CN114469802B - Prinsepia utilis royle oil-containing composition and dispersing method and application thereof - Google Patents
Prinsepia utilis royle oil-containing composition and dispersing method and application thereof Download PDFInfo
- Publication number
- CN114469802B CN114469802B CN202210082291.8A CN202210082291A CN114469802B CN 114469802 B CN114469802 B CN 114469802B CN 202210082291 A CN202210082291 A CN 202210082291A CN 114469802 B CN114469802 B CN 114469802B
- Authority
- CN
- China
- Prior art keywords
- prinsepia utilis
- utilis royle
- oil
- royle oil
- containing composition
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/85—Products or compounds obtained by fermentation, e.g. yoghurt, beer, wine
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Veterinary Medicine (AREA)
- Public Health (AREA)
- General Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- Epidemiology (AREA)
- Birds (AREA)
- Mycology (AREA)
- Microbiology (AREA)
- Botany (AREA)
- Biotechnology (AREA)
- Engineering & Computer Science (AREA)
- Dermatology (AREA)
- Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Cosmetics (AREA)
Abstract
The invention provides a prinsepia utilis royle oil-containing composition, and a dispersing method and application thereof. The prinsepia utilis royle oil-containing composition comprises: prinsepia utilis oil and Prinsepia utilis fermented extract; the Prinsepia utilis royle fermentation extract comprises glycerin, a pecan seed extract and a yeast fermentation product extract. The dispersion method comprises the following steps: and mixing the prinsepia utilis royle oil and the prinsepia utilis royle fermentation extract, and homogenizing to obtain the prinsepia utilis royle oil-containing composition. The invention mainly relates to a processing method capable of making prinsepia utilis royle oil droplets disperse less.
Description
Technical Field
The invention belongs to the technical field of cosmetics, and particularly relates to a prinsepia utilis royle oil-containing composition, and a dispersing method and application thereof.
Background
The Prinsepia utilis Royle is a perennial shrub plant of the genus Orchidaceae, and is known as Panicum miliaceum. The Prinsepia utilis Royle has a long history and wide application in the aspects of eating, skin care, beauty treatment, single traditional Chinese medicine and the like. The Prinsepia utilis royle oil contains three types of fatty acids which are very important to human health, wherein the content composition ratio of saturated fatty acids (palmitic acid and stearic acid), monounsaturated fatty acids (oleic acid) and polyunsaturated fatty acids (linoleic acid and linolenic acid) is (0.6-0.7): 1.
The emulsified cosmetic is prepared by high-speed shearing of water phase and oil phase, and the emulsified particle size is 1-10 μm. The emulsified particle size is related to the product formula and the production process. The shearing speed of the cosmetic emulsifying equipment is usually between 0 and 3000r/min, and the cosmetic emulsifying equipment belongs to medium and low rotating speeds. However, the existing prinsepia utilis royle oil is difficult to disperse and has the defects of larger particle size after emulsification.
CN109589278A discloses a preparation process of high-stability Prinsepia utilis Royle oil liposome, which adopts a high-low temperature alternating and high-pressure homogenizing composite process to prepare the Prinsepia utilis Royle oil liposome, thus solving the problems of stability, encapsulation rate, slow release effect, convenient addition to water and the like of Prinsepia utilis Royle oil, and effectively improving the encapsulation rate of the Prinsepia utilis Royle oil, wherein the encapsulation rate is more than 98%. The Prinsepia utilis Royle oil liposome is in a nanometer level, improves bioavailability, can be mutually dissolved with water at any ratio, and can be widely applied to preparation of various cosmetics. However, the preparation process of the method is complex, a coating object needs to be adopted for coating, high-temperature and low-temperature alternation needs to be carried out in the emulsification process, and the problem of small amount of prinsepia utilis royle oil loss still exists in the emulsification process.
CN106031705A discloses a high-content stable Prinsepia utilis royle oil microemulsion and a preparation method thereof, belonging to the technical field of oil microemulsion. The Prinsepia utilis royle oil microemulsion comprises 10-20 parts of Prinsepia utilis royle oil, 3-7 parts of tween 65, 2-7 parts of span 80, 2-6 parts of dioctyl sodium sulfosuccinate, 3-7 parts of polyethylene glycol monoricinoleate, 4-8 parts of cocamidopropyl betaine, 5-12 parts of glycerol, 2-4 parts of n-butyl alcohol, 0.1-0.3 part of preservative and 130-160 parts of deionized water. The preparation method of the Prinsepia utilis royle oil microemulsion comprises the steps of mixing, stirring, shearing and the like. The Prinsepia utilis royle oil microemulsion prepared by the method has the characteristics of small particle size, excellent storage stability and excellent solubility. Although the particle size of the emulsion prepared by the method is small, a large amount of emulsifier needs to be added for emulsification so as to improve the dispersibility and the solubility.
Therefore, it is an important research in the art to develop a treatment method that can make the droplet of the prinsepia utilis royle oil less dispersed.
Disclosure of Invention
Aiming at the defects of the prior art, the invention aims to provide a prinsepia utilis royle oil-containing composition, a dispersing method and application thereof.
In order to achieve the purpose, the invention adopts the following technical scheme:
in a first aspect, the present invention provides a prinsepia utilis oil-containing composition comprising: prinsepia utilis oil and Prinsepia utilis fermented extract;
the Prinsepia utilis royle fermented extract comprises glycerol, a carya cathayensis seed extract and a yeast fermented product extract.
In the invention, the combined group comprises prinsepia utilis royle oil and the prinsepia utilis royle fermentation extract, and the prinsepia utilis royle fermentation extract can enable the prinsepia utilis royle oil droplets to be dispersed smaller. Its advantage is: 1, the particle size of the droplets in the product can be reduced, and the arrangement and distribution are more uniform; 2 can make the product more stable.
Preferably, the mass ratio of the prinsepia utilis royle oil to the prinsepia utilis royle fermentation extract is (1-4): (4-1), and can be, for example, 1.
In the present invention, the mass ratio of the prinsepia utilis royle oil to the prinsepia utilis royle fermentation extract is within the above range, so that the particle size of the phase droplets in the product can be further reduced, and the phase droplets can be dispersed more uniformly. If the content of the Prinsepia utilis Royle oil is too much and the content of the Prinsepia utilis Royle fermentation extract is too little, the optimal dispersion effect is difficult to achieve; however, if the content of the Prinsepia utilis Royle oil is too low and the content of the Prinsepia utilis Royle fermentation extract is too high, the droplet size cannot be further reduced.
Preferably, the prinsepia utilis royle fermented extract comprises the following components in percentage by mass: 76-84% of glycerol, 3.42-3.78% of a juglans sigillata seed extract and 15.58-17.55% of a yeast fermentation product extract.
In the present invention, the glycerol content in the prinsepia utilis royle fermented extract is 76 to 84%, and may be, for example, 76%, 77%, 78%, 79%, 80%, 81%, 82%, 83%, 84%, or the like.
In the invention, the content of the juglans sigillata seed extract in the prinsepia utilis royle fermented extract is 3.42-3.78%, for example, 3.42%, 3.45%, 3.5%, 3.52%, 3.55%, 3.6%, 3.62%, 3.65%, 3.7%, 3.75%, 3.78% and the like.
In the present invention, the content of the yeast fermentation product extract in the prinsepia utilis royle fermentation extract is 15.58-17.55%, for example, 15.58%, 16.6%, 16.7%, 16.8%, 16.9%, 17%, 17.2%, 17.5%, 17.55%, etc.
Preferably, the particle size of the prinsepia utilis royle oil-containing composition is 0.1-10 μm, and may be, for example, 0.1 μm, 0.2 μm, 0.3 μm, 0.4 μm, 0.5 μm, 0.6 μm, 0.7 μm, 0.8 μm, 1 μm, 2 μm, 3 μm, 4 μm, 5 μm, 6 μm, 7 μm, 8 μm, 9 μm, 10 μm, etc., preferably 0.1-1 μm.
In a second aspect, the present invention provides a method of dispersing a prinsepia utilis royle oil-containing composition as described in the first aspect, the method of dispersing comprising the steps of: and mixing the prinsepia utilis royle oil and the prinsepia utilis royle fermentation extract, and homogenizing to obtain the prinsepia utilis royle oil-containing composition.
Preferably, the mixing temperature is 5-25 ℃, for example, can be 5 degrees, 6 degrees, 8 degrees, 10 degrees, 12 degrees, 14 degrees, 16 degrees, 18 degrees, 20 degrees, 22 degrees, 25 degrees.
Preferably, the homogenization is high-pressure homogenization, the pressure of the high-pressure homogenization is 800-1000bar, such as 800bar, 850bar, 900bar, 950bar, 1000bar and the like, and the time of the high-pressure homogenization is 1-3min, such as 1min, 1.2min, 1.4min, 1.6min, 1.8min, 2min, 2.2min, 2.4min, 2.6min, 2.8min, 3min and the like.
In the invention, the high-pressure homogenization pressure is in the range of 800-1000bar, the obtained liquid drop has smaller particle size and is more uniformly dispersed; outside this range, the particle size obtained is large, both with increasing and decreasing pressure, and even results in the Prinsepia utilis oil and the Prinsepia utilis fermented extract not being miscible.
Preferably, the homogenization is ordinary homogenization, the rotation speed of the ordinary homogenization is 1000-10000r/min, such as 1000r/min, 2000r/min, 3000r/min, 4000r/min, 5000r/min, 6000r/min, 7000r/min, 8000r/min, 9000r/min, 10000r/min and the like, and the time of the ordinary homogenization is 1-3min, such as 1min, 1.2min, 1.4min, 1.6min, 1.8min, 2min, 2.2min, 2.4min, 2.6min, 2.8min, 3min and the like.
In a third aspect, the present invention provides the use of a composition comprising prinsepia utilis royle oil as described in the first aspect in the preparation of a cosmetic product.
In a fourth aspect, the present invention provides a cosmetic comprising the prinsepia utilis royle oil-containing composition according to the first aspect.
Compared with the prior art, the invention has the following beneficial effects:
in the invention, the combined group comprises prinsepia utilis royle oil and the prinsepia utilis royle fermentation extract, and the prinsepia utilis royle fermentation extract can enable the prinsepia utilis royle oil droplets to be dispersed smaller. The advantages are as follows: 1, the particle size of the droplets in the product can be reduced, and the arrangement and distribution are more uniform; 2 can make the product more stable.
Detailed Description
The technical solution of the present invention is further described below by way of specific embodiments. It should be understood by those skilled in the art that the examples are only for the understanding of the present invention and should not be construed as the specific limitations of the present invention.
The following examples and comparative examples were purchased from the following sources:
example 1
This example provides a prinsepia utilis royle oil-containing composition obtained by the following dispersion method:
mixing Prinsepia utilis Royle oil and Prinsepia utilis Royle fermented extract at 20 deg.C in a mass ratio of 1.
Example 2
This example provides a prinsepia utilis royle oil-containing composition obtained by the following dispersion method:
mixing the prinsepia utilis royle oil and the prinsepia utilis royle fermentation extract in a mass ratio of 1.
Example 3
This example provides a prinsepia utilis royle oil-containing composition obtained by the following dispersion method:
mixing Prinsepia utilis Royle oil and Prinsepia utilis Royle fermented extract at 20 deg.C in a mass ratio of 1.
Example 4
This example provides a prinsepia utilis royle oil-containing composition obtained by the following dispersion method:
mixing Prinsepia utilis Royle oil and Prinsepia utilis Royle fermented extract at 20 deg.C in a mass ratio of 1.
Example 5
This example provides a prinsepia utilis royle oil-containing composition obtained by the following dispersion method:
mixing the prinsepia utilis royle oil and the prinsepia utilis royle fermentation extract in a mass ratio of 1.
Example 6
This example provides a prinsepia utilis royle oil-containing composition obtained by the following dispersion method:
mixing Prinsepia utilis Royle oil and Prinsepia utilis Royle fermented extract at 20 deg.C in a mass ratio of 1.
Example 7
This example provides a prinsepia utilis royle oil-containing composition obtained by the following dispersion method:
mixing Prinsepia utilis Royle oil and Prinsepia utilis Royle fermented extract at 20 deg.C in a mass ratio of 1.
Example 8
This example provides a prinsepia utilis royle oil-containing composition obtained by the following dispersion method:
mixing the prinsepia utilis royle oil and the prinsepia utilis royle fermentation extract in a mass ratio of 1.
Example 9
This example provides a prinsepia utilis royle oil-containing composition obtained by the following dispersion method:
mixing Prinsepia utilis Royle oil and Prinsepia utilis Royle fermented extract at 20 deg.C in a mass ratio of 1.
Example 10
This example provides a prinsepia utilis royle oil-containing composition obtained by the following dispersion method:
mixing Prinsepia utilis Royle oil and Prinsepia utilis Royle fermented extract at 20 deg.C in a mass ratio of 1.
Example 11
This example provides a prinsepia utilis royle oil-containing composition obtained by the following dispersion method:
mixing Prinsepia utilis Royle oil and Prinsepia utilis Royle fermented extract at 20 deg.C in a mass ratio of 1.
Example 12
This example provides a prinsepia utilis royle oil-containing composition obtained by the following dispersion method:
mixing the prinsepia utilis royle oil and the prinsepia utilis royle fermentation extract in a mass ratio of 1.
Example 13
This example provides a prinsepia utilis royle oil-containing composition obtained by the following dispersion method:
mixing Prinsepia utilis Royle oil and Prinsepia utilis Royle fermented extract at 20 deg.C in a mass ratio of 1.
Example 14
This example provides a prinsepia utilis royle oil-containing composition obtained by the following dispersion method:
mixing Prinsepia utilis Royle oil and Prinsepia utilis Royle fermented extract at 20 deg.C in a mass ratio of 1.
Example 15
This example provides a prinsepia utilis royle oil-containing composition obtained by the following dispersion method:
mixing Prinsepia utilis Royle oil and Prinsepia utilis Royle fermented extract at 20 deg.C in a mass ratio of 1.
Example 16
This example provides a prinsepia utilis royle oil-containing composition obtained by the following dispersion method:
mixing Prinsepia utilis Royle oil and Prinsepia utilis Royle fermented extract at 20 deg.C in a mass ratio of 1.
Example 17
This example provides a prinsepia utilis royle oil-containing composition obtained by the following dispersion method:
mixing Prinsepia utilis Royle oil and Prinsepia utilis Royle fermented extract at 20 deg.C in a mass ratio of 1.
Example 18
This example provides a prinsepia utilis royle oil-containing composition obtained by the following dispersion method:
mixing Prinsepia utilis Royle oil and Prinsepia utilis Royle fermented extract at 20 deg.C in a mass ratio of 1.
Example 19
This example provides a prinsepia utilis royle oil-containing composition obtained by the following dispersion method:
mixing Prinsepia utilis Royle oil and Prinsepia utilis Royle fermented extract at 20 deg.C in a mass ratio of 1.
Example 20
This example provides a prinsepia utilis royle oil-containing composition obtained by the following dispersion method:
mixing the prinsepia utilis royle oil and the prinsepia utilis royle fermentation extract in a mass ratio of 1.
Example 21
This example provides a prinsepia utilis royle oil-containing composition obtained by the following dispersion method:
mixing Prinsepia utilis Royle oil and Prinsepia utilis Royle fermented extract at 20 deg.C in a mass ratio of 1.
Example 22
This example provides a prinsepia utilis royle oil-containing composition obtained by the following dispersion method:
mixing Prinsepia utilis Royle oil and Prinsepia utilis Royle fermented extract at 20 deg.C in a mass ratio of 1.
Example 23
This example provides a prinsepia utilis royle oil-containing composition obtained by the following dispersion method:
mixing Prinsepia utilis Royle oil and Prinsepia utilis Royle fermented extract at 20 deg.C in a mass ratio of 1.
Example 24
This example provides a prinsepia utilis royle oil-containing composition obtained by the following dispersion method:
mixing Prinsepia utilis Royle oil and Prinsepia utilis Royle fermented extract at 20 deg.C in a mass ratio of 1.
Example 25
This example provides a prinsepia utilis royle oil-containing composition obtained by the following dispersion method:
mixing Prinsepia utilis Royle oil and Prinsepia utilis Royle fermented extract at 20 deg.C in a mass ratio of 1.
Example 26
This example provides a prinsepia utilis royle oil-containing composition obtained by the following dispersion method:
mixing Prinsepia utilis Royle oil and Prinsepia utilis Royle fermented extract at 20 deg.C in a mass ratio of 1.
Example 27
This example provides a prinsepia utilis royle oil-containing composition obtained by the following dispersion method:
mixing Prinsepia utilis Royle oil and Prinsepia utilis Royle fermented extract at 20 deg.C in a mass ratio of 1.
Example 28
This example provides a prinsepia utilis royle oil-containing composition obtained by the following dispersion method:
mixing the prinsepia utilis royle oil and the prinsepia utilis royle fermentation extract in a mass ratio of 2.
Example 29
This example provides a prinsepia utilis royle oil-containing composition obtained by the following dispersion method:
mixing the prinsepia utilis royle oil and the prinsepia utilis royle fermentation extract in a mass ratio of 2.
Example 30
This example provides a prinsepia utilis royle oil-containing composition obtained by the following dispersion method:
mixing the prinsepia utilis royle oil and the prinsepia utilis royle fermentation extract in a mass ratio of 2.
Example 31
This example provides a prinsepia utilis royle oil-containing composition obtained by the following dispersion method:
mixing the prinsepia utilis royle oil and the prinsepia utilis royle fermentation extract in a mass ratio of 2.
Example 32
This example provides a prinsepia utilis royle oil-containing composition obtained by the following dispersion method:
mixing the prinsepia utilis royle oil and the prinsepia utilis royle fermentation extract in a mass ratio of 2.
Example 33
This example provides a prinsepia utilis royle oil-containing composition obtained by the following dispersion method:
mixing the prinsepia utilis royle oil and the prinsepia utilis royle fermentation extract in a mass ratio of 2.
Example 34
This example provides a prinsepia utilis royle oil-containing composition obtained by the following dispersion method:
mixing the prinsepia utilis royle oil and the prinsepia utilis royle fermentation extract in a mass ratio of 2.
Example 35
This example provides a prinsepia utilis royle oil-containing composition obtained by the following dispersion method:
mixing the prinsepia utilis royle oil and the prinsepia utilis royle fermentation extract in a mass ratio of 2.
Example 36
This example provides a prinsepia utilis royle oil-containing composition obtained by the following dispersion method:
mixing the prinsepia utilis royle oil and the prinsepia utilis royle fermentation extract in a mass ratio of 2.
Example 37
This example provides a prinsepia utilis royle oil-containing composition obtained by the following dispersion method:
mixing Prinsepia utilis Royle oil and Prinsepia utilis Royle fermented extract at 20 deg.C in a mass ratio of 4.
Example 38
This example provides a prinsepia utilis royle oil-containing composition obtained by the following dispersion method:
mixing the prinsepia utilis royle oil and the prinsepia utilis royle fermentation extract in a mass ratio of 4.
Example 39
This example provides a prinsepia utilis royle oil-containing composition obtained by the following dispersion method:
mixing the prinsepia utilis royle oil and the prinsepia utilis royle fermentation extract in a mass ratio of 4.
Example 40
This example provides a prinsepia utilis royle oil-containing composition obtained by the following dispersion method:
mixing the prinsepia utilis royle oil and the prinsepia utilis royle fermentation extract in a mass ratio of 4.
Example 41
This example provides a prinsepia utilis royle oil-containing composition obtained by the following dispersion method:
mixing Prinsepia utilis Royle oil and Prinsepia utilis Royle fermented extract at 20 deg.C in a mass ratio of 4.
Example 42
This example provides a prinsepia utilis royle oil-containing composition obtained by the following dispersion method:
mixing Prinsepia utilis Royle oil and Prinsepia utilis Royle fermented extract at 20 deg.C in a mass ratio of 4.
Example 43
This example provides a prinsepia utilis royle oil-containing composition obtained by the following dispersion method:
mixing Prinsepia utilis Royle oil and Prinsepia utilis Royle fermented extract at 20 deg.C in a mass ratio of 4.
Example 44
This example provides a prinsepia utilis royle oil-containing composition obtained by the following dispersion method:
mixing the prinsepia utilis royle oil and the prinsepia utilis royle fermentation extract in a mass ratio of 4.
Example 45
This example provides a prinsepia utilis royle oil-containing composition obtained by the following dispersion method:
mixing Prinsepia utilis Royle oil and Prinsepia utilis Royle fermented extract at 20 deg.C in a mass ratio of 4.
Example 46
This example provides a prinsepia utilis royle oil-containing composition obtained by the following dispersion method:
mixing the prinsepia utilis royle oil and the prinsepia utilis royle fermentation extract in a mass ratio of 1.
Example 47
This example provides a prinsepia utilis royle oil-containing composition obtained by the following dispersion method:
mixing the prinsepia utilis royle oil and the prinsepia utilis royle fermentation extract in a mass ratio of 1.
Example 48
This example provides a prinsepia utilis royle oil-containing composition obtained by the following dispersion method:
mixing the prinsepia utilis royle oil and the prinsepia utilis royle fermentation extract in a mass ratio of 1.
Example 49
This example provides a prinsepia utilis royle oil-containing composition obtained by the following dispersion method:
mixing the prinsepia utilis royle oil and the prinsepia utilis royle fermentation extract in a mass ratio of 1.
Example 50
This example provides a prinsepia utilis royle oil-containing composition obtained by the following dispersion method:
mixing the prinsepia utilis royle oil and the prinsepia utilis royle fermentation extract in a mass ratio of 1.
Example 51
This example provides a prinsepia utilis royle oil-containing composition obtained by the following dispersion method:
mixing Prinsepia utilis Royle oil and Prinsepia utilis Royle fermented extract at a mass ratio of 1.
Example 52
This example provides a prinsepia utilis royle oil-containing composition obtained by the following dispersion method:
mixing the prinsepia utilis royle oil and the prinsepia utilis royle fermentation extract in a mass ratio of 1.
Example 53
This example provides a prinsepia utilis royle oil-containing composition obtained by the following dispersion method:
mixing the prinsepia utilis royle oil and the prinsepia utilis royle fermentation extract in a mass ratio of 1.
Example 54
This example provides a prinsepia utilis royle oil-containing composition obtained by the following dispersion method:
mixing the prinsepia utilis royle oil and the prinsepia utilis royle fermentation extract in a mass ratio of 1.
Example 55
This example provides a prinsepia utilis royle oil-containing composition obtained by the following dispersion method:
mixing the prinsepia utilis royle oil and the prinsepia utilis royle fermentation extract in a mass ratio of 1.
Example 56
This example provides a prinsepia utilis royle oil-containing composition obtained by the following dispersion method:
mixing the prinsepia utilis royle oil and the prinsepia utilis royle fermentation extract in a mass ratio of 1.
Example 57
This example provides a prinsepia utilis royle oil-containing composition obtained by the following dispersion method:
mixing the prinsepia utilis royle oil and the prinsepia utilis royle fermentation extract in a mass ratio of 1.
Example 58
This example provides a prinsepia utilis royle oil-containing composition obtained by the following dispersion method:
mixing the prinsepia utilis royle oil and the prinsepia utilis royle fermentation extract in a mass ratio of 1.
Example 59
This example provides a prinsepia utilis royle oil-containing composition obtained by the following dispersion method:
mixing the prinsepia utilis royle oil and the prinsepia utilis royle fermentation extract in a mass ratio of 1.
Example 60
This example provides a prinsepia utilis royle oil-containing composition obtained by the following dispersion method:
mixing the prinsepia utilis royle oil and the prinsepia utilis royle fermentation extract in a mass ratio of 1.
Example 61
This example provides a prinsepia utilis royle oil-containing composition obtained by the following dispersion method:
mixing the prinsepia utilis royle oil and the prinsepia utilis royle fermentation extract in a mass ratio of 1.
Example 62
This example provides a prinsepia utilis royle oil-containing composition obtained by the following dispersion method:
mixing the prinsepia utilis royle oil and the prinsepia utilis royle fermentation extract in a mass ratio of 1.
Example 63
This example provides a prinsepia utilis royle oil-containing composition obtained by the following dispersion method:
mixing the prinsepia utilis royle oil and the prinsepia utilis royle fermentation extract in a mass ratio of 1.
Example 64
This example provides a prinsepia utilis royle oil-containing composition obtained by the following dispersion method:
mixing the prinsepia utilis royle oil and the prinsepia utilis royle fermentation extract in a mass ratio of 1.
Example 65
This example provides a prinsepia utilis royle oil-containing composition obtained by the following dispersion method:
mixing Prinsepia utilis Royle oil and Prinsepia utilis Royle fermented extract at a mass ratio of 1.
Example 66
This example provides a prinsepia utilis royle oil-containing composition obtained by the following dispersion method:
mixing the prinsepia utilis royle oil and the prinsepia utilis royle fermentation extract in a mass ratio of 1.
Example 67
This example provides a prinsepia utilis royle oil-containing composition obtained by the following dispersion method:
mixing the prinsepia utilis royle oil and the prinsepia utilis royle fermentation extract in a mass ratio of 2.
Example 68
This example provides a prinsepia utilis royle oil-containing composition obtained by the following dispersion method:
mixing the prinsepia utilis royle oil and the prinsepia utilis royle fermentation extract in a mass ratio of 2.
Example 69
This example provides a prinsepia utilis royle oil-containing composition obtained by the following dispersion method:
mixing the prinsepia utilis royle oil and the prinsepia utilis royle fermentation extract in a mass ratio of 2.
Example 70
This example provides a prinsepia utilis royle oil-containing composition obtained by the following dispersion method:
mixing the prinsepia utilis royle oil and the prinsepia utilis royle fermentation extract in a mass ratio of 2.
Example 71
This example provides a prinsepia utilis royle oil-containing composition obtained by the following dispersion method:
mixing the prinsepia utilis royle oil and the prinsepia utilis royle fermentation extract in a mass ratio of 2.
Example 72
This example provides a prinsepia utilis royle oil-containing composition obtained by the following dispersion method:
mixing the prinsepia utilis royle oil and the prinsepia utilis royle fermentation extract in a mass ratio of 2.
Example 73
This example provides a prinsepia utilis royle oil-containing composition obtained by the following dispersion method:
mixing the prinsepia utilis royle oil and the prinsepia utilis royle fermentation extract in a mass ratio of 2.
Example 74
This example provides a prinsepia utilis royle oil-containing composition obtained by the following dispersion method:
mixing the prinsepia utilis royle oil and the prinsepia utilis royle fermentation extract in a mass ratio of 4:1 at 20 ℃, and carrying out common homogenization for 3min at a rotating speed of 100r/min to obtain the prinsepia utilis royle oil-containing composition.
Example 75
This example provides a prinsepia utilis royle oil-containing composition obtained by the following dispersion method:
mixing the prinsepia utilis royle oil and the prinsepia utilis royle fermentation extract in a mass ratio of 4.
Example 76
This example provides a prinsepia utilis royle oil-containing composition obtained by the following dispersion method:
mixing the prinsepia utilis royle oil and the prinsepia utilis royle fermentation extract in a mass ratio of 4.
Example 77
This example provides a prinsepia utilis royle oil-containing composition obtained by the following dispersion method:
mixing the prinsepia utilis royle oil and the prinsepia utilis royle fermentation extract in a mass ratio of 4.
Example 78
This example provides a prinsepia utilis royle oil-containing composition obtained by the following dispersion method:
mixing the prinsepia utilis royle oil and the prinsepia utilis royle fermentation extract in a mass ratio of 4.
Example 79
This example provides a prinsepia utilis royle oil-containing composition obtained by the following dispersion method:
mixing the prinsepia utilis royle oil and the prinsepia utilis royle fermentation extract in a mass ratio of 4:1 at 20 ℃, and carrying out common homogenization for 3min at a rotating speed of 8000r/min to obtain the prinsepia utilis royle oil-containing composition.
Example 80
This example provides a prinsepia utilis royle oil-containing composition obtained by the following dispersion method:
mixing the prinsepia utilis royle oil and the prinsepia utilis royle fermentation extract in a mass ratio of 4.
Comparative example 1
The present comparative example provides a prinsepia utilis royle oil-containing composition obtained by the following dispersion method:
mixing the prinsepia utilis royle oil and glycerol in a mass ratio of 1.
Comparative example 2
This example provides a prinsepia utilis royle oil-containing composition obtained by the following dispersion method:
mixing the prinsepia utilis royle oil and glycerol in a mass ratio of 1.
Performance test
Test samples: the prinsepia utilis royle oil-containing compositions provided in examples 1-80 and the prinsepia utilis royle oil-containing compositions provided in comparative examples 1-2;
the test method comprises the following steps: dispersing the samples to obtain mixed liquid, and observing the liquid drop particle diameter of the mixed liquid under an optical microscope (model: MF52-N, manufacturer: mingmei photoelectricity);
the specific test results of high pressure homogenization are shown in table 1 below, and the specific test results of general homogenization are shown in table 2 below, wherein "-" represents no mixing:
TABLE 1
TABLE 2
As can be seen from the test data in tables 1 and 2, the combined group of the invention comprises prinsepia utilis royle oil and prinsepia utilis royle fermentation extract, and the prinsepia utilis royle fermentation extract can enable the prinsepia utilis royle oil droplets to be dispersed smaller. Its advantage is: 1, the particle size of the droplets in the product can be reduced, and the arrangement and distribution are more uniform; 2 can make the product more stable.
The applicant states that the composition containing prinsepia utilis royle oil, the dispersion method and the application thereof are illustrated by the above examples, but the invention is not limited to the above examples, that is, the invention is not limited to the above examples. It should be understood by those skilled in the art that any modifications of the present invention, equivalent substitutions of the raw materials of the product of the present invention, and the addition of auxiliary components, selection of specific modes, etc., are within the scope and disclosure of the present invention.
Claims (4)
1. The composition containing the prinsepia utilis royle oil is characterized by consisting of the prinsepia utilis royle oil and a prinsepia utilis royle fermentation extract according to the mass ratio of (1-4) to (4-1);
the prinsepia utilis royle fermentation extract comprises 76-84% of glycerol, 3.42-3.78% of a carya oblata seed extract and 15.58-17.55% of a yeast fermentation product extract in percentage by mass;
the prinsepia utilis royle oil-containing composition is dispersed by the following method: mixing the prinsepia utilis royle oil and the prinsepia utilis royle fermentation extract, and homogenizing to obtain the prinsepia utilis royle oil-containing composition, wherein the mixing temperature is 5-25 ℃, the homogenizing is high-pressure homogenizing, the pressure of the high-pressure homogenizing is 800-1000bar, and the time of the high-pressure homogenizing is 1-3min.
2. The prinsepia utilis royle oil-containing composition according to claim 1, wherein the particle size of the prinsepia utilis royle oil-containing composition is 0.1-1 μm.
3. Use of the prinsepia utilis royle oil-containing composition according to any one of claims 1-2 for the preparation of a cosmetic product.
4. A cosmetic comprising the prinsepia utilis royle oil-containing composition according to any one of claims 1 to 2.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202210082291.8A CN114469802B (en) | 2022-01-24 | 2022-01-24 | Prinsepia utilis royle oil-containing composition and dispersing method and application thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202210082291.8A CN114469802B (en) | 2022-01-24 | 2022-01-24 | Prinsepia utilis royle oil-containing composition and dispersing method and application thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN114469802A CN114469802A (en) | 2022-05-13 |
| CN114469802B true CN114469802B (en) | 2023-03-31 |
Family
ID=81474344
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202210082291.8A Active CN114469802B (en) | 2022-01-24 | 2022-01-24 | Prinsepia utilis royle oil-containing composition and dispersing method and application thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN114469802B (en) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115721586B (en) * | 2022-09-05 | 2023-09-15 | 广东丸美生物技术股份有限公司 | Skin care matrix |
| CN116376731B (en) * | 2023-05-25 | 2023-08-15 | 云南英格生物技术有限公司 | Application of Wilkham yeast in preparing Prinsepia utilis extract |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101199461A (en) * | 2006-12-12 | 2008-06-18 | 王洪飞 | Skin-protecting and hair-protecting products containing prinsepia utilis royle oil |
| CN109589278A (en) * | 2018-10-10 | 2019-04-09 | 昆明贝泰妮生物科技有限公司 | The preparation process of high stable prinsepia utilis royle oil liposome and its application in cosmetics |
-
2022
- 2022-01-24 CN CN202210082291.8A patent/CN114469802B/en active Active
Also Published As
| Publication number | Publication date |
|---|---|
| CN114469802A (en) | 2022-05-13 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN114469802B (en) | Prinsepia utilis royle oil-containing composition and dispersing method and application thereof | |
| CN107252400A (en) | Vegetable fat nanoemulsions prepared by a kind of use D phases emulsion process and preparation method thereof | |
| CN103283866B (en) | camellia oil microemulsion and preparation method thereof | |
| CN102389378B (en) | Compound grease microemulsion used in cosmetics and preparation method thereof | |
| CN103301038A (en) | Tea tree oil nanoemulsion and preparation method thereof | |
| CN114848533A (en) | Preparation method of nano-liposome efficiently-coated composite ceramide | |
| CN112006923B (en) | High internal phase emulsion stabilized by low-content surfactant and preparation method thereof | |
| CN109527120B (en) | Food-grade bacteriostatic oil gel based on vegetable oil and rich in polyunsaturated fatty acid and preparation method thereof | |
| CN108498376B (en) | Methyl silicone oil emulsion and preparation method thereof | |
| CN111803427B (en) | Oil-in-water type cosmetic composition and preparation method thereof | |
| CN111449975A (en) | Microemulsion and preparation method thereof | |
| CN110771692A (en) | Camellia seed oil nano-emulsion and preparation method thereof | |
| CN107582493B (en) | Dendrobium polysaccharide emulsion containing coconut oil and preparation method thereof | |
| JP4950511B2 (en) | Emulsifier derived from red yeast | |
| JPS6153208A (en) | Skin cosmetic | |
| CN100536826C (en) | Sheep oil nano emulsions and preparation and application thereof | |
| CN112168737A (en) | Nano emulsion and preparation method thereof | |
| CN113925800A (en) | Method for improving emulsifying capacity of glycerin monostearate emulsifying system | |
| Prima et al. | Techniques of additional Kappaphycus alvarezii on seaweed face mask production | |
| CN105994345A (en) | Efficient cyfluthrin nano-emulsion composition and preparation method thereof | |
| CN109248131A (en) | A kind of energy of a quantum implantation modified version creams preparation process | |
| CN108635241A (en) | One kind having thixotropic oiliness slurry and preparation method thereof | |
| CN113693977A (en) | Rose essential oil and preparation method thereof | |
| CN115778831B (en) | Oil-in-water type brightening liquid and preparation method thereof | |
| DE4104053A1 (en) | DISPERSION OF FATTY ACID PARTICLE GLYCERIDES |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant |