CN114766702A - Original flavor for Chinese style heating non-combustible cigarette, preparation method and application thereof - Google Patents
Original flavor for Chinese style heating non-combustible cigarette, preparation method and application thereof Download PDFInfo
- Publication number
- CN114766702A CN114766702A CN202210394814.2A CN202210394814A CN114766702A CN 114766702 A CN114766702 A CN 114766702A CN 202210394814 A CN202210394814 A CN 202210394814A CN 114766702 A CN114766702 A CN 114766702A
- Authority
- CN
- China
- Prior art keywords
- weight
- parts
- flavor
- tobacco
- yunyan
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 77
- 239000000796 flavoring agent Substances 0.000 title claims abstract description 75
- 235000019634 flavors Nutrition 0.000 title claims abstract description 75
- 238000002360 preparation method Methods 0.000 title claims abstract description 19
- 238000010438 heat treatment Methods 0.000 title claims description 55
- 241000208125 Nicotiana Species 0.000 claims abstract description 96
- 235000002637 Nicotiana tabacum Nutrition 0.000 claims abstract description 96
- OXQOBQJCDNLAPO-UHFFFAOYSA-N 2,3-Dimethylpyrazine Chemical compound CC1=NC=CN=C1C OXQOBQJCDNLAPO-UHFFFAOYSA-N 0.000 claims abstract description 70
- YKVWPZJHENXDAJ-VOTSOKGWSA-N Megastigmatrienone Chemical compound CC1=CC(=O)CC(C)(C)C1\C=C\C=C YKVWPZJHENXDAJ-VOTSOKGWSA-N 0.000 claims abstract description 38
- JVTAAEKCZFNVCJ-UHFFFAOYSA-N lactic acid Chemical compound CC(O)C(O)=O JVTAAEKCZFNVCJ-UHFFFAOYSA-N 0.000 claims abstract description 36
- IMKHDCBNRDRUEB-UHFFFAOYSA-N Dihydroactinidiolide Natural products C1CCC(C)(C)C2=CC(=O)OC21C IMKHDCBNRDRUEB-UHFFFAOYSA-N 0.000 claims abstract description 21
- IMKHDCBNRDRUEB-LLVKDONJSA-N dihydroactinidiolide Chemical compound C1CCC(C)(C)C2=CC(=O)O[C@@]21C IMKHDCBNRDRUEB-LLVKDONJSA-N 0.000 claims abstract description 21
- POIARNZEYGURDG-FNORWQNLSA-N beta-damascenone Chemical compound C\C=C\C(=O)C1=C(C)C=CCC1(C)C POIARNZEYGURDG-FNORWQNLSA-N 0.000 claims abstract description 19
- POIARNZEYGURDG-UHFFFAOYSA-N beta-damascenone Natural products CC=CC(=O)C1=C(C)C=CCC1(C)C POIARNZEYGURDG-UHFFFAOYSA-N 0.000 claims abstract description 19
- 229930007850 β-damascenone Natural products 0.000 claims abstract description 19
- 239000004310 lactic acid Substances 0.000 claims abstract description 18
- 235000014655 lactic acid Nutrition 0.000 claims abstract description 18
- 229960004903 invert sugar Drugs 0.000 claims abstract description 17
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims description 93
- 239000011248 coating agent Substances 0.000 claims description 32
- 238000000576 coating method Methods 0.000 claims description 32
- 239000011162 core material Substances 0.000 claims description 30
- 239000007788 liquid Substances 0.000 claims description 27
- 239000002994 raw material Substances 0.000 claims description 25
- 238000000034 method Methods 0.000 claims description 18
- 238000002156 mixing Methods 0.000 claims description 8
- 238000001035 drying Methods 0.000 claims description 7
- 239000000779 smoke Substances 0.000 abstract description 27
- 239000003205 fragrance Substances 0.000 abstract description 20
- 230000001953 sensory effect Effects 0.000 abstract description 9
- 238000001914 filtration Methods 0.000 description 20
- 238000003756 stirring Methods 0.000 description 20
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 18
- 235000019505 tobacco product Nutrition 0.000 description 13
- 239000000047 product Substances 0.000 description 12
- 238000000605 extraction Methods 0.000 description 10
- 238000010992 reflux Methods 0.000 description 10
- 239000007789 gas Substances 0.000 description 8
- 230000008569 process Effects 0.000 description 8
- 238000002791 soaking Methods 0.000 description 8
- 238000002485 combustion reaction Methods 0.000 description 7
- 238000011156 evaluation Methods 0.000 description 7
- 239000000706 filtrate Substances 0.000 description 7
- 230000007794 irritation Effects 0.000 description 7
- 238000007865 diluting Methods 0.000 description 6
- CHHHXKFHOYLYRE-UHFFFAOYSA-M 2,4-Hexadienoic acid, potassium salt (1:1), (2E,4E)- Chemical compound [K+].CC=CC=CC([O-])=O CHHHXKFHOYLYRE-UHFFFAOYSA-M 0.000 description 5
- 229930091371 Fructose Natural products 0.000 description 5
- RFSUNEUAIZKAJO-ARQDHWQXSA-N Fructose Chemical compound OC[C@H]1O[C@](O)(CO)[C@@H](O)[C@@H]1O RFSUNEUAIZKAJO-ARQDHWQXSA-N 0.000 description 5
- 239000005715 Fructose Substances 0.000 description 5
- 235000009508 confectionery Nutrition 0.000 description 5
- 239000004302 potassium sorbate Substances 0.000 description 5
- 235000010241 potassium sorbate Nutrition 0.000 description 5
- 229940069338 potassium sorbate Drugs 0.000 description 5
- 230000000391 smoking effect Effects 0.000 description 5
- 239000002253 acid Substances 0.000 description 4
- 239000000919 ceramic Substances 0.000 description 4
- 238000004140 cleaning Methods 0.000 description 4
- 239000012528 membrane Substances 0.000 description 4
- 238000011160 research Methods 0.000 description 4
- 239000000126 substance Substances 0.000 description 4
- 206010013911 Dysgeusia Diseases 0.000 description 3
- 238000011161 development Methods 0.000 description 3
- 238000012986 modification Methods 0.000 description 3
- 230000004048 modification Effects 0.000 description 3
- 210000000214 mouth Anatomy 0.000 description 3
- 238000012827 research and development Methods 0.000 description 3
- SNICXCGAKADSCV-JTQLQIEISA-N (-)-Nicotine Chemical compound CN1CCC[C@H]1C1=CC=CN=C1 SNICXCGAKADSCV-JTQLQIEISA-N 0.000 description 2
- HGINCPLSRVDWNT-UHFFFAOYSA-N Acrolein Chemical compound C=CC=O HGINCPLSRVDWNT-UHFFFAOYSA-N 0.000 description 2
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 2
- 240000008866 Ziziphus nummularia Species 0.000 description 2
- 239000003546 flue gas Substances 0.000 description 2
- -1 invert sugar Chemical compound 0.000 description 2
- 230000002045 lasting effect Effects 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 229960002715 nicotine Drugs 0.000 description 2
- SNICXCGAKADSCV-UHFFFAOYSA-N nicotine Natural products CN1CCCC1C1=CC=CN=C1 SNICXCGAKADSCV-UHFFFAOYSA-N 0.000 description 2
- 238000013441 quality evaluation Methods 0.000 description 2
- 239000013589 supplement Substances 0.000 description 2
- 230000001502 supplementing effect Effects 0.000 description 2
- 206010016322 Feeling abnormal Diseases 0.000 description 1
- 238000005054 agglomeration Methods 0.000 description 1
- 230000002776 aggregation Effects 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- VYQRBKCKQCRYEE-UHFFFAOYSA-N ctk1a7239 Chemical compound C12=CC=CC=C2N2CC=CC3=NC=CC1=C32 VYQRBKCKQCRYEE-UHFFFAOYSA-N 0.000 description 1
- 230000003111 delayed effect Effects 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 238000009776 industrial production Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- WSFSSNUMVMOOMR-NJFSPNSNSA-N methanone Chemical compound O=[14CH2] WSFSSNUMVMOOMR-NJFSPNSNSA-N 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 230000033764 rhythmic process Effects 0.000 description 1
- 230000000638 stimulation Effects 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 230000002195 synergetic effect Effects 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 231100000331 toxic Toxicity 0.000 description 1
- 230000002588 toxic effect Effects 0.000 description 1
- 238000012795 verification Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
- A24B15/241—Extraction of specific substances
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24C—MACHINES FOR MAKING CIGARS OR CIGARETTES
- A24C5/00—Making cigarettes; Making tipping materials for, or attaching filters or mouthpieces to, cigars or cigarettes
- A24C5/01—Making cigarettes for simulated smoking devices
Abstract
The invention provides a primary flavor for Chinese-style non-combustible heated cigarettes, which uses red date extract, Yunyan tobacco extract, lactic acid, megastigmatrienone, dihydroactinidiolide, Yunyan absolute oil, beta-damascenone, invert sugar and 2, 3-dimethyl pyrazine in a proper proportion, so that the flavor can effectively improve the tobacco fragrance of flue-cured tobaccos, improve the smoke state, has comfortable mouthfeel, meets the taste requirements of Chinese consumers on Chinese-style flue-cured tobaccos, and improves the sensory experience of the consumers. The application also provides a preparation method and application of the original flavor.
Description
Technical Field
The invention relates to the technical field of tobacco, in particular to an original flavor for Chinese style heating non-combustible cigarettes, a preparation method and application thereof.
Background
A heating non-combustible tobacco product (also called low temperature cigarette, IQOS) is a novel tobacco product which heats tobacco shreds through a special heating source, and nicotine and aroma substances in the tobacco shreds are volatilized to generate smoke gas to meet the requirements of smokers during heating. In recent years, the heat-not-burn product represented by IQOS is rapidly the focus of attention in the field of domestic and foreign tobacco products by virtue of the characteristics of high development speed, high customer conversion rate, outstanding technological content and the like, and the novel tobacco product is really pushed to the air opening of public opinion.
Compared with the traditional cigarette, the 'low temperature' design of heating the non-burning cigarette can ensure that the tobacco leaves are just heated to the degree of giving off the taste under the condition of not igniting the tobacco leaves. Generally, when a common cigarette is smoked, the high temperature of 600 ℃ to 900 ℃ is achieved, a plurality of harmful substances are generated, and when the low-temperature cigarette is heated below 500 ℃, the harmful substances are obviously reduced. At present, in the analysis discussion of substances generated by heating non-combustible products, the Swiss researchers' opinion on representative products of heating non-combustible products, namely IQOS, is more mainstream, and the IQOS generated nicotine, formaldehyde, toxic acrolein and the like are reduced by 84% compared with the traditional cigarettes.
Since the 70 s of the last century, international tobacco enterprises invest a great deal of capital in market research, product research and development and advertising of novel tobacco products and successively release related products. And the market is strongly and quickly seized through commercial merger, brand sharing and other means, and the research on the aspect obtains greater technical breakthrough and leap-over development. The growth rate is expected to remain around 15% to 20% in the coming years. China starts late in the research aspect of novel tobacco products, has a great gap compared with international leading enterprises, and has high importance in the future, so that the research investment is increased, and the promotion rhythm is accelerated; only by one step, innovative products with unique flavor, convenient use and low harmfulness can be researched and developed, and the initiative of domestic and international market competition can be mastered.
The market scale of Chinese tobacco reaches trillion level, China is still in the beginning stage in the research and development field and the commercialization field of novel heating non-combustible tobacco products, and domestic traditional consumers are used to the taste, the taste and the smoking method of Chinese flue-cured tobacco, but at present, the original taste of the heating non-combustible product represented by IQOS is taken as the mixed taste, and the requirements of the domestic traditional consumers are difficult to meet. Therefore, the research and development of novel tobacco products are urgently needed to face the consumption requirements of vast consumers in China and develop novel tobacco products which are low in harm, high in quality and unique in Chinese style flavor. Because the development of the original flavor for Chinese heating non-combustible tobacco products is delayed, the original flavor for Chinese heating non-combustible cigarettes is urgently needed to develop Chinese heating non-combustible cigarettes, so that the taste requirements of Chinese consumers are met, and the problems are avoided.
Disclosure of Invention
The invention aims to provide the original flavor for Chinese style heating non-combustible cigarettes, which can supplement the original flavor of tobacco, improve the smoke state and improve the taste requirements of consumers when applied to the heating non-combustible cigarettes.
In view of the above, the application provides an original flavor for Chinese style non-combustible heating cigarettes, which comprises the following raw materials in 100 parts by weight:
preferably, the content of the red date extract is 2-8 parts by weight.
Preferably, the content of the lactic acid is 0.02-0.06 weight part, and the content of the dihydroactinidiolide is 0.1-0.6 weight part.
Preferably, the content of the megastigmatrienone is 0.02-0.08 weight part, the megastigmatrienone is added in the form of 10-15 wt% of megastigmatrienone solution, and the megastigmatrienone solution is prepared by dissolving propylene glycol with megastigmatrienone.
Preferably, the content of the Yunyan absolute oil is 0.2-0.8 part by weight, and the content of the beta-damascenone is 0.2-0.8 part by weight.
Preferably, the content of the 2, 3-dimethylpyrazine is 0.02-0.08 part by weight, the 2, 3-dimethylpyrazine is added in the form of 10-15 wt% of 2, 3-dimethylpyrazine, and the 2, 3-dimethylpyrazine solution is prepared by dissolving propylene glycol in the 2, 3-dimethylpyrazine.
The application also provides a preparation method of the primary flavor essence, which comprises the following steps:
mixing the red date extract, the Yunyan extract, lactic acid, megastigmatrienone, dihydroactinidiolide, Yunyan absolute, beta-damascenone, invert sugar, 2, 3-dimethyl pyrazine and propylene glycol according to the raw material ratio to obtain the original flavor for Chinese style cigarette which is not combusted by heating.
Preferably, the mixing further comprises:
dissolving megastigmatrienone and 2, 3-dimethyl pyrazine respectively by adopting propylene glycol until the concentration is 10-15 wt%.
The application also provides a preparation method of the cigarette core material of the cigarette without burning by heating, which comprises the following steps:
mixing the coating liquid of the cigarette which is not combusted by heating with the original flavor to obtain mixed coating liquid;
coating and flavoring the tobacco sheet base by adopting the mixed coating liquid, and drying to obtain a tobacco core material;
the primary flavor is the primary flavor or the primary flavor prepared by the preparation method.
Preferably, the primary flavor essence accounts for 2-10 wt% of the coating liquid, and the mixed coating liquid accounts for 5-15 wt% of the tobacco sheet base.
The application provides an original flavor for Chinese-style cigarettes which are not combusted by heating, and the original flavor comprises a red date extract, a Yunyan extract, lactic acid, megastigmatrienone, dihydroactinidiolide, Yunyan absolute, beta-damascenone, invert sugar, 2, 3-dimethyl pyrazine and propylene glycol with specific content; in the original flavor provided by the application, the Yunyan tobacco extract and the Yunyan tobacco absolute oil can endow cigarettes with fresh and sweet fragrance; the red date extract can provide sweet fragrance of the jujube and enrich tobacco fragrance; megastigmatrienone, dihydroactinidiolide, beta-damascenone and 2, 3-dimethylpyrazine are all flue-cured tobacco aroma components and can play a role in supplementing flue-cured tobacco aroma; lactic acid can play a role in reducing thorns, so that the soft and exquisite feeling of smoke is improved; the invert sugar can make the smoke conglobate and become elegant, and the components have synergistic effect, so that the herbal fragrance of the smoke can be supplemented, the smoke state can be improved, and the taste can be improved; experimental results show that the heating non-combustion tobacco product produced by adding the Chinese style heating non-combustion cigarette primary flavor into the tobacco core material has the advantages of comfortable and natural tobacco fragrance, soft and fine smoke, clean oral cavity and improved comfort in smoking.
Detailed Description
For a further understanding of the invention, reference will now be made to the preferred embodiments of the invention by way of example, and it is to be understood that the description is intended to further illustrate features and advantages of the invention, and not to limit the scope of the claims.
In view of the problem that the original flavor of Chinese style non-burning cigarettes in the prior art cannot meet the taste requirements of Chinese consumers, the application provides the original flavor for Chinese style non-burning cigarettes, which adopts red date extract, Yunyan extract, lactic acid, megastigmatrienone, dihydroactinidiolide, Yunyan absolute oil, beta-damascenone, invert sugar and 2, 3-dimethyl pyrazine and is prepared in a proper proportion. Specifically, the embodiment of the invention discloses a primary flavor for Chinese style heating non-combustible cigarettes, which comprises the following raw materials in 100 parts by weight:
in the original flavor provided by the application, the red date extract can make the fragrance become thin and rich, the penetrability is enhanced, the fragrance of aged tobacco becomes mellow, the smooth smoke feeling is good, the smoke is thickened, and the sweet feeling is enhanced; the content of the red date extract is 2 to 10 parts by weight, more specifically 2 to 8 parts by weight, and in specific embodiments, the content of the red date extract is 2.2 parts by weight, 2.8 parts by weight, 3.0 parts by weight, 3.2 parts by weight, 3.5 parts by weight, 4.2 parts by weight, 4.5 parts by weight, 4.8 parts by weight, 5.2 parts by weight, 5.5 parts by weight, 6.1 parts by weight, 6.3 parts by weight, 6.7 parts by weight, 6.9 parts by weight, 7.2 parts by weight, 7.5 parts by weight, or 7.8 parts by weight. If the content of the red date extract is not within the above range, the overall taste is deteriorated, the irritation and the dry feeling are increased, and the aftertaste is not clean.
In evaluation and analysis, the Yunyan tobacco extract has rich fragrance, natural aged tobacco fragrance, good smooth smoke and increased convergence. The content of the yunyan tobacco extract is 3 to 15 parts by weight, more specifically 3.5 to 12 parts by weight, and in specific embodiments, the content of the yunyan tobacco extract is 3.8 parts by weight, 4.5 parts by weight, 5.2 parts by weight, 5.6 parts by weight, 6.2 parts by weight, 6.6 parts by weight, 6.9 parts by weight, 7.2 parts by weight, 7.7 parts by weight, 7.9 parts by weight, 8.2 parts by weight, 8.6 parts by weight, 8.8 parts by weight, 9.2 parts by weight, 9.6 parts by weight, 9.8 parts by weight, 10.2 parts by weight, 10.5 parts by weight, 11.2 parts by weight, or 11.8 parts by weight.
The lactic acid makes the smoke smooth and has less dryness and irritation. The content of the lactic acid is 0.02 to 0.10 part by weight, specifically 0.02 to 0.06 part by weight, more specifically 0.03 part by weight, 0.05 part by weight, 0.06 part by weight, or 0.08 part by weight.
The megastigmatrienone can thin and enrich smoke, cover miscellaneous gas, increase lasting feeling, and increase smooth feeling and concentration of smoke. The megastigmatrienone is a 10-15 wt% megastigmatrienone solution, and the megastigmatrienone solution is prepared by dissolving propylene glycol in megastigmatrienone. The megastigmatrienone content is 0.02-0.10 parts by weight, more specifically 0.02-0.08 parts by weight, and in specific embodiments, the megastigmatrienone content is 0.03 parts by weight, 0.055 parts by weight, 0.065 parts by weight, 0.070 parts by weight, or 0.075 parts by weight. If the megastigmatrienone content is not within the above range, the throat portion may have heavy residue and the mouth feel may be uncomfortable.
The dihydro actinidiolide enables smoke to be elegant and rich, covers miscellaneous gas, increases lasting feeling, enables the smoke to be soft, improves comfortable feeling, and reduces dry feeling. The content of the dihydroactinidiolide is 0.1-1.0 part by weight, specifically, the content of the dihydroactinidiolide is 0.1-0.6 part by weight, more specifically, the content of the dihydroactinidiolide is 0.15 part by weight, 0.30 part by weight, 0.32 part by weight, 0.45 part by weight, 0.55 part by weight or 0.60 part by weight. If the content of dihydroactinidiolide is out of the above range, the taste is deteriorated and the residual and dry feeling are increased.
The Yunyan absolute can make the smoke gas rich, the aged tobacco is fragrant and natural, the smoke gas has good smooth feeling, and the dry feeling and the irritation are appropriate. The content of the Yunyan absolute is 0.2-1.0 part by weight, specifically, the content of the Yunyan absolute is 0.2-0.8 part by weight, more specifically, the content of the Yunyan absolute is 0.3 part by weight, 0.5 part by weight, 0.55 part by weight, 0.70 part by weight or 0.75 part by weight. When the content of the yunyan absolute exceeds the above range, the dry feeling and the irritation are enhanced.
The beta-damascenone has the advantages of fine fragrance, rich fragrance, enhanced penetrability and covering up miscellaneous gas; smooth feeling and soft feeling are improved; improving comfort, relieving irritation and dryness, and improving aftertaste. The content of the beta-damascenone is 0.2 to 1.0 part by weight, specifically, 0.2 to 0.8 part by weight, more specifically, 0.25 part by weight, 0.30 part by weight, 0.35 part by weight, 0.40 part by weight, 0.45 part by weight, 0.55 part by weight, 0.68 part by weight, or 0.75 part by weight. If the content of the beta-damascenone exceeds the above range, the taste becomes poor, the irritation and the dry feeling increase, and the aftertaste becomes unclean.
The invert sugar improves the penetrability, covers miscellaneous gases and enhances the natural sense of the cigarette fragrance; the smooth feeling is improved, and the smoke concentration and the agglomeration property are increased; reducing irritation and feeling of dryness. The invert sugar is present in an amount of 3 to 8 parts by weight, more specifically 3 to 6 parts by weight, and in specific embodiments 3.5, 4.2, 4.8, 5.2, or 5.5 parts by weight. If the content of the invert sugar is too large, the smoke becomes rough.
The 2, 3-dimethyl pyrazine enables the tobacco fragrance to become fine and smooth and covers miscellaneous gases; the smoke becomes smooth and soft, and the smoke concentration is increased. The content of the 2, 3-dimethylpyrazine is 0.02-0.10 parts by weight, specifically, the content of the 2, 3-dimethylpyrazine is 0.02-0.08 parts by weight, more specifically, the content of the 2, 3-dimethylpyrazine is 0.03 parts by weight, 0.040 parts by weight, 0.042 parts by weight, 0.055 parts by weight, 0.060 parts by weight, 0.062 parts by weight, 0.070 parts by weight, or 0.075 parts by weight, and if the content of the 2, 3-dimethylpyrazine is too high, the taste residue increases.
The raw materials in the primary flavor essence described in the present application may be commercially available products, or may be prepared according to conventional methods in the prior art, and the source of the raw materials is not particularly limited in the present application.
The invention also provides a preparation method of the original flavor, which comprises the following steps:
mixing the red date extract, the Yunyan extract, lactic acid, megastigmatrienone, dihydroactinidiolide, Yunyan absolute oil, beta-damascenone, invert sugar, 2, 3-dimethyl pyrazine and propylene glycol according to the raw material ratio to obtain the original flavor for Chinese style non-combustible heating cigarettes.
The red date extract is prepared by the following method:
removing cores of dried red dates, crushing, soaking for 3-6 hours by using 66.5% ethanol with the mass 6-12 times of that of the dried red dates, performing hot reflux extraction for 3-5 hours at 70-95 ℃, filtering while hot by using a duplex filter (200 meshes), standing for 12-48 hours after filtering, taking supernate, concentrating the supernate until the relative density (20 ℃) is 1.0280 +/-0.008, standing in a refrigerator for 12-24 hours, taking supernate, filtering by using a 100nm ceramic membrane, adding 32% of fructose, 32% of propylene glycol and 0.15% of potassium sorbate into filtrate, and uniformly stirring to obtain the red date extract.
The preparation method of the Yunyan tobacco extract comprises the following steps:
cleaning and crushing Yunyan tobacco leaves, soaking the Yunyan tobacco leaves in 42.85% ethanol with the mass 8-20 times of that of the Yunyan tobacco leaves for 3-6 hours, carrying out hot reflux extraction for 4-6 hours at the temperature of 70-95 ℃, filtering the Yunyan tobacco leaves while the Yunyan tobacco leaves are hot through a duplex filter (200 meshes), filtering the obtained filtrate through a 0.8 mu m plate frame, and concentrating the filtrate until the relative density is (20 ℃): 1.2866 + -0.0080, refractive index (20 deg.C): 1.3650. + -. 0.0080, acid number: 6.5 +/-2.0, thus obtaining the Yunyan tobacco extract.
In the process of preparing the red date extract and the yunyan extract, the dry red date is denucleated, crushed and soaked, then is subjected to hot reflux extraction, and is filtered by a 200-mesh duplex filter while hot; the Yunyan tobacco leaves are cleaned, crushed, soaked in ethanol, subjected to hot reflux extraction, and filtered by a 200-mesh duplex filter and a plate frame.
Before the raw materials are mixed, the method also comprises the following steps: dissolving megastigmatrienone and 2, 3-dimethyl pyrazine respectively by adopting propylene glycol until the concentration is 10-15 wt%.
The application also provides a preparation method of the cigarette core material of the cigarette without burning by heating, which comprises the following steps:
mixing the coating liquid of the cigarette which is not burnt by heating with the original flavor to obtain mixed coating liquid;
coating and perfuming a tobacco sheet base by adopting the mixed coating liquid, and drying to obtain a tobacco core material;
the original flavor is the original flavor in the scheme.
The above process is more specifically: A) slowly adding the original flavor for the Chinese style heating non-combustible cigarette, which accounts for 2-8% of the weight of the coating liquid, into the coating liquid for the Chinese style heating non-combustible cigarette, stirring at the speed of 150-180 rpm in the process of adding the flavor, wherein the stirring temperature is 20-28 ℃, the relative humidity is 40-70%, and continuously stirring for 2-3 hours under the stirring condition after the flavor is completely added to prepare the coating liquid containing the original flavor for the Chinese style heating non-combustible cigarette;
B) preparing a tobacco sheet base by papermaking, adding the coating liquid obtained in the step A) according to the proportion of 6-12% of the total weight of the tobacco sheet base, and then adding fragrance and drying according to the normal process of heating the non-combustible cigarette core material to prepare the cigarette core material of the non-combustible cigarette.
The coating solution and the tobacco sheet base are materials well known to those skilled in the art, and the present application is not particularly limited thereto.
The cigarette is endowed with fresh and sweet fragrance by the Yunyan extract and the Yunyan absolute oil which are used as raw materials of the Chinese-style heating non-combustible cigarette primary flavor provided by the invention; the red date extract can provide the fruit sweet fragrance of the jujube, and enrich the tobacco fragrance; megastigmatrienone, dihydroactinidiolide, beta-damascenone and 2, 3-dimethylpyrazine are all flue-cured tobacco aroma components and can play a role in supplementing flue-cured tobacco aroma; the lactic acid can play a role in reducing thorns, so that the soft and exquisite feeling of the smoke is improved; the invert sugar can make the smoke agglomerate and become through and elegant, and all the components can supplement the original fragrance of the tobacco to different degrees, improve the smoke state and improve the taste. The Chinese-style heating non-combustible cigarette original flavor and the coating liquid can be mutually soluble without impurity precipitation, and the feasibility of the prepared cigarette core material is reliably guaranteed through production verification; the heating non-combustion tobacco product produced by adding the Chinese heating non-combustion cigarette primary flavor into the tobacco core material has the advantages of comfortable and natural tobacco fragrance of flue-cured tobacco in the smoking process, soft and fine smoke, clean oral cavity and improved comfort. Through a cigarette core material test, the coating liquid of the Chinese style heating non-combustible cigarette original flavor essence is added, the cigarette core material is not influenced, and the normal production can be realized. The preparation method is simple and convenient, has low cost, can be used for large-scale industrial production, and has strong practicability.
For further understanding of the present invention, the following examples are given to illustrate details of the original flavor, its preparation method and its application, and the scope of the present invention is not limited by the following examples.
Embodiment 1A Chinese style heating non-burning cigarette original flavor essence is specifically prepared by the following steps:
(1) preparation of raw materials
a. Removing cores of dried red dates, crushing, soaking in 66.5% ethanol with the mass 6.2 times that of the dried red dates for 3.2 hours, carrying out hot reflux extraction for 3.1 hours at 73 ℃, then filtering while hot by using a duplex filter (200 meshes), standing for 12.8 hours after filtering, taking supernate, concentrating the supernate until the relative density (20 ℃) is 1.0280 +/-0.008, standing for 12.5 hours in a refrigerator, filtering the supernate by using a 100nm ceramic membrane, adding fructose, propylene glycol and potassium sorbate into the filtrate, wherein the weight of the fructose, the propylene glycol and the potassium sorbate is 32% of the weight of the filtrate, and uniformly stirring to obtain a red date extract for later use;
b. cleaning and crushing Yunyan tobacco leaves, soaking the Yunyan tobacco leaves in 42.85% ethanol with the mass 9 times that of the Yunyan tobacco leaves for 3.2 hours, carrying out hot reflux extraction for 4.3 hours at the temperature of 72 ℃, filtering the Yunyan tobacco leaves while hot through a duplex filter (200 meshes), filtering the filtered tobacco leaves through a 0.8 mu m plate frame, and concentrating the filtered tobacco leaves until the relative density is (20 ℃): 1.2866 + -0.0080, refractive index (20 ℃): 1.3650. + -. 0.0080, acid number: 6.5 +/-2.0, thus obtaining the yunyan tobacco extract for later use;
(2) pretreatment of essence raw material
a. Diluting a certain amount of megastigmatrienone propylene glycol into a solution with the mass concentration of 10%, and shaking up until the megastigmatrienone propylene glycol is completely dissolved for later use;
b. diluting a certain amount of 2, 3-dimethyl pyrazine into a solution with the mass concentration of 10% by using propylene glycol, and shaking up until the solution is completely dissolved for later use;
(3) preparing essence according to the following raw materials in parts by weight: 2.2 parts of red date extract prepared in the step (1), 3.8 parts of Yunyan tobacco extract prepared in the step (1), 0.3 part of megastigmatrienone solution with the mass concentration of 10% prepared in the step (2), 0.3 part of 2, 3-dimethyl pyrazine solution with the mass concentration of 10% prepared in the step (2), 0.03 part of lactic acid, 0.15 part of dihydroactinidiolide, 0.3 part of Yunyan absolute, 0.25 part of beta-damascenone, 3.5 parts of invert sugar and 89.17 parts of propylene glycol, and 100 parts of raw materials in total weight are uniformly mixed to obtain the Chinese-style heating non-combustible cigarette primary flavor essence A;
the total mass percent of the Chinese style heating non-burning cigarette primary flavor A prepared in the example 1 is 100%, wherein the mass percent of each raw material is as follows: 2.2 percent of red date extract, 3.8 percent of Yunyan tobacco extract, 0.03 percent of lactic acid, 0.03 percent of megastigmatrienone, 0.15 percent of dihydroactinidiolide, 0.3 percent of Yunyan tobacco absolute, 0.25 percent of beta-damascenone, 3.5 percent of invert sugar, 0.03 percent of 2, 3-dimethyl pyrazine and the balance of propylene glycol.
Embodiment 2 an essence for Chinese style cigarette with heat and non-combustible property, which has a primary flavor, is prepared by the following steps:
(1) preparing raw materials:
a. removing cores of dried red dates, crushing, soaking for 5.5 hours by using ethanol with the concentration of 66.5% and the mass of the dried red dates being 11 times of that of the dried red dates, carrying out hot reflux extraction for 4.8 hours at the temperature of 90 ℃, then filtering while hot by using a duplex filter (200 meshes), standing for 45 hours after filtering, concentrating supernate until the relative density (20 ℃) is 1.0280 +/-0.008, placing the supernate in a cold storage for 22 hours, filtering the supernate by using a 100nm ceramic membrane, adding fructose with the weight of 32%, propylene glycol with the weight of 32% and potassium sorbate with the weight of 0.15% into the filtrate, and uniformly stirring to obtain a red date extract for later use;
b. cleaning and crushing Yunyan tobacco leaves, soaking the Yunyan tobacco leaves in 42.85% ethanol with the mass being 18 times of that of the Yunyan tobacco leaves for 5.8 hours, carrying out hot reflux extraction for 5.8 hours at the temperature of 92 ℃, filtering the Yunyan tobacco leaves while hot through a duplex filter (200 meshes), filtering the filtered liquid through a 0.8 mu m plate frame, and concentrating the filtered liquid until the relative density is (20 ℃): 1.2866 + -0.0080, refractive index (20 deg.C): 1.3650. + -. 0.0080, acid number: 6.5 +/-2.0, thus obtaining the yunyan tobacco extract for later use;
(2) pretreatment of essence raw materials:
a. diluting a certain amount of megastigmatrienone propylene glycol into a solution with the mass concentration of 10%, and shaking up until the solution is completely dissolved for later use;
b. diluting a certain amount of 2, 3-dimethyl pyrazine into a solution with the mass concentration of 10% by using propylene glycol, and shaking up until the solution is completely dissolved for later use;
(3) preparing essence according to the following raw materials in parts by weight: 7.5 parts of red date extract prepared in the step (1), 14.5 parts of Yunyan tobacco extract prepared in the step (1), 0.75 part of megastigmatrienone solution with the mass concentration of 10% prepared in the step (2), 0.75 part of 2, 3-dimethyl pyrazine solution with the mass concentration of 10% prepared in the step (2), 0.05 part of lactic acid, 0.55 part of dihydroactinidiolide, 0.75 part of Yunyan absolute, 0.75 part of beta-damascenone, 5.5 parts of invert sugar and 68.9 parts of propylene glycol, and 100 parts of raw materials in total weight are uniformly mixed to obtain the Chinese-style heating non-combustible cigarette primary flavor essence B;
example 2 the total mass percent of the primary flavor B for Chinese style heat non-combustible cigarettes is 100%, wherein the mass percent of the raw materials is as follows: 7.5% of red date extract, 14.5% of yunyan tobacco extract, 0.05% of lactic acid, 0.075% of megastigmatrienone, 0.55% of dihydroactinidiolide, 0.75% of yunyan neat oil, 0.75% of beta-damascenone, 5.5% of invert sugar, 0.075% of 2, 3-dimethyl pyrazine and the balance of propylene glycol.
Example 3 an essence with original flavor for Chinese style cigarette without heat and combustion is prepared by the following steps:
(1) preparing raw materials:
a. removing cores of dried red dates, crushing, soaking for 4.6 hours by using 66.5% ethanol with the mass 9.2 times of that of the dried red dates, performing hot reflux extraction for 4.2 hours at the temperature of 70-95 ℃, then filtering while hot by using a duplex filter (200 meshes), standing for 32 hours after filtering, taking supernate, concentrating the supernate until the relative density (20 ℃) is 1.0280 +/-0.008, standing in a refrigerator for 20 hours, taking supernate, filtering by using a 100nm ceramic membrane, adding 32% of fructose, 32% of propylene glycol and 0.15% of potassium sorbate into the filtrate, and uniformly stirring to obtain a red date extract for later use;
b. cleaning and crushing Yunyan tobacco leaves, soaking the Yunyan tobacco leaves in 42.85% ethanol with the mass 14.2 times of that of the Yunyan tobacco leaves for 4.6 hours, carrying out hot reflux extraction for 5.2 hours at 82 ℃, filtering the Yunyan tobacco leaves while hot through a duplex filter (200 meshes), filtering the filtered tobacco leaves through a 0.8 mu m plate frame, and concentrating the filtered tobacco leaves until the relative density is (20 ℃): 1.2866 + -0.0080, refractive index (20 deg.C): 1.3650. + -. 0.0080, acid number: 6.5 +/-2.0, thus obtaining the yunyan tobacco extract for later use;
(2) pretreatment of essence raw materials:
a. diluting a certain amount of megastigmatrienone propylene glycol into a solution with the mass concentration of 10%, and shaking up until the solution is completely dissolved for later use;
b. diluting a certain amount of 2, 3-dimethyl pyrazine into a solution with the mass concentration of 10% by using propylene glycol, and shaking up until the solution is completely dissolved for later use;
(3) preparing essence according to the following raw materials in parts by weight: 5.2 parts of red date extract prepared in the step (1), 10 parts of Yunyan tobacco extract prepared in the step (1), 0.55 part of megastigmatrienone solution with the mass concentration of 10% prepared in the step (2), 0.56 part of 2, 3-dimethyl pyrazine solution with the mass concentration of 10% prepared in the step (2), 0.05 part of lactic acid, 0.55 part of dihydroactinidiolide, 0.55 part of Yunyan absolute, 0.55 part of beta-damascenone, 4.8 parts of invert sugar and 77.19 parts of propylene glycol, and 100 parts of raw materials in total weight are uniformly mixed to obtain the Chinese-style heating non-combustible cigarette original flavor essence C;
example 3 the total mass percent of the original flavor C for the Chinese style heating non-burning cigarette is 100%, wherein the mass percent of the raw materials is as follows: 5.2% of red date extract, 10% of yunyan tobacco extract, 0.05% of lactic acid, 0.055% of megastigmatrienone, 0.55% of dihydroactinidiolide, 0.55% of yunyan tobacco absolute oil, 0.55% of beta-damascenone, 4.8% of invert sugar, 0.055% of 2, 3-dimethyl pyrazine and the balance of propylene glycol.
Example 4 the Chinese style heating non-burning cigarette primary flavor essence A prepared in example 1 is applied to a cigarette core material, and the steps thereof include:
a. slowly adding the Chinese style essence A which is prepared in the embodiment 1 and has the weight of 2.8 percent of the coating liquid into the coating liquid, stirring at the speed of 160rpm in the process of adding the original flavor A, wherein the stirring temperature is 22 ℃, the relative humidity is 45 percent, and continuously stirring for 2.2 hours under the condition of keeping the stirring after the flavor A is completely added, thus finishing the preparation process;
b. and (b) preparing a tobacco sheet base by a papermaking method, adding the Chinese style heating non-combustible cigarette original flavor A in the a according to the proportion of 6.2 percent of the total weight of the tobacco sheet base, coating, perfuming and drying to prepare the tobacco core material A used in the heating non-combustible cigarette.
Example 5 applying the primary flavor B of a chinese style heated non-burning cigarette prepared in example 2 to a core material, the steps include:
a. slowly adding 7.8% of the Chinese-style essence B which is prepared in the embodiment 2 and is not combusted in the weight of the coating liquid into the coating liquid, stirring at the speed of 175rpm in the process of adding the original essence at the stirring temperature of 27 ℃ and the relative humidity of 67%, and keeping the stirring condition for continuously stirring for 2.8 hours after the essence B is completely added, thus finishing the preparation process;
b. and (3) preparing a tobacco sheet base by papermaking, adding the Chinese style heating non-combustion cigarette original flavor B in the component a according to the proportion of 11.5 percent of the total weight of the tobacco sheet base, coating, perfuming and drying to prepare the tobacco core material B used in the heating non-combustion cigarette.
Example 6 applying the primary flavor C of a chinese style heated non-burning cigarette prepared in example 3 to a core material, the steps include:
a. slowly adding the Chinese style essence C which is prepared in the embodiment 3 and accounts for 5.3 percent of the weight of the coating liquid into the coating liquid, stirring at the speed of 165rpm in the process of adding the original flavor, wherein the stirring temperature is 24 ℃, the relative humidity is 57 percent, and after the flavor C is completely added, keeping the stirring condition and continuing stirring for 2.5 hours to finish the preparation process;
b. and (3) preparing a tobacco sheet base by papermaking, adding the essence C containing the Chinese style heating non-combustible cigarette primary taste in the step a according to the proportion of 9.2 percent of the total weight of the tobacco sheet base, coating, perfuming and drying to prepare the tobacco core material C used in the heating non-combustible cigarette.
The cigarette core materials A, B, C in application examples 4, 5 and 6 were made into a non-burning heated cigarette product, and the same method as in example 4 was used to make a blank cigarette core material without the addition of the original flavor, and then the blank cigarette core material was made into a non-burning heated cigarette product, which was evaluated according to the national bureau smoking assessment standards, and the smoking panel consisted of 13 cigarette sensory evaluation experts, and sensory evaluations and scores were performed in a dark evaluation mode, and the comprehensive sensory quality evaluation results are shown in table 1, and the sensory evaluation scores are shown in table 2:
TABLE 1 comprehensive sensory quality evaluation result data sheet of heated non-burning cigarette product made of cigarette core material A, B, C
TABLE 2 sensory evaluation score sheet
As can be seen from tables 1 and 2, the tobacco core material is added with the heating non-combustible tobacco product containing the Chinese style heating non-combustible cigarette original flavor, so that the tobacco aroma of the flue-cured tobacco can be effectively improved, the smoke state is improved, the taste is comfortable, the taste requirement of Chinese style flue-cured tobacco by consumers in China is met, and the sensory experience of the consumers is improved.
Comparative example 1
The original flavor is prepared according to the method in the example 1, except that no yunyan tobacco extract is added, the method in the example 4 is applied to the tobacco core material, and sensory comparison and evaluation analysis shows that the flue gas volume of the Chinese style flue-cured tobacco prepared in the example is reduced, the richness is reduced, the stimulation is increased, and the softness of the flue gas is reduced.
The above description of the embodiments is only intended to facilitate the understanding of the method of the invention and its core idea. It should be noted that, for those skilled in the art, it is possible to make various improvements and modifications to the present invention without departing from the principle of the present invention, and those improvements and modifications also fall within the scope of the claims of the present invention.
The previous description of the disclosed embodiments is provided to enable any person skilled in the art to make or use the present invention. Various modifications to these embodiments will be readily apparent to those skilled in the art, and the generic principles defined herein may be applied to other embodiments without departing from the spirit or scope of the invention. Thus, the present invention is not intended to be limited to the embodiments shown herein but is to be accorded the widest scope consistent with the principles and novel features disclosed herein.
Claims (10)
1. The original flavor for Chinese style non-combustible heating cigarettes comprises the following raw materials in 100 parts by weight:
the balance of propylene glycol.
2. The primary flavor according to claim 1, wherein the content of the red date extract is 2-8 parts by weight.
3. The primary taste essence according to claim 1, wherein the content of lactic acid is 0.02-0.06 parts by weight, and the content of dihydroactinidiolide is 0.1-0.6 parts by weight.
4. The primary taste essence according to claim 1, wherein the megastigmatrienone is 0.02-0.08 weight part, and is added in the form of 10-15 wt% megastigmatrienone solution, and the megastigmatrienone solution is prepared by dissolving propylene glycol with megastigmatrienone.
5. The primary flavor according to claim 1, wherein the content of the yunyan absolute is 0.2-0.8 weight part, and the content of the beta-damascenone is 0.2-0.8 weight part.
6. The primary flavor according to claim 1, wherein the 2, 3-dimethylpyrazine is contained in an amount of 0.02-0.08 parts by weight, the 2, 3-dimethylpyrazine is added in the form of 10-15 wt% of 2, 3-dimethylpyrazine, and the 2, 3-dimethylpyrazine solution is prepared by dissolving 2, 3-dimethylpyrazine in propylene glycol.
7. The method for preparing the primary flavor according to claim 1, comprising the steps of:
mixing the red date extract, the Yunyan extract, lactic acid, megastigmatrienone, dihydroactinidiolide, Yunyan absolute oil, beta-damascenone, invert sugar, 2, 3-dimethyl pyrazine and propylene glycol according to the raw material ratio to obtain the original flavor for Chinese style non-combustible heating cigarettes.
8. The method of claim 7, further comprising, prior to the mixing:
dissolving megastigmatrienone and 2, 3-dimethyl pyrazine respectively by adopting propylene glycol until the concentration is 10-15 wt%.
9. A preparation method of a cigarette core material for heating non-combustible cigarettes comprises the following steps:
mixing the coating liquid of the cigarette which is not combusted by heating with the original flavor to obtain mixed coating liquid;
coating and flavoring the tobacco sheet base by adopting the mixed coating liquid, and drying to obtain a tobacco core material;
the primary flavor is the primary flavor described in any one of claims 1 to 6 or the primary flavor prepared by the preparation method described in any one of claims 7 to 8.
10. The preparation method according to claim 1, wherein the primary flavor is 2 to 10 wt% of the coating liquid, and the mixed coating liquid is 5 to 15 wt% of the tobacco sheet base.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202210394814.2A CN114766702A (en) | 2022-04-15 | 2022-04-15 | Original flavor for Chinese style heating non-combustible cigarette, preparation method and application thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202210394814.2A CN114766702A (en) | 2022-04-15 | 2022-04-15 | Original flavor for Chinese style heating non-combustible cigarette, preparation method and application thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN114766702A true CN114766702A (en) | 2022-07-22 |
Family
ID=82429714
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202210394814.2A Pending CN114766702A (en) | 2022-04-15 | 2022-04-15 | Original flavor for Chinese style heating non-combustible cigarette, preparation method and application thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN114766702A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115505458A (en) * | 2022-11-02 | 2022-12-23 | 江西中烟工业有限责任公司 | Aroma style tobacco essence |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102302217A (en) * | 2011-03-17 | 2012-01-04 | 广州市澳键丰泽生物科技有限公司 | Formula of Chinese flue-cured tobacco flavoring essence |
| CN108893195A (en) * | 2018-06-08 | 2018-11-27 | 南通金源新材料有限公司 | A kind of composition suitable for heating the cigarette that do not burn |
| CN108991588A (en) * | 2018-10-09 | 2018-12-14 | 湖北中烟工业有限责任公司 | For improving the essence and its preparation method and application for heating not burning tobacco mouthfeel |
-
2022
- 2022-04-15 CN CN202210394814.2A patent/CN114766702A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102302217A (en) * | 2011-03-17 | 2012-01-04 | 广州市澳键丰泽生物科技有限公司 | Formula of Chinese flue-cured tobacco flavoring essence |
| CN108893195A (en) * | 2018-06-08 | 2018-11-27 | 南通金源新材料有限公司 | A kind of composition suitable for heating the cigarette that do not burn |
| CN108991588A (en) * | 2018-10-09 | 2018-12-14 | 湖北中烟工业有限责任公司 | For improving the essence and its preparation method and application for heating not burning tobacco mouthfeel |
Non-Patent Citations (1)
| Title |
|---|
| 毛多斌等: "烟草工艺与调香技术", vol. 1, 河南科学技术出版社, pages: 153 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115505458A (en) * | 2022-11-02 | 2022-12-23 | 江西中烟工业有限责任公司 | Aroma style tobacco essence |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN108451001B (en) | Dry-process reconstituted tobacco for heating non-combustible cigarettes and preparation method thereof | |
| CN106235376A (en) | A kind of reconstituted tobacco being applicable to heat non-combustion-type Medicated cigarette | |
| CN1957777A (en) | Method for preparing slices reconstituted from tea, and application in tobacco product | |
| CN103462203B (en) | Method for producing novel blended type cigarettes with flue-cured tobacco styles | |
| CN109288121B (en) | Novel cigarette suitable for different smoking modes and manufacturing method thereof | |
| WO2020177266A1 (en) | Cigarette core material capable of being lit and capable of being heated at low temperature for suction and preparation method therefor | |
| CN108576932B (en) | Raw material formula of mixed type flavor cooling and blending section, preparation method thereof and base rod of cigarette without burning during heating | |
| CN108968138B (en) | Essence for improving smoke state of tobacco not burning during heating and preparation method and application thereof | |
| CN114766702A (en) | Original flavor for Chinese style heating non-combustible cigarette, preparation method and application thereof | |
| CN108991589B (en) | Essence for reducing thorn and covering impurities in non-burning tobacco after heating and preparation method and application thereof | |
| CN108998241B (en) | Cured flue-cured tobacco flavor essence for heating non-combustible cigarettes and preparation method and application thereof | |
| CN108618192A (en) | A kind of 15 are formulated electronic cigarette tobacco tar and preparation method thereof | |
| CN112006321A (en) | Method for making tobacco shred and sheet mixed quasi-ordered heating non-combustible cigarette | |
| CN105029684B (en) | Utilize the method that compounded amino acid fermentation prepares cigar tobacco | |
| CN111362434A (en) | Wine aroma base mainly prepared from vinasse extract and used for cigarettes | |
| CN109757759B (en) | Composition and application thereof in field of cigarettes/cartridges | |
| CN214071751U (en) | Orderly heating non-combustible cigarette with mixed tobacco shreds and sheets | |
| CN114587010A (en) | Cigar flavor smoking and heating dual-purpose cigarette | |
| CN110432536B (en) | Sweet and fragrant sauce type heating non-combustion tobacco product and preparation method thereof | |
| CN110655985A (en) | Spices with Chinese flue-cured tobacco characteristic aroma and heating non-combustible cigarette prepared from spices | |
| CN110367579B (en) | Milk-sweet-fragrant type heating non-combustion tobacco product and preparation method thereof | |
| CN103385537B (en) | Burley tobaccos alcohol n-hexane mixed solution extract and its preparation method and application | |
| CN115748303B (en) | Glutinous rice fragrant cigarette paper and application thereof | |
| CN115005495B (en) | Cigar-flavored heating non-combustible cigarette | |
| CN115584297B (en) | Preparation method and application of plum extract |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination |