provided with a first screw rod (409) through welding, the outer wall of the first screw rod (409) is connected with a connecting rod (410) through a thread, the bottom of connecting rod (410) is through welded fastening has first baffle (411), one side of spliced pole (404) is provided with complementary unit (5) for the operation of clearing up the residue that drops to first filter (405) below.
2. The selenium-rich saccharicterpenin preparation device according to claim 1, wherein the auxiliary mechanism (5) comprises a third bevel gear (501) fixed on one side of a connecting column (404) by welding, the bottom end of the third bevel gear (501) is engaged with a fourth bevel gear (502), the bottom end of the fourth bevel gear (502) is fixed with a second worm (503) by welding, one side of the second worm (503) is engaged with a second worm gear (504), one end of the second worm gear (504) is fixed with a second screw rod (505) by welding, the outer wall of the second screw rod (505) is connected with a cleaning brush (506) by screw threads, one end of the cleaning brush (506) is connected with a fixing block (507) by bolts, the inner wall of the filter pipe (2) is fixed with a second filter plate (508) attached to the bottom end of the cleaning brush (506) by bolts, one end, far away from cleaning brush (506), of the inner wall of filter pipe (2) is connected with a rotating rod (509) through a bearing, and the outer wall of rotating rod (509) is fixedly connected with a second baffle (510).
3. The device for preparing the selenium-rich saccharicterpenin as claimed in claim 2, wherein the second worm (503) and the second screw rod (505) are rotatably connected with the inner wall of the filtering pipe (2) through a bearing, and the second worm wheel (504) is rotatably connected with the inner wall of the filtering pipe (2) through a rotating shaft.
4. The preparation device of selenium-enriched saccharicterpenin according to claim 2, wherein a sliding groove matched with the moving track of the cleaning brush (506) is formed in the inner wall of the filter pipe (2), the fixing block (507) and the second baffle (510) are located at the same horizontal height, a rotating groove matched with the rotating track of the second baffle (510) is arranged in the filter pipe (2), and a sealing element is arranged at the joint of the rotating rod (509) and the filter pipe (2).
5. The apparatus for preparing Se-enriched saccharicterpenins according to claim 1, wherein the number of the first worms (402) is two and symmetrically distributed at two ends of the rotating rod (406), the number of the first filter plates (405) is two, and the first filter plates (405) are located above the second filter plates (508).
6. The device for preparing selenium-rich saccharicterpenin according to claim 1, wherein the connecting column (404) is rotatably connected with the inner wall of the filtering pipe (2) through a bearing with the first screw rod (409), a sealing element is arranged at the joint of the connecting column (404) and the filtering pipe (2), one side of the first worm wheel (403) is connected with a rotating shaft, the rotating shaft is connected with a fixing plate through a bearing, and the fixing plate is fixedly connected with the inner wall of the filtering pipe (2).
7. The device for preparing selenium-rich saccharicterpenin according to claim 1, wherein a sliding groove matched with the connecting rod (410) is arranged inside the filtering pipe (2), a sliding groove matched with the first baffle (411) is arranged inside the filtering pipe (2), and a sealing element is arranged at the joint of the first baffle (411) and the filtering pipe (2).
8. A preparation process of selenium-rich saccharicterpenin, which is characterized by using the preparation device of the selenium-rich saccharicterpenin according to any one of claims 1 to 7, and comprises the following steps:
step 1, crushing raw materials: carrying out ultrafine grinding on the degreased camellia seed meal to 100 meshes;
step 2, adding ethanol, heating and filtering: adding 85% ethanol in volume fraction into defatted camellia seed meal, wherein the ratio of material to liquid is 1: leaching for 2 times at 70 deg.C for 2 hr each time, mixing filtrates, filtering, and concentrating to obtain concentrated solution;
step 3, preparing the total saponins of camellia oleifera: adding 1% chitosan with a volume of 16% of the concentrated solution into the concentrated solution, standing for 4h, removing precipitate, reserving the concentrated solution, and then performing spray drying on the concentrated solution to obtain the camellia oleifera total saponin;
step 4, preparing the oil tea total sugar: adding water in a ratio of 1:10 into the oil tea seed meal filtration residue filtered in the step 2, extracting for 2 times at the temperature of 80 ℃, extracting for 2 hours each time, combining the filtrates, filtering, concentrating to obtain a concentrated solution, adding ethanol with the volume fraction of 3 times being 85%, standing for 24 hours, removing the supernatant, leaving a precipitate, and freeze-drying to obtain oil tea total sugar;
step 5, preparing saccharicterpenin: mixing the obtained total saponins and total sugar of Camellia oleifera Abel at a ratio of 2:1 to obtain saccharicterpenin.
9. The preparation process of the selenium-rich saccharicterpenin according to claim 8, wherein in the step 2, the mixing operation of the camellia seed meal and the ethanol and the filtering operation of the camellia seed meal residue are performed through a collection box (1), a filter pipe (2) and a stirring bin (3).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202210781685.2A CN115104673A (en) | 2022-07-04 | 2022-07-04 | Preparation process and device of selenium-rich saccharicterpenin |
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| Application Number | Priority Date | Filing Date | Title |
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| CN202210781685.2A CN115104673A (en) | 2022-07-04 | 2022-07-04 | Preparation process and device of selenium-rich saccharicterpenin |
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| CN202210781685.2A Withdrawn CN115104673A (en) | 2022-07-04 | 2022-07-04 | Preparation process and device of selenium-rich saccharicterpenin |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115521943A (en) * | 2022-10-10 | 2022-12-27 | 湖南文理学院 | Method for extracting saccharicterpenin from oil tea cake |
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- 2022-07-04 CN CN202210781685.2A patent/CN115104673A/en not_active Withdrawn
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115521943A (en) * | 2022-10-10 | 2022-12-27 | 湖南文理学院 | Method for extracting saccharicterpenin from oil tea cake |
| CN115521943B (en) * | 2022-10-10 | 2024-05-14 | 湖南文理学院 | Method for extracting saccharicterpenin from oil tea cake |
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Application publication date: 20220927 |