CN114886821A - Hair nourishing essence and preparation method thereof - Google Patents

Hair nourishing essence and preparation method thereof Download PDF

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Publication number
CN114886821A
CN114886821A CN202210669235.4A CN202210669235A CN114886821A CN 114886821 A CN114886821 A CN 114886821A CN 202210669235 A CN202210669235 A CN 202210669235A CN 114886821 A CN114886821 A CN 114886821A
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parts
extract
hair
essence
heating
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CN114886821B (en
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平荷梅
钟向阳
章华东
章旦红
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Zhejiang Savol Health & Beauty Hair Industry Co ltd
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Zhejiang Savol Health & Beauty Hair Industry Co ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/36Carboxylic acids; Salts or anhydrides thereof
    • A61K8/365Hydroxycarboxylic acids; Ketocarboxylic acids
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/44Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/67Vitamins
    • A61K8/673Vitamin B group
    • A61K8/675Vitamin B3 or vitamin B3 active, e.g. nicotinamide, nicotinic acid, nicotinyl aldehyde
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9728Fungi, e.g. yeasts
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00Preparations for care of the hair
    • A61Q5/002Preparations for repairing the hair, e.g. hair cure
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00Preparations for care of the hair
    • A61Q5/004Preparations used to protect coloured hair
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00Preparations for care of the hair
    • A61Q5/12Preparations containing hair conditioners
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q7/00Preparations for affecting hair growth
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • A61K2800/592Mixtures of compounds complementing their respective functions
    • A61K2800/5922At least two compounds being classified in the same subclass of A61K8/18

Abstract

The invention discloses a hair nourishing essence which comprises the following raw materials in parts by weight: 15-24 parts of water, 5-8 parts of cetearyl alcohol, 2-3 parts of an antistatic agent, 3-5 parts of ethylhexyl palmitate, 4-6 parts of propylene glycol, 4-6 parts of polydimethylsiloxane, 5-7 parts of ethanol, 0.3-0.8 part of essence, 2-5 parts of acrylate copolymer, 2-4 parts of hydrolyzed wheat protein, 0.1-0.4 part of citric acid, 0.08-0.18 part of shea butter fruit resin extract, 0.06-0.12 part of polygonum multiflorum root extract, 0.06-0.2 part of olive oil fruit extract, 0.08-0.26 part of silk amino acid, 0.06-0.14 part of ginseng root extract, 0.18-0.28 part of eclipta prostrata leaf extract, 0.04-0.16 part of black mulberry fruit extract, 0.04-0.12 part of ganoderma lucidum stem extract, 0.18-0.3 part of nicotinamide and 0.18-0.32 part of preservative. The hair nourishing essence disclosed by the invention can effectively repair damaged hair after hair dyeing, increases the dry and wet combing performance of hair and has a good color fixing and protecting effect.

Description

Hair nourishing essence and preparation method thereof
Technical Field
The invention relates to the technical field of hair care products, and particularly relates to a hair nourishing essence and a preparation method thereof.
Background
Along with the improvement of living standard, the pursuit of external image by people is not only simple and tidy and elegant, but also the color of clothes is changeable, and a plurality of designs are added on hair color, the hair color is usually dyed by hair dye, however, because chemical preparations are added in the hair dye, the damage of the hair by dyeing is large, the hair is easy to be withered, knotted, broken and not easy to comb, and the hair is seriously faded after being washed for many times after being dyed, so the design of the essence for repairing and maintaining the dyed hair has important significance.
Disclosure of Invention
An object of the present invention is to solve at least the above problems and to provide at least the advantages described later.
The invention also aims to provide the hair nourishing essence which is prepared by adding citric acid, ginseng root extract and black mulberry extract into the components to increase the toughness of hair, prevent hair from breaking, improve the dry and wet combing performance of hair and simultaneously achieve the purposes of color protection and fixation through the synergistic effect of the eclipta prostrata leaf extract, nicotinamide and citric acid.
To achieve these objects and other advantages in accordance with the present invention, there is provided a hair nourishing essence comprising the following raw materials in parts by weight:
15-24 parts of water, 5-8 parts of cetearyl alcohol, 2-3 parts of an antistatic agent, 3-5 parts of ethylhexyl palmitate, 4-6 parts of propylene glycol, 4-6 parts of polydimethylsiloxane, 5-7 parts of ethanol, 0.3-0.8 part of essence, 2-5 parts of acrylate copolymer, 2-4 parts of hydrolyzed wheat protein, 0.1-0.4 part of citric acid, 0.08-0.18 part of shea butter fruit resin extract, 0.06-0.12 part of polygonum multiflorum root extract, 0.06-0.2 part of olive oil fruit extract, 0.08-0.26 part of silk amino acid, 0.06-0.14 part of ginseng root extract, 0.18-0.28 part of eclipta prostrata leaf extract, 0.04-0.16 part of black mulberry fruit extract, 0.04-0.12 part of ganoderma lucidum stem extract, 0.18-0.3 part of nicotinamide and 0.18-0.32 part of preservative.
Preferably, in the hair nourishing essence, the antistatic agent is stearyl trimethyl ammonium chloride or polyquaternium-7.
Preferably, in the hair nourishing essence, the silk amino acids comprise at least two of serine, alanine, glycine and tyrosine.
Preferably, in the hair nourishing essence, the essence is: one of mint essence, green tea essence and rose essence.
Preferably, in the hair nourishing essence, the preservative is kasong.
The cason in the invention is a mixture of methylchloroisothiazolinone, methylisothiazolinone, magnesium chloride and magnesium nitrate, wherein the weight ratio of the methylchloroisothiazolinone to the methylisothiazolinone is 3: 1.
The invention also provides a preparation method of the hair nourishing essence, which comprises the following steps:
step one, adding 1/3 water into a certain proportion of polydimethylsiloxane, heating to 30-45 ℃, stirring and mixing for 15-25 min, sequentially adding 1/4 certain proportion of citric acid, certain proportion of ginseng root extract, black mulberry extract, shea butter fruit resin extract, polygonum multiflorum root extract, olive fruit extract, silk amino acids and ganoderma lucidum stem extract while stirring and mixing for 10-20 min, uniformly mixing, and standing for 30-60 min to obtain a first conditioner;
step two, mixing propylene glycol, hydrolyzed wheat protein and acrylate copolymer in proportion, adding ethanol in proportion, heating to 35-50 ℃, stirring and mixing for 15-25 min, adding water in proportion of 1/3, continuously stirring and mixing for 15-35 min at constant temperature, then adding citric acid in proportion of 3/4, eclipta prostrata leaf extract in proportion and nicotinamide in proportion, heating to 50-55 ℃, stirring for 10-20 min, uniformly mixing, and standing for 30-60 min to obtain a second conditioner;
mixing cetearyl alcohol and ethyl palmitate in proportion to form an oil phase, mixing water in 1/3 proportion and an antistatic agent in proportion to form a water phase, respectively heating to 80-85 ℃, adding the water phase into the oil phase to emulsify for 3-5 min, and cooling to obtain an emulsion matrix;
and step four, sequentially adding the first conditioner, the second conditioner, the preservative and the essence into the emulsion matrix, stirring while adding, uniformly mixing, and standing at normal temperature for 20-35 min to obtain the hair nourishing essence.
Preferably, in the preparation method of the hair nourishing essence, the preparation method of the snakehead gut leaf extract comprises the following steps: cleaning and airing the snakehead gut leaves with clear water, adding an ethanol solution with the volume of 1.2-1.5 times of that of the snakehead gut leaves, heating to 45-55 ℃, preserving heat and stirring for 15-30 min, filtering to obtain a first extracting solution, adding an ethanol solution with the volume of 1.2-1.5 times of that of the rest solid, heating to 45-55 ℃, preserving heat and stirring for 30-60 min, filtering to obtain a second extracting solution, adding an ethanol solution with the volume of 1.2-1.5 times of that of the rest solid, heating to 35-40 ℃, preserving heat and stirring for 60-80 min, filtering to obtain a third extracting solution, mixing and heating the first extracting solution, the second extracting solution and the third extracting solution until the volumes are concentrated to 0.5-0.6 time of the volumes of all ethanol solutions, and filtering to obtain the snakehead gut leaf extract.
Preferably, in the preparation method of the hair nourishing essence, the preparation method of the ginseng root extract comprises the following steps: weighing a proper amount of ginseng root, drying, crushing, adding water with the volume being 3-5 times of that of the ginseng root and the temperature of 50-60 ℃, soaking for 30-60 min, heating, decocting and extracting for 2-3 h, filtering, heating and concentrating the filtrate until the volume of the filtrate is equal to that of ginseng root powder, and obtaining the ginseng root extract.
The invention at least comprises the following beneficial effects:
the shea butter fruit resin extract is a pure natural product extracted from plants, has the effects of moisturizing and moistening, can be used in personal care and cleaning products, has a good conditioning effect on hair and skin, makes the hair and the skin soft and smooth, can deeply nourish the hair, and can permanently lock water for cells.
The polygonum multiflorum is a precious traditional Chinese medicine, and the extract of the polygonum multiflorum is added into hair washing and caring products to achieve the effects of hair nourishing, hair blacking and hair nourishing.
The olive fruit extract has the main functions of relieving, resisting allergy, resisting inflammation, whitening and removing freckles in the washing and protecting products.
The silk amino acids can provide essential nutrients for skin and hair, and keep skin and hair moist and glossy.
The hair care product can expand the capillary vessels of the head, increase the nutrition of the hair, improve the toughness of the hair, reduce the hair loss and the hair breakage and has the protection effect on the damaged hair.
The black mulberry extract mainly has the effects of skin conditioner, anti-inflammatory agent, antioxidant and whitening agent in cosmetics and skin care products, and can promote blood circulation, strengthen hair roots and prevent alopecia.
Citric acid can be used for neutralizing alkaline hair, refreshing hair, and softening scalp, and has effects in promoting blood circulation, preventing thin hair and alopecia, and improving split hair and broken hair.
The snakehead intestine is also called eclipta and medicinal herbs, has the functions of cooling blood, stopping bleeding, nourishing liver and kidney and clearing heat and toxic materials, is used for treating odontoseisis and early white beard and hair, and can be used as a skin conditioner in cosmetics.
The nicotinamide can repair damaged stratum corneum lipid barrier, improve skin resistance, improve skin darkness, and promote hair growth.
The Ganoderma lucidum stem extract has the main functions of an antioxidant, an anti-inflammatory agent, whitening and freckle removing in cosmetics and skin care products. Ganoderma lucidum is one of Ganoderma lucidum, has effects of promoting the generation of collagen and ceramide, enhancing skin cell metabolism, and has effects of resisting wrinkle and antiaging by combining its antioxidation; has activating effect on luciferase and shows anti-inflammatory effect; has the effect of inhibiting tyrosinase, can whiten the skin, and has more obvious whitening effect by combining the moisturizing capability of the skin.
According to the invention, the citric acid, the ginseng root extract and the black mulberry extract are added to perform synergistic action so as to enhance the toughness of the hair, improve the bifurcation, strengthen the hair root, enhance the effects of preventing the hair from being broken and preventing the hair from falling off, and effectively improve the dry and wet combing performance of the hair; the synergistic effect of the eclipta prostrata leaf extract, the nicotinamide and the citric acid is added, so that the adhesion capability of the pigment in the coloring agent on the hair cortex is increased, and the purposes of color protection and color fixation are achieved; the hair nourishing essence disclosed by the invention can effectively repair damaged and beautiful hair after hair dyeing, improves the defect that the hair is easy to break due to withered, split and alopecia, enables the hair to be elastic, moist and glossy, has a good consolidation effect on the color of the dyed hair, and enables the hair not to fade easily.
Additional advantages, objects, and features of the invention will be set forth in part in the description which follows and in part will become apparent to those having ordinary skill in the art upon examination of the following or may be learned from practice of the invention.
Detailed Description
The present invention is further described in detail with reference to specific examples, so that those skilled in the art can implement the invention with reference to the description.
It will be understood that terms such as "having," "including," and "comprising," as used herein, do not preclude the presence or addition of one or more other elements or groups thereof.
It is to be noted that the experimental methods described in the following embodiments are all conventional methods unless otherwise specified, and the reagents and materials are commercially available unless otherwise specified. In the description of the present invention, it should be noted that unless otherwise explicitly stated or limited, the terms "mounted," "connected" and "disposed" are to be construed broadly and can be, for example, fixedly connected, disposed, detachably connected, disposed or integrally connected and disposed. The specific meanings of the above terms in the present invention can be understood in specific cases to those skilled in the art. The terms "transverse," "longitudinal," "upper," "lower," "front," "rear," "left," "right," "vertical," "horizontal," "top," "bottom," "inner," "outer," and the like are used in the indicated orientations and positional relationships to indicate orientations and positional relationships based on those shown, merely to facilitate description of the invention and to simplify description, and do not indicate or imply that the referenced devices or elements must have a particular orientation, be constructed and operated in a particular orientation, and are therefore not to be construed as limiting the present invention.
Example 1
Preparing the hair nourishing essence:
taking 4 parts by weight of polydimethylsiloxane, adding 5 parts by weight of water, heating to 30 ℃, stirring and mixing for 15min, sequentially adding 0.025 part by weight of citric acid, 0.06 part by weight of ginseng root extract, 0.04 part by weight of black mulberry extract, 0.08 part by weight of shea butter extract, 0.06 part by weight of polygonum multiflorum root extract, 0.06 part by weight of olive fruit extract, 0.08 part by weight of mixture of serine and tyrosine and 0.04 part by weight of ganoderma lucidum stem extract, stirring and mixing for 10min while adding, uniformly mixing, and standing for 30min to obtain a first conditioner;
step two, mixing 4 parts by weight of propylene glycol, 2 parts by weight of hydrolyzed wheat protein and 2 parts by weight of acrylate copolymer, adding 5 parts by weight of ethanol, heating to 35 ℃, stirring and mixing for 15min, adding 5 parts by weight of water, continuously stirring and mixing for 15min at constant temperature, then adding 0.075 part by weight of citric acid, 0.18 part by weight of eclipta prostrata leaf extract and 0.18 part by weight of nicotinamide, heating to 50 ℃, stirring for 10min, uniformly mixing, and standing for 30min to obtain a second conditioner;
mixing 5 parts by weight of cetearyl alcohol and 3 parts by weight of ethylhexyl palmitate to obtain an oil phase, mixing 5 parts by weight of water and 2 parts by weight of polyquaternium-7 to obtain a water phase, respectively heating to 80-85 ℃, adding the water phase into the oil phase to emulsify for 3-5 min, and cooling to obtain an emulsion matrix;
and step four, sequentially adding the first conditioner, the second conditioner, 0.18 part by weight of the kasong and 0.3 part by weight of the green tea essence into the emulsion matrix, stirring while adding, uniformly mixing, and standing at normal temperature for 20min to obtain the hair nourishing essence.
The preparation method of the snakehead gut leaf extract comprises the following steps: cleaning eclipta prostrata leaves with clear water, drying in the air, adding an ethanol solution with the volume 1.2 times of the eclipta prostrata leaves, heating to 45 ℃, preserving heat and stirring for 30min, filtering to obtain a first extracting solution, adding an ethanol solution with the volume 1.2 times of the remaining solid, heating to 45 ℃, preserving heat and stirring for 60min, filtering to obtain a second extracting solution, adding an ethanol solution with the volume 1.2 times of the remaining solid, heating to 35 ℃, preserving heat and stirring for 80min, filtering to obtain a third extracting solution, mixing and heating the first extracting solution, the second extracting solution and the third extracting solution until the volumes are concentrated to 0.5 time of the volumes of all the ethanol solutions, and filtering to obtain eclipta prostrata leaf extracts;
the preparation method of the ginseng root extract comprises the following steps: weighing appropriate amount of Ginseng radix, drying, pulverizing, adding 3 times of 50 deg.C water, soaking for 60min, heating, decocting for 2 hr, filtering, and heating and concentrating the filtrate to equal volume with Ginseng radix powder to obtain Ginseng radix extract.
Example 2
Preparing the hair nourishing essence:
taking 5 parts by weight of polydimethylsiloxane, adding 6.5 parts by weight of water, heating to 40 ℃, stirring and mixing for 20min, sequentially adding 0.0625 part by weight of citric acid, 0.1 part by weight of ginseng root extract, 0.1 part by weight of black mulberry extract, 0.13 part by weight of shea butter fruit resin extract, 0.09 part by weight of polygonum multiflorum root extract, 0.13 part by weight of olive fruit extract, 0.17 part by weight of mixture of serine, alanine, glycine and tyrosine, and 0.08 part by weight of ganoderma lucidum stem extract, stirring and mixing for 15min while adding, uniformly mixing, and standing for 45min to obtain a first conditioner;
step two, mixing 5 parts by weight of propylene glycol, 3 parts by weight of hydrolyzed wheat protein and 3.5 parts by weight of acrylate copolymer, adding 6 parts by weight of ethanol, heating to 40 ℃, stirring and mixing for 20min, adding 6.5 parts by weight of water, continuously stirring and mixing for 25min at constant temperature, then adding 0.1875 part by weight of citric acid, 0.23 part by weight of eclipta prostrata leaf extract and 0.24 part by weight of nicotinamide, heating to 53 ℃, stirring for 15min, uniformly mixing, and standing for 45min to obtain a second conditioner;
mixing 6.5 parts by weight of cetearyl alcohol and 4 parts by weight of ethylhexyl palmitate to obtain an oil phase, mixing 6.5 parts by weight of water and 2.5 parts by weight of stearyltrimethyl ammonium chloride to obtain a water phase, respectively heating to 80-85 ℃, adding the water phase into the oil phase to emulsify for 3-5 min, and cooling to obtain an emulsion matrix;
and step four, sequentially adding the first conditioner, the second conditioner, 0.25 weight part of kasong and 0.55 weight part of mint essence into the emulsion matrix, stirring while adding, uniformly mixing, and standing at normal temperature for 28min to obtain the hair nourishing essence.
The preparation method of the snakehead gut leaf extract comprises the following steps: cleaning eclipta prostrata leaves with clear water, airing, adding an ethanol solution with the volume being 1.35 times of the eclipta prostrata leaves, heating to 50 ℃, preserving heat and stirring for 23min, filtering to obtain a first extracting solution, adding an ethanol solution with the volume being 1.35 times of the volume of the rest solid, heating to 50 ℃, preserving heat and stirring for 45min, filtering to obtain a second extracting solution, adding an ethanol solution with the volume being 1.35 times of the volume of the rest solid, heating to 38 ℃, preserving heat and stirring for 70min, filtering to obtain a third extracting solution, mixing the first extracting solution, the second extracting solution and the third extracting solution, heating to the volume concentration of the first extracting solution, the second extracting solution and the third extracting solution until the volume is 0.55 times of the volume of all the ethanol solution is added, and filtering to obtain eclipta prostipta prostrata extract;
the preparation method of the ginseng root extract comprises the following steps: weighing a proper amount of ginseng root, drying, crushing, adding 4 times of volume of 55 ℃ water for soaking for 45min, then heating, decocting and extracting for 2.5h, filtering, heating and concentrating the filtrate until the volume of the filtrate is equal to that of ginseng root powder, thus obtaining the ginseng root extract.
Example 3
Preparing the hair nourishing essence:
step one, adding 8 parts by weight of water into 6 parts by weight of polydimethylsiloxane, heating to 45 ℃, stirring and mixing for 25min, sequentially adding 0.1 part by weight of citric acid, 0.14 part by weight of ginseng root extract, 0.16 part by weight of black mulberry extract, 0.18 part by weight of shea butter fruit resin extract, 0.12 part by weight of polygonum multiflorum root extract, 0.2 part by weight of olive fruit extract, 0.26 part by weight of mixture of serine, alanine and tyrosine, and 0.12 part by weight of ganoderma lucidum stem extract, stirring and mixing for 20min while adding, uniformly mixing, and standing for 60min to obtain a first conditioner;
step two, mixing 6 parts by weight of propylene glycol, 4 parts by weight of hydrolyzed wheat protein and 5 parts by weight of acrylate copolymer, adding 7 parts by weight of ethanol, heating to 50 ℃, stirring and mixing for 25min, adding 8 parts by weight of water, continuously stirring and mixing for 35min at constant temperature, then adding 0.3 part by weight of citric acid, 0.28 part by weight of eclipta prostrata leaf extract and 0.3 part by weight of nicotinamide, heating to 55 ℃, stirring for 20min, uniformly mixing, and standing for 60min to obtain a second conditioner;
mixing 8 parts by weight of cetearyl alcohol and 3 parts by weight of ethylhexyl palmitate to obtain an oil phase, mixing 8 parts by weight of water and 3 parts by weight of stearyltrimethyl ammonium chloride to obtain a water phase, respectively heating to 80-85 ℃, adding the water phase into the oil phase to emulsify for 3-5 min, and cooling to obtain an emulsion matrix;
and step four, sequentially adding the first conditioner, the second conditioner, 0.32 weight part of kasong and 0.8 weight part of rose essence into the emulsion matrix, stirring while adding, uniformly mixing, and standing at normal temperature for 35min to obtain the hair nourishing essence.
The preparation method of the snakehead gut leaf extract comprises the following steps: cleaning eclipta prostrata leaves with clear water, drying in the air, adding an ethanol solution with the volume 1.5 times of the eclipta prostrata leaves, heating to 55 ℃, preserving heat and stirring for 15min, filtering to obtain a first extracting solution, adding an ethanol solution with the volume 1.5 times of the remaining solid, heating to 55 ℃, preserving heat and stirring for 30min, filtering to obtain a second extracting solution, adding an ethanol solution with the volume 1.5 times of the remaining solid, heating to 40 ℃, preserving heat and stirring for 60min, filtering to obtain a third extracting solution, mixing and heating the first extracting solution, the second extracting solution and the third extracting solution until the volumes are concentrated to 0.6 time of the volumes of all the ethanol solutions, and filtering to obtain eclipta prostrata leaf extracts;
the preparation method of the ginseng root extract comprises the following steps: weighing a proper amount of ginseng root, drying, crushing, adding 5 times of water with the volume of 60 ℃ for soaking for 30min, then heating, decocting and extracting for 3h, filtering, heating and concentrating the filtrate until the volume of the filtrate is equal to that of the ginseng root powder, thus obtaining the ginseng root extract.
The products of the above embodiments are all proper in viscosity, cool and comfortable, good in stability, fragrant in smell, fine and uniform.
The products of the above examples were subjected to irritation experiments, allergy experiments: the hair of the back of the white mouse is cut off, and the hair nourishing essence product is respectively coated on the cut-off part and the non-coated part, so that no irritation and anaphylactic reaction are caused. A proper amount of the hair nourishing essence product is taken and put on the hand of a volunteer (25-65 years old, 150 persons), and after 40 minutes, the phenomena of redness, eruption and bubbles are avoided.
The use method of the hair nourishing essence comprises the following steps: after washing hair and wetting hair, smearing a proper amount of the product on the hair, rubbing for 2-5 minutes, and washing with clear water.
Comparative example 1:
the difference from example 2 is that no ginseng root extract or no black mulberry extract is contained in the ingredients.
Comparative example 2:
the difference from the example 2 is that no citric acid and no black mulberry extract are contained in the components.
Comparative example 3:
the difference from example 2 is that no ginseng root extract and no citric acid are contained in the ingredients.
Comparative example 4:
the same as example 2, except that no black mulberry extract was contained in the composition.
Comparative example 5:
the same as example 2, except that no ginseng root extract was contained in the composition.
Comparative example 6:
the difference from example 2 is that no citric acid is present in the composition.
Comparative example 7:
the same as example 2, except that the snakehead leaf extract was contained in the composition.
Comparative example 8
The same as example 2 except that no nicotinamide was present in the composition.
Comparative example 9
The same as example 2, except that the components contained in the composition were citric acid-free and snakehead gut leaf extract-free.
Comparative example 10
The difference is that no citric acid and no nicotinamide are contained in the components as in example 2.
Comparative example 11
The same as example 2, except that the ingredients contained smokeless amide and snakehead gut leaf extract.
Comparative example 12
The difference from the example 2 is that the second step is: mixing 5 parts by weight of propylene glycol, 3 parts by weight of hydrolyzed wheat protein, 3.5 parts by weight of acrylate copolymer, 0.1875 part by weight of citric acid, 0.23 part by weight of eclipta prostrata leaf extract and 0.24 part by weight of nicotinamide, adding 6 parts by weight of ethanol, heating to 40 ℃, stirring and mixing for 20min, adding 6.5 parts by weight of water, continuously stirring and mixing for 25min at constant temperature, heating to 53 ℃, stirring for 15min, uniformly mixing, and standing for 45min to obtain the second conditioner.
Comparative example 13
Is a common commercial hair conditioner.
Sensory evaluation was performed on the hair care comprehensive effects of the hair care products (hair tonic essence, hair conditioner, etc.) in the above examples and comparative examples: 390 colored (including newly colored and colored) people in the age range of 25-65 years are selected as trial objects by adopting a civil survey grading method, are randomly and equally divided into 13 groups (each group contains the newly colored and colored people), and the hair is respectively treated by the hair care products in the above examples and comparative examples. After washing hair twice a week, the hair is nursed for three months. The total using effect of each item is 10 points, the higher the score is, the better the sensory effect is: 10 points are the highest points, which means that the product is good and very satisfactory; preferably 8 minutes or more; scores of 6 and above are acceptable; when the amount is less than 6 points, the results are not acceptable. The average score of each item is as follows. The color protection effect is that the smaller the hair color change is, the higher the score is, the larger the color change is, the more serious the hair color loss is, the lower the score is, the scoring result is shown in table 1:
TABLE 1
Wet combing property Dry combing property Moisture retention Gloss of Color protection effect
Example 1 10 10 10 10 10
Example 2 10 10 10 10 10
Example 3 10 10 10 10 10
Comparative example 1 5 7 10 10 10
Comparative example 2 7 7 10 10 10
Comparative example 3 7 7 10 10 10
Comparative example 4 7 7 10 10 10
Comparative example 5 7 7 10 10 10
Comparative example 6 7 7 10 10 5
Comparative example 7 10 10 10 9 5
Comparative example 8 10 10 10 10 5
Comparative example 9 10 10 10 9 4
Comparative example 10 10 10 10 10 5
Comparative example 11 10 10 10 9 5
Comparative example 12 10 10 10 10 7
Comparative example 13 6 6 6 7 3
Through the analysis of the evaluation results in the table 1, the comparison of the evaluation score results of the examples 1-3 and the comparative example 13 shows that the product of the invention has much better use experience compared with the common hair conditioner products sold in the market, wherein the dry and wet combing performance, the moisture retention performance, the glossiness and the color protection effect are all increased, and particularly, the color protection effect is obviously better than that of the common products sold in the market;
the hair care product is characterized in that multiple nutrient substances are added to the hair care product to provide multiple nutrients and repair components for hair, especially, the ginseng root extract, the black mulberry fruit extract, the citric acid, the snakehead intestine leaf extract and the nicotinamide are added, and the ginseng root extract, the black mulberry fruit extract and the citric acid have synergistic effect to improve the dry and wet combing performance of the hair care product on the hair through the evaluation result analysis of the embodiment 2 and the comparative examples 1-6; although the ginseng extract, the black mulberry extract and the citric acid have the hair loss or hair breakage preventing performance and can indirectly improve the hair combing performance, the effect is not obvious or even poor when the ginseng extract, the black mulberry extract and the citric acid are independently used or added, and only in the product disclosed by the invention, when the ginseng extract, the black mulberry extract and the citric acid are used, the sensory evaluation effect of the dry and wet combing performance of the hair is greatly increased, so that the hair breakage and hair loss preventing effect is increased under the synergistic effect of the ginseng extract, the black mulberry extract and the citric acid, and the toughness of the hair is increased, so that the dry and wet combing performance of the hair is greatly increased;
the evaluation results of the embodiment 2, the comparative examples 6 to 11 and the comparative example 13 are analyzed, when one or two of the citric acid, the snakehead gut leaf extract and the nicotinamide exist, although the color protection effect is increased compared with that of the commercially available hair care product, the color protection effect cannot be accepted by users, only after the citric acid, the snakehead gut leaf extract and the nicotinamide are added simultaneously in the product, the color protection effect score of the hair care product is obviously and greatly improved, because the three-component synergistic effect can greatly increase the adhesion capability of the pigment in the coloring agent on a hair cortex layer, so that the pigment cannot easily and quickly separate from the hair, and the purpose of color protection and fixation is achieved;
from the analysis of the evaluation results of example 2 and comparative example 12, the color-protecting effect is reduced after changing the preparation mode of the second conditioner, namely changing the mode of adding the citric acid, the eclipta prostrata leaf extract and the nicotinamide into the product of the invention, and only the oxidation essence prepared by the method of the invention can achieve the satisfactory color-fixing and color-protecting effect.
The number of apparatuses and the scale of the process described herein are intended to simplify the description of the present invention. Applications, modifications and variations of the present invention will be apparent to those skilled in the art.
While embodiments of the invention have been described above, it is not limited to the applications set forth in the description and the embodiments, which are fully applicable to various fields of endeavor for which the invention may be embodied with additional modifications as would be readily apparent to those skilled in the art, and the invention is therefore not limited to the details given herein and to the embodiments shown and described without departing from the generic concept as defined by the claims and their equivalents.

Claims (8)

1. The hair nourishing essence is characterized by comprising the following raw materials in parts by weight:
15-24 parts of water, 5-8 parts of cetearyl alcohol, 2-3 parts of an antistatic agent, 3-5 parts of ethylhexyl palmitate, 4-6 parts of propylene glycol, 4-6 parts of polydimethylsiloxane, 5-7 parts of ethanol, 0.3-0.8 part of essence, 2-5 parts of acrylate copolymer, 2-4 parts of hydrolyzed wheat protein, 0.1-0.4 part of citric acid, 0.08-0.18 part of shea butter fruit resin extract, 0.06-0.12 part of polygonum multiflorum root extract, 0.06-0.2 part of olive oil fruit extract, 0.08-0.26 part of silk amino acid, 0.06-0.14 part of ginseng root extract, 0.18-0.28 part of eclipta prostrata leaf extract, 0.04-0.16 part of black mulberry fruit extract, 0.04-0.12 part of ganoderma lucidum stem extract, 0.18-0.3 part of nicotinamide and 0.18-0.32 part of preservative.
2. The hair nourishing essence according to claim 1, wherein the antistatic agent is stearyltrimethylammonium chloride or polyquaternium-7.
3. The hair nourishing essence of claim 1 wherein the silk amino acids comprise at least two of serine, alanine, glycine, tyrosine.
4. The hair nourishing essence of claim 1, wherein the essence is: one of mint essence, green tea essence and rose essence.
5. The hair nourishing essence of claim 1 wherein the preservative is cason.
6. The method for preparing the hair nourishing essence according to any one of claims 1 to 5, comprising the following steps:
step one, adding 1/3 water into a certain proportion of polydimethylsiloxane, heating to 30-45 ℃, stirring and mixing for 15-25 min, sequentially adding 1/4 certain proportion of citric acid, certain proportion of ginseng root extract, black mulberry extract, shea butter fruit resin extract, polygonum multiflorum root extract, olive fruit extract, silk amino acids and ganoderma lucidum stem extract while stirring and mixing for 10-20 min, uniformly mixing, and standing for 30-60 min to obtain a first conditioner;
step two, mixing propylene glycol, hydrolyzed wheat protein and acrylate copolymer in proportion, adding ethanol in proportion, heating to 35-50 ℃, stirring and mixing for 15-25 min, adding water in proportion of 1/3, continuously stirring and mixing for 15-35 min at constant temperature, then adding citric acid in proportion of 3/4, eclipta prostrata leaf extract in proportion and nicotinamide in proportion, heating to 50-55 ℃, stirring for 10-20 min, uniformly mixing, and standing for 30-60 min to obtain a second conditioner;
mixing cetearyl alcohol and ethyl palmitate in proportion to form an oil phase, mixing water in 1/3 proportion and an antistatic agent in proportion to form a water phase, respectively heating to 80-85 ℃, adding the water phase into the oil phase to emulsify for 3-5 min, and cooling to obtain an emulsion matrix;
and step four, sequentially adding the first conditioner, the second conditioner, the preservative and the essence into the emulsion matrix, stirring while adding, uniformly mixing, and standing at normal temperature for 20-35 min to obtain the hair nourishing essence.
7. The method for preparing the hair nourishing essence according to claim 6, wherein the method for preparing the snakehead leaf extract comprises the following steps: cleaning and airing the snakehead gut leaves with clear water, adding an ethanol solution with the volume of 1.2-1.5 times of that of the snakehead gut leaves, heating to 45-55 ℃, preserving heat and stirring for 15-30 min, filtering to obtain a first extracting solution, adding an ethanol solution with the volume of 1.2-1.5 times of that of the rest solid, heating to 45-55 ℃, preserving heat and stirring for 30-60 min, filtering to obtain a second extracting solution, adding an ethanol solution with the volume of 1.2-1.5 times of that of the rest solid, heating to 35-40 ℃, preserving heat and stirring for 60-80 min, filtering to obtain a third extracting solution, mixing and heating the first extracting solution, the second extracting solution and the third extracting solution until the volumes are concentrated to 0.5-0.6 time of the volumes of all ethanol solutions, and filtering to obtain the snakehead gut leaf extract.
8. The method of preparing the hair nourishing essence according to claim 6, wherein the ginseng root extract is prepared by: weighing a proper amount of ginseng root, drying, crushing, adding water with the volume being 3-5 times of that of the ginseng root and the temperature of 50-60 ℃, soaking for 30-60 min, heating, decocting and extracting for 2-3 h, filtering, heating and concentrating the filtrate until the volume of the filtrate is equal to that of ginseng root powder, and obtaining the ginseng root extract.
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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114796026A (en) * 2022-05-13 2022-07-29 广州千羽化妆品有限公司 Permanent wave agent with damaged hair repairing effect

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2000302653A (en) * 1999-04-27 2000-10-31 Hoyu Co Ltd Oxidative hair dye composition and hair treating agent composition for hair dyeing
CN107693460A (en) * 2017-12-01 2018-02-16 成都易创思生物科技有限公司 A kind of preparation method of hair conditioner

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2000302653A (en) * 1999-04-27 2000-10-31 Hoyu Co Ltd Oxidative hair dye composition and hair treating agent composition for hair dyeing
CN107693460A (en) * 2017-12-01 2018-02-16 成都易创思生物科技有限公司 A kind of preparation method of hair conditioner

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114796026A (en) * 2022-05-13 2022-07-29 广州千羽化妆品有限公司 Permanent wave agent with damaged hair repairing effect

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