CN115074188A - Detergent product composition - Google Patents
Detergent product composition Download PDFInfo
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- CN115074188A CN115074188A CN202210882080.2A CN202210882080A CN115074188A CN 115074188 A CN115074188 A CN 115074188A CN 202210882080 A CN202210882080 A CN 202210882080A CN 115074188 A CN115074188 A CN 115074188A
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- detergent product
- antibacterial peptide
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- VJYFKVYYMZPMAB-UHFFFAOYSA-N ethoprophos Chemical compound CCCSP(=O)(OCC)SCCC VJYFKVYYMZPMAB-UHFFFAOYSA-N 0.000 description 1
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- WIGCFUFOHFEKBI-UHFFFAOYSA-N gamma-tocopherol Natural products CC(C)CCCC(C)CCCC(C)CCCC1CCC2C(C)C(O)C(C)C(C)C2O1 WIGCFUFOHFEKBI-UHFFFAOYSA-N 0.000 description 1
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Images
Classifications
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
- C11D7/22—Organic compounds
- C11D7/40—Products in which the composition is not well defined
- C11D7/44—Vegetable products
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/48—Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
- C11D7/22—Organic compounds
- C11D7/32—Organic compounds containing nitrogen
- C11D7/3263—Amides or imides
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
- C11D7/22—Organic compounds
- C11D7/40—Products in which the composition is not well defined
-
- C11D2111/14—
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
Abstract
The invention provides a detergent product composition, which relates to the technical field of detergents and comprises the following raw materials: shell powder, honeysuckle, wild chrysanthemum, chamomile, loquat leaves, rabdosia lophanthide, gordon malachite and antibacterial peptide. According to the invention, through research, the raw materials in the detergent have good synergistic effect, and a product with excellent efficacy can be obtained through reasonable compounding, wherein the synergistic decontamination and deodorization effects of the rabdosia lophanthide and the malachite flaccida are particularly obvious. In addition, the shell powder, the antibacterial peptide and the plant components are added to effectively replace the addition of chemical components such as hydrocarbons, so that the product is more environment-friendly and safer, meanwhile, the usage amount of the antibacterial peptide is relatively reduced, the cost is further controlled, and the industrial development of the product is facilitated. The finally obtained detergent product composition is safe, has good antibacterial and bactericidal effects, has multifunctional effects, and can be used for cleaning fruits and vegetables, fresh fruits and feeding bottles.
Description
Technical Field
The invention relates to the technical field of detergents, in particular to a detergent product composition.
Background
The detergent is a product prepared for cleaning purposes, and the main components of the detergent are mostly surfactants and other additives, and the detergent is used for cleaning dirt of utensils such as bowls and chopsticks. In addition to bowls and chopsticks, the demand of special detergents for foods such as fruits and vegetables, fresh products, feeding bottles and the like and daily necessities is gradually increased, but the fruits and the vegetables have a large amount of pesticide residues, the fresh products have fishy and mutton smells, blood stains, grease floating foam, various bacteria and the like, and the feeding bottles have milk stains which are easy to breed the bacteria after being used and are often difficult to clean.
However, many detergents contain various chemical components, such as fluorescent agents with carcinogenic factors, which are easily accumulated in the liver or other organs, acidic and alkaline substances which are easily damaged by the skin, and hydrocarbon substances which are easily caused to be sterile, so that secondary residues of related substances are likely to be left when fruits and vegetables, fresh food or milk bottles are cleaned, and health and safety are affected. In order to reduce the use of various chemical components, part of researchers use shell powder or antibacterial peptide in detergents instead of adding part of chemical components to maintain or promote the efficacy of sterilization, bacteriostasis and the like of products.
For example, patent CN112940877A discloses a cleaning agent for shell fruits and vegetables, a preparation method and application thereof, the raw materials include: 40-80 parts of calcined shell powder, 5-10 parts of sodium percarbonate, 5-10 parts of chitosan, 3-10 parts of water-soluble starch, 0.1-3 parts of surfactant, 0.1-5 parts of traditional Chinese medicine extract and 0.1-5 parts of additive. The cleaning agent can achieve the effects of removing residues and sterilizing by matching calcined shell powder with sodium percarbonate, chitosan and water-soluble starch. However, the cleaning agent contains sodium percarbonate which is not stored or transported, and meanwhile, the product is mainly used for cleaning pesticide residues such as propoxur, cypermethrin and the like on fruits and vegetables, and has a single function. The patent CN109456860A discloses a shell powder fruit and vegetable cleaning agent and a preparation method thereof, the cleaning agent comprises 30-70 parts of shell powder, 30-50 parts of tea seed cake powder, 0.15-3 parts of common cnidium fruit and 0.1 part of lightyellow sophora root powder, and finally the obtained product can clean oily pesticide residues on fruits and vegetables, and can inhibit bacteria and resist bacteria for a long time after cleaning. However, the invention also mainly carries out researches on related pesticide residues such as dichlorvos, ethoprophos, monocrotophos and the like, and other effects of the product are unknown.
For another example, patent CN110283669A discloses a green antibacterial detergent containing NP10 antibacterial peptide, its preparation method and application, the detergent comprises the following components by mass percent: 14 to 20 percent of anionic surfactant, 4 to 12 percent of nonionic surfactant, 0.10 to 0.15 percent of NP10 antibacterial peptide, 0.08 to 0.12 percent of sodium citrate, 1 to 3 percent of urea, 0.08 to 0.12 percent of EDTA disodium, 0.1 to 0.3 percent of sorbitol, 0.1 to 0.3 percent of vitamin E and the balance of water. The NP10 antibacterial peptide is cooperated with sodium citrate, so that the antibacterial activity is enhanced. The detergent has good decontamination capability, and the antibacterial effect of the antibacterial peptide is less than that of a chemical bacteriostatic agent and is healthier. However, the application of the antibacterial peptide in the market is limited due to high cost of the antibacterial peptide, so that the addition amount of the antibacterial peptide is still at a high level for the product in the invention, the development of the market is limited as a whole, and in addition, the product in the invention still has the use of a large amount of components such as surfactants and the like.
Aiming at the problems of difficult storage of raw materials, single product function, high price and the like in the detergent in the prior art, the multifunctional detergent which has good effect and low cost and can be used for cleaning fruits and vegetables, fresh fruits and milk bottles is very necessary to be found.
Disclosure of Invention
The invention provides a detergent product composition aiming at the problems in the prior art, the detergent product composition has excellent effect and multifunctional function, and can be used for cleaning fruits and vegetables, fresh fruits and feeding bottles.
In order to achieve the purpose, the technical scheme adopted by the invention is as follows:
the invention provides a detergent product composition, which comprises the following raw materials: shell powder, honeysuckle, wild chrysanthemum, chamomile, loquat leaves, rabdosia lophanthide, gordon malachite and antibacterial peptide.
Further, the detergent product composition comprises the following raw materials in parts by weight: 50-70 parts of shell powder, 10-12 parts of honeysuckle, 5-10 parts of wild chrysanthemum flower, 5-8 parts of chamomile, 3-5 parts of loquat leaf, 1-2 parts of linea rabdosia, 0.3-1.2 parts of sparrow's broom, and 0.01-0.03 part of antibacterial peptide.
In some embodiments, the detergent product composition comprises, in parts by weight: 60 parts of shell powder, 10 parts of honeysuckle, 6 parts of wild chrysanthemum flower, 6 parts of chamomile, 4 parts of loquat leaf, 1 part of linea rabdosia, 0.8 part of sparrow's broom, and 0.02 part of antibacterial peptide.
In other specific embodiments, the detergent product composition comprises, in parts by weight: 65 parts of shell powder, 11 parts of honeysuckle, 8 parts of wild chrysanthemum flower, 7 parts of chamomile, 3 parts of loquat leaf, 1.5 parts of linea rabdosia, 1 part of sparrow's broom and 0.02 part of antibacterial peptide.
Further, the detergent product composition comprises the following raw materials: perilla leaf, lophatherum gracile, momordica grosvenori and radish seed.
Preferably, the detergent product composition further comprises the following raw materials in parts by weight: 5-8 parts of perilla leaf, 5-8 parts of lophatherum gracile, 4-10 parts of momordica grosvenori and 7-10 parts of radish seed.
Further preferably, the detergent product composition comprises the following raw materials in parts by weight: 7 parts of perilla leaf, 7 parts of lophatherum gracile, 7 parts of momordica grosvenori and 9 parts of radish seed.
Further, the detergent product composition comprises the following raw materials: mint and reed rhizome.
Preferably, the detergent product composition further comprises the following raw materials in parts by weight: 10-12 parts of mint and 10-15 parts of reed rhizome.
Further preferably, the detergent product composition further comprises the following raw materials in parts by weight: 11 parts of mint and 12 parts of reed rhizome.
Further, the detergent product composition comprises the following raw materials: mulberry leaf, purslane and seville orange flower.
Preferably, the detergent product composition further comprises the following raw materials in parts by weight: 5-12 parts of mulberry leaves, 4-8 parts of purslane and 4-6 parts of seville orange flowers.
Further preferably, the detergent product composition further comprises the following raw materials in parts by weight: 10 parts of mulberry leaf, 5 parts of purslane and 5 parts of seville orange flower.
Furthermore, the weight ratio of the shell powder to the honeysuckle to the loquat leaves to the linearstripe rabdosia herb is 50-70:10-12:3-5: 1-2. Preferably 60:10:4:1 or 65:11:3: 1.5.
Further, the weight ratio of the loquat leaves, the broom cypress leaves and the antibacterial peptide is as follows: 3-5:0.3-1.2:0.01-0.03. Preferably 4:0.8:0.02 or 3:1: 0.02.
Further, the present invention also provides a process for the preparation of the above detergent product composition comprising the steps of:
(1) pulverizing flos Lonicerae, flos Chrysanthemi Indici, flos Matricariae Chamomillae, folium Eriobotryae, herba Rabdosiae Lophanthoidis and flos Caraganae Sinicae, soaking in water, decocting with slow fire for the first time, filtering to obtain first filtrate and residue, adding water to the residue again, decocting with slow fire, filtering to obtain second filtrate, mixing the filtrates, and diluting to obtain diluent;
(2) and (2) adding the shell powder and the antibacterial peptide into the diluent obtained in the step (1) to obtain the antibacterial peptide.
Further, the method for preparing the shell powder used in the present invention comprises the steps of:
s1, cleaning the shell, soaking the shell with hydrochloric acid, soaking the shell with sodium hydroxide, and drying the shell for later use;
s2, crushing the dried shell to obtain coarse shell micro powder;
s3, calcining and puffing the shell coarse micro powder obtained in the step S2, and naturally cooling;
and S4, nano-crushing the shell coarse micro powder cooled in the step S3 to obtain nano shell powder.
Further, the hydrochloric acid dipping time and the sodium hydroxide dipping time are both 30-60 minutes;
further, the specific calcining process comprises the following steps: calcining at 400 ℃ for 30-60 minutes, heating to 800 ℃ for 30-60 minutes, and heating to 1200 ℃ for 30-60 minutes.
Further, the shell is derived from one or more of mussel shell, scallop shell, oyster shell, flower shell and corbicula fluminea shell.
The antibacterial peptide originally refers to a kind of basic polypeptide substance with antibacterial activity produced by insect in vivo induction, the molecular weight is about 2000-7000, and the basic polypeptide substance is composed of 20-60 amino acid residues. It has broad-spectrum antibacterial activity, has strong killing effect on bacteria, can be used as a substitute for health products and antibacterial substances, and has related applications in medicine, agriculture and industry.
The technical effects obtained by the invention are as follows:
1. the detergent disclosed by the invention is prepared by compounding the shell powder with various components including honeysuckle, wild chrysanthemum, chamomile, loquat leaves, rabdosia lophanthide, gorgon euryale and antibacterial peptide, is safe, has good antibacterial and bactericidal effects, and can be used for cleaning pesticide residues, stains, milk stains and the like. In addition, the composition disclosed by the invention is mixed with perilla leaf, lophatherum gracile, momordica grosvenori and radish seed, and if the radish seed contains rich fat-soluble components, pesticide residues can be effectively removed, and the effect of cleaning fruits and vegetables is further improved; the composition is further compounded with the mint and the reed rhizome, and partial components in related extracts can participate in the dispersion of oil stains and milk stains, so that the extract is easier to separate from the wall of a container, and the effect of cleaning the milk bottle is further improved; the composition is further compounded with mulberry leaves, purslane and seville orange flowers, wherein the volatile oil component has a certain fishy smell removing effect, and part of flavonoids also has the effect of removing substances such as methyl mercaptan and the like, so that the cleaning and fresh effect of the composition is further improved; in addition, the raw materials are rich in antioxidant components or components with sterilization and bacteriostasis effects, such as peppermint oil, anthraquinone and the like, and can realize good sterilization and bacteriostasis effects when being mutually compounded with other components.
2. The invention mainly utilizes natural raw material components and combines the friction performance between shell powder or plant fibers, thereby realizing the improvement of the decontamination effect. Meanwhile, researches show that the synergistic interaction effect among the components can be realized by adding specific contents of shell powder, honeysuckle, loquat leaves and linearstripe rabdosia herb or adjusting the proportioning conditions of loquat leaves, gorgon euryale leaves and antibacterial peptide, so that the antibacterial and bactericidal performance of the product or the decontamination and stain removal capability of the product on the surfaces of fruits and vegetables, milk bottles and fresh fruits and vegetables can be effectively improved. The invention can fully exert the anti-pollution function of diterpenoid substances in the rabdosia lophanthide, realize combined synergism with the decontamination and deodorization function of flavonoid substances in the gorse lineolate, and further realize combined compounding with other components in the detergent, thereby improving the removal rate of the detergent on stains and acetaldehyde to a certain extent.
3. According to the invention, the shell powder, the antibacterial peptide and the plant components are used to replace the addition of chemical components, so that the prepared detergent is more environment-friendly and safer, the use of the antibacterial peptide is reduced while the detergent has a better washing effect, and the cost of the detergent is reduced, which has very important significance in industrial application.
Drawings
FIG. 1 is an electron microscope image of shell powder in the raw material of the present invention;
FIG. 2 is an infrared test result of shell powder in the feedstock of the present invention;
fig. 3 shows the bacteriostatic effect of shell powder in the raw material of the present invention, wherein (a) shows the bacteriostatic effect on escherichia coli, and (b) shows the bacteriostatic effect on staphylococcus aureus.
Detailed Description
The embodiments of the present invention are described below with reference to specific embodiments, and other advantages and effects of the present invention will be easily understood by those skilled in the art from the disclosure of the present specification. The invention is capable of other and different embodiments and of being practiced or of being carried out in various ways, and its several details are capable of modification in various respects, all without departing from the spirit and scope of the present invention.
Before the present embodiments are further described, it is to be understood that the scope of the invention is not limited to the particular embodiments described below; it is also to be understood that the terminology used in the examples is for the purpose of describing particular embodiments only, and is not intended to limit the scope of the present invention.
When numerical ranges are given in the examples, it is understood that both endpoints of each of the numerical ranges and any value therebetween can be selected unless the invention otherwise indicated. Unless defined otherwise, all technical and scientific terms used herein have the same meaning as commonly understood by one of ordinary skill in the art to which this invention belongs.
It is worth to be noted that the antibacterial peptide used in the invention is purchased from Shenzhen Dadi kang En Biotech Limited (the content is more than 95%, the antibacterial peptide can be applied to food, daily chemical products and maternal and infant products), and the other raw materials are all common commercial products, so the source of the antibacterial peptide is not particularly limited, and the preparation of the shell powder is described in detail in the following description.
TABLE 1
| Formulation of | Example 1 | Example 2 | Example 3 | Example 4 | Example 5 | Example 6 | Example 7 |
| Shell powder | 50 | 70 | 60 | 65 | 60 | 60 | 60 |
| Honeysuckle | 10 | 12 | 10 | 11 | 10 | 10 | 10 |
| Wild chrysanthemum flower | 5 | 10 | 6 | 8 | 6 | 6 | 6 |
| Chamomile | 5 | 8 | 6 | 7 | 6 | 6 | 6 |
| Folium Eriobotryae | 3 | 5 | 4 | 3 | 4 | 4 | 4 |
| Rabdosia lophanthide (Hemsl.) |
1 | 2 | 1 | 1.5 | 1 | 1 | 1 |
| All-grass of Largeleaf Caragana | 0.3 | 1.2 | 0.8 | 1 | 0.8 | 0.8 | 0.8 |
| Antibacterial peptide | 0.01 | 0.03 | 0.02 | 0.02 | 0.02 | 0.02 | 0.02 |
| Folium Perillae | - | - | - | - | 7 | - | - |
| Lophatherum gracile (Lophatherum gracile) Var) | - | - | - | - | 7 | - | - |
| Momordica grosvenori | - | - | - | - | 7 | - | - |
| Radish seed | - | - | - | - | 9 | - | - |
| Mint | - | - | - | - | - | 11 | - |
| Rhizoma Phragmitis | - | - | - | - | - | 12 | - |
| Mulberry Leaves | - | - | - | - | - | - | 10 |
| Herba Portulacae | - | - | - | - | - | - | 5 |
| Substitute flower | - | - | - | - | - | - | 5 |
Comparative example 1
The difference from the embodiment 1 is mainly that honeysuckle, wild chrysanthemum and linearstripe rabdosia herb are respectively replaced by the same amount of orange peels, honey locust and chitosan. That is, the raw materials of the detergent product composition comprise, by weight: 50 parts of shell powder, 10 parts of orange peel, 5 parts of gleditsia sinensis lam, 5 parts of chamomile, 3 parts of loquat leaf, 1 part of chitosan, 0.3 part of gorse lineariifolia and 0.01 part of antibacterial peptide.
Comparative example 2
The difference from the example 1 is mainly that the weight ratio of the shell powder, the honeysuckle, the loquat leaves and the rabdosia lophanthide is 40:15:2:7 (the total weight is not changed), namely, the raw materials of the detergent product composition comprise the following components in parts by weight: 40 parts of shell powder, 15 parts of honeysuckle, 5 parts of wild chrysanthemum flower, 5 parts of chamomile, 2 parts of loquat leaf, 7 parts of linea rabdosia, 0.3 part of sparrow's broom, and 0.01 part of antibacterial peptide.
Comparative example 3
The difference from example 2 is mainly that the brook herb in the raw material is replaced by the same amount of gorse canary. That is, the raw materials of the detergent product composition comprise, by weight: 70 parts of shell powder, 12 parts of honeysuckle, 10 parts of wild chrysanthemum flower, 8 parts of chamomile, 5 parts of loquat leaf, 3.2 parts of gordon malachite and 0.03 part of antibacterial peptide.
Comparative example 4
The difference from example 2 is mainly that the raw material of the sparrow's broom was replaced by an equal amount of isovalerian. That is, the raw materials of the detergent product composition comprise, by weight: 70 parts of shell powder, 12 parts of honeysuckle, 10 parts of wild chrysanthemum flower, 8 parts of chamomile, 5 parts of loquat leaf, 3.2 parts of rabdosia lophanthide and 0.03 part of antibacterial peptide.
In the above examples and comparative examples, the preparation method of the detergent comprises the steps of:
(1) pulverizing flos Lonicerae, flos Chrysanthemi Indici, flos Matricariae Chamomillae, folium Eriobotryae, herba Rabdosiae Lophanthoidis and flos Caraganae Sinicae, soaking in water, decocting with slow fire for the first time, filtering to obtain first filtrate and residue, adding water to the residue again, decocting with slow fire, filtering to obtain second filtrate, mixing the filtrates, and diluting to obtain diluent;
(2) adding the shell powder and the antibacterial peptide into the diluent obtained in the step (1) to obtain the antibacterial peptide.
The preparation methods of the products in comparative example 1 and comparative examples 3 to 4 mainly replace the related raw materials, and the feeding sequence of the preparation methods is not changed.
The preparation method of the shell powder comprises the following steps:
s1, cleaning mussel shell, soaking in hydrochloric acid for 50 minutes, soaking in sodium hydroxide for 50 minutes, and drying for later use;
s2, crushing the dried shell to obtain coarse shell micro powder;
s3, calcining and puffing the shell coarse micro powder obtained in the step S2, wherein the specific calcining process comprises the following steps: calcining at 400 ℃ for 40 minutes, heating to 800 ℃ for 40 minutes, heating to 1200 ℃ for 40 minutes, and naturally cooling;
and S4, carrying out nano grinding on the shell coarse micro powder cooled in the step S3 to obtain nano shell powder. The detail of the electron microscope image of the finally obtained shell powder is shown in figure 1, the detail of the infrared test result is shown in figure 2, the detail of the bacteriostasis effect of the shell powder is shown in figure 3, and the calcined shell powder is shown to have uneven surface structure and a porous state, is attached with various groups and has excellent bacteriostasis effect.
Firstly, the cleaning effect of the product of the invention
The test method comprises the following steps:
test 1: the test is carried out by referring to a verification method of GB/T24691-. Wherein the vegetable sample is sweet kidney beans.
Test 2: the stain is derived from edible butter, and the weight is m 0 Coating edible cream on the enamel sheet and drying, and recording the weight of the enamel sheet as m 1 The enamel piece coated with the cream was immersed in a 1% aqueous solution of the sample of each example for 1 minute, shaken in a shaker for 7 minutes, and then dried, and the mass of the enamel piece was recorded as m 2 The removal rate [ (m) is calculated 2 -m 1 )/(m 1 -m 0 )]×100％。
Test 3: the main component of the fishy smell of the seawater is trimethylamine, the main components of the fresh water and the fishy smell are mainly combined with acetaldehyde on the surface of a fish body by hexahydropyridine compounds generated by actinomycetes in soil, a gas chromatography combination instrument is used for detecting the removing capability of the product in each embodiment, and the results are counted in a table 2.
TABLE 2
As can be seen from table 2, the detergent of the present invention is remarkably effective in removing cypermethrin, propoxur, stains, and acetaldehyde. In particular, when the detergent composition is compounded with perilla leaf, lophatherum gracile, momordica grosvenori and radish seed, the removal effect of cypermethrin and propoxur can be improved, when the detergent composition is used with mint and reed rhizome, the removal effect of stains can be improved, and when the detergent composition is used with mulberry leaf, purslane and seville orange flower, acetaldehyde can be effectively removed. In contrast, when the raw materials in the composition were replaced with orange peels, honey locust and chitosan, which had similar effects, the final removal effect was somewhat reduced. In the compound test of shell powder, honeysuckle, loquat leaves and linearstripe rabdosia herb and the test between the gorse senna and the linearstripe rabdosia herb, the compound between the gorse senna and the linearstripe rabdosia herb can be seen to have obvious synergistic effect on removing stains and acetaldehyde when the detergent is applied. Similarly, the proportion of the shell powder, the honeysuckle, the loquat leaves and the linearstripe rabdosia herb also has a critical influence on the efficacy of the detergent.
Secondly, the sterilization and bacteriostasis performance of the product of the invention
The test refers to GB4789.2-2016 food safety national standard food microbiology test colony total number determination and European Union standard BP2002 XVICIFFICAIYOFANTICROBIALPHRESERVATION, and the results show that the product of the invention has good bacteriostatic effect on staphylococcus aureus, escherichia coli, bacillus subtilis, salmonella and the like, the bacteriostatic rate reaches over 99.99 percent, and the bacteriostatic effective time can reach over 24 hours.
In addition, the product of the invention also has good bactericidal performance, the test is carried out according to 2.1.1.7.4 of the quantitative bactericidal test of the disinfection technical code of the Ministry of public health of the people's republic of China, and the bactericidal rate of pseudomonas aeruginosa ATCC 15442 (test time 10 minutes), escherichia coli 8099 (test time 10 minutes), klebsiella pneumoniae ATCC 4352 (test time 10 minutes) or staphylococcus aureus ATCC6538 (test time 30 minutes) can reach more than 99.99 percent. In contrast, the bacteriostatic and bactericidal effects of the other comparative examples are slightly weaker than those of the examples.
Finally, it should be noted that the above-mentioned contents are only used for illustrating the technical solutions of the present invention, and not for limiting the protection scope of the present invention, and that the simple modifications or equivalent substitutions of the technical solutions of the present invention by those of ordinary skill in the art can be made without departing from the spirit and scope of the technical solutions of the present invention.
Claims (10)
1. A detergent product composition characterized by: the raw materials comprise: shell powder, honeysuckle, wild chrysanthemum, chamomile, loquat leaves, rabdosia lophanthide, gordon malachite and antibacterial peptide.
2. A detergent product composition according to claim 1, characterized in that: the raw materials comprise the following components in parts by weight: 50-70 parts of shell powder, 10-12 parts of honeysuckle, 5-10 parts of wild chrysanthemum flower, 5-8 parts of chamomile, 3-5 parts of loquat leaf, 1-2 parts of linea rabdosia, 0.3-1.2 parts of sparrow's broom, and 0.01-0.03 part of antibacterial peptide.
3. A detergent product composition according to claim 1, characterized in that: the raw materials also comprise: perilla leaf, lophatherum gracile, momordica grosvenori and radish seed.
4. A detergent product composition according to claim 3, characterized in that: the raw materials also comprise, by weight: 5-8 parts of perilla leaf, 5-8 parts of lophatherum gracile, 4-10 parts of momordica grosvenori and 7-10 parts of radish seed.
5. A detergent product composition according to claim 1, characterized in that: the raw materials also comprise: mint and reed rhizome.
6. A detergent product composition according to claim 5, characterized in that: the raw materials also comprise the following components in parts by weight: 10-12 parts of mint and 10-15 parts of reed rhizome.
7. A detergent product composition according to claim 1, characterized in that: the raw materials also comprise: mulberry leaf, purslane and seville orange flower.
8. A detergent product composition according to claim 7 wherein: the raw materials also comprise, by weight: 5-12 parts of mulberry leaves, 4-8 parts of purslane and 4-6 parts of seville orange flowers.
9. A detergent product composition according to claim 1, characterized in that: the weight ratio of the shell powder to the honeysuckle to the loquat leaves to the linearstripe rabdosia herb is 50-70:10-12:3-5: 1-2.
10. A process for the preparation of a detergent product composition as claimed in claim 1 or claim 2, wherein: the method comprises the following steps:
(1) pulverizing flos Lonicerae, flos Chrysanthemi Indici, flos Matricariae Chamomillae, folium Eriobotryae, herba Rabdosiae Lophanthoidis and flos Caraganae Sinicae, soaking in water, decocting with slow fire for the first time, filtering to obtain first filtrate and residue, adding water to the residue again, decocting with slow fire, filtering to obtain second filtrate, mixing the filtrates, and diluting to obtain diluent;
(2) adding the shell powder and the antibacterial peptide into the diluent obtained in the step (1) to obtain the antibacterial peptide.
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