CN210905007U - Drying device for purifying metal ruthenium trichloride from waste residues - Google Patents

Drying device for purifying metal ruthenium trichloride from waste residues Download PDF

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Publication number
CN210905007U
CN210905007U CN201921857296.3U CN201921857296U CN210905007U CN 210905007 U CN210905007 U CN 210905007U CN 201921857296 U CN201921857296 U CN 201921857296U CN 210905007 U CN210905007 U CN 210905007U
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China
Prior art keywords
drying device
base
circular
ruthenium trichloride
carousel
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CN201921857296.3U
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Inventor
文劲松
柴湖军
李云鹏
朱海江
秦永红
张海燕
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Yunnan Guiyue Metal Materials Technology Co ltd
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Yunnan Guiyue Metal Materials Technology Co ltd
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Abstract

The utility model discloses a follow drying device of purification metal ruthenium trichloride in waste residue, including the drying device main part, be equipped with the heat lamp in the drying device main part, and placed the distillation container in the drying device main part to be connected with the pipe on the distillation container, drying device main part lower extreme is equipped with the base, and installs the motor on the base to the motor has the carousel through the coupling joint, the gyro wheel is installed to the carousel lower extreme, and is equipped with on the carousel and places the seat, circular recess has evenly been seted up on the carousel, and the circular recess interpolation of carousel is equipped with the dead lever to the dead lever is connected with the heat lamp. This drying device of metal ruthenium trichloride purifies in follow waste residue can make the distillation container thermally equivalent when purifying for the distillation container can be in certain reaction time efficient purification ruthenium trichloride.

Description

Drying device for purifying metal ruthenium trichloride from waste residues
Technical Field
The utility model relates to a ruthenium trichloride purification device technical field specifically is a drying device of purification metal ruthenium trichloride in follow waste residue.
Background
Ruthenium trichloride is a glossy crystal particle, generally in a grayish brown or dark red color, corrosive, very easy to deliquesce, dissolved in water, alcohol, acetone and ethyl acetate, and decomposed in hot water. It is used for heterogeneous catalysis or homogeneous catalysis, electroplating, electrolytic anode, electronic industry and other important chemical materials. Ruthenium trichloride can be purified from industrial ruthenium-containing waste, active ruthenium black is obtained through smelting activation and acid leaching, then oxidized and distilled, placed in hydrochloric acid for absorption, and then the absorption liquid is concentrated and dried to obtain ruthenium trichloride.
The existing drying device for purifying ruthenium trichloride heats absorption liquid in a distillation container through a heating lamp, a guide pipe for discharging corrosive gas generated by drying is arranged on the distillation container, but the heating lamp is fixed on the side surface of the distillation container in a static mode, so that the distillation container is easily heated unevenly, and the drying efficiency is reduced.
SUMMERY OF THE UTILITY MODEL
An object of the utility model is to provide a follow drying device of purification metal ruthenium trichloride in waste residue to solve the static fixing in the distillation vessel side of the heat lamp that is used for following the drying device of purification metal ruthenium trichloride in the waste residue on the existing market that above-mentioned background art provided, lead to the distillation vessel to be heated inhomogeneous easily, reduce drying efficiency's problem.
In order to achieve the above object, the utility model provides a following technical scheme: the utility model provides a follow drying device of purification metal ruthenium trichloride in waste residue, includes the drying device main part, be equipped with the heat lamp in the drying device main part, and placed the distillation container in the drying device main part to be connected with the pipe on the distillation container, drying device main part lower extreme is equipped with the base, and installs the motor on the base to the motor has the carousel through the coupling joint, the gyro wheel is installed to the carousel lower extreme, and is equipped with on the carousel and places the seat, circular recess has evenly been seted up to the carousel upper end, and the circular recess interpolation of carousel is equipped with the dead lever to the dead lever is connected with the heat lamp.
Preferably, the upper end of the base is provided with a circular groove, and the width of the circular groove at the upper end of the base is equal to the thickness of the roller.
Preferably, a circular through hole is formed in the middle of the base, and a fixing frame is fixed to the circular through hole of the base through a bolt in a clamping mode.
Preferably, the fixed frame is of a cylindrical frame structure, the fixed frame is sleeved outside the motor, the lower end of the base is further provided with a trapezoidal groove, and the height of the base is higher than that of the fixed frame.
Preferably, the lower part of the placing seat is of a circular ring structure, the upper part of the placing seat is of a disc structure, and the size of the disc structure of the placing seat is equal to that of the bottom of the distillation container.
Preferably, a circular groove is formed in the turntable, the diameter of the circular groove of the turntable is equal to that of the disc of the placing seat, a circular through hole is further formed in the groove of the turntable, and the circular through hole of the turntable is matched with the circular ring structure of the placing seat in shape.
Compared with the prior art, the beneficial effects of the utility model are that: this drying device of metal ruthenium trichloride purifies in follow waste residue can make the distillation container thermally equivalent when purifying for the distillation container can be in certain reaction time efficient purification ruthenium trichloride. This drying device of purification metal ruthenium trichloride from waste residue passes through the dead lever with the heat lamp and fixes on the carousel, and the carousel can rotate at the uniform velocity under the effect of motor, and the base lower extreme is seted up flutedly simultaneously, can make things convenient for the motor heat dissipation.
Drawings
FIG. 1 is a schematic structural view of a drying apparatus for purifying ruthenium trichloride from waste residues according to the present invention;
FIG. 2 is a schematic view of a three-dimensional structure of the bottom of a placing seat of a drying device for purifying ruthenium trichloride from waste residue;
FIG. 3 is a schematic view of the three-dimensional structure of the base of the drying apparatus for purifying ruthenium trichloride from the waste residue according to the present invention;
FIG. 4 is a schematic view of a connecting structure of a rotary plate and a fixing rod of a drying device for purifying ruthenium trichloride from waste residue;
FIG. 5 is a schematic diagram of the groove structure of the base of the drying device for purifying ruthenium trichloride from the waste residue.
In the figure: 1. drying device main part, 2, dead lever, 3, distillation vessel, 4, gyro wheel, 5, base, 6, pipe, 7, heating lamp, 8, place the seat, 9, carousel, 10, fixed frame, 11, motor.
Detailed Description
The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments. Based on the embodiments in the present invention, all other embodiments obtained by a person skilled in the art without creative work belong to the protection scope of the present invention.
Referring to fig. 1-5, the present invention provides a technical solution: a drying device for purifying metal ruthenium trichloride from waste residues comprises a drying device main body 1, wherein a heating lamp 7 is arranged on the drying device main body 1, the heating lamp 7 is a heating lamp tube with the model number of YR-2410-430 manufactured by ESLIGHT, a distillation container 3 is placed on the drying device main body 1, the distillation container 3 is a distillation vessel on the existing drying device for purifying metal ruthenium trichloride from waste residues, a conduit 6 is connected on the distillation container 3, the conduit 6 is used for discharging corrosive gas generated by reaction in the distillation container 3 in the drying process, so that the corrosion of the distillation container 3 caused by the fact that the corrosive gas stays in the distillation container 3 for a long time is avoided, a base 5 is arranged at the lower end of the drying device main body 1, a motor 11 is installed on the base 5, a circular through hole is formed in the middle of the base 5, and a fixing frame 10 is fixed on the circular through hole of the base 5, the circular through hole of the base 5 of the structure is convenient for connecting and fixing the fixed frame 10, the motor 11 is connected with the rotary disc 9 through the coupler, the rotary disc 9 can rotate at a constant speed under the drive of the motor 11, the fixed frame 10 is a cylindrical frame structure, the fixed frame 10 is sleeved outside the motor 11, the lower end of the base 5 is also provided with a trapezoidal groove, the height of the base 5 is higher than that of the fixed frame 10, the fixed frame 10 of the structure plays a role of supporting the motor 11, meanwhile, the trapezoidal grooves at the lower ends of the fixed frame 10 and the base 5 can facilitate the timely heat dissipation of the motor 11, the lower end of the rotary disc 9 is provided with the roller 4, the upper end of the base 5 is provided with a circular groove, the width of the circular groove at the upper end of the base 5 is equal to the thickness of the roller 4, the rotary disc 9 of the structure, the roller 4 plays a role in limiting and supporting in the rotation of the turntable 9, so that the turntable 9 can conveniently and stably rotate, the turntable 9 is provided with the placing seat 8, the lower part of the placing seat 8 is of a circular ring structure, the upper part of the placing seat 8 is of a circular disc structure, the size of the circular disc structure of the placing seat 8 is equal to that of the bottom of the distillation container 3, the structure can place the distillation container 3 on the circular disc of the placing seat 8, the upper end of the turntable 9 is uniformly provided with a circular groove, a fixing rod 2 is inserted into the circular groove of the turntable 9 and is connected with a heating lamp 7, the turntable 9 is internally provided with a circular groove, the diameter of the circular groove of the turntable 9 is equal to that of the circular disc of the placing seat 8, the groove of the turntable 9 is also provided with a circular ring-shaped through hole, the circular ring-shaped through hole of the turntable 9 is matched with the circular ring structure of the placing seat, so that the placing seat 8 can be still unaffected when the turntable 9 rotates.
The working principle is as follows: when the drying device for purifying the metal ruthenium trichloride from the waste residue is used, firstly, a fixing frame 10 and a motor 11 are clamped and fixed in a circular through hole of a base 5, then the motor 11 is connected with a rotary disc 9 through a coupler, a roller 4 at the lower end of the rotary disc 9 is clamped into an annular groove at the upper end of the base 5, then an annular bulge at the lower end of a placing seat 8 is inserted into the annular through hole of the rotary disc 9, the placing seat 8 and the base 5 are fixed through bolts, after the placing seat 8 is fixed, a fixing rod 2 is uniformly inserted into the circular groove of the rotary disc 9, then a heating lamp 7 is arranged on the fixing rod 2, after the drying device main body 1 is arranged, a distillation container 3 filled with absorption liquid is arranged on the placing seat 8, a guide pipe 6 is connected into a device for treating corrosive gas, then the drying device main body 1 is started, the rotary disc 9 drives the heating lamp 7 to rotate at a constant speed under the action of the motor 11 to heat the, the gas generated by the drying of the distillation vessel 3 is discharged through the conduit 6, thereby completing a series of works.
Although the present invention has been described in detail with reference to the foregoing embodiments, it will be apparent to those skilled in the art that modifications may be made to the embodiments or portions thereof without departing from the spirit and scope of the invention.

Claims (6)

1. The utility model provides a purification metal ruthenium trichloride's drying device in follow waste residue, includes drying device main part (1), be equipped with heat lamp (7) on drying device main part (1), and placed distillation container (3) on drying device main part (1) to be connected with pipe (6), its characterized in that on distillation container (3): drying device main part (1) lower extreme is equipped with base (5), and installs motor (11) on base (5) to motor (11) have carousel (9) through coupling joint, gyro wheel (4) are installed to carousel (9) lower extreme, and are equipped with on carousel (9) and place seat (8), circular recess has evenly been seted up to carousel (9) upper end, and the circular recess interpolation of carousel (9) is equipped with dead lever (2) to dead lever (2) are connected with heat lamp (7).
2. The drying device for purifying ruthenium trichloride from waste residue as claimed in claim 1, wherein: the upper end of the base (5) is provided with a circular groove, and the width of the circular groove at the upper end of the base (5) is equal to the thickness of the roller (4).
3. The drying device for purifying ruthenium trichloride from waste residue as claimed in claim 1, wherein: a circular through hole is formed in the middle of the base (5), and a fixing frame (10) is fixed to the circular through hole of the base (5) through a bolt in a clamping mode.
4. The drying device for purifying ruthenium trichloride from waste residue as claimed in claim 3, wherein: the fixing frame (10) is of a cylindrical frame structure, the fixing frame (10) is sleeved outside the motor (11), the lower end of the base (5) is further provided with a trapezoidal groove, and the height of the base (5) is higher than that of the fixing frame (10).
5. The drying device for purifying ruthenium trichloride from waste residue as claimed in claim 1, wherein: the lower part of the placing seat (8) is of a circular ring structure, the upper part of the placing seat (8) is of a disc structure, and the size of the disc structure of the placing seat (8) is equal to that of the bottom of the distillation container (3).
6. The drying device for purifying ruthenium trichloride from waste residue as claimed in claim 1, wherein: a circular groove is formed in the rotary table (9), the diameter of the circular groove of the rotary table (9) is equal to that of the disc of the placing seat (8), a circular through hole is further formed in the groove of the rotary table (9), and the circular through hole of the rotary table (9) is identical to the circular ring structure of the placing seat (8).
CN201921857296.3U 2019-10-31 2019-10-31 Drying device for purifying metal ruthenium trichloride from waste residues Active CN210905007U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201921857296.3U CN210905007U (en) 2019-10-31 2019-10-31 Drying device for purifying metal ruthenium trichloride from waste residues

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201921857296.3U CN210905007U (en) 2019-10-31 2019-10-31 Drying device for purifying metal ruthenium trichloride from waste residues

Publications (1)

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CN210905007U true CN210905007U (en) 2020-07-03

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114949898A (en) * 2022-08-03 2022-08-30 陕西赛恩锶钽新材料科技有限公司 Drying device for preparing ruthenium trichloride

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114949898A (en) * 2022-08-03 2022-08-30 陕西赛恩锶钽新材料科技有限公司 Drying device for preparing ruthenium trichloride

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