CN114796084A - Camellia oil with beauty and oxidation resistance effects and preparation method thereof - Google Patents
Camellia oil with beauty and oxidation resistance effects and preparation method thereof Download PDFInfo
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- CN114796084A CN114796084A CN202210521355.XA CN202210521355A CN114796084A CN 114796084 A CN114796084 A CN 114796084A CN 202210521355 A CN202210521355 A CN 202210521355A CN 114796084 A CN114796084 A CN 114796084A
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- 239000010495 camellia oil Substances 0.000 title claims abstract description 105
- 230000000694 effects Effects 0.000 title claims abstract description 33
- 238000002360 preparation method Methods 0.000 title claims abstract description 22
- 230000003796 beauty Effects 0.000 title claims abstract description 17
- 230000003647 oxidation Effects 0.000 title claims abstract description 10
- 238000007254 oxidation reaction Methods 0.000 title claims abstract description 10
- 239000000284 extract Substances 0.000 claims abstract description 44
- 240000005959 Abelmoschus manihot Species 0.000 claims abstract description 32
- 235000001075 Abelmoschus manihot Nutrition 0.000 claims abstract description 32
- 240000001548 Camellia japonica Species 0.000 claims abstract description 25
- 235000018597 common camellia Nutrition 0.000 claims abstract description 25
- 241000168517 Haematococcus lacustris Species 0.000 claims abstract description 22
- 239000001683 mentha spicata herb oil Substances 0.000 claims abstract description 22
- 235000019721 spearmint oil Nutrition 0.000 claims abstract description 22
- JLPULHDHAOZNQI-ZTIMHPMXSA-N 1-hexadecanoyl-2-(9Z,12Z-octadecadienoyl)-sn-glycero-3-phosphocholine Chemical compound CCCCCCCCCCCCCCCC(=O)OC[C@H](COP([O-])(=O)OCC[N+](C)(C)C)OC(=O)CCCCCCC\C=C/C\C=C/CCCCC JLPULHDHAOZNQI-ZTIMHPMXSA-N 0.000 claims abstract description 17
- 244000077995 Coix lacryma jobi Species 0.000 claims abstract description 17
- 235000012907 honey Nutrition 0.000 claims abstract description 17
- 229940083466 soybean lecithin Drugs 0.000 claims abstract description 17
- 235000015112 vegetable and seed oil Nutrition 0.000 claims abstract description 17
- 239000002994 raw material Substances 0.000 claims abstract description 13
- 230000003078 antioxidant effect Effects 0.000 claims abstract description 11
- 230000003064 anti-oxidating effect Effects 0.000 claims abstract description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 17
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 16
- 238000003825 pressing Methods 0.000 claims description 16
- 238000011085 pressure filtration Methods 0.000 claims description 14
- 239000000047 product Substances 0.000 claims description 14
- 241001075517 Abelmoschus Species 0.000 claims description 13
- 238000007605 air drying Methods 0.000 claims description 12
- 238000001816 cooling Methods 0.000 claims description 12
- 238000010438 heat treatment Methods 0.000 claims description 12
- 238000002156 mixing Methods 0.000 claims description 12
- 239000000243 solution Substances 0.000 claims description 12
- 238000009210 therapy by ultrasound Methods 0.000 claims description 12
- 239000003513 alkali Substances 0.000 claims description 8
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 claims description 6
- 238000004108 freeze drying Methods 0.000 claims description 6
- 239000002244 precipitate Substances 0.000 claims description 6
- 238000003756 stirring Methods 0.000 claims description 6
- 238000005406 washing Methods 0.000 claims description 6
- 238000005303 weighing Methods 0.000 claims description 6
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 claims description 4
- 238000000227 grinding Methods 0.000 claims description 4
- 238000010790 dilution Methods 0.000 claims description 2
- 239000012895 dilution Substances 0.000 claims description 2
- 238000001035 drying Methods 0.000 claims description 2
- 239000003480 eluent Substances 0.000 claims description 2
- IDGUHHHQCWSQLU-UHFFFAOYSA-N ethanol;hydrate Chemical compound O.CCO IDGUHHHQCWSQLU-UHFFFAOYSA-N 0.000 claims description 2
- 239000012046 mixed solvent Substances 0.000 claims description 2
- 239000000843 powder Substances 0.000 claims description 2
- 238000010298 pulverizing process Methods 0.000 claims description 2
- 239000011347 resin Substances 0.000 claims description 2
- 229920005989 resin Polymers 0.000 claims description 2
- 238000002390 rotary evaporation Methods 0.000 claims description 2
- 229910000030 sodium bicarbonate Inorganic materials 0.000 claims description 2
- 235000017557 sodium bicarbonate Nutrition 0.000 claims description 2
- 238000000034 method Methods 0.000 claims 4
- 239000002537 cosmetic Substances 0.000 claims 2
- 239000003921 oil Substances 0.000 abstract description 9
- 235000019198 oils Nutrition 0.000 abstract description 9
- 229910052760 oxygen Inorganic materials 0.000 abstract description 8
- 239000001301 oxygen Substances 0.000 abstract description 8
- JEBFVOLFMLUKLF-IFPLVEIFSA-N Astaxanthin Natural products CC(=C/C=C/C(=C/C=C/C1=C(C)C(=O)C(O)CC1(C)C)/C)C=CC=C(/C)C=CC=C(/C)C=CC2=C(C)C(=O)C(O)CC2(C)C JEBFVOLFMLUKLF-IFPLVEIFSA-N 0.000 abstract description 6
- 235000013793 astaxanthin Nutrition 0.000 abstract description 6
- 239000001168 astaxanthin Substances 0.000 abstract description 6
- MQZIGYBFDRPAKN-ZWAPEEGVSA-N astaxanthin Chemical compound C([C@H](O)C(=O)C=1C)C(C)(C)C=1/C=C/C(/C)=C/C=C/C(/C)=C/C=C/C=C(C)C=CC=C(C)C=CC1=C(C)C(=O)[C@@H](O)CC1(C)C MQZIGYBFDRPAKN-ZWAPEEGVSA-N 0.000 abstract description 6
- 229940022405 astaxanthin Drugs 0.000 abstract description 6
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 abstract description 5
- 238000012423 maintenance Methods 0.000 abstract description 5
- 244000020551 Helianthus annuus Species 0.000 abstract description 3
- 235000003222 Helianthus annuus Nutrition 0.000 abstract description 3
- 230000008451 emotion Effects 0.000 abstract description 3
- 235000020238 sunflower seed Nutrition 0.000 abstract description 3
- 239000000463 material Substances 0.000 abstract description 2
- 238000012545 processing Methods 0.000 abstract description 2
- 230000001276 controlling effect Effects 0.000 description 10
- 230000009759 skin aging Effects 0.000 description 8
- 230000032683 aging Effects 0.000 description 6
- 230000001815 facial effect Effects 0.000 description 6
- 230000006872 improvement Effects 0.000 description 6
- 239000000203 mixture Substances 0.000 description 6
- 238000002474 experimental method Methods 0.000 description 5
- 230000000052 comparative effect Effects 0.000 description 4
- 239000003963 antioxidant agent Substances 0.000 description 3
- 235000006708 antioxidants Nutrition 0.000 description 3
- 230000036039 immunity Effects 0.000 description 3
- 150000008442 polyphenolic compounds Chemical class 0.000 description 3
- 235000013824 polyphenols Nutrition 0.000 description 3
- 235000021122 unsaturated fatty acids Nutrition 0.000 description 3
- 150000004670 unsaturated fatty acids Chemical class 0.000 description 3
- YYGNTYWPHWGJRM-UHFFFAOYSA-N (6E,10E,14E,18E)-2,6,10,15,19,23-hexamethyltetracosa-2,6,10,14,18,22-hexaene Chemical compound CC(C)=CCCC(C)=CCCC(C)=CCCC=C(C)CCC=C(C)CCC=C(C)C YYGNTYWPHWGJRM-UHFFFAOYSA-N 0.000 description 2
- BHEOSNUKNHRBNM-UHFFFAOYSA-N Tetramethylsqualene Natural products CC(=C)C(C)CCC(=C)C(C)CCC(C)=CCCC=C(C)CCC(C)C(=C)CCC(C)C(C)=C BHEOSNUKNHRBNM-UHFFFAOYSA-N 0.000 description 2
- 241001122767 Theaceae Species 0.000 description 2
- LRFDUPNLCDXZOE-UHFFFAOYSA-N camellianin b Chemical compound OC1C(O)C(O)C(C)OC1OC1C(O)C(O)C(OC=2C=3C(=O)C=C(OC=3C=C(O)C=2)C=2C=CC(O)=CC=2)OC1CO LRFDUPNLCDXZOE-UHFFFAOYSA-N 0.000 description 2
- HVYWMOMLDIMFJA-DPAQBDIFSA-N cholesterol Chemical compound C1C=C2C[C@@H](O)CC[C@]2(C)[C@@H]2[C@@H]1[C@@H]1CC[C@H]([C@H](C)CCCC(C)C)[C@@]1(C)CC2 HVYWMOMLDIMFJA-DPAQBDIFSA-N 0.000 description 2
- 201000010099 disease Diseases 0.000 description 2
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 2
- PRAKJMSDJKAYCZ-UHFFFAOYSA-N dodecahydrosqualene Natural products CC(C)CCCC(C)CCCC(C)CCCCC(C)CCCC(C)CCCC(C)C PRAKJMSDJKAYCZ-UHFFFAOYSA-N 0.000 description 2
- XMGQYMWWDOXHJM-UHFFFAOYSA-N limonene Chemical compound CC(=C)C1CCC(C)=CC1 XMGQYMWWDOXHJM-UHFFFAOYSA-N 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 229940031439 squalene Drugs 0.000 description 2
- TUHBEKDERLKLEC-UHFFFAOYSA-N squalene Natural products CC(=CCCC(=CCCC(=CCCC=C(/C)CCC=C(/C)CC=C(C)C)C)C)C TUHBEKDERLKLEC-UHFFFAOYSA-N 0.000 description 2
- 239000011782 vitamin Substances 0.000 description 2
- 229940088594 vitamin Drugs 0.000 description 2
- 229930003231 vitamin Natural products 0.000 description 2
- 235000013343 vitamin Nutrition 0.000 description 2
- GRWFGVWFFZKLTI-UHFFFAOYSA-N α-pinene Chemical compound CC1=CCC2C(C)(C)C1C2 GRWFGVWFFZKLTI-UHFFFAOYSA-N 0.000 description 2
- TZCPCKNHXULUIY-RGULYWFUSA-N 1,2-distearoyl-sn-glycero-3-phosphoserine Chemical compound CCCCCCCCCCCCCCCCCC(=O)OC[C@H](COP(O)(=O)OC[C@H](N)C(O)=O)OC(=O)CCCCCCCCCCCCCCCCC TZCPCKNHXULUIY-RGULYWFUSA-N 0.000 description 1
- GRWFGVWFFZKLTI-IUCAKERBSA-N 1S,5S-(-)-alpha-Pinene Natural products CC1=CC[C@@H]2C(C)(C)[C@H]1C2 GRWFGVWFFZKLTI-IUCAKERBSA-N 0.000 description 1
- CFWRDBDJAOHXSH-UHFFFAOYSA-N 2-azaniumylethyl 2,3-diacetyloxypropyl phosphate Chemical compound CC(=O)OCC(OC(C)=O)COP(O)(=O)OCCN CFWRDBDJAOHXSH-UHFFFAOYSA-N 0.000 description 1
- 241000894006 Bacteria Species 0.000 description 1
- 241000526900 Camellia oleifera Species 0.000 description 1
- 206010008570 Chloasma Diseases 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 102000004190 Enzymes Human genes 0.000 description 1
- 108090000790 Enzymes Proteins 0.000 description 1
- ZWZWYGMENQVNFU-UHFFFAOYSA-N Glycerophosphorylserin Natural products OC(=O)C(N)COP(O)(=O)OCC(O)CO ZWZWYGMENQVNFU-UHFFFAOYSA-N 0.000 description 1
- 206010019233 Headaches Diseases 0.000 description 1
- 206010061218 Inflammation Diseases 0.000 description 1
- 208000003351 Melanosis Diseases 0.000 description 1
- 208000008589 Obesity Diseases 0.000 description 1
- GAMYVSCDDLXAQW-AOIWZFSPSA-N Thermopsosid Natural products O(C)c1c(O)ccc(C=2Oc3c(c(O)cc(O[C@H]4[C@H](O)[C@@H](O)[C@H](O)[C@H](CO)O4)c3)C(=O)C=2)c1 GAMYVSCDDLXAQW-AOIWZFSPSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- MVNCAPSFBDBCGF-UHFFFAOYSA-N alpha-pinene Natural products CC1=CCC23C1CC2C3(C)C MVNCAPSFBDBCGF-UHFFFAOYSA-N 0.000 description 1
- 235000001014 amino acid Nutrition 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- 230000003712 anti-aging effect Effects 0.000 description 1
- 230000001093 anti-cancer Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000017531 blood circulation Effects 0.000 description 1
- 210000004204 blood vessel Anatomy 0.000 description 1
- 210000004556 brain Anatomy 0.000 description 1
- 230000019522 cellular metabolic process Effects 0.000 description 1
- 230000004098 cellular respiration Effects 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 235000012000 cholesterol Nutrition 0.000 description 1
- 230000006378 damage Effects 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 238000013100 final test Methods 0.000 description 1
- 229930003944 flavone Natural products 0.000 description 1
- 150000002212 flavone derivatives Chemical class 0.000 description 1
- 235000011949 flavones Nutrition 0.000 description 1
- 229930003935 flavonoid Natural products 0.000 description 1
- 150000002215 flavonoids Chemical class 0.000 description 1
- 235000017173 flavonoids Nutrition 0.000 description 1
- 230000002431 foraging effect Effects 0.000 description 1
- 150000004676 glycans Chemical class 0.000 description 1
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 description 1
- 229910052737 gold Inorganic materials 0.000 description 1
- 239000010931 gold Substances 0.000 description 1
- 231100000869 headache Toxicity 0.000 description 1
- 230000004054 inflammatory process Effects 0.000 description 1
- 229940087305 limonene Drugs 0.000 description 1
- 235000001510 limonene Nutrition 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000002932 luster Substances 0.000 description 1
- 244000005700 microbiome Species 0.000 description 1
- 230000036651 mood Effects 0.000 description 1
- 230000003472 neutralizing effect Effects 0.000 description 1
- 230000000050 nutritive effect Effects 0.000 description 1
- 235000020824 obesity Nutrition 0.000 description 1
- 210000000056 organ Anatomy 0.000 description 1
- 239000001814 pectin Substances 0.000 description 1
- 235000010987 pectin Nutrition 0.000 description 1
- 229920001277 pectin Polymers 0.000 description 1
- 150000003904 phospholipids Chemical class 0.000 description 1
- 229920001282 polysaccharide Polymers 0.000 description 1
- 239000005017 polysaccharide Substances 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 239000001397 quillaja saponaria molina bark Substances 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 230000008439 repair process Effects 0.000 description 1
- 229930182490 saponin Natural products 0.000 description 1
- 150000007949 saponins Chemical class 0.000 description 1
- 230000037380 skin damage Effects 0.000 description 1
- 208000024891 symptom Diseases 0.000 description 1
- 235000018553 tannin Nutrition 0.000 description 1
- 239000001648 tannin Substances 0.000 description 1
- 229920001864 tannin Polymers 0.000 description 1
- 238000010998 test method Methods 0.000 description 1
- 239000011573 trace mineral Substances 0.000 description 1
- 235000013619 trace mineral Nutrition 0.000 description 1
- VHBFFQKBGNRLFZ-UHFFFAOYSA-N vitamin p Natural products O1C2=CC=CC=C2C(=O)C=C1C1=CC=CC=C1 VHBFFQKBGNRLFZ-UHFFFAOYSA-N 0.000 description 1
- 230000037303 wrinkles Effects 0.000 description 1
- 229910052725 zinc Inorganic materials 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/35—Ketones, e.g. benzophenone
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/55—Phosphorus compounds
- A61K8/553—Phospholipids, e.g. lecithin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/63—Steroids; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9706—Algae
- A61K8/9722—Chlorophycota or Chlorophyta [green algae], e.g. Chlorella
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
- A61K8/988—Honey; Royal jelly, Propolis
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
Abstract
The invention discloses camellia oil with beauty and oxidation resistance effects and a preparation method thereof, and belongs to the technical field of processing of camellia oil. The invention provides camellia oil with beauty and antioxidation effects, which comprises the following preparation raw materials in parts by weight: 100 parts of camellia seed, 1.5-2.5 parts of abelmoschus manihot seed, 13-18 parts of abelmoschus manihot leaf extract, 1-3 parts of haematococcus pluvialis extract, 1-4 parts of phytosterol, 0.8-1.5 parts of spearmint oil, 4-6 parts of coix seed oil, 3-10 parts of soybean lecithin and 4-8 parts of honey. According to the camellia oil press, various auxiliary materials such as the yellow sunflower seeds, the yellow sunflower leaf extract, the astaxanthin, the spearmint oil and the like are adopted, and the oil is pressed from the yellow sunflower seeds and the camellia seeds step by step, so that the finally obtained camellia oil has a strong antioxidant effect. The camellia oil can effectively remove excessive oxygen free radicals in a human body, enhance cell activity, reduce pressure and improve emotion, thereby achieving good maintenance and beauty effects.
Description
Technical Field
The invention belongs to the technical field of tea oil processing, and particularly relates to camellia oil with beauty treatment and antioxidation effects and a preparation method thereof.
Background
Oxygen is an important element for life, and is transported to the whole body through the blood circulation to satisfy cellular respiration, but in this case, part of oxygen is catalyzed by enzymes to form oxygen free radicals for various reasons. The main reasons for aging, physical weakness and skin luster loss of people are excessive free radicals in the body. In young age, the body has a better neutralizing system to eliminate free radicals and reduce the damage caused by the free radicals, but the ability of the body to repair free radicals is reduced along with the age of the body. Normally, free radicals in a human body are in a balanced state, but when the free radicals exceed a certain amount and are out of control, the free radicals attack the human body and greatly promote the aging process, so that symptoms such as organ aging, skin relaxation, physical strength decline, immunity reduction and the like appear.
The reason why the skin aging speed of women is accelerated after 30 years old is that oxygen radicals invade to slow down the metabolism of cells in the skin, reduce stored water, lose elasticity, cause chloasma, darkness and wrinkles, and many women easily ignore the real reason of aging.
Camellia oil is extracted from Camellia oleifera fruit of wild woody oil family, and is known as liquid gold because it is rich in unsaturated fatty acid, camellin, tea polyphenol, phospholipids and saponin, tannin, squalene, flavonoids, Ca, Fe, Zn, Se and various vitamins. Unsaturated fatty acid is called as 'beauty acid', which can make skin tender and moist, and in addition, the unsaturated fatty acid is easy to be absorbed by human body and is not easy to be accumulated and converted into fat to cause obesity; the squalene and the tea polyphenol can diminish inflammation, remove bacteria and prevent sunshine; vitamins and other antioxidant components can prevent skin damage and aging. Based on the camellia oil, the camellia oil is expected to be a natural, beautifying and antioxidant product.
Disclosure of Invention
Aiming at the problems of multiple negative effects on human bodies caused by excessive oxygen radicals, particularly the rapid aging of skin along with the aging, the invention provides camellia oil with the effects of beautifying and resisting oxidation and a preparation method thereof, aims to provide natural camellia oil with the effects of resisting oxidation and beautifying, and provides a new way for beautifying, maintaining, improving immunity and preventing diseases.
The invention is realized by the following technical scheme:
the invention provides camellia oil with beauty and antioxidation effects, which comprises the following preparation raw materials in parts by weight:
100 parts of camellia seed, 1.5-2.5 parts of abelmoschus seed,
13-18 parts of abelmoschus manihot leaf extract, 1-3 parts of haematococcus pluvialis extract,
1-4 parts of phytosterol, 0.8-1.5 parts of spearmint oil, 4-6 parts of coix seed oil,
3-10 parts of soybean lecithin and 4-8 parts of honey.
Further, the camellia oil with the beautifying and antioxidant effects comprises the following preparation raw materials in parts by weight:
100 parts of camellia seed, 2.0-2.5 parts of abelmoschus seed,
14-16 parts of abelmoschus manihot leaf extract, 1-3 parts of haematococcus pluvialis extract,
2-4 parts of phytosterol, 1.0-1.4 parts of spearmint oil, 4-6 parts of coix seed oil,
4-8 parts of soybean lecithin and 5-7 parts of honey.
Further, the camellia oil with the beautifying and antioxidant effects comprises the following preparation raw materials in parts by weight:
100 parts of camellia seed, 2.4 parts of abelmoschus seed,
15.5 parts of abelmoschus manihot leaf extract, 2.5 parts of haematococcus pluvialis extract,
3 parts of phytosterol, 1.3 parts of spearmint oil, 5 parts of coix seed oil,
6 parts of soybean lecithin and 6 parts of honey.
Further, the preparation method of the yellow sunflower leaf extract comprises the following steps: grinding and crushing the dry leaves of the abelmoschus manihot, adding water for dilution, adjusting the pH value, adsorbing by adopting macroporous resin, eluting by adopting ethanol water solution to obtain eluent, and performing rotary evaporation and concentration to obtain the abelmoschus manihot extract.
Further, the preparation method of the haematococcus pluvialis extract comprises the following steps: drying Haematococcus pluvialis at low temperature under vacuum to control water content to 1% -2%, grinding, pulverizing, extracting the obtained powder with mixed solvent of ethanol and ethyl acetate at equal volume ratio, and saponifying.
Alpha cephalin contained in the abelmoschus manihot seeds has good antioxidation, and phosphatidylserine can play a role in relieving blood vessels, relieving pressure and regulating negative emotion; the abelmoschus manihot leaves are rich in protein, free amino acid, flavone, pectin, polysaccharide and various trace elements, not only have high nutritive value, but also have the effects of maintaining beauty and keeping young, reducing cholesterol, delaying aging and the like. Haematococcus pluvialis is a microorganism which synthesizes and accumulates most astaxanthin in nature, and astaxanthin is a natural antioxidant and has strong anticancer and anti-aging effects. In addition, the spearmint oil and the crude tea oil are mixed to prepare the raw tea oil, on one hand, the alpha-pinene, the limonene and other components contained in the raw tea oil can coordinate the antioxidation effect of the abelmoschus manihot and the astaxanthin, on the other hand, the raw tea oil keeps various plant polyphenols, and can refresh the brain, relieve the headache and relieve the mood.
The invention also provides a preparation method of the camellia oil with the effects of beautifying and resisting oxidation, which comprises the following steps:
1) weighing the raw materials according to the parts by formula for later use;
2) taking 3-4 parts of camellia seeds, air-drying, controlling water content to 3% -10%, performing ultraviolet irradiation treatment for 40-80min, performing negative pressure freeze-drying, then shelling, and performing low-temperature coarse pressing to obtain a crude camellia oil product I for later use;
3) mixing the residual camellia seeds and abelmoschus manihot seeds, air-drying, controlling water content to 10% -12%, shelling, and performing low-temperature coarse pressing to obtain a crude camellia oil product II for later use;
4) adding phytosterol, an extract of abelmoschus manihot leaves and an extract of haematococcus pluvialis into the crude tea oil I prepared in the step 2) in sequence, heating to 75-90 ℃, performing ultrasonic treatment for 25-55min, cooling, washing with ethanol and an alkali solution in sequence, performing pressure filtration, and removing precipitates to obtain crude tea oil I;
5) adding spearmint oil, coix seed oil, soybean lecithin and honey into the crude tea oil II prepared in the step 3), heating to 120-135 ℃, stirring for 1-2h, slowly cooling to room temperature, and standing overnight to obtain crude tea oil II;
6) mixing the crude tea oil I and the crude tea oil II prepared in the steps 4) and 5), performing ultrasonic treatment at normal temperature for 50-70min, and performing pressure filtration to obtain the camellia oil.
Further, the temperatures of the shelling and low-temperature rough pressing in the steps 2) and 3) are both 2-12 ℃.
Further, the alkali solution in the step 4) is sodium bicarbonate; the pressure condition of the filter pressing is 1.2-2.5 MPa.
Further, the pressure filtration pressure condition of the step 6) is 1.4-1.8 MPa.
Compared with the prior art, the invention has the beneficial effects that:
the invention provides camellia oil with beauty and antioxidation effects, compared with the common conventional camellia oil, the camellia oil has unobvious beauty effects, the invention adopts various auxiliary materials such as abelmoschus seeds, abelmoschus leaf extracts, astaxanthin, spearmint oil and the like, and the camellia oil finally obtained has strong antioxidation effects by gradually extracting oil with camellia seeds step by step. The camellia oil can effectively remove excessive oxygen free radicals in a human body, enhance cell activity, reduce pressure and improve emotion, thereby achieving good maintenance and beauty effects.
Detailed Description
In order to make the objects, technical solutions and advantages of the present invention more apparent, the technical solutions of the present invention will be clearly and completely described below with reference to the embodiments. The examples, in which specific conditions are not specified, were conducted under conventional conditions or conditions recommended by the manufacturer. The reagents or instruments used are not indicated by the manufacturer, and are all conventional products available commercially.
Unless defined otherwise, all technical and scientific terms used herein have the same meaning as commonly understood by one of ordinary skill in the art to which this invention belongs. The terminology used in the description of the invention herein is for the purpose of describing particular embodiments only and is not intended to be limiting of the invention. As used herein, the term "and/or" includes any and all combinations of one or more of the associated listed items.
Example 1
1. Weighing the following preparation raw materials in parts by weight: 100 parts of camellia seed, 2.4 parts of abelmoschus seed, 15.5 parts of abelmoschus leaf extract, 2.5 parts of haematococcus pluvialis extract, 3 parts of phytosterol, 1.3 parts of spearmint oil, 5 parts of coix seed oil, 6 parts of soybean lecithin and 6 parts of honey.
2. Taking 3 parts of camellia seeds, air-drying, controlling water content to 8%, performing ultraviolet irradiation treatment for 60min, performing negative pressure freeze-drying, then shelling, and performing coarse pressing at 8 ℃ to obtain a crude camellia oil product I for later use; and mixing the residual camellia seeds and the abelmoschus manihot seeds, air-drying, controlling water to 10% and then shelling at 10 ℃ for coarse pressing to obtain a crude camellia oil product II for later use.
3. Adding phytosterol, an extract of Abelmoschus manihot leaves and an extract of Haematococcus pluvialis into the prepared crude tea oil I in sequence, heating to 85 ℃, performing ultrasonic treatment for 35min, cooling, washing with ethanol and an alkali solution in sequence, performing pressure filtration at 2.2MPa, and removing precipitates to obtain crude tea oil I; adding spearmint oil, coix seed oil, soybean lecithin and honey into the prepared crude tea oil II, heating to 125 ℃, stirring for 1.5h, slowly cooling to room temperature, and standing overnight to obtain crude tea oil II.
4. Mixing the crude tea oil I prepared in the step 4) and the step 5) with the crude tea oil II, and performing ultrasonic treatment at normal temperature for 60min and then performing pressure filtration at 1.6MPa to obtain the camellia oil.
The camellia oil sample prepared in the embodiment is tested for the skin care efficacy: the experimental method is that the camellia oil replaces the traditional edible blend oil and is smeared on the face for one month, and the final experimental result is that: the facial skin aging is obviously improved for 82 persons, 15 persons with certain effect and 3 persons without obvious improvement.
Example 2
1. Weighing the following preparation raw materials in parts by weight: 100 parts of camellia seed, 1.5 parts of abelmoschus seed, 13 parts of abelmoschus leaf extract, 3 parts of haematococcus pluvialis extract, 3 parts of phytosterol, 1.3 parts of spearmint oil, 5 parts of coix seed oil, 6 parts of soybean lecithin and 6 parts of honey.
2. Taking 3 parts of camellia seeds, air-drying, controlling water content to 8%, performing ultraviolet irradiation treatment for 60min, performing negative pressure freeze-drying, then shelling, and performing coarse pressing at 8 ℃ to obtain a crude camellia oil product I for later use; and mixing the residual camellia seeds and the abelmoschus manihot seeds, air-drying, controlling water to 10% and then shelling at 10 ℃ for coarse pressing to obtain a crude camellia oil product II for later use.
3. Adding phytosterol, an extract of Abelmoschus manihot leaves and an extract of Haematococcus pluvialis into the prepared crude tea oil I in sequence, heating to 85 ℃, performing ultrasonic treatment for 35min, cooling, washing with ethanol and an alkali solution in sequence, performing pressure filtration at 2.2MPa, and removing precipitates to obtain crude tea oil I; adding spearmint oil, coix seed oil, soybean lecithin and honey into the prepared crude tea oil II, heating to 125 ℃, stirring for 1.5h, slowly cooling to room temperature, and standing overnight to obtain crude tea oil II.
4. Mixing the crude tea oil I prepared in the step 4) and the step 5) with the crude tea oil II, and performing ultrasonic treatment at normal temperature for 60min and then performing pressure filtration at 1.6MPa to obtain the camellia oil.
The camellia oil sample prepared in the embodiment is tested for the skin care efficacy: the experimental method is that the camellia oil replaces the traditional edible blend oil and is smeared on the face for one month, and the final experimental result is that: the facial skin aging is obviously improved for 76 persons, has a certain effect for 20 persons, and does not obviously improve for 4 persons.
Example 3
1. Weighing the following preparation raw materials in parts by weight: 100 parts of camellia seed, 2.4 parts of abelmoschus manihot seed, 18 parts of abelmoschus manihot leaf extract, 2.5 parts of haematococcus pluvialis extract, 3 parts of phytosterol, 0.8 part of spearmint oil, 5 parts of coix seed oil, 6 parts of soybean lecithin and 6 parts of honey.
2. Taking 3 parts of camellia seeds, air-drying, controlling water content to 8%, performing ultraviolet irradiation treatment for 60min, performing negative pressure freeze-drying, then shelling, and performing coarse pressing at 8 ℃ to obtain a crude camellia oil product I for later use; and mixing the residual camellia seeds and the abelmoschus manihot seeds, air-drying, controlling water to 10% and then shelling at 10 ℃ for coarse pressing to obtain a crude camellia oil product II for later use.
3. Adding phytosterol, an extract of Abelmoschus manihot leaves and an extract of Haematococcus pluvialis into the prepared crude tea oil I in sequence, heating to 85 ℃, performing ultrasonic treatment for 35min, cooling, washing with ethanol and an alkali solution in sequence, performing pressure filtration at 2.2MPa, and removing precipitates to obtain crude tea oil I; adding spearmint oil, coix seed oil, soybean lecithin and honey into the prepared crude tea oil II, heating to 125 ℃, stirring for 1.5h, slowly cooling to room temperature, and standing overnight to obtain crude tea oil II.
4. Mixing the crude tea oil I prepared in the step 4) and the step 5) with the crude tea oil II, and performing ultrasonic treatment at normal temperature for 60min and then performing pressure filtration at 1.6MPa to obtain the camellia oil.
The camellia oil sample prepared in the embodiment is tested for the skin care efficacy: the experimental method is that the camellia oil replaces the traditional edible blend oil and is smeared on the face for one month, and the final experimental result is that: the facial skin aging is obviously improved for 79 persons, 16 persons with certain effect and 5 persons without obvious improvement.
Example 4
1. Weighing the following preparation raw materials in parts by weight: 100 parts of camellia seed, 2.4 parts of abelmoschus seed, 15.5 parts of abelmoschus leaf extract, 2.5 parts of haematococcus pluvialis extract, 3 parts of phytosterol, 1.3 parts of spearmint oil, 5 parts of coix seed oil, 6 parts of soybean lecithin and 6 parts of honey.
2. Taking 3 parts of camellia seeds, air-drying, controlling water content to 8%, performing ultraviolet irradiation treatment for 60min, performing negative pressure freeze-drying, then shelling, and performing coarse pressing at 8 ℃ to obtain a crude camellia oil product I for later use; and mixing the residual camellia seeds and the abelmoschus manihot seeds, air-drying, controlling water to 10% and then shelling at 10 ℃ for coarse pressing to obtain a crude camellia oil product II for later use.
3. Adding phytosterol, an extract of Abelmoschus manihot leaves and an extract of Haematococcus pluvialis into the prepared crude tea oil I in sequence, heating to 85 ℃, performing ultrasonic treatment for 35min, cooling, washing with ethanol and an alkali solution in sequence, performing pressure filtration at 1.2MPa, and removing precipitates to obtain crude tea oil I; adding spearmint oil, coix seed oil, soybean lecithin and honey into the prepared crude tea oil II, heating to 125 ℃, stirring for 1.8h, slowly cooling to room temperature, and standing overnight to obtain crude tea oil II.
4. Mixing the crude tea oil I prepared in the step 4) and the step 5) with the crude tea oil II, and performing ultrasonic treatment at normal temperature for 60min and then performing pressure filtration at 1.6MPa to obtain the camellia oil.
The camellia oil sample prepared in the embodiment is tested for the skin care efficacy: the experimental method is that the camellia oil replaces the traditional edible blend oil and is smeared on the face for one month, and the final experimental result is that: the facial skin aging is obviously improved for 74 persons, 19 persons with certain effect and 7 persons without obvious improvement.
Comparative example 1
Reference is made to the preparation process and parameters of example 1, except that the extracts of seeds and leaves of abelmoschus manihot are not added.
And (3) detecting the maintenance and beauty effects of the camellia oil sample prepared in the comparative example: the test method is that the camellia oil replaces the traditional edible blend oil and is coated on the face for one month, and the final test result is that: the facial skin aging is obviously improved for 51 persons, 31 persons with certain effect and 18 persons without obvious improvement.
Comparative example 2
Reference is made to the preparation and parameters of example 1, except that no spearmint oil is added.
And (3) detecting the maintenance and beauty effects of the camellia oil sample prepared in the comparative example: the experimental method is that the camellia oil replaces the traditional edible blend oil and is smeared on the face for one month, and the final experimental result is that: the facial skin aging is obviously improved for 59 persons, 22 persons with certain effect and 19 persons without obvious improvement.
In conclusion, the yellow sunflower seeds, the yellow sunflower leaf extract, the astaxanthin, the spearmint oil and the like adopted by the invention can improve the maintenance and beauty effects of the camellia oil. The camellia oil prepared by the invention is pure natural and pollution-free, has good effects of resisting oxidation and removing oxygen radicals, provides a new way for people to maintain beauty, improve immunity and prevent diseases, and has good market competitiveness.
The embodiments described above merely represent some preferred embodiments of the present invention, which are described in more detail and detail, but are not intended to limit the present invention. It should be understood that various changes and modifications can be made by those skilled in the art, and any modification, equivalent replacement, improvement and the like made within the spirit and principle of the present invention should be included in the scope of the present invention.
Claims (9)
1. The camellia oil with the effects of beautifying and resisting oxidation is characterized by comprising the following preparation raw materials in parts by weight:
100 parts of camellia seed, 1.5-2.5 parts of abelmoschus manihot seed,
13-18 parts of abelmoschus manihot leaf extract, 1-3 parts of haematococcus pluvialis extract,
1-4 parts of phytosterol, 0.8-1.5 parts of spearmint oil, 4-6 parts of coix seed oil,
3-10 parts of soybean lecithin and 4-8 parts of honey.
2. The camellia oil with the effects of beautifying and resisting oxidation according to claim 1, which is characterized by comprising the following preparation raw materials in parts by weight:
100 parts of camellia seed, 2.0-2.5 parts of abelmoschus seed,
14-16 parts of abelmoschus manihot leaf extract, 1-3 parts of haematococcus pluvialis extract,
2-4 parts of phytosterol, 1.0-1.4 parts of spearmint oil, 4-6 parts of coix seed oil,
4-8 parts of soybean lecithin and 5-7 parts of honey.
3. The camellia oil with the effects of beautifying and resisting oxidation according to claim 1, which is characterized by comprising the following preparation raw materials in parts by weight:
100 parts of camellia seed, 2.4 parts of abelmoschus seed,
15.5 parts of abelmoschus manihot leaf extract, 2.5 parts of haematococcus pluvialis extract,
3 parts of phytosterol, 1.3 parts of spearmint oil, 5 parts of coix seed oil,
6 parts of soybean lecithin and 6 parts of honey.
4. The camellia oil with beauty and anti-oxidation effects as claimed in claim 1, wherein the preparation method of the abelmoschus manihot leaf extract comprises the following steps: grinding and crushing the dry leaves of the abelmoschus manihot, adding water for dilution, adjusting the pH value, adsorbing by adopting macroporous resin, eluting by adopting ethanol water solution to obtain eluent, and performing rotary evaporation and concentration to obtain the abelmoschus manihot extract.
5. The camellia oil with cosmetic and antioxidant effects as claimed in claim 1, wherein the haematococcus pluvialis extract is prepared by the following steps: drying Haematococcus pluvialis at low temperature under vacuum to control water content to 1% -2%, grinding, pulverizing, extracting the obtained powder with mixed solvent of ethanol and ethyl acetate at equal volume ratio, and saponifying.
6. A method for preparing camellia oil with cosmetic antioxidant effect as claimed in any one of claims 1-5, comprising the steps of:
1) weighing the raw materials according to the parts by formula for later use;
2) taking 3-4 parts of camellia seeds, air-drying, controlling water content to 3% -10%, performing ultraviolet irradiation treatment for 40-80min, performing negative pressure freeze-drying, then shelling, and performing low-temperature coarse pressing to obtain a crude camellia oil product I for later use;
3) mixing the residual camellia seeds and abelmoschus manihot seeds, air-drying, controlling water content to 10% -12%, shelling, and performing low-temperature coarse pressing to obtain a crude camellia oil product II for later use;
4) adding phytosterol, an extract of abelmoschus manihot leaves and an extract of haematococcus pluvialis into the crude tea oil I prepared in the step 2) in sequence, heating to 75-90 ℃, performing ultrasonic treatment for 25-55min, cooling, washing with ethanol and an alkali solution in sequence, performing pressure filtration, and removing precipitates to obtain crude tea oil I;
5) adding spearmint oil, coix seed oil, soybean lecithin and honey into the crude tea oil II prepared in the step 3), heating to 120-135 ℃, stirring for 1-2h, slowly cooling to room temperature, and standing overnight to obtain crude tea oil II;
6) mixing the crude tea oil I prepared in the step 4) and the step 5) with the crude tea oil II, performing ultrasonic treatment at normal temperature for 50-70min, and performing pressure filtration to obtain the camellia oil.
7. The method for preparing camellia oil with skin-beautifying and antioxidant effects as claimed in claim 6, wherein the temperatures of the shelling and low-temperature rough pressing in steps 2) and 3) are both 2-12 ℃.
8. The method for preparing camellia oil with skin-beautifying and antioxidant effects as claimed in claim 6, wherein the alkali solution in step 4) is sodium bicarbonate; the pressure condition of the filter pressing is 1.2-2.5 MPa.
9. The method for preparing camellia oil with skin-beautifying and antioxidant effects as claimed in claim 6, wherein the pressure filtration pressure condition in step 6) is 1.4-1.8 MPa.
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