CN115068378A - 一种真空装置提取的植物提取物及应用 - Google Patents

一种真空装置提取的植物提取物及应用 Download PDF

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CN115068378A
CN115068378A CN202110953725.2A CN202110953725A CN115068378A CN 115068378 A CN115068378 A CN 115068378A CN 202110953725 A CN202110953725 A CN 202110953725A CN 115068378 A CN115068378 A CN 115068378A
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extract
vacuum device
plant extract
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孙宗军
刘晓彬
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Qingdao Ruihan Tiancheng Biotechnology Co ltd
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Abstract

本发明公开了一种真空装置提取的植物提取物及其应用。本申请中植物提取物的提取步骤为:1)、将新鲜的樱花花清洗、沥干,投放到真空装置的物料仓内,关闭仓门;2)、开启电蒸汽发生器、制冷机组、水处理设备,启动真空装置,设置运行时间;3)、控制整个樱花花原液提取过程中的温度、真空度,收集冷凝提取液于收液罐中;4)、待无提取液滴出,停止提取操作,进行排气驱动,确定干燥物状态,排出干燥物,收集浸出液。通过该装置实现非溶剂常温负压樱花花提取,避免了热分解对热敏活性物质的影响,保证了樱花花提取物的100%活性应用。将樱花提取物用于面霜,协同其他组分可以使面霜具有良好的美白抗氧化效果。

Description

一种真空装置提取的植物提取物及应用
技术领域
本发明涉及的是植物提取物设备技术领域,B01D11/02,尤其涉及一种真空装置提取的植物提取物及应用。
背景技术
植物提取物常用的提取方法有溶剂提取法、超声波提取法、微波辅助提取法和酶提取法。溶剂提取法:是一种根据原料中各种化学成分在溶剂中溶解能力,选择合适的溶剂将成分从原料中溶解提出的方法,常用的有冷提法、渗漉法、煎煮法、回流提取法、连续回流提取法;超声波提取法:是一种利用超声波振动使溶剂快速进入固体原料中,使多种成分尽可能溶于溶剂中被提取出的一种方法;微波辅助提取法:是一种在特定微波反应器中,添加适合的溶剂从原料中提取各种化学成分的方法;酶提取法:是一种通过添加特定酶法作用于目标产物,改善其理化性质,进而提高其在溶剂中的溶解度,实现目标产物提取的方法。
超临界流体萃取法、半仿生、动态逆流则作为新的提取技术被广泛使用。超临界流体萃取法:是以超临界流体为溶剂,从固体或液体原料中萃取并分离特定有效组分的方法;半仿生提取:是经消化道口服给药的制剂设计的一种新的提取工艺,是将整体药物研究方法与分子药物研究法相结合,模拟口服药物经胃肠道转运吸收的环境,采用活性指导下的导向分离方法;动态逆流提取:在增加药材比表面积的情况下,利用机械手段,采用强制循环方式,以增加固液相接触,从而提取出药物中有效成分的一种提取方法。这些新技术虽然提取周期短、提取率高、有效成分损失少,但不同程度上需要有机溶剂溶解,提取物中真正做到无残留仍在改进。除超临界萃取法采用接近室温(35~40℃)及CO2气体笼罩下进行提取外,其他方法提取过程温度一般在60℃左右,并不能完全防止一些热敏性物质的氧化和逸散,而超临界萃取法设备和所需车间的投资比较昂贵,不适合中小型提取生产企业使用。
新鲜樱花花体内富含以小分子水为主的多种活性成分,在美容护肤领域具有广泛的应用前景。目前,樱花提取物主要的提取方式为溶剂提取法。专利CN201610887110.3提供了一种富含天然樱花花瓣及其纯露,利用乙醇作为溶剂,将樱花花瓣和乙醇的混合液加热回流收集滤液,然后减压浓缩至无醇味后用大孔树脂吸附洗脱,最后减压浓缩得到樱花花提取物。专利CN202011194127.3公开了一种樱花花提取物及其提取方法和应用,采用提取剂(C3~C6小分子多元醇、乙醇和水的组合物)浸提樱花花瓣。提取剂组分的筛选和优化,有利于樱花花瓣中不同极性和溶解性的组分的浸出,且所述樱花花提取物能够适用于水剂或乳化剂等多种剂型,应用性能好。然而,溶剂提取法需要大量溶剂,损失率大,提取所需时间长,收液率低,纯度差;而且植物所含有的热敏性物质在提取过程中容易被氧化分解,造成活性成分应用效果降低。此外,提取物中的农药、化肥和重金属残留容易超标,使植物提取物使用过程中具有安全隐患。
发明内容
为了解决上述问题,本发明第一方面提供一种真空装置提取的植物提取物:
利用一种用于新鲜植物组织提取设备来得到樱花花提取物,设备参考专利号:CN202010510600.8。
提取步骤:
1)、将新鲜的樱花花清洗、沥干,投放到真空装置的物料仓内,关闭仓门;
2)、开启电蒸汽发生器、制冷机组、水处理设备,启动真空装置,设置运行时间;
3)、控制整个樱花花原液提取过程中的温度、真空度,收集冷凝提取液于收液罐中;
4)、待无提取液滴出,停止提取操作,进行排气驱动,确定干燥物状态,排出干燥物,收集浸出液即植物提取物;
所述植物提取物为樱花花提取物;
所述的樱花花为新鲜的樱花(PrunusSpeciosa)花,即采摘到使用的时间最多为半天或当即冷冻保存的;
所述运行时间为1~3h;
所述樱花花原液提取过程中温度为35℃~40℃;
所述樱花花原液提取过程中真空度为-90kPa~95kPa;
本发明第二方面提供一种真空装置提取的植物提取物的应用:
由上述方法提取所得的植物提取物用于美白面霜,按重量计,其原料的组成及含量如下:
溶剂:60-70份;螯合剂:0.1-0.2份;保湿剂:8-13份;皮肤调理剂:6-17份;增稠剂:0.3-0.7份;乳化剂:2-6份;润肤剂:13-18份;抗氧化剂:0.5-1份;防腐剂:0.3-1.0份。
溶剂:选自去离子水和PEG-40氢化蓖麻油,水:61-70份,PEG-40氢化蓖麻油0.4-1份;
螯合剂:选自EDTA-2Na;
保湿剂:选自甘油、甘油聚醚-26、丙二醇、山梨醇、银耳多糖、海藻糖、二甲基甲硅烷醇透明质酸酯、透明质酸钠中的一种或多种;优选为甘油、甘油聚醚-26、银耳多糖、海藻糖、透明质酸钠、乙酰壳糖胺中的一种或多种;
皮肤调理剂:选自植物甾醇油酸酯、泛醇、氢化卵磷脂、甘油硬脂酸酯、双丙甘醇、神经酰胺、红没药醇、尿囊素、角鲨烷、咖啡黄葵(AbelmoschusEsclentus)果提取物、柠檬酸、乳酸杆菌发酵产物、姜黄根提取物(Cercuma Longa)、二裂酵母发酵产物溶胞物、乙酸、乳酸、视黄醇棕榈酸酯、烟酰胺、四氢甲基嘧啶羧酸、精氨酸、蜂蜜(Mel)提取物的一种或几种;
增稠剂:选自黄原胶、羟乙基丙烯酸盐、丙烯酰二甲基牛磺酸钠共聚物、卡波姆941中的一种或几种;优选为黄原胶和卡波姆941;
所述黄原胶和卡波姆941的重量份比为1~2;1~3;
乳化剂:选自聚硬脂酰谷氨酸钠、鲸蜡醇、甘油-3甲基葡糖二硬脂酸酯、双-PEG/PPG-20/5PEG/PPG-20/5聚二甲基硅氧烷、甲氧基PEG/PPG-25/4聚二甲基硅氧烷、鲸蜡硬脂醇、PEG-100硬脂酸酯、PEG-60硬脂酸酯中的一种或几种;优选为硬脂酰谷氨酸钠、鲸蜡醇、鲸蜡硬脂醇、PEG-100硬脂酸酯甲氧基PEG/PPG-25/4聚二甲基硅氧烷中的一种或几种;
润肤剂:选自辛酸/癸酸甘油三酯、霍霍巴(SimmondsiaChinensis)籽油、肉豆蔻醇肉豆蔻酸酯、聚二甲基硅氧烷、牛油果树(Butyrosp-ErumumParkii)果脂、新戊二醇二庚酸酯、甘油三(乙基己酸)酯、辛基聚甲基硅氧烷中的一种或多种;优选为霍霍巴籽油、肉豆蔻醇肉豆蔻酸酯、牛油果树果脂、生育酚乙酸酯、甘油三(乙基己酸)酯中的一种或多种;
抗氧化剂:选自樱花花提取物、超氧化物歧化酶(SOD)、季戊四醇四(双-叔丁基羟基氢化肉桂酸)酯、半胱氨酸、抗坏血酸、维生素C、维生素E中的一种或多种;
防腐剂:选自1,2己二醇,对羟基苯乙酮、甲基异噻唑啉酮、苯甲酸钠中的一种或多种;
与现有技术相比,本发明具有以下有益效果:
(1)本申请通过真空装置实现常温负压条件下就能促使樱花花水分蒸发进行樱花花的提取。通过常温提取,可有效防止热分解和氧化,保证樱花花内含的热敏性活性成分不变质,使得到的提取液、干燥粉、水溶性精油等100%活性应用。
(2)本申请能够在物料仓内不加任何溶剂的情况下得到新鲜樱花花的提取物,避免了有机溶剂的使用,整个过程简单、环保,而且产率高,可以一定程度避免樱花花提取物被污染,使得到的樱花花提取物具有使用安全性。
(3)本发明中含有牛油果树果脂成分,但是其所含脂肪酸会对樱花提取物以及咖啡黄葵果提取物的有效成分造成一定影响。本发明人意外发现,使用一定比例的黄原胶和卡波姆941增稠剂组成的增稠剂,配合特定组成的保湿剂和乳化剂,可以有效改善其负面影响,减少美白面霜中沉淀的产生,提升美白面霜的储存稳定性。可能原因是卡波姆941增稠剂可以协同特定组成的保湿剂和乳化剂,促进体系内有序相的形成,提升产品稳定性。并且实验过程中发现黄原胶卡和波姆941重量份比为2:3时,制得的美白面霜的稳定性最佳。
(4)美白面霜中包含樱花花提取物、咖啡黄葵果提取物等天然提取物,组分含量较为复杂,其所制备得到的面霜有效成分溶解性变差,会出现分层或絮凝等现象。但本申请人发现保湿剂中含有的海藻糖可以与皮肤调理剂协同作用,有效改善产品低温和高温条件下分层或絮凝等现象。这是由于一定比例海藻糖与乙酰壳糖胺所形成的特有结构,使其与其他成分上的有效基团一起将美白保湿组合物包覆其中,不仅有利于皮肤对有效成分的吸收,同时有利于体系各组分均匀分布于爽肤水产品中,显著降低温度对于稳定性的影响。
(5)本发明通过使用新鲜植物组织提取设备来获得樱花花提取物,设备设置巧妙,安装和操作简便。而且真空提取装置可维持常温下真空度要求,无臭气,经济环保。
具体实施方式:
实施例1:一种真空装置提取的植物提取物:
利用一种用于新鲜植物组织提取设备来得到樱花花提取物,设备参考专利号:CN202010510600.8。
提取步骤:
1)、将新鲜的樱花花清洗、沥干,投放到真空装置的物料仓内,关闭仓门;
2)、开启电蒸汽发生器、制冷机组、水处理设备,启动真空装置,设置运行时间;
3)、控制整个樱花花原液提取过程中的温度、真空度,收集冷凝提取液于收液罐中;
4)、待无提取液滴出,停止提取操作,进行排气驱动,确定干燥物状态,排出干燥物,收集浸出液即樱花花提取物。
所述的樱花花为新鲜的樱花花,即采摘到使用的时间最多为半天或当即冷冻保存的;
所述运行时间为2h;
所述樱花花原液提取过程中温度为35℃;
所述樱花花原液提取过程中真空度为-50kPa;
一种真空装置提取的植物提取物的应用:美白面霜
由上述方法提取所得的植物提取物用于美白面霜,按重量计,其原料的组成及含量如下:
溶剂:64.5份;螯合剂:0.1份;保湿剂:10份;皮肤调理剂:8份;增稠剂:0.5份;乳化剂:3份;润肤剂:13份;抗氧化剂:0.6份;防腐剂:0.3份。
溶剂:去离子水(64份)、PEG-40氢化蓖麻油(0.5份);
螯合剂:EDTA-2Na(0.1份);
保湿剂:甘油(4份)、甘油聚醚-26(3份)、银耳多糖(1.8份)、海藻糖(1.0份)、透明质酸钠(0.2份);
皮肤调理剂:植物甾醇油酸酯(1份)、泛醇(0.3份)、氢化卵磷脂(0.05份)、双丙甘醇(0.07份)、神经酰胺(0.05份)、红没药醇(0.5份)、尿囊素(0.5份)、角鲨烷(2份)、乳酸杆菌发酵产物(0.5份)、姜黄根提取物(0.01份)(购自斯百全化学(上海)有限公司)、二裂酵母发酵产物溶胞物(0.01)、视黄醇棕榈酸酯(0.1份)、烟酰胺(2份)、四氢甲基嘧啶羧酸(0.01份)、精氨酸(0.25份)、柠檬酸(0.25)、乙酰壳糖胺(0.2份)、蜂蜜提取物(0.2份)(购自扶风斯诺特生物科技有限公司);
增稠剂:卡波姆941(0.3份)、黄原胶(0.2份);
乳化剂:硬脂酰谷氨酸钠(0.3份)、鲸蜡硬脂醇(2份)、PEG-100硬脂酸酯(0.4份)、甲氧基PEG/PPG-25/4聚二甲基硅氧烷(0.3份);
润肤剂:霍霍巴籽油(5份)、肉豆蔻醇肉豆蔻酸酯(3份)、牛油果树果脂(2份)(购买自上海协瑞化工,型号为SHEA BUTTER产品)、生育酚乙酸酯(2份)、甘油三(乙基己酸)酯(1份);
抗氧化剂:选自樱花花提取物(0.3份)、季戊四醇四(双-叔丁基羟基氢化肉桂酸)酯(0.1份)、咖啡黄葵果提取物(0.2份)(购自上海钊馨化学);
防腐剂:1,2己二醇(0.2份)、对羟基苯乙酮(0.1份);
实施例2:一种真空装置提取的植物提取物:
利用一种用于新鲜植物组织提取设备来得到樱花花提取物,设备参考专利号:CN202010510600.8。
提取步骤:
1)、将新鲜的樱花花清洗、沥干,投放到真空装置的物料仓内,关闭仓门;
2)、开启电蒸汽发生器、制冷机组、水处理设备,启动真空装置,设置运行时间;
3)、控制整个樱花花原液提取过程中的温度、真空度,收集冷凝提取液于收液罐中;
4)、待无提取液滴出,停止提取操作,进行排气驱动,确定干燥物状态,排出干燥物,收集浸出液即樱花花提取物。
所述的樱花花为新鲜的樱花花,即采摘到使用的时间最多为半天或当即冷冻保存的;
所述运行时间为2h;
所述樱花花原液提取过程中温度为40℃;
所述樱花花原液提取过程中真空度为-50kPa;
一种真空装置提取的植物提取物的应用:美白面霜
由上述方法提取所得的植物提取物用于美白面霜,按重量份计,其原料的组成及含量如下:
溶剂:64.5份;螯合剂:0.1份;保湿剂:10份;皮肤调理剂:8份;增稠剂:0.5份;乳化剂:3份;润肤剂:13份;抗氧化剂:0.6份;防腐剂:0.3份。
溶剂:去离子水(64份)、PEG-40氢化蓖麻油(0.5份);
螯合剂:EDTA-2Na(0.1份);
保湿剂:甘油(4份)、甘油聚醚-26(3份)、银耳多糖(1.8份)、海藻糖(1.0份)、透明质酸钠(0.2份);
皮肤调理剂:植物甾醇油酸酯(1份)、泛醇(0.3份)、氢化卵磷脂(0.05份)、双丙甘醇(0.07份)、神经酰胺(0.05份)、红没药醇(0.5份)、尿囊素(0.5份)、角鲨烷(2份)、乳酸杆菌发酵产物(0.5份)、姜黄根提取物(0.01份)、二裂酵母发酵产物溶胞物(0.01)、视黄醇棕榈酸酯(0.1份)、烟酰胺(2份)、四氢甲基嘧啶羧酸(0.01份)、精氨酸(0.25份)、柠檬酸(0.25)、乙酰壳糖胺(0.2份)、蜂蜜提取物(0.2份);
增稠剂:卡波姆941(0.3份)、黄原胶(0.2份);
乳化剂:硬脂酰谷氨酸钠(0.3份)、鲸蜡硬脂醇(2份)、PEG-100硬脂酸酯(0.4份)、甲氧基PEG/PPG-25/4聚二甲基硅氧烷(0.3份);
润肤剂:霍霍巴籽油(5份)、肉豆蔻醇肉豆蔻酸酯(3份)、牛油果树果脂(2份)、生育酚乙酸酯(2份)、甘油三(乙基己酸)酯(1份);
抗氧化剂:选自樱花花提取物(0.3份)、季戊四醇四(双-叔丁基羟基氢化肉桂酸)酯(0.1份)、咖啡黄葵果提取物(0.2份);
防腐剂:1,2己二醇(0.2份)、对羟基苯乙酮(0.1份);
对比例1:一种真空装置提取的植物提取物:
利用一种用于新鲜植物组织提取设备来得到樱花花提取物,设备参考专利号:CN202010510600.8。
提取步骤:
1)、将新鲜的樱花花清洗、沥干,投放到真空装置的物料仓内,关闭仓门;
2)、开启电蒸汽发生器、制冷机组、水处理设备,启动真空装置,设置运行时间;
3)、控制整个樱花花原液提取过程中的温度、真空度,收集冷凝提取液于收液罐中;
4)、待无提取液滴出,停止提取操作,进行排气驱动,确定干燥物状态,排出干燥物,收集浸出液即樱花花提取物。
所述的樱花花为新鲜的樱花花,即采摘到使用的时间最多为半天或当即冷冻保存的;
所述运行时间为2h;
所述樱花花原液提取过程中温度为35℃;
所述樱花花原液提取过程中真空度为-50kPa;
一种真空装置提取的植物提取物的应用:美白面霜
由上述方法提取所得的植物提取物用于美白面霜,按重量计,其原料的组成及含量如下:
溶剂:64.5份;螯合剂:0.1份;保湿剂:10份;皮肤调理剂:8份;增稠剂:0.5份;乳化剂:3份;润肤剂:13份;抗氧化剂:0.6份;防腐剂:0.3份。
溶剂:去离子水(64份)、PEG-40氢化蓖麻油(0.5份);
螯合剂:EDTA-2Na(0.1份);
保湿剂:甘油(4.5份)、甘油聚醚-26(3.5份)、银耳多糖(1.8份)、透明质酸钠(0.2份);
皮肤调理剂:植物甾醇油酸酯(1份)、泛醇(0.3份)、氢化卵磷脂(0.05份)、双丙甘醇(0.07份)、神经酰胺(0.05份)、红没药醇(0.5份)、尿囊素(0.5份)、角鲨烷(2份)、乳酸杆菌发酵产物(0.5份)、姜黄根提取物(0.01份)、二裂酵母发酵产物溶胞物(0.01)、视黄醇棕榈酸酯(0.1份)、烟酰胺(2份)、四氢甲基嘧啶羧酸(0.01份)、精氨酸(0.25份)、柠檬酸(0.25)、乙酰壳糖胺(0.2份)、蜂蜜提取物(0.2份);
增稠剂:卡波姆941(0.3份)、黄原胶(0.2份);
乳化剂:硬脂酰谷氨酸钠(0.3份)、鲸蜡硬脂醇(2份)、PEG-100硬脂酸酯(0.4份)、甲氧基PEG/PPG-25/4聚二甲基硅氧烷(0.3份);
润肤剂:霍霍巴籽油(5份)、肉豆蔻醇肉豆蔻酸酯(3份)、牛油果树果脂(2份)、生育酚乙酸酯(2份)、甘油三(乙基己酸)酯(1份);
抗氧化剂:选自樱花花提取物(0.3份)、季戊四醇四(双-叔丁基羟基氢化肉桂酸)酯(0.1份)、咖啡黄葵果提取物(0.2份);
防腐剂:1,2己二醇(0.2份)、对羟基苯乙酮(0.1份);
对比例2:一种真空装置提取的植物提取物:
利用一种用于新鲜植物组织提取设备来得到樱花花提取物,设备参考专利号:CN202010510600.8。
提取步骤:
1)、将新鲜的樱花花清洗、沥干,投放到真空装置的物料仓内,关闭仓门;
2)、开启电蒸汽发生器、制冷机组、水处理设备,启动真空装置,设置运行时间;
3)、控制整个樱花花原液提取过程中的温度、真空度,收集冷凝提取液于收液罐中;
4)、待无提取液滴出,停止提取操作,进行排气驱动,确定干燥物状态,排出干燥物,收集浸出液即樱花花提取物。
所述的樱花花为新鲜的樱花花,即采摘到使用的时间最多为半天或当即冷冻保存的;
所述运行时间为2h;
所述樱花花原液提取过程中温度为35℃;
所述樱花花原液提取过程中真空度为-50kPa;
一种真空装置提取的植物提取物的应用:美白面霜
由上述方法提取所得的植物提取物用于美白面霜,按重量计,其原料的组成及含量如下:
溶剂:64.5份;螯合剂:0.1份;保湿剂:10份;皮肤调理剂:8份;增稠剂:0.5份;乳化剂:3份;润肤剂:13份;抗氧化剂:0.6份;防腐剂:0.3份。
溶剂:去离子水(64份)、PEG-40氢化蓖麻油(0.5份);
螯合剂:EDTA-2Na(0.1份);
保湿剂:甘油(4份)、甘油聚醚-26(3份)、银耳多糖(1.8份)、海藻糖(1.0份)、透明质酸钠(0.2份);
皮肤调理剂:植物甾醇油酸酯(1份)、泛醇(0.3份)、氢化卵磷脂(0.05份)、双丙甘醇(0.07份)、神经酰胺(0.05份)、红没药醇(0.5份)、尿囊素(0.5份)、角鲨烷(2份)、乳酸杆菌发酵产物(0.5份)、姜黄根提取物(0.01份)、二裂酵母发酵产物溶胞物(0.01)、视黄醇棕榈酸酯(0.1份)、烟酰胺(2份)、四氢甲基嘧啶羧酸(0.01份)、精氨酸(0.25份)、柠檬酸(0.25)、乙酰壳糖胺(0.2份)、蜂蜜提取物(0.2份);
增稠剂:卡波姆941(0.3份)、黄原胶(0.2份);
乳化剂:硬脂酰谷氨酸钠(0.3份)、鲸蜡硬脂醇(2份)、PEG-100硬脂酸酯(0.4份)、甲氧基PEG/PPG-25/4聚二甲基硅氧烷(0.3份);
润肤剂:霍霍巴籽油(5份)、肉豆蔻醇肉豆蔻酸酯(3份)、牛油果树果脂(2份)、生育酚乙酸酯(2份)、甘油三(乙基己酸)酯(1份);
抗氧化剂:选自樱花花提取物(0.3份)、季戊四醇四(双-叔丁基羟基氢化肉桂酸)酯(0.1份)、咖啡黄葵果提取物(0.2份);
防腐剂:1,2己二醇(0.2份)、对羟基苯乙酮(0.1份);
对比例3:一种美白面霜:按重量计,其原料的组成及含量如下:
溶剂:64.5份;螯合剂:0.1份;保湿剂:10份;皮肤调理剂:8份;增稠剂:0.5份;乳化剂:3份;润肤剂:13份;抗氧化剂:0.6份;防腐剂:0.3份。
溶剂:去离子水(64份)、PEG-40氢化蓖麻油(0.5份);
螯合剂:EDTA-2Na(0.1份);
保湿剂:甘油(4份)、甘油聚醚-26(3份)、银耳多糖(1.8份)、海藻糖(1.0份)、透明质酸钠(0.2份);
皮肤调理剂:植物甾醇油酸酯(1份)、泛醇(0.3份)、氢化卵磷脂(0.05份)、双丙甘醇(0.07份)、神经酰胺(0.05份)、红没药醇(0.5份)、尿囊素(0.5份)、角鲨烷(2份)、乳酸杆菌发酵产物(0.5份)、姜黄根提取物(0.01份)、二裂酵母发酵产物溶胞物(0.01)、视黄醇棕榈酸酯(0.1份)、烟酰胺(2份)、四氢甲基嘧啶羧酸(0.01份)、精氨酸(0.25份)、柠檬酸(0.25)、乙酰壳糖胺(0.2份)、蜂蜜提取物(0.2份);
增稠剂:卡波姆941(0.3份)、黄原胶(0.2份);
乳化剂:硬脂酰谷氨酸钠(0.3份)、鲸蜡硬脂醇(2份)、PEG-100硬脂酸酯(0.4份)、甲氧基PEG/PPG-25/4聚二甲基硅氧烷(0.3份);
润肤剂:霍霍巴籽油(5份)、肉豆蔻醇肉豆蔻酸酯(3份)、牛油果树果脂(2份)、生育酚乙酸酯(2份)、甘油三(乙基己酸)酯(1份);
抗氧化剂:选自樱花花提取物(0.3份)(购自西安全奥生物科技有限公司)、季戊四醇四(双-叔丁基羟基氢化肉桂酸)酯(0.1份)、咖啡黄葵果提取物(0.2份);
防腐剂:1,2己二醇(0.2份)、对羟基苯乙酮(0.1份);
性能测试:
性能测试:
1、提取产率:通过准确称量新鲜樱花花和提取后的樱花花干燥物、浸出液的质量,计算评估樱花花提取物的提取产率。实施例1新鲜樱花花的干燥物产出率为33.4%,出液率为66.2%,产率高;实施例2新鲜樱花花的干燥物产出率为33.6%,出液率为66.1%,产率高。
2、稳定性:将实施例和对比例所得面霜进行机械稳定性的产品性能测试。将样品置于2000r/min转速的离心机中,离心30分钟后,观察是否有沉淀或分层现象发生。评价标准为:看不出外观上的变化记为A,观察到少量混浊记为B,观察到部分混浊甚至出现沉淀物记为C,观察到大量沉淀物甚至出现分层现象,记为D。实施例1和2的稳定性评级为A,对比例1的评级为C,对比例2的评级为B;对比例3的稳定性评级为B。

Claims (10)

1.一种真空装置提取的植物提取物,其特征在于,包括以下步骤:
1)、将新鲜的樱花花清洗、沥干,投放到真空装置的物料仓内,关闭仓门;
2)、开启电蒸汽发生器、制冷机组、水处理设备,启动真空装置,设置运行时间;
3)、控制整个樱花花原液提取过程中的温度、真空度,收集冷凝提取液于收液罐中;
4)、待无提取液滴出,停止提取操作,进行排气驱动,确定干燥物状态,排出干燥物,收集浸出液即植物提取物;
所述植物提取物为樱花花提取物。
2.如权利要求1所述的一种真空装置提取的植物提取物,其特征在于,所述樱花花原液提取过程中温度为35℃~40℃。
3.如权利要求1所述的一种真空装置提取的植物提取物在化妆品中的应用。
4.如权利要求3所述的一种真空装置提取的植物提取物在化妆品中的应用,其特征在于,应用于美白面霜、美白爽肤水、美白保湿乳、沐浴露中。
5.一种美白面霜,其特征在于,按重量份计,其原料的组成及含量如下:
溶剂:60-70份;螯合剂:0.1-0.2份;保湿剂:8-13份;皮肤调理剂:6-17份;增稠剂:0.3-0.7份;乳化剂:2-6份;润肤剂:13-18份;抗氧化剂:0.5-1份;防腐剂:0.3-1.0份;
所述抗氧化剂包括权利要求1-2任一项所述的樱花花提取物。
6.如权利要求5所述的一种美白面霜,其特征在于,所述保湿剂选自甘油、甘油聚醚-26、丙二醇、山梨醇、银耳多糖、海藻糖、二甲基甲硅烷醇透明质酸酯、透明质酸钠中的一种或多种。
7.如权利要求5所述的一种美白面霜,其特征在于,所述皮肤调理剂选自植物甾醇油酸酯、泛醇、氢化卵磷脂、甘油硬脂酸酯、双丙甘醇、神经酰胺、红没药醇、尿囊素、角鲨烷、咖啡黄葵果提取物、柠檬酸、乳酸杆菌发酵产物、姜黄根提取物、二裂酵母发酵产物溶胞物、乙酸、乳酸、视黄醇棕榈酸酯、烟酰胺、四氢甲基嘧啶羧酸、精氨酸、蜂蜜提取物的一种或几种。
8.如权利要求5所述的一种美白面霜,其特征在于,所述增稠剂选自黄原胶、羟乙基丙烯酸盐、丙烯酰二甲基牛磺酸钠共聚物、卡波姆941中的一种或几种。
9.如权利要求8所述的一种美白面霜,其特征在于,所述增稠剂选自黄原胶和卡波姆941。
10.如权利要求5所述的一种美白面霜,其特征在于,所述抗氧化剂还包括超氧化物歧化酶、季戊四醇四(双-叔丁基羟基氢化肉桂酸)酯、半胱氨酸、抗坏血酸、维生素C、维生素E中的一种或多种。
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