CN211486584U - Drying device for preparing ruthenium trichloride - Google Patents
Drying device for preparing ruthenium trichloride Download PDFInfo
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- CN211486584U CN211486584U CN201922401320.9U CN201922401320U CN211486584U CN 211486584 U CN211486584 U CN 211486584U CN 201922401320 U CN201922401320 U CN 201922401320U CN 211486584 U CN211486584 U CN 211486584U
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Abstract
The utility model discloses a drying device of preparation ruthenium trichloride, the on-line screen storage device comprises a base, fixed mounting has the mounting panel on the roof of base, fixed mounting has the distillation vessel on the roof of mounting panel, the top of base is rotated and is installed annular carousel, and annular carousel dismantles and install on the lateral wall of mounting panel, fixed mounting has annular bottom plate on the diapire of annular carousel, set up the annular movable groove of mutually supporting with annular bottom plate on the roof of base, symmetrical movable mounting has two stoppers on the inside wall of annular carousel, and the one end of stopper is all inserted and is established on the mounting panel, set up the annular spacing groove of mutually supporting with two stoppers on the lateral wall of mounting panel. The utility model discloses in be equipped with annular seal plate in the outside of heating lamp and distillation vessel, and seal heating lamp and distillation vessel in annular seal plate during the heating, not only improved distillation vessel's heating effect, also avoided thermal waste, reasonable in design, practical function is good.
Description
Technical Field
The utility model relates to a noble metal draws reaction instrument technical field, especially relates to a drying device of preparation ruthenium trichloride.
Background
Ruthenium trichloride is an important chemical raw material, and is usually prepared by ruthenium-containing waste liquid at present, in the process of preparing ruthenium trichloride by using the ruthenium-containing waste liquid, the last step is to heat and dry ruthenium-containing solution obtained after ruthenium tetroxide and hydrochloric acid react to separate out ruthenium trichloride crystals, at present, ruthenium-containing solution in a container is usually dried by a heating device, and in the drying process, steam with corrosivity is emitted from the container to corrode the heating device, so that the heating device needs to be frequently replaced, and the production cost is undoubtedly increased.
Through retrieval, the Chinese patent No. CN207342233U discloses a drying device for preparing ruthenium trichloride, which comprises a base, a support rod, a heating lamp and a distillation container, wherein the base is provided with the distillation container, the side surface of the distillation container is provided with the support rod, the support rod is arranged on the base, and the heating lamp is arranged on the support rod; the distillation container is provided with a top cover, and a conduit for communicating the inside and the outside of the distillation container is arranged on the top cover.
The existing drying device for preparing ruthenium trichloride has the following defects: the heating device is completely exposed, so that the heating effect of the distillation container is poor, the heat waste is serious, and the practical effect is poor.
SUMMERY OF THE UTILITY MODEL
The utility model aims at solving the unreasonable design problem of the drying device for preparing ruthenium trichloride in the prior art and providing a drying device for preparing ruthenium trichloride.
In order to achieve the above purpose, the utility model adopts the following technical scheme:
a drying device for preparing ruthenium trichloride comprises a base, wherein a mounting plate is fixedly mounted on the top wall of the base, a distillation container is fixedly mounted on the top wall of the mounting plate, an annular rotary table is rotatably mounted at the top end of the base and detachably mounted on the outer side wall of the mounting plate, an annular bottom plate is fixedly mounted on the bottom wall of the annular rotary table, an annular movable groove matched with the annular bottom plate is formed in the top wall of the base, two limit blocks are symmetrically and movably mounted on the inner side wall of the annular rotary table, one end of each limit block is inserted into the mounting plate, an annular limit groove matched with the two limit blocks is formed in the outer side wall of the mounting plate, a driving device is connected onto the annular rotary table, a plurality of mounting rods are fixedly mounted on the top wall of the annular rotary table, and a plurality of heating lamps are mounted on each mounting, the top wall of the annular rotary table is fixedly provided with an annular sealing plate, the distillation container, the mounting rod and the heating lamp are all located in the annular sealing plate, the top end of the distillation container is detachably provided with a top cover, a guide pipe is inserted into the top wall of the top cover and is communicated with the distillation container, the top wall of the top cover is fixedly provided with a handle, and the top cover is provided with a sealing device matched with the annular sealing plate.
Preferably, two mounting grooves mutually supporting with the stopper, two are seted up to the symmetry on the inside wall of annular carousel equal fixed mounting has the threaded rod on the roof of stopper, and the top of threaded rod all runs through the roof of annular carousel and extends to the upside of annular carousel, two movable grooves mutually supporting with the threaded rod are seted up to the symmetry on the roof of annular carousel, two equal threaded connection has fastening nut on the lateral wall on threaded rod top, and fastening nut's diameter all is greater than the width in movable groove.
Preferably, drive arrangement includes the driving motor of fixed mounting in base one side, driving motor's output fixed mounting has the pivot, the top fixed mounting of pivot has the toothed disc, evenly set up the gear with toothed disc intermeshing on the lateral wall of annular turntable.
Preferably, a plurality of balls are uniformly arranged on the top wall of the base, and the balls are in mutual contact with the annular turntable.
Preferably, the sealing device comprises an annular mounting plate fixedly mounted on the outer side wall of the top end of the top cover, an annular connecting plate is fixedly mounted on the bottom wall of the annular mounting plate, the bottom end of the annular connecting plate is inserted into the top wall of the annular sealing plate, and an annular connecting groove matched with the annular connecting plate is formed in the top wall of the annular sealing plate.
Compared with the prior art, the utility model discloses there is following beneficial effect:
1. the annular sealing plates are arranged on the outer sides of the heating lamp and the distillation container, and the heating lamp and the distillation container are sealed in the annular sealing plates during heating, so that the heating effect of the distillation container is improved, the waste of heat is avoided, the design is reasonable, and the practical effect is good;
2. the annular turntable, the mounting rod and the heating lamp can be driven to rotate around the distillation container by starting the driving motor, so that the distillation container can be uniformly heated, and the heating effect of the distillation container is further improved.
Drawings
FIG. 1 is a front sectional view of a drying apparatus for producing ruthenium trichloride;
FIG. 2 is a schematic front structural view of a drying apparatus for producing ruthenium trichloride;
fig. 3 is an enlarged view of a part a of the structure of the drying device for preparing ruthenium trichloride.
In the figure: the device comprises a base 1, a mounting plate 2, a distillation container 3, a ring-shaped rotary table 4, a ring-shaped bottom plate 5, a limiting block 6, a mounting groove 7, a threaded rod 8, a movable groove 9, a fastening nut 10, a driving motor 11, a rotating shaft 12, a gear plate 13, a ball 14, a mounting rod 15, a heating lamp 16, a ring-shaped sealing plate 17, a top cover 18, a guide pipe 19, a handle 20, a ring-shaped mounting plate 21 and a ring-shaped connecting plate 22.
Detailed Description
The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments.
Referring to fig. 1-3, a drying device for preparing ruthenium trichloride comprises a base 1, a mounting plate 2 is fixedly mounted on the top wall of the base 1, a distillation container 3 is fixedly mounted on the top wall of the mounting plate 2, an annular rotary table 4 is rotatably mounted at the top end of the base 1, the annular rotary table 4 is detachably mounted on the outer side wall of the mounting plate 2, an annular bottom plate 5 is fixedly mounted on the bottom wall of the annular rotary table 4, an annular movable groove mutually matched with the annular bottom plate 5 is formed on the top wall of the base 1, two limit blocks 6 are symmetrically and movably mounted on the inner side wall of the annular rotary table 4, one end of each limit block 6 is inserted into the mounting plate 2, an annular limit groove mutually matched with the two limit blocks 6 is formed on the outer side wall of the mounting plate 2, two mounting grooves 7 mutually matched with the limit blocks 6 are symmetrically formed on the inner side wall of the, and the top of threaded rod 8 all runs through the roof of annular carousel 4 and extends to the upside of annular carousel 4, two movable grooves 9 that mutually support with threaded rod 8 have been seted up to the symmetry on the roof of annular carousel 4, equal threaded connection has fastening nut 10 on the lateral wall on two threaded rod 8 tops, and fastening nut 10's diameter all is greater than the width of movable groove 9, can be convenient install annular carousel 4 to mounting panel 2 on or pull down from mounting panel 2, and annular carousel 4 can be relative mounting panel 2 free rotation.
Be connected with drive arrangement on annular carousel 4, drive arrangement includes the driving motor 11 of fixed mounting in base 1 one side, driving motor 11's output fixed mounting has pivot 12, the top fixed mounting of pivot 12 has toothed disc 13, evenly set up the gear with toothed disc 13 intermeshing on annular carousel 4's the lateral wall, driving motor 11 can drive pivot 12 and drive toothed disc 13 and rotate, toothed disc 13 and 4 intermeshing gear of annular carousel, consequently, toothed disc 13 rotates and can drive annular carousel 4 and rotate.
Evenly install a plurality of balls 14 on the roof of base 1, and ball 14 all contacts each other with annular turntable 4, can promote annular turntable 4 pivoted stability.
A plurality of mounting rods 15 are fixedly mounted on the top wall of the annular rotary table 4, a plurality of heating lamps 16 are mounted on each mounting rod 15, an annular sealing plate 17 is fixedly mounted on the top wall of the annular rotary table 4, the distillation container 3, the mounting rods 15 and the heating lamps 16 are all positioned in the annular sealing plate 17, a top cover 18 is demountably mounted at the top end of the distillation container 3, a guide pipe 19 is inserted on the top wall of the top cover 18 and is communicated with the distillation container 3, a handle 20 is fixedly mounted on the top wall of the top cover 18, a sealing device matched with the annular sealing plate 17 is mounted on the top cover 18 and comprises an annular mounting plate 21 fixedly mounted on the outer side wall of the top end of the top cover 18, an annular connecting plate 22 is fixedly mounted on the bottom wall of the annular mounting plate 21, the bottom end of the annular connecting plate 22 is inserted on the top wall of the annular sealing plate 17, an annular connecting groove, the heating lamps 16 and the retort 3 are sealed in the annular sealing plate 17 by mounting the top cover 18 on the top end of the retort 3 and inserting the annular connecting plate 22 into the corresponding annular connecting groove.
The utility model discloses in, install top cap 18 on distillation container 3's top and insert corresponding annular connecting groove with annular connecting plate 22 during the use, just can seal heating lamp 16 and distillation container 3 in annular seal board 17, start driving motor 11, driving motor 11 can drive pivot 12 and drive toothed disc 13 and rotate, toothed disc 13 and 4 intermeshing gears of annular carousel, consequently toothed disc 13 rotates and to drive annular carousel 4, installation pole 15 and heating lamp 16 rotate around distillation container 3, thereby can carry out the even heating to distillation container 3.
Further, unless otherwise specifically stated or limited, the above-described fixed connection is to be understood in a broad sense, and may be, for example, welded, glued, or integrally formed as is conventional in the art.
It is noted that, herein, relational terms such as first and second, and the like may be used solely to distinguish one entity or action from another entity or action without necessarily requiring or implying any actual such relationship or order between such entities or actions. Also, the terms "comprises," "comprising," or any other variation thereof, are intended to cover a non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such process, method, article, or apparatus.
The above, only be the concrete implementation of the preferred embodiment of the present invention, but the protection scope of the present invention is not limited thereto, and any person skilled in the art is in the technical scope of the present invention, according to the technical solution of the present invention and the utility model, the concept of which is equivalent to replace or change, should be covered within the protection scope of the present invention.
Claims (5)
1. The utility model provides a prepare drying device of ruthenium trichloride, includes base (1), its characterized in that: the distillation container is characterized in that a mounting plate (2) is fixedly mounted on the top wall of the base (1), a distillation container (3) is fixedly mounted on the top wall of the mounting plate (2), an annular rotary table (4) is rotatably mounted at the top end of the base (1), the annular rotary table (4) is detachably mounted on the outer side wall of the mounting plate (2), an annular bottom plate (5) is fixedly mounted on the bottom wall of the annular rotary table (4), an annular movable groove matched with the annular bottom plate (5) is formed in the top wall of the base (1), two limiting blocks (6) are symmetrically and movably mounted on the inner side wall of the annular rotary table (4), one ends of the limiting blocks (6) are inserted into the mounting plate (2), annular limiting grooves matched with the two limiting blocks (6) are formed in the outer side wall of the mounting plate (2), and a driving device is connected to the annular rotary table, fixed mounting has a plurality of installation poles (15) on the roof of annular carousel (4), every all install a plurality of heating lamps (16) on installation pole (15), fixed mounting has annular seal board (17) on the roof of annular carousel (4), and distillation container (3), installation pole (15) and heating lamps (16) all are located annular seal board (17), the top dismantlement of distillation container (3) is installed top cap (18), it is equipped with pipe (19) to insert on the roof of top cap (18), and pipe (19) and distillation container (3) communicate each other, fixed mounting has handle (20) on the roof of top cap (18), install the sealing device who mutually supports with annular seal board (17) on top cap (18).
2. The drying device for preparing ruthenium trichloride according to claim 1, wherein: two mounting grooves (7) of mutually supporting with stopper (6) are seted up to the symmetry on the inside wall of annular carousel (4), two equal fixed mounting has threaded rod (8) on the roof of stopper (6), and the top of threaded rod (8) all runs through the roof of annular carousel (4) and extends to the upside of annular carousel (4), two movable groove (9) of mutually supporting with threaded rod (8), two are seted up to the symmetry on the roof of annular carousel (4) equal threaded connection has fastening nut (10) on the lateral wall on threaded rod (8) top, and the diameter of fastening nut (10) all is greater than the width of movable groove (9).
3. The drying device for preparing ruthenium trichloride according to claim 1, wherein: drive arrangement includes driving motor (11) of fixed mounting in base (1) one side, the output fixed mounting of driving motor (11) has pivot (12), the top fixed mounting of pivot (12) has toothed disc (13), evenly set up the gear with toothed disc (13) intermeshing on the lateral wall of annular carousel (4).
4. The drying device for preparing ruthenium trichloride according to claim 1, wherein: a plurality of balls (14) are uniformly installed on the top wall of the base (1), and the balls (14) are in mutual contact with the annular turntable (4).
5. The drying device for preparing ruthenium trichloride according to claim 1, wherein: the sealing device comprises an annular mounting plate (21) fixedly mounted on the outer side wall of the top end of the top cover (18), an annular connecting plate (22) is fixedly mounted on the bottom wall of the annular mounting plate (21), the bottom end of the annular connecting plate (22) is inserted into the top wall of the annular sealing plate (17), and an annular connecting groove matched with the annular connecting plate (22) is formed in the top wall of the annular sealing plate (17).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201922401320.9U CN211486584U (en) | 2019-12-27 | 2019-12-27 | Drying device for preparing ruthenium trichloride |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201922401320.9U CN211486584U (en) | 2019-12-27 | 2019-12-27 | Drying device for preparing ruthenium trichloride |
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| CN211486584U true CN211486584U (en) | 2020-09-15 |
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| CN201922401320.9U Active CN211486584U (en) | 2019-12-27 | 2019-12-27 | Drying device for preparing ruthenium trichloride |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115031156A (en) * | 2022-05-09 | 2022-09-09 | 北京天海低温设备有限公司 | Automatic sand filling system of low-temperature storage tank |
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2019
- 2019-12-27 CN CN201922401320.9U patent/CN211486584U/en active Active
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115031156A (en) * | 2022-05-09 | 2022-09-09 | 北京天海低温设备有限公司 | Automatic sand filling system of low-temperature storage tank |
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