CN114949898B - Prepare drying device of ruthenium trichloride - Google Patents
Prepare drying device of ruthenium trichloride Download PDFInfo
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- CN114949898B CN114949898B CN202210924258.5A CN202210924258A CN114949898B CN 114949898 B CN114949898 B CN 114949898B CN 202210924258 A CN202210924258 A CN 202210924258A CN 114949898 B CN114949898 B CN 114949898B
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- rod
- workbench
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- YBCAZPLXEGKKFM-UHFFFAOYSA-K ruthenium(iii) chloride Chemical compound [Cl-].[Cl-].[Cl-].[Ru+3] YBCAZPLXEGKKFM-UHFFFAOYSA-K 0.000 title claims abstract description 32
- 238000001035 drying Methods 0.000 title claims abstract description 20
- 238000004821 distillation Methods 0.000 claims abstract description 96
- 230000007246 mechanism Effects 0.000 claims abstract description 51
- 238000010438 heat treatment Methods 0.000 claims abstract description 42
- 238000003756 stirring Methods 0.000 claims description 18
- 230000000149 penetrating effect Effects 0.000 claims description 2
- 239000013078 crystal Substances 0.000 abstract description 14
- 238000007599 discharging Methods 0.000 abstract description 6
- 238000006243 chemical reaction Methods 0.000 abstract description 3
- 230000009286 beneficial effect Effects 0.000 abstract description 2
- 238000000605 extraction Methods 0.000 abstract description 2
- 238000001556 precipitation Methods 0.000 abstract description 2
- 239000010970 precious metal Substances 0.000 abstract 1
- KJTLSVCANCCWHF-UHFFFAOYSA-N Ruthenium Chemical compound [Ru] KJTLSVCANCCWHF-UHFFFAOYSA-N 0.000 description 9
- 229910052707 ruthenium Inorganic materials 0.000 description 9
- 238000000034 method Methods 0.000 description 8
- 239000002994 raw material Substances 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- 230000008901 benefit Effects 0.000 description 2
- 230000002146 bilateral effect Effects 0.000 description 2
- 238000009434 installation Methods 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 230000008569 process Effects 0.000 description 2
- 238000007789 sealing Methods 0.000 description 2
- 239000002699 waste material Substances 0.000 description 2
- 238000003466 welding Methods 0.000 description 2
- -1 base 1 Chemical compound 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 230000008878 coupling Effects 0.000 description 1
- 238000010168 coupling process Methods 0.000 description 1
- 238000005859 coupling reaction Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000009713 electroplating Methods 0.000 description 1
- 239000002360 explosive Substances 0.000 description 1
- 238000007210 heterogeneous catalysis Methods 0.000 description 1
- 238000007172 homogeneous catalysis Methods 0.000 description 1
- 238000005984 hydrogenation reaction Methods 0.000 description 1
- 239000003999 initiator Substances 0.000 description 1
- 238000006317 isomerization reaction Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 229910000510 noble metal Inorganic materials 0.000 description 1
- 238000006116 polymerization reaction Methods 0.000 description 1
- 238000004321 preservation Methods 0.000 description 1
- 150000003303 ruthenium Chemical class 0.000 description 1
- 229910001927 ruthenium tetroxide Inorganic materials 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/02—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping in boilers or stills
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D9/00—Crystallisation
- B01D9/02—Crystallisation from solutions
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G55/00—Compounds of ruthenium, rhodium, palladium, osmium, iridium, or platinum
- C01G55/005—Halides
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/10—Process efficiency
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Crystallography & Structural Chemistry (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
The invention relates to the technical field of precious metal extraction reaction instruments, in particular to a drying device for preparing ruthenium trichloride. The invention provides a drying device for preparing ruthenium trichloride, which is convenient for discharging and is beneficial to crystal precipitation. The invention provides a drying device for preparing ruthenium trichloride, which comprises: the supporting mechanisms for adjusting and guiding the distillation container are symmetrically arranged on the workbench, and the distillation container is arranged between the two supporting mechanisms; and the sliding heating device is arranged at the position between the arc-shaped support and the distillation container on the top of the workbench. Can adjust the distance of arc heating lamp and distillation vessel according to operating condition, cross cutting ferrule and cross card axle joint, the rotating electrical machines can drive the distillation vessel rotation and carry out the even heating, moves upward when driving the distillation vessel, and cross card axle will break away from with the cross cutting ferrule, alright upset distillation vessel makes to appear ruthenium trichloride crystal and can collect fast.
Description
Technical Field
The invention relates to the technical field of noble metal extraction reaction instruments, in particular to a drying device for preparing ruthenium trichloride.
Background
Ruthenium trichloride is an important inorganic substance, can react with a plurality of reagents to generate a plurality of complexes, and is also an initiator for preparing a plurality of ruthenium complexes, the ruthenium trichloride can be used for heterogeneous catalysis or homogeneous catalysis, can be used as a catalyst for polymerization, isomerization, hydrogenation and other reactions of a plurality of organic substances, can also be used for electroplating, electrolytic anodes, electronic industry and other important chemical raw materials, is generally prepared by ruthenium-containing waste liquid at present, and in the process of preparing ruthenium trichloride by utilizing the ruthenium-containing waste liquid, the last step is to heat and dry ruthenium-containing solution after ruthenium tetroxide reacts with hydrochloric acid to separate out ruthenium trichloride crystals.
At present, a heating device is generally used for drying ruthenium-containing solution in a container, and in the drying process, corrosive steam is emitted from the container and corrodes the heating device, so that the heating device needs to be frequently replaced, and through retrieval, chinese patent No. CN207342233U discloses a drying device for preparing ruthenium trichloride, which comprises a base, a support rod, a heating lamp and a distillation container, wherein the base is provided with the distillation container, the side surface of the distillation container is provided with the support rod, the support rod is arranged on the base, and the heating lamp is arranged on the support rod; the distillation container is provided with a top cover, and a conduit for communicating the inside and the outside of the distillation container is arranged on the top cover.
Foretell drying device who prepares ruthenium trichloride collects the ruthenium trichloride crystal of appearing inconvenient, and the cooperation of heat lamp and distillation container is inseparable, can not collect fast, consequently, designs one kind and can make things convenient for the ejection of compact and do benefit to the drying device who prepares ruthenium trichloride that the crystal appeared.
Disclosure of Invention
In order to overcome the defects that the existing drying device for preparing ruthenium trichloride is inconvenient to collect precipitated ruthenium trichloride crystals, a heating lamp is tightly matched with a distillation container, and the ruthenium trichloride crystals cannot be collected quickly, the invention has the technical problems that: provides a drying device for preparing ruthenium trichloride, which is convenient for discharging and is beneficial to crystal precipitation.
The technical scheme is as follows: a drying device for preparing ruthenium trichloride comprises: the workbench is fixedly arranged on the base; the rotating electrical machines is provided with rotating electrical machines on the base, still includes: the supporting mechanism is symmetrically arranged on the workbench and used for adjusting and guiding the distillation container; the distillation container is arranged between the two supporting mechanisms; the bottom of the distillation container is provided with a cross cutting sleeve; the cross clamping shaft is rotatably arranged on the workbench and is positioned right below the cross clamping sleeve, and an output shaft of the rotating motor is connected with the cross clamping shaft through a coupler; the arc-shaped support is arranged on one side, away from the supporting mechanism, of the workbench; the top of the workbench is provided with a sliding heating device between the arc-shaped bracket and the distillation container; the upper part of the arc-shaped bracket is provided with a guide seat close to one side of the distillation container; the guide rod is arranged on the guide seat in a sliding manner; the lower end of the guide rod is provided with a top cover, the edge of the bottom of the top cover is provided with a circle of clamping rings, the top cover is positioned right above the distillation container, and the edge of the top of the distillation container is provided with a circular clamping groove matched with the clamping rings at the bottom of the top cover; the top cover is provided with a guide pipe for guiding out steam in a penetrating manner.
Further, the support mechanism includes: the supporting seat is symmetrically arranged on the workbench; the top of each supporting seat is provided with a sliding rail; the sliding blocks are arranged in the sliding rails in a sliding manner; the rotating shafts are rotatably arranged on the sliding blocks; the annular ring is arranged between the two rotating shafts; the annular track is arranged at the inner ring position of the annular ring, and the distillation container is installed in a sliding mode through the annular groove in the outer side wall and the annular track on the annular ring.
Further, the sliding heating apparatus includes: the top of the workbench is provided with a first sliding groove between the arc-shaped bracket and the distillation container, and the first sliding groove on the workbench is internally provided with a sliding block in a sliding manner; the sliding block is provided with a mounting frame; the arc heating lamps are symmetrically arranged on one side, close to the distillation container, of the mounting frame up and down.
Further, the method also comprises the following steps: jacking mechanism is provided with on the workstation and can adjusts fixed jacking mechanism to supporting mechanism, and jacking mechanism includes: the top of the workbench is provided with a second sliding chute close to the supporting seat, the second sliding chutes are internally provided with wedge-shaped ejector blocks in a sliding manner, and the wedge-shaped ejector blocks are in contact fit with one end of the rotating shaft away from the distillation container; the connecting rod is arranged between one sides of the two wedge-shaped top blocks, which are far away from the distillation container; the middle part of one side of the connecting rod, which is far away from the distillation container, is provided with a first connecting frame, and one side of the first connecting frame, which is far away from the connecting rod, is connected with the mounting frame; the push rod is arranged on the lower portion of one side, away from the connecting rod, of the mounting frame.
Further, the method also comprises the following steps: push-and-pull institution installs the push-and-pull institution that can drive jack-up mechanism and carry out the removal regulation on the top cap, and push-and-pull institution includes: the edge positions of the top cover are uniformly provided with four second connecting frames at intervals; the mounting rings are arranged among the tops of the four second connecting frames; the mounting rod is arranged on one side, close to the push rod, of the mounting ring; the installation rod is provided with a telescopic rod; the bottom end of the telescopic rod is provided with two inclined groove plates; and one end of the push rod, which is far away from the distillation container, is provided with a slide shaft, and the two ends of the slide shaft are respectively positioned in the inclined chutes of the adjacent inclined chute plates.
Further, the method also comprises the following steps: rabbling mechanism, central point puts and is provided with the rabbling mechanism that can be two state regulation of vertical and level in the top cap, and the rabbling mechanism includes: the mounting seat is arranged at the central position in the top cover; the mounting shaft is rotatably arranged on the mounting seat; stirring blades are arranged on the mounting shaft at intervals.
Further, the method also comprises the following steps: and the rotary heater is rotatably arranged at the position of the side wall of the sliding rail far away from the mounting frame.
Further, the method also comprises the following steps: the guide rod is provided with a pull rod; the mounting plate is arranged on the upper part of the side wall of the arc-shaped support close to the distillation container; the rotary clamping frame is rotatably arranged on the mounting plate and matched with the pull rod.
Compared with the prior art, the invention has the following advantages:
1. the position of heating device that slides is adjusted to the accessible, realizes that the distance of arc heating lamp and distillation container is adjusted, and cross cutting ferrule and cross card axle joint when the distillation container bottom, the rotating electrical machines can drive the distillation container rotation and carry out the even heating, through driving the distillation container upward movement, and cross card axle breaks away from with the cross cutting ferrule, conveniently overturns the distillation container for it pours into to the collecting vessel fast to appear ruthenium trichloride crystal.
2. Through the cooperation of jack-up mechanism and push-and-pull institution, when needs top cap to move away from, can realize keeping away from of slip heating device to and distillation vessel's automation lifts up, conveniently feeds in raw material and ejection of compact operation.
3. Because the top cap is in sealing fit with the distillation container, the stirring blade can be in contact with the ruthenium-containing solution for stirring, so that the ruthenium trichloride crystal can be conveniently separated out. Can rotate installation axle and stirring vane to the horizontality during the ejection of compact, prevent to influence the ejection of compact of distillation container.
4. When heating operation is carried out, the rotary heater on the side wall of the mounting rack can be rotated to be close to the distillation container, auxiliary heating is carried out, and when discharging is needed, the rotary heater can be rotated to two sides to be separated.
Drawings
Fig. 1 is a schematic perspective view of the present invention.
Fig. 2 is a partial perspective view of the present invention.
Fig. 3 is a schematic view of a partial three-dimensional explosive structure according to the present invention.
Fig. 4 is a schematic perspective view of the jacking mechanism and the push-pull mechanism of the present invention.
Fig. 5 is a schematic perspective view of the stirring mechanism of the present invention.
Fig. 6 is a schematic perspective view of the pull rod, the mounting plate and the rotating clamp frame according to the present invention.
The meaning of the reference symbols in the figures: 1: base, 2: workbench, 3: support mechanism, 31: support seat, 32: slide rail, 33: slider, 34: rotating shaft, 35: annular ring, 36: circular orbit, 4: distillation vessel, 5: cross cutting ferrule, 6: rotating electric machine, 7: cross shaft, 8: slide heating device, 81: first chute, 82: sliding block, 83: mounting frame, 84: arc heating lamp, 9: arc support, 10: guide holder, 11: guide rod, 12: top cover, 13: catheter, 14: jack-up mechanism, 141: second chute, 142: wedge-shaped top block, 143: connecting rod, 144: first link frame, 145: push rod, 15: push-pull mechanism, 151: second link, 152: mounting ring, 1521: mounting rod, 153: telescopic rod, 154: chute plate, 155: slide shaft, 16: stirring mechanism, 161: mount, 162: mounting shaft, 163: stirring blade, 17: rotary heater, 18: pull rod, 19: mounting plate, 20: the clamping frame is rotated.
Detailed Description
The invention is further described below with reference to the drawings and examples.
Example 1
As shown in fig. 1-2, a drying device for preparing ruthenium trichloride, including base 1, workstation 2 and rotating electrical machines 6, workstation 2 fixed mounting is on base 1, be provided with rotating electrical machines 6 on the base 1, still including supporting mechanism 3, distillation container 4, cross cutting ferrule 5, cross trip shaft 7, sliding heating device 8, arc support 9, guide holder 10, guide arm 11, top cap 12 and pipe 13, workstation 2 top bilateral symmetry is provided with supporting mechanism 3, be provided with distillation container 4 between two supporting mechanism 3, distillation container 4 bottom welding has cross cutting ferrule 5, workstation 2 upper rotating type is provided with cross trip shaft 7, cross trip shaft 7 is located under cross cutting ferrule 5, the output shaft of rotating electrical machines 6 passes through the coupling joint with cross trip shaft 7, workstation 2 rear side is provided with arc support 9, workstation 2 top is located between arc support 9 and distillation container 4 and is provided with sliding heating device 8, arc support 9 upper portion front side is provided with guide holder 10 through the bolted connection, guide holder 10 upper sliding type is provided with guide arm 11, the lower extreme of workstation 11 is provided with distillation container 12, the top cap 12 edge is provided with the top cap 12 and is used for the top cap 12 edge of the top cap 12 and the top cap 12 runs through the steam outlet of the top cap and is used for opening the cooperation of the top cap.
As shown in fig. 3, the supporting mechanism 3 includes a supporting seat 31, a sliding rail 32, a sliding block 33, a rotating shaft 34, an annular ring 35 and an annular rail 36, the supporting seat 31 is arranged at the top of the worktable 2 in a bilateral symmetry manner, the sliding rail 32 is arranged at the top of the supporting seat 31, the sliding block 33 is arranged in the sliding rail 32 in a sliding manner, the rotating shaft 34 is arranged on the sliding block 33 in a rotating manner, the annular ring 35 is arranged between the two rotating shafts 34 in a bolt connection manner, the annular rail 36 is arranged at the inner ring position of the annular ring 35 in a screw connection manner, and the distillation container 4 is slidably mounted with the annular rail 36 on the annular ring 35 through the annular groove on the outer side wall.
As shown in fig. 3, the slide heating device 8 includes: sliding block 82, mounting bracket 83 and arc heating lamp 84, workstation 2 top rear side is opened has first spout 81, and first spout 81 is located between arc support 9 and the distillation vessel 4, and the slidingtype is provided with sliding block 82 in the first spout 81 on the workstation 2, and the mode through bolted connection is provided with mounting bracket 83 on the sliding block 82, and mounting bracket 83 is close to distillation vessel 4 one side longitudinal symmetry and is provided with arc heating lamp 84.
When the equipment is used, a worker injects a ruthenium-containing solution into the distillation container 4, then moves the top cover 12 downwards, the top cover 12 drives the guide pipe 13 to move downwards, the top cover 12 is closed with the distillation container 4, and then the worker leads the guide pipe 13 on the top cover 12 to a steam collecting position. At this time, the worker pushes the mounting frame 83 to move closer to the retort 4, and the arc-shaped heating lamps 84 are close to the retort 4. The cross cutting ferrule 5 and the cross clamping shaft 7 joint of distillation container 4 bottom, staff control arc heating lamp 84 and rotating electrical machines 6 work this moment, and arc heating lamp 84 heats distillation container 4 and dries, and in the heating stoving in-process, the corrosive steam that contains ruthenium solution and continuously escape in the distillation container 4 will get into steam collection department through pipe 13. Simultaneously, rotating electrical machines 6 drives cross cutting ferrule 5 and distillation vessel 4 rotation through cross card axle 7, then make arc heating lamp 84 to distillation vessel 4 even heating, after appearing the ruthenium trichloride crystal, staff's control arc heating lamp 84 and rotating electrical machines 6 stop work, then pulling mounting bracket 83 is to keeping away from 4 directions of distillation vessel and remove, and then arc heating lamp 84 keeps away from distillation vessel 4, wait after 4 heat preservation cooling of distillation vessel, staff alright drive distillation vessel 4 upward movement, cross card axle 7 drives cross cutting ferrule 5 and breaks away from, then upset distillation vessel 4 can make to appear the ruthenium trichloride crystal and pour into to the collecting vessel in fast.
Example 2
As shown in fig. 4, based on embodiment 1, the distillation container further includes a jacking mechanism 14, the work table 2 is provided with the jacking mechanism 14 capable of adjusting and fixing the supporting mechanism 3, the jacking mechanism 14 includes a wedge-shaped jacking block 142, a connecting rod 143, a first connecting frame 144 and a push rod 145, the top of the work table 2 is bilaterally symmetrically provided with a second sliding groove 141, the second sliding groove 141 is internally provided with the wedge-shaped jacking block 142 in a sliding manner, the wedge-shaped jacking block 142 is in contact fit with one end of the rotating shaft 34 far away from the distillation container 4, the connecting rod 143 is arranged between the rear sides of the two wedge-shaped jacking blocks 142, the middle position of the rear side of the connecting rod 143 is provided with the first connecting frame 144, the rear end of the first connecting frame 144 is connected with the mounting frame 83, and the lower part of the rear side of the mounting frame 83 is provided with the push rod 145.
As shown in fig. 4, the distillation container further includes a push-pull mechanism 15, the top cover 12 is provided with the push-pull mechanism 15 capable of driving the jacking mechanism 14 to move and adjust, the push-pull mechanism 15 includes four second connecting frames 151, four mounting rings 152, four mounting rods 1521, a telescopic rod 153, two chute plates 154 and a sliding shaft 155, the edge positions of the top cover 12 are provided with the second connecting frames 151 at uniform intervals, the four second connecting frames 151 are provided with the mounting rings 152 between the tops of the four second connecting frames 151, the mounting rods 1521 are arranged on the rear sides of the mounting rings 152, the telescopic rod 153 is arranged on the mounting rod 1521, the two chute plates 154 are symmetrically arranged at the bottom ends of the telescopic rod 153 in the left-right direction, the end of the push rod 145, which is far away from the distillation container 4, is provided with the sliding shaft 155, and the two ends of the sliding shaft 155 are respectively located in the oblique chutes of the adjacent chute plates 154.
As shown in fig. 6, the device further includes a pull rod 18, a mounting plate 19 and a rotary clamping frame 20, the pull rod 18 is arranged on the guide rod 11 in a welding manner, the mounting plate 19 is arranged on the upper portion of the right side wall of the arc-shaped support 9, the rotary clamping frame 20 is rotatably arranged on the mounting plate 19, and the rotary clamping frame 20 is matched with the pull rod 18.
When the distillation container 4 needs to be lifted, the pull rod 18 drives the guide rod 11 and the top cover 12 to move upwards when a worker holds the pull rod 18 to move upwards. Then, the second connecting frame 151, the mounting ring 152, the mounting rod 1521 and the telescopic rod 153 on the top cover 12 move upward together, when the telescopic rod 153 drives the chute plate 154 to move upward, the chute of the chute plate 154 drives the sliding shaft 155 to move to the side far away from the distillation container 4, the sliding shaft 155 drives the mounting frame 83 and the arc-shaped heating lamp 84 to move away from the distillation container 4 through the push rod 145, the mounting frame 83 drives the connecting rod 143 and the first connecting frame 144 to move, so that the connecting rod 143 drives the wedge-shaped ejecting block 142 to move, the inclined plane of the wedge-shaped ejecting block 142 lifts the rotating shaft 34 upward, when the horizontal plane of the upper part of the wedge-shaped ejecting block 142 is located below the cross-shaped rotating shaft 34, the lifting of the distillation container 4 is achieved, and the clamping shaft 7 drives the cross-shaped clamping sleeve 5 to be separated. At this time, the worker rotates the rotating jig 20, and the rotating jig 20 can stop the downward movement of the pull rod 18, and keep the top cover 12 staying at the upper side. At this moment, the staff can conveniently add raw materials into the distillation container 4 or collect the processed precipitated ruthenium trichloride crystals, when heating operation needs to be carried out again, only the rotary clamping frame 20 needs to be rotated again, the pull rod 18 is held to move downwards to drive the guide rod 11 and the top cover 12 to move downwards, when the inclined groove plate 154 moves downwards, the inclined groove of the inclined groove plate 154 drives the sliding shaft 155 to move towards one side close to the distillation container 4, when the inclined groove plate 154 drives the sliding shaft 155 to move towards the position closest to the distillation container 4, the inclined groove plate 154 stops moving downwards, the top cover 12 continues to move downwards to be closed with the distillation container 4, at the moment, the telescopic rod 153 contracts along with the inclined groove plate, the device is simple in structure, when the top cover 12 needs to be moved away, the top cover can be separated from the sliding heating device 8 through the jacking mechanism 14 and the push-pull mechanism 15, and the distillation container 4 can be lifted automatically, and discharging operation is further facilitated.
Example 3
As shown in fig. 5, in addition to embodiment 2, the stirring device further includes a stirring mechanism 16, the stirring mechanism 16 capable of being adjusted in two states, namely, a vertical state and a horizontal state, is disposed at a central position in the top cover 12, the stirring mechanism 16 includes a mounting seat 161, a mounting shaft 162 and stirring blades 163, the mounting seat 161 is disposed at the central position in the top cover 12 in a screw connection manner, the mounting shaft 162 is rotatably disposed on the mounting seat 161, and the stirring blades 163 are disposed on the mounting shaft 162 at intervals.
When ruthenium-containing solution in the distillation container 4 is heated, the rotation of the distillation container 4 can be realized by the operation of the rotating motor 6, and the top cover 12 is in sealing fit with the distillation container 4, so that the stirring blades 163 can be in contact with the ruthenium-containing solution for stirring, and the separation of ruthenium trichloride crystals is facilitated. When the material needs to be discharged, the top cover 12 drives the mounting seat 161, the mounting shaft 162 and the stirring blade 163 to move upwards together, and then the mounting shaft 162 and the stirring blade 163 can be rotated to the horizontal state, so that the influence on the discharging of the distillation container 4 is prevented.
As shown in fig. 1, the distillation container further comprises a rotary heater 17, the rotary heater 17 is rotatably disposed at a position of a front side wall of the slide rail 32, when heating is performed, the rotary heater 17 on the side wall of the mounting frame 83 can be rotated to be close to the distillation container 4, so as to achieve auxiliary heating of the distillation container 4, and when discharging is needed, the rotary heater 17 can be rotated away to two sides.
The above description is only an embodiment of the present invention, and not intended to limit the scope of the present invention, and all modifications of equivalent structures and equivalent processes, which are made by the present specification, or directly or indirectly applied to other related technical fields, are included in the scope of the present invention.
Claims (5)
1. A drying device for preparing ruthenium trichloride comprises: the workbench (2), the workbench (2) is fixedly arranged on the base (1); rotating electrical machines (6), be provided with rotating electrical machines (6) on base (1), its characterized in that still includes: the supporting mechanism (3) is symmetrically arranged on the workbench (2) and used for adjusting and guiding the distillation container (4); the distillation container (4), the distillation container (4) is arranged between the two supporting mechanisms (3); the bottom of the distillation container (4) is provided with a cross cutting sleeve (5); the rotary table comprises a cross clamping shaft (7), the workbench (2) is rotatably provided with the cross clamping shaft (7), the cross clamping shaft (7) is positioned right below a cross clamping sleeve (5), and an output shaft of a rotary motor (6) is connected with the cross clamping shaft (7) through a coupler; the arc-shaped support (9) is arranged on one side of the workbench (2) far away from the supporting mechanism (3); the top of the workbench (2) is provided with a sliding heating device (8) between the arc-shaped support (9) and the distillation container (4); the upper part of the arc-shaped bracket (9) close to one side of the distillation container (4) is provided with a guide seat (10); the guide rod (11) is arranged on the guide seat (10) in a sliding manner; the lower end of the guide rod (11) is provided with a top cover (12), the edge of the bottom of the top cover (12) is provided with a ring of clamping rings, the top cover (12) is positioned right above the distillation container (4), and the edge of the top of the distillation container (4) is provided with a circular clamping groove matched with the clamping rings at the bottom of the top cover (12); a conduit (13) for leading out steam is arranged on the top cover (12) in a penetrating way; the support mechanism (3) includes: the supporting seat (31) is symmetrically arranged on the workbench (2); the top of each supporting seat (31) is provided with a sliding rail (32); the sliding blocks (33) are arranged in the sliding rails (32) in a sliding manner; the rotating shafts (34) are arranged on the sliding blocks (33) in a rotating mode; the annular ring (35) is arranged between the two rotating shafts (34); the distillation container (4) is arranged in a sliding manner through the annular groove on the outer side wall and the annular rail (36) on the annular ring (35); the slide heating device (8) comprises: a first sliding groove (81) is formed in the position, located between the arc-shaped support (9) and the distillation container (4), of the top of the workbench (2), and the sliding block (82) is arranged in the first sliding groove (81) in the workbench (2) in a sliding mode; the sliding block (82) is provided with the mounting frame (83); the distillation container is characterized by comprising arc-shaped heating lamps (84), wherein the arc-shaped heating lamps (84) are symmetrically arranged on one side, close to the distillation container (4), of the mounting frame (83) from top to bottom; further comprising: jack-up mechanism (14), be provided with on workstation (2) and adjust fixed jack-up mechanism (14) to supporting mechanism (3), jack-up mechanism (14) include: the top of the workbench (2) is provided with second sliding chutes (141) close to the supporting seat (31), the second sliding chutes (141) are internally provided with wedge-shaped top blocks (142) in a sliding manner, and the wedge-shaped top blocks (142) are in contact fit with one end, far away from the distillation container (4), of the rotating shaft (34); the connecting rod (143) is arranged between one sides of the two wedge-shaped top blocks (142) far away from the distillation container (4); the middle part of one side, far away from the distillation container (4), of the connecting rod (143) is provided with a first connecting frame (144), and one side, far away from the connecting rod (143), of the first connecting frame (144) is connected with the mounting frame (83); the push rod (145) is arranged on the lower portion of one side, away from the connecting rod (143), of the mounting frame (83).
2. The drying device for preparing ruthenium trichloride according to claim 1, further comprising: push-and-pull institution (15), install on top cap (12) and can drive jack-up mechanism (14) and carry out push-and-pull institution (15) that remove the regulation, push-and-pull institution (15) include: the second connecting frames (151) are arranged at the edge of the top cover (12) at uniform intervals, and the number of the second connecting frames (151) is four; the mounting rings (152) are arranged among the tops of the four second connecting frames (151); the mounting rod (1521) is arranged on one side, close to the push rod (145), of the mounting ring (152); the telescopic rod (153), the mounting rod (1521) is provided with the telescopic rod (153); the bottom end of the telescopic rod (153) is provided with two chute plates (154); a sliding shaft (155) is arranged at one end of the push rod (145) far away from the distillation container (4), and two ends of the sliding shaft (155) are respectively positioned in the inclined chutes of the adjacent inclined chute plates (154).
3. The drying device for preparing ruthenium trichloride according to claim 2, further comprising: rabbling mechanism (16), central point puts in top cap (12) and is provided with rabbling mechanism (16) that can be vertical and two state regulation of level, and rabbling mechanism (16) include: the mounting seat (161) is arranged at the central position in the top cover (12); a mounting shaft (162), wherein the mounting base (161) is rotatably provided with the mounting shaft (162); the stirring blades (163) are arranged on the mounting shaft (162) at intervals.
4. The drying device for preparing ruthenium trichloride according to claim 3, further comprising: the rotary heater (17) is rotatably arranged at the position, far away from the side wall of the mounting frame (83), of the slide rail (32).
5. The drying device for preparing ruthenium trichloride according to claim 4, further comprising: the pull rod (18) is arranged on the guide rod (11); the mounting plate (19) is arranged on the upper part of the side wall of the arc-shaped bracket (9) close to the distillation container (4); the rotary clamping frame (20) is rotatably arranged on the mounting plate (19), and the rotary clamping frame (20) is matched with the pull rod (18).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202210924258.5A CN114949898B (en) | 2022-08-03 | 2022-08-03 | Prepare drying device of ruthenium trichloride |
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| Application Number | Priority Date | Filing Date | Title |
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| CN202210924258.5A CN114949898B (en) | 2022-08-03 | 2022-08-03 | Prepare drying device of ruthenium trichloride |
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| CN114949898B true CN114949898B (en) | 2022-10-25 |
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| CN208932106U (en) * | 2018-11-13 | 2019-06-04 | 李海鹏 | A kind of plastic containers for portable fever |
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| JP2001010893A (en) * | 1999-06-24 | 2001-01-16 | Toshiba Ceramics Co Ltd | Single crystal pulling device |
| CN2937162Y (en) * | 2005-12-16 | 2007-08-22 | 中国科学院福建物质结构研究所 | Turn-over device of large size KDP crystal |
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| CN114949898A (en) | 2022-08-30 |
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Denomination of invention: A drying device for producing ruthenium trichloride Effective date of registration: 20231205 Granted publication date: 20221025 Pledgee: Xi'an innovation financing Company limited by guarantee Pledgor: Shaanxi Saien Strontium Tantalum New Material Technology Co.,Ltd. Registration number: Y2023980069357 |
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