CN114480004B - 一种微乳脱模光亮剂 - Google Patents
一种微乳脱模光亮剂 Download PDFInfo
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- CN114480004B CN114480004B CN202210162917.6A CN202210162917A CN114480004B CN 114480004 B CN114480004 B CN 114480004B CN 202210162917 A CN202210162917 A CN 202210162917A CN 114480004 B CN114480004 B CN 114480004B
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- parts
- sodium
- paraffin
- brightening agent
- mixture
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- 239000003795 chemical substances by application Substances 0.000 title claims abstract description 46
- 238000005282 brightening Methods 0.000 title claims abstract description 24
- 239000004530 micro-emulsion Substances 0.000 title claims abstract description 15
- 229920002545 silicone oil Polymers 0.000 claims abstract description 46
- 239000012188 paraffin wax Substances 0.000 claims abstract description 33
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 24
- 229920001577 copolymer Polymers 0.000 claims abstract description 21
- 239000008367 deionised water Substances 0.000 claims abstract description 19
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 19
- 239000003995 emulsifying agent Substances 0.000 claims abstract description 18
- 229910021538 borax Inorganic materials 0.000 claims abstract description 12
- 239000011521 glass Substances 0.000 claims abstract description 12
- 239000000843 powder Substances 0.000 claims abstract description 12
- 239000004328 sodium tetraborate Substances 0.000 claims abstract description 12
- 235000010339 sodium tetraborate Nutrition 0.000 claims abstract description 12
- FTLYMKDSHNWQKD-UHFFFAOYSA-N (2,4,5-trichlorophenyl)boronic acid Chemical compound OB(O)C1=CC(Cl)=C(Cl)C=C1Cl FTLYMKDSHNWQKD-UHFFFAOYSA-N 0.000 claims abstract description 11
- 150000001336 alkenes Chemical class 0.000 claims abstract description 11
- 229910000365 copper sulfate Inorganic materials 0.000 claims abstract description 11
- ARUVKPQLZAKDPS-UHFFFAOYSA-L copper(II) sulfate Chemical compound [Cu+2].[O-][S+2]([O-])([O-])[O-] ARUVKPQLZAKDPS-UHFFFAOYSA-L 0.000 claims abstract description 11
- 229960001617 ethyl hydroxybenzoate Drugs 0.000 claims abstract description 11
- 235000010228 ethyl p-hydroxybenzoate Nutrition 0.000 claims abstract description 11
- 239000004403 ethyl p-hydroxybenzoate Substances 0.000 claims abstract description 11
- NUVBSKCKDOMJSU-UHFFFAOYSA-N ethylparaben Chemical compound CCOC(=O)C1=CC=C(O)C=C1 NUVBSKCKDOMJSU-UHFFFAOYSA-N 0.000 claims abstract description 11
- JRZJOMJEPLMPRA-UHFFFAOYSA-N olefin Natural products CCCCCCCC=C JRZJOMJEPLMPRA-UHFFFAOYSA-N 0.000 claims abstract description 11
- 229940085605 saccharin sodium Drugs 0.000 claims abstract description 11
- 239000013530 defoamer Substances 0.000 claims abstract description 10
- VVSMKOFFCAJOSC-UHFFFAOYSA-L disodium;dodecylbenzene;sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O.CCCCCCCCCCCCC1=CC=CC=C1 VVSMKOFFCAJOSC-UHFFFAOYSA-L 0.000 claims abstract description 10
- 239000000203 mixture Substances 0.000 claims description 40
- 238000003756 stirring Methods 0.000 claims description 26
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 claims description 15
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 15
- -1 liquid paraffin Substances 0.000 claims description 12
- 239000002994 raw material Substances 0.000 claims description 11
- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 claims description 10
- NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims description 10
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims description 10
- 239000004115 Sodium Silicate Substances 0.000 claims description 10
- 235000021355 Stearic acid Nutrition 0.000 claims description 10
- 238000006243 chemical reaction Methods 0.000 claims description 10
- FPYJFEHAWHCUMM-UHFFFAOYSA-N maleic anhydride Chemical compound O=C1OC(=O)C=C1 FPYJFEHAWHCUMM-UHFFFAOYSA-N 0.000 claims description 10
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 claims description 10
- OQCDKBAXFALNLD-UHFFFAOYSA-N octadecanoic acid Natural products CCCCCCCC(C)CCCCCCCCC(O)=O OQCDKBAXFALNLD-UHFFFAOYSA-N 0.000 claims description 10
- WXZMFSXDPGVJKK-UHFFFAOYSA-N pentaerythritol Chemical compound OCC(CO)(CO)CO WXZMFSXDPGVJKK-UHFFFAOYSA-N 0.000 claims description 10
- 229920002635 polyurethane Polymers 0.000 claims description 10
- 239000004814 polyurethane Substances 0.000 claims description 10
- 229910052911 sodium silicate Inorganic materials 0.000 claims description 10
- 239000008117 stearic acid Substances 0.000 claims description 10
- 239000004721 Polyphenylene oxide Substances 0.000 claims description 9
- 229920000570 polyether Polymers 0.000 claims description 9
- GVGUFUZHNYFZLC-UHFFFAOYSA-N dodecyl benzenesulfonate;sodium Chemical compound [Na].CCCCCCCCCCCCOS(=O)(=O)C1=CC=CC=C1 GVGUFUZHNYFZLC-UHFFFAOYSA-N 0.000 claims description 6
- 229940080264 sodium dodecylbenzenesulfonate Drugs 0.000 claims description 6
- VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 claims description 5
- 239000004698 Polyethylene Substances 0.000 claims description 5
- GXBURFIAORMJHZ-UHFFFAOYSA-M [Si]([O-])(O)(O)O.[Na+].[OH-].[Na+] Chemical compound [Si]([O-])(O)(O)O.[Na+].[OH-].[Na+] GXBURFIAORMJHZ-UHFFFAOYSA-M 0.000 claims description 5
- 239000000908 ammonium hydroxide Substances 0.000 claims description 5
- XGZRAKBCYZIBKP-UHFFFAOYSA-L disodium;dihydroxide Chemical compound [OH-].[OH-].[Na+].[Na+] XGZRAKBCYZIBKP-UHFFFAOYSA-L 0.000 claims description 5
- 238000005886 esterification reaction Methods 0.000 claims description 5
- 229940057995 liquid paraffin Drugs 0.000 claims description 5
- 229920000573 polyethylene Polymers 0.000 claims description 5
- 229910000029 sodium carbonate Inorganic materials 0.000 claims description 5
- 239000001488 sodium phosphate Substances 0.000 claims description 5
- 229910000162 sodium phosphate Inorganic materials 0.000 claims description 5
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 claims description 5
- POWFTOSLLWLEBN-UHFFFAOYSA-N tetrasodium;silicate Chemical compound [Na+].[Na+].[Na+].[Na+].[O-][Si]([O-])([O-])[O-] POWFTOSLLWLEBN-UHFFFAOYSA-N 0.000 claims description 5
- RYFMWSXOAZQYPI-UHFFFAOYSA-K trisodium phosphate Chemical compound [Na+].[Na+].[Na+].[O-]P([O-])([O-])=O RYFMWSXOAZQYPI-UHFFFAOYSA-K 0.000 claims description 5
- 239000001993 wax Substances 0.000 claims description 5
- 238000007334 copolymerization reaction Methods 0.000 claims description 3
- 238000002844 melting Methods 0.000 claims description 3
- 230000008018 melting Effects 0.000 claims description 3
- 238000010438 heat treatment Methods 0.000 claims description 2
- 238000002360 preparation method Methods 0.000 claims description 2
- 229960000355 copper sulfate Drugs 0.000 claims 1
- 239000004094 surface-active agent Substances 0.000 abstract description 13
- 239000012535 impurity Substances 0.000 abstract description 5
- 230000000694 effects Effects 0.000 abstract description 4
- 239000003921 oil Substances 0.000 abstract description 3
- 239000000463 material Substances 0.000 abstract description 2
- 230000002542 deteriorative effect Effects 0.000 abstract 1
- 239000002518 antifoaming agent Substances 0.000 description 11
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 4
- 238000004140 cleaning Methods 0.000 description 4
- 238000000034 method Methods 0.000 description 4
- 229910052710 silicon Inorganic materials 0.000 description 4
- 239000010703 silicon Substances 0.000 description 4
- WBIQQQGBSDOWNP-UHFFFAOYSA-N 2-dodecylbenzenesulfonic acid Chemical compound CCCCCCCCCCCCC1=CC=CC=C1S(O)(=O)=O WBIQQQGBSDOWNP-UHFFFAOYSA-N 0.000 description 3
- 239000004593 Epoxy Substances 0.000 description 3
- 125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 description 3
- 229940060296 dodecylbenzenesulfonic acid Drugs 0.000 description 3
- 150000002191 fatty alcohols Chemical class 0.000 description 3
- 229920000056 polyoxyethylene ether Polymers 0.000 description 3
- 229940051841 polyoxyethylene ether Drugs 0.000 description 3
- 125000002924 primary amino group Chemical group [H]N([H])* 0.000 description 3
- 125000003396 thiol group Chemical class [H]S* 0.000 description 3
- KCXVZYZYPLLWCC-UHFFFAOYSA-N EDTA Chemical compound OC(=O)CN(CC(O)=O)CCN(CC(O)=O)CC(O)=O KCXVZYZYPLLWCC-UHFFFAOYSA-N 0.000 description 2
- 241001122767 Theaceae Species 0.000 description 2
- 239000003054 catalyst Substances 0.000 description 2
- 239000000839 emulsion Substances 0.000 description 2
- 230000007935 neutral effect Effects 0.000 description 2
- 238000005406 washing Methods 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 1
- 230000000844 anti-bacterial effect Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000003749 cleanliness Effects 0.000 description 1
- 230000006835 compression Effects 0.000 description 1
- 238000007906 compression Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 125000000118 dimethyl group Chemical group [H]C([H])([H])* 0.000 description 1
- 238000010292 electrical insulation Methods 0.000 description 1
- 238000011010 flushing procedure Methods 0.000 description 1
- 239000006082 mold release agent Substances 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- 230000005855 radiation Effects 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 239000002689 soil Substances 0.000 description 1
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- C10M169/04—Mixtures of base-materials and additives
- C10M169/048—Mixtures of base-materials and additives the additives being a mixture of compounds of unknown or incompletely defined constitution, non-macromolecular and macromolecular compounds
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Abstract
本发明公开了一种微乳脱模光亮剂，该脱模光亮剂旨在解决现有技术下无法除去停留在模具表面的油污、氧化及未氧化的表面杂质，不能保持模具的光泽度，成品表面有毛刺，降低了成品质感的技术问题。该脱模光亮剂包括如下重量份的组分：石蜡50‑200份、硅油100‑200份、乳化剂50‑80份、硼砂100‑150份、玻璃粉200‑300份、表面活性剂70‑150份、碱剂10‑30份、尼泊金乙酯10‑30、去离子水60‑100份、消泡剂30‑50、混合共聚物100‑200份、聚合烯烃50‑100份、糖精钠80‑160份、乙氧基化丁炔二醇30‑60份、硫酸铜30‑60份、十二烷基苯硫酸钠10‑30份。该脱模光亮剂采用硅油和石蜡为主料，因此使脱模光亮剂具有较好的脱模效果，保证了成品的光泽度，防止脱模光亮剂变质，提高脱模光亮剂的抗刮伤性能，有效减少脱模光亮剂中的气泡。
Description
技术领域
本发明属于脱模光亮剂技术领域，具体涉及一种微乳脱模光亮剂。
背景技术
现今，针对日常茶具及相关杯具的清洗，一般是使用手动的毛刷杆或海绵杆进行手动清洗，其通常是一边冲水一边进行手动的刷洗，这种方式虽然直接，但其清洗效率慢，花费的时间较长；同时，这种方式容易在清洗过程中出现部分位置漏洗的情况，导致清洗不全面，从而对日常茶具在使用后难以实现全面快速的清洁。
目前，专利号为CN101406928A的发明专利公开了有机硅微乳脱模剂及其制备方法，它由如下组份组成:二甲基环硅氧烷20-35％，烷基三乙氧基硅烷3-7％，脂肪醇聚氧乙烯醚2-6％，乙二胺四乙酸0.1-0.5％，十二烷基苯磺酸4-8％，去离子水50-70％，各百分比均为重量百分比，各组分之和为百分之百，PH值为中性。有机硅微乳脱模剂的制备方法，其特征在于它包括如下步骤:①.在均质机中加入二甲基环硅氧烷20-35％，烷基三乙氧基硅烷3-7％，乙二胺四乙酸0.1-0.5％，去离子水25-35％，投入作为催化剂的十二烷基苯磺酸2-4％，调整PH值至5-7，加入乳化剂脂肪醇聚氧乙烯醚1-3％，在速度为2800转/分钟,压力为40-50mpa的条件下，均质20-50分钟，制成均质预制体乳液待用；②.在反应釜中加入去离子水25-35％，加入乳化剂脂肪醇聚氧乙烯醚1-3％，加入催化剂十二烷基苯磺酸2-4％，升温度至80"C土1C,将均质后预制体乳液滴加至反应釜中，加入时间为1小时，保温3-4小时,冷却至45C，调PH值至中性，即得有机硅微乳脱模剂，其中各百分比均为重量百分比，各组分之和为百分之百。其以有机硅中间体为原料主体，安全无毒，但该脱模剂无法除去停留在模具表面的油污、氧化及未氧化的表面杂质，不能保持模具的光泽度，成品表面有毛刺，降低了成品的质感。
因此，针对上述脱模剂不能增加成品表面光泽度的问题，亟需得到解决，以改善脱模剂的使用场景。
发明内容
(1)要解决的技术问题
针对现有技术的不足，本发明的目的在于提供一种微乳脱模光亮剂，该脱模光亮剂旨在解决现有技术下无法除去停留在模具表面的油污、氧化及未氧化的表面杂质，不能保持模具的光泽度，成品表面有毛刺，降低了成品质感的技术问题。
(2)技术方案
为了解决上述技术问题，本发明提供了这样一种微乳脱模光亮剂，该脱模光亮剂包括如下重量份的组分：石蜡50-200份、硅油100-200份、乳化剂50-80份、硼砂100-150份、玻璃粉200-300份、表面活性剂70-150份、碱剂10-30份、尼泊金乙酯10-30、去离子水60-100份、消泡剂30-50、混合共聚物100-200份、聚合烯烃50-100份、糖精钠80-160份、乙氧基化丁炔二醇30-60份、硫酸铜30-60份、十二烷基苯硫酸钠10-30份；
混合共聚物中含有季戊四醇1-3重量份、硬脂酸3-9重量份、丙烯酸1-3重量份、顺丁烯二酸酐2-5重量份；
其步骤如下：
步骤一：将季戊四醇、硬脂酸和丙烯酸按比例放入反应釜中进行酯化反应，分别于65℃、70℃和75℃下，反应10分钟，然后在80℃下反应1.5-2H，得到聚氨酯，然后往聚氨酯中加入顺丁烯二酸酐共聚，得到混合共聚物；
步骤二：碱剂中加入去离子水，得到溶液备用，往混合共聚物中加入溶液和乳化剂，以180转/分钟的转速，搅拌1个小时，得到混合物一；
步骤三：把石蜡、硅油和乳化剂放入恒温水浴锅中，在60-80℃下，将原料熔化，将熔化后的原料放入搅拌机内，并加入硼砂和玻璃粉，以150转/分钟的转速，搅拌半个小时，得到混合物二；
步骤四：将糖精钠、乙氧基化丁炔二醇、硫酸铜、十二烷基苯硫酸钠、表面活性剂、尼泊金乙酯、去离子水、聚合烯烃放入另一搅拌机内，并加热至80-90℃，以150转/分钟的转速，搅拌半个小时，得到混合物三。
步骤五：待混合物三温度与混合物二温度基本保持一致时，将混合物三慢慢加入混合物二中，以200转/分钟的转速，搅拌半个小时后，加入消泡剂和混合物一，然后以180转/分钟的转速，继续搅拌1个小时，最后以150转/分钟的转速，继续搅拌半个小时，得到成品。
优选地，所述碱剂为氢氧化钠、氢氧化钾、氢氧化铵、碳酸钠、磷酸钠、原硅酸钠、硅酸钠、氢氧化钠—原硅酸钠、氢氧化钠-硅酸钠中的任一种。
优选地，所述石蜡为微晶石蜡、液体石蜡、聚乙烯蜡、半精炼石蜡、氯化石蜡中的任一种或多种。
优选地，所述硅油为氨基改性硅油、环氧基改性硅油、聚醚改性硅油、羧基改性硅油、醇羧基改性硅油、酚羧基改性硅油、巯基改性硅油。
优选地，所述消泡剂为聚醚改性有机硅型消泡剂，所述表面活性剂为十二烷基苯磺酸钠。
(3)有益效果
与现有技术相比，本发明的有益效果在于：本发明的脱模光亮剂采用硅油和石蜡为主料，硅油具有耐热性、电绝缘性、耐候性、疏水性、生理惰性和较小的表面张力，此外还具有低的粘温系数、较高的抗压缩性、有的品种还具有耐辐射的性能，因此使脱模光亮剂具有较好的脱模效果，并且保证了成品的光泽度，利用硼砂用以净化成品表面，保障成品的整洁性，且硼砂具有一定的抑菌作用，可以防止脱模光亮剂变质，提高脱模光亮剂的使用寿命，通过添加玻璃粉，可增加脱模光亮剂的硬度和韧度，提高脱模光亮剂的抗刮伤性能，从而便于成品更好的脱模，通过消泡剂的设计，有效减少脱模光亮剂中的气泡，通过将糖精钠、乙氧基化丁炔二醇、硫酸铜和十二烷基苯硫酸钠，可以除去停留在成品表面的油污、氧化及未氧化的表面杂质，保持成品和模具的洁净、光泽度、色牢度，提高了成品的质感。
具体实施方式
为使本发明实现的技术手段、创作特征、达成目的与功效易于明白了解，下面对本发明具体实施方式中的技术方案进行清楚、完整的描述，以进一步阐述本发明，显然，所描述的具体实施方式仅仅是本发明的一部分实施方式，而不是全部的样式。
实施例1
本具体实施方式是微乳脱模光亮剂，该脱模光亮剂包括如下重量份的组分：石蜡150份、硅油100份、乳化剂50份、硼砂130份、玻璃粉200份、表面活性剂80份、碱剂10份、尼泊金乙酯30、去离子水80份、消泡剂30、混合共聚物120份、聚合烯烃80份、糖精钠160份、乙氧基化丁炔二醇50份、硫酸铜50份、十二烷基苯硫酸钠10份；
混合共聚物中含有季戊四醇2重量份、硬脂酸6重量份、丙烯酸2重量份、顺丁烯二酸酐3重量份；
其步骤如下：
步骤一：将季戊四醇2份、硬脂酸6份和丙烯酸2份放入反应釜中进行酯化反应，分别于65℃、70℃和75℃下，反应10分钟，然后在80℃下反应1.5-2H，得到聚氨酯，然后往聚氨酯中加入顺丁烯二酸酐共聚3份，得到混合共聚物；
步骤二：碱剂10份中加入去离子水20份，得到溶液备用，往混合共聚物中加入溶液和乳化剂15份，以180转/分钟的转速，搅拌1个小时，得到混合物一；
步骤三：把石蜡150份、硅油100份和乳化剂35份放入恒温水浴锅中，在60-80℃下，将原料熔化，将熔化后的原料放入搅拌机内，并加入硼砂130份和玻璃粉200份，以150转/分钟的转速，搅拌半个小时，得到混合物二；
步骤四：将糖精钠160份、乙氧基化丁炔二醇50份、硫酸铜50份、十二烷基苯硫酸钠10份、表面活性剂80份、尼泊金乙酯30份、去离子水60份、聚合烯烃80份放入另一搅拌机内，并加热至80-90℃，以150转/分钟的转速，搅拌半个小时，得到混合物三。
步骤五：待混合物三温度与混合物二温度基本保持一致时，将混合物三慢慢加入混合物二中，以200转/分钟的转速，搅拌半个小时后，加入消泡剂30份和混合物一，然后以180转/分钟的转速，继续搅拌1个小时，最后以150转/分钟的转速，继续搅拌半个小时，得到成品。
进一步的，碱剂为氢氧化钠、氢氧化钾、氢氧化铵、碳酸钠、磷酸钠、原硅酸钠、硅酸钠、氢氧化钠—原硅酸钠、氢氧化钠-硅酸钠中的任一种。
进一步的，石蜡为微晶石蜡、液体石蜡、聚乙烯蜡、半精炼石蜡、氯化石蜡中的任一种或多种。
进一步的，硅油为氨基改性硅油、环氧基改性硅油、聚醚改性硅油、羧基改性硅油、醇羧基改性硅油、酚羧基改性硅油、巯改性硅油。
进一步的，消泡剂为聚醚改性有机硅型消泡剂，表面活性剂为十二烷基苯磺酸钠。
实施例2
本具体实施方式是微乳脱模光亮剂，该脱模光亮剂包括如下重量份的组分：石蜡180份、硅油120份、乳化剂80份、硼砂120份、玻璃粉250份、表面活性剂100份、碱剂10份、尼泊金乙酯10、去离子水60份、消泡剂40、混合共聚物150份、聚合烯烃50份、糖精钠120份、乙氧基化丁炔二醇60份、硫酸铜40份、十二烷基苯硫酸钠20份；
混合共聚物中含有季戊四醇2重量份、硬脂酸6重量份、丙烯酸2重量份、顺丁烯二酸酐3重量份；
其步骤如下：
步骤一：将季戊四醇1份、硬脂酸3份和丙烯酸1份放入反应釜中进行酯化反应，分别于65℃、70℃和75℃下，反应10分钟，然后在80℃下反应1.5-2H，得到聚氨酯，然后往聚氨酯中加入顺丁烯二酸酐共聚2份，得到混合共聚物；
步骤二：碱剂10份中加入去离子水20份，得到溶液备用，往混合共聚物中加入溶液和乳化剂25份，以180转/分钟的转速，搅拌1个小时，得到混合物一；
步骤三：把石蜡180份、硅油120份和乳化剂55份放入恒温水浴锅中，在60-80℃下，将原料熔化，将熔化后的原料放入搅拌机内，并加入硼砂120份和玻璃粉250份，以150转/分钟的转速，搅拌半个小时，得到混合物二；
步骤四：将糖精钠120份、乙氧基化丁炔二醇60份、硫酸铜40份、十二烷基苯硫酸钠20份、表面活性剂100份、尼泊金乙酯10份、去离子水40份、聚合烯烃50份放入另一搅拌机内，并加热至80-90℃，以150转/分钟的转速，搅拌半个小时，得到混合物三。
步骤五：待混合物三温度与混合物二温度基本保持一致时，将混合物三慢慢加入混合物二中，以200转/分钟的转速，搅拌半个小时后，加入消泡剂40份和混合物一，然后以180转/分钟的转速，继续搅拌1个小时，最后以150转/分钟的转速，继续搅拌半个小时，得到成品。
进一步的，碱剂为氢氧化钠、氢氧化钾、氢氧化铵、碳酸钠、磷酸钠、原硅酸钠、硅酸钠、氢氧化钠—原硅酸钠、氢氧化钠-硅酸钠中的任一种。
进一步的，石蜡为微晶石蜡、液体石蜡、聚乙烯蜡、半精炼石蜡、氯化石蜡中的任一种或多种。
进一步的，硅油为氨基改性硅油、环氧基改性硅油、聚醚改性硅油、羧基改性硅油、醇羧基改性硅油、酚羧基改性硅油、巯改性硅油。
进一步的，消泡剂为聚醚改性有机硅型消泡剂，表面活性剂为十二烷基苯磺酸钠。
实施例3
本具体实施方式是微乳脱模光亮剂，该脱模光亮剂包括如下重量份的组分：石蜡180份、硅油180份、乳化剂80份、硼砂130份、玻璃粉220份、表面活性剂130份、碱剂15份、尼泊金乙酯15、去离子水100份、消泡剂40、混合共聚物150份、聚合烯烃90份、糖精钠130份、乙氧基化丁炔二醇50份、硫酸铜40份、十二烷基苯硫酸钠20份；
混合共聚物中含有季戊四醇2重量份、硬脂酸6重量份、丙烯酸2重量份、顺丁烯二酸酐3重量份；
其步骤如下：
步骤一：将季戊四醇2份、硬脂酸6份和丙烯酸2份放入反应釜中进行酯化反应，分别于65℃、70℃和75℃下，反应10分钟，然后在80℃下反应1.5-2H，得到聚氨酯，然后往聚氨酯中加入顺丁烯二酸酐共聚3份，得到混合共聚物；
步骤二：碱剂15份中加入去离子水30份，得到溶液备用，往混合共聚物中加入溶液和乳化剂20份，以180转/分钟的转速，搅拌1个小时，得到混合物一；
步骤三：把石蜡180份、硅油180份和乳化剂60份放入恒温水浴锅中，在60-80℃下，将原料熔化，将熔化后的原料放入搅拌机内，并加入硼砂130份和玻璃粉220份，以150转/分钟的转速，搅拌半个小时，得到混合物二；
步骤四：将糖精钠130份、乙氧基化丁炔二醇50份、硫酸铜40份、十二烷基苯硫酸钠20份、表面活性剂130份、尼泊金乙酯15份、去离子水70份、聚合烯烃90份放入另一搅拌机内，并加热至80-90℃，以150转/分钟的转速，搅拌半个小时，得到混合物三。
步骤五：待混合物三温度与混合物二温度基本保持一致时，将混合物三慢慢加入混合物二中，以200转/分钟的转速，搅拌半个小时后，加入消泡剂40份和混合物一，然后以180转/分钟的转速，继续搅拌1个小时，最后以150转/分钟的转速，继续搅拌半个小时，得到成品。
进一步的，碱剂为氢氧化钠、氢氧化钾、氢氧化铵、碳酸钠、磷酸钠、原硅酸钠、硅酸钠、氢氧化钠—原硅酸钠、氢氧化钠-硅酸钠中的任一种。
进一步的，石蜡为微晶石蜡、液体石蜡、聚乙烯蜡、半精炼石蜡、氯化石蜡中的任一种或多种。
进一步的，硅油为氨基改性硅油、环氧基改性硅油、聚醚改性硅油、羧基改性硅油、醇羧基改性硅油、酚羧基改性硅油、巯改性硅油。
进一步的，消泡剂为聚醚改性有机硅型消泡剂，表面活性剂为十二烷基苯磺酸钠。
表1
通过实施例3所得的成品颜色通透、无杂质、无刺激性气味，同时表面不含气泡，涂抹在模具内后，脱模后的成品表面光滑、有光泽，且无毛刺。
以上描述了本发明的主要技术特征和基本原理及相关优点，对于本领域技术人员而言，显然本发明不限于上述示范性具体实施方式的细节，而且在不背离本发明的构思或基本特征的情况下，能够以其他的具体形式实现本发明。因此，无论从哪一点来看，均应将上述具体实施方式看作是示范性的，而且是非限制性的，本发明的范围由所附权利要求而不是上述说明限定，因此旨在将落在权利要求的等同要件的含义和范围内的所有变化囊括在本发明内。
此外，应当理解，虽然本说明书按照各实施方式加以描述，但并非每个实施方式仅包含一个独立的技术方案，说明书的这种叙述方式仅仅是为清楚起见，本领域技术人员应当将说明书作为一个整体，各实施方式中的技术方案也可以经适当组合，形成本领域技术人员可以理解的其他实施方式。
Claims (3)
1.一种微乳脱模光亮剂，该脱模光亮剂由如下重量份的组分组成：石蜡50-200份、硅油100-200份、乳化剂50-80份、硼砂100-150份、玻璃粉200-300份、十二烷基苯磺酸钠70-150份、碱剂10-30份、尼泊金乙酯10-30、去离子水60-100份、聚醚改性有机硅型消泡剂30-50、混合共聚物100-200份、聚合烯烃50-100份、糖精钠80-160份、乙氧基化丁炔二醇30-60份、硫酸铜30-60份、十二烷基苯硫酸钠10-30份；
混合共聚物中含有季戊四醇1-3重量份、硬脂酸3-9重量份、丙烯酸1-3重量份、顺丁烯二酸酐2-5重量份；
其制备方法如下：
步骤一：将季戊四醇、硬脂酸和丙烯酸按比例放入反应釜中进行酯化反应，分别于65℃、70℃和75℃下，反应10分钟，然后在80℃下反应1.5-2H，得到聚氨酯，然后往聚氨酯中加入顺丁烯二酸酐共聚，得到混合共聚物；
步骤二：碱剂中加入去离子水，得到溶液备用，往混合共聚物中加入溶液和乳化剂，以180转/分钟的转速，搅拌1个小时，得到混合物一；
步骤三：把石蜡、硅油和乳化剂放入恒温水浴锅中，在60-80℃下，将原料熔化，将熔化后的原料放入搅拌机内，并加入硼砂和玻璃粉，以150转/分钟的转速，搅拌半个小时，得到混合物二；
步骤四：将糖精钠、乙氧基化丁炔二醇、硫酸铜、十二烷基苯硫酸钠、十二烷基苯磺酸钠、尼泊金乙酯、去离子水、聚合烯烃放入另一搅拌机内，并加热至80-90℃，以150转/分钟的转速，搅拌半个小时，得到混合物三；
步骤五：待混合物三温度与混合物二温度基本保持一致时，将混合物三慢慢加入混合物二中，以200转/分钟的转速，搅拌半个小时后，加入聚醚改性有机硅型消泡剂和混合物一，然后以180转/分钟的转速，继续搅拌1个小时，最后以150转/分钟的转速，继续搅拌半个小时，得到成品。
2.根据权利要求1所述的一种微乳脱模光亮剂，其特征在于，所述碱剂为氢氧化钠、氢氧化钾、氢氧化铵、碳酸钠、磷酸钠、原硅酸钠、硅酸钠、氢氧化钠—原硅酸钠、氢氧化钠-硅酸钠中的任一种。
3.根据权利要求1所述的一种微乳脱模光亮剂，其特征在于，所述石蜡为微晶石蜡、液体石蜡、聚乙烯蜡、半精炼石蜡、氯化石蜡中的任一种或多种。
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